Patent ID: 7692023

Claim:
A process for preparing candesartan cilexetil Form I comprising the steps of: (a) preparing a slurry of the candesartan cilexetil Form XIV, Form XIV-1, Form XXII, or Form XXIII in a C 1 -C 4 alcohol; (b) cooling the slurry to precipitate candesartan cilexetil: (c) isolating the precipitated candesartan cilexetil; and (d) drying the precipitated candesartan cilexetil to constant weight to obtain candesartan cilexetil Form I, wherein Form XIV has x-ray diffraction peaks at 6.1, 7.3, 8.1, 10.4, 14.2, 15.3, 17.5, 20.5, 22.4, and 25.3 degrees two-theta, ±0.2 degrees two theta, Form XIV-1 has x-ray diffraction peaks at 6.4, 7.3, 8.2, 9.3, 14.3, 16.7, 20.5, 23.8, 25.3, and 28.0 degrees two-theta, ±0.2 degrees two theta, Form XXII has x-ray diffraction peaks at 7.1, 8.9, 10.6, 12.1, 16.3, 17.8, 19.4, 20.5, 21.7, and 24.0 degrees two-theta, ±0.2 degrees two theta and Form XXIII has x-ray diffraction peaks at 6.0, 10.3, 12.0, 16.3, 18.0, 19.8, 21.0, 21.6, 22.4, and 23.1 degrees two-theta, ±0.2 degrees two theta.