Patent ID: 8362006

Claim:
A process for making a zilpaterol intermediate, or a salt thereof, wherein the process comprises: making chloro 2,3-dihydro-2-oxo-1H-benzimidazol-1-butanoate (or a salt thereof) by a process comprising reacting 4-(2-oxo-2,3-dihydrobenzimidazol-1-yl)butyric acid (or a salt thereof) with at least one chlorinating agent selected from the group consisting of oxalyl chloride, phosgene, and triphosgene; or making 4,5-dihydro-imidazo[4,5,1-jk][1]benzazepin-2,6,7[1H]-trione-6-oxime (or a salt thereof) by a process comprising reacting 8,9-dihydro-2H,7H-2,9a-diazabenzo[cd]azulene-1,6-dione (or a salt thereof) with an inorganic nitrite.