Patent Description:
Raw milk typically contains microorganisms/pathogens which may be unsafe for human consumption. Processes are known to treat raw milk in order to produce milk with safe pathogenic levels for human consumption. These processes, termed pasteurization, involve exposing milk to elevated temperatures.

The most common pasteurization process involves heating the milk to a temperature of about <NUM> for about <NUM> seconds, producing milk with safe pathogenic levels for human consumption with a shelf life of approximately <NUM> days. Milk produced by this process is often simply referred to as pasteurized milk, fresh milk or fresh pasteurized milk.

Ultra heat treatment (UHT) treatment of milk involves pasteurizing milk at a temperature in excess of <NUM> for a period of about <NUM> seconds to produce a milk referred to as UHT milk, which has a relatively stable shelf life. Pasteurizing milk at a temperature of about <NUM> to produce milk referred to as extended shelf life milk (ESL), which has a shelf life of about <NUM> to <NUM> days.

The temperatures required to pasteurize milk results in significant denaturing of milk proteins and enzymes as well as alterations to some organoleptic characteristics of the milk as the processing heat increases. As a result, the nutritional quality of milk is degraded by the pasteurization process, with the degree of degradation increasing as the temperature of processing is increased. Accordingly, a trade-off between nutritional value and shelf life occurs, with pasteurized milk having a higher nutritional quality and a shorter shelf life than ESL or UHT milk. The short shelf life of pasteurized milk makes if difficult to transport and sell in certain markets, and in particularly markets where the consumers of the milk are located in an area without a significant dairy industry. These types of markets are often only provided with the nutritionally inferior but longer lasting ESL or UHT milk. <CIT> describes a continuous system and procedure of sterilization and physical stabilization of pumpable fluids, food, or other type of fluids, through ultra-high pressure homogenization (UHPH) comprising a first heat exchanger <NUM> which preheats the fluid at temperature Tp between <NUM> and <NUM>; an ultra-homogenizer <NUM> through which fluid at temperature Tp is introduced at a pressure Pu between <NUM> and 600MPa increasing its temperature up to a final value.

Accordingly, there is a need to produce a milk with a high nutritional value through retention of key proteins and enzymes and with an extended shelf life.

The reference in this specification to any prior publication (or information derived from it), or to any matter which is known, is not, and should not be taken as, an acknowledgement or admission or any form of suggestion that prior publication (or information derived from it) or known matter forms part of the common general knowledge in the field of endeavour to which this specification relates.

The present invention seeks to provide a process and product with improved features and properties.

According to a first aspect the present invention provides process for treating milk including the steps of: a homogenization step wherein the milk is maintained at a temperature of below about <NUM>; and, a high pressure processing step, wherein the milk is subjected to an elevated pressure above about <NUM> MPa wherein the elevated pressure of the high pressure processing step does not induce an increase in the temperature of the milk in excess of a limiting temperature of about <NUM> during the high pressure processing step.

The process according to the invention wherein the elevated pressure of the high pressure processing step induces a temperature increase in the milk such that the temperature of the milk is increased to at least about <NUM> during the high pressure processing step.

According to further aspect the present invention provides the process according to the first aspect wherein the elevated pressure of the high pressure process step induces a temperature increase in the milk such that the temperature of the milk is increased to between about <NUM> to about <NUM> during the high pressure processing step.

According to further aspect the present invention provides the process according to the first aspect wherein the milk is subjected to an elevated pressure of between about 500MPa to about 750MPa during the high pressure processing step.

According to further aspect the present invention provides the process according to the first aspect wherein the milk is subjected to an elevated pressure of about 600MPa.

According to further aspect the present invention provides the process according to the first aspect wherein the milk is subjected to the elevated pressure in the high pressure processing step for a period of time such that pathogen levels in the milk are reduced to substantially safe levels for human consumption.

According to further aspect the present invention provides the process according to the first aspect wherein the milk is subjected to the elevated pressure in the high pressure processing step for about <NUM> minutes or less or about <NUM> minutes or less.

According to further aspect the present invention provides the process according to the first aspect further including the step of chilling the milk to an initial temperature prior to the high pressure processing step, wherein the initial temperature is selected such that the temperature of the milk does not exceed <NUM> during the high pressure processing step.

According to further aspect the present invention provides the process according to the preceding aspect wherein the initial temperature is selected such that the temperature of the milk is increased to between the range of about <NUM> to about <NUM> during the high pressure processing step.

According to further aspect the present invention provides the process according to the preceding aspect wherein the initial temperature is between about <NUM> to about <NUM>.

According to further aspect the present invention provides the process according to the first aspect wherein the high pressure processing step is performed by packaging milk into sealed containers and immersing the sealed containers in a fluid, wherein the fluid is subsequently pressurized thereby subjecting the milk to the elevated pressure.

According to further aspect the present invention provides the process according to the first aspect wherein the temperature of the fluid before pressurization is about the same temperature as the initial temperature.

According to further aspect the present invention provides the process according to the first aspect further including the step of subjecting the milk to UV treatment and/or ozone treatment and/or bactofugation.

According to further aspect the present invention provides the process according to the first aspect wherein the process is used to treat milk obtained from bovine animals, ovine animals, caprine animals, bubaline animals or camelus animals.

According to further aspect the present invention provides the process according to the first aspect wherein the process further includes the step of cooling milk to a temperature of below about <NUM> after the high pressure processing step.

According to further aspect the present invention provides the process according to the first aspect wherein the process further includes the step of standardizing the milk to a certain fat content.

According to further aspect the present invention provides the process according to the first aspect wherein the process is completed within about <NUM> hours from obtaining the milk from an animal or about <NUM> hours from obtaining the milk from an animal.

A process for treating milk is described, including the steps of (a) obtaining milk from an animal and storing the milk at a temperature of between about <NUM> and about <NUM>; and, (b) clarifying the milk; and, (c) homogenizing the milk at a temperature of between about <NUM> and about <NUM>; and, (d) packaging the milk into sealed containers; and, (e) cooling the milk to an initial temperature; and, (f) high pressure processing the homogenized milk wherein the packaged milk is immersed in a fluid subjected to elevated pressures of greater than about 500MPa; and, (g) cooling the packaged milk to a temperature of below about <NUM> after the high pressure processing step, wherein the initial temperature is chosen such that the temperature of the milk is increased to between about <NUM> to about <NUM> during the high pressure processing step.

Milk is produced by any one of the preceding aspects.

The milk has a shelf life of about <NUM> days to about <NUM> days.

According to an aspect, the present invention provides a process for treating milk, wherein the process includes the following steps: a homogenization step; and, a high pressure processing step, wherein the milk is subject to an elevated pressure.

Advantageously, the process of the above aspects may produce milk with reduced levels of pathogens whilst providing milk with improved nutritional values, organoleptic properties and shelf life compared to milk produced by conventional processes.

Example embodiments should become apparent from the following description, which is given by way of example only, of at least one preferred embodiment, described in connection with the accompanying figures.

<FIG> illustrates a flowchart of the process according to the present invention.

In the figures, incorporated to illustrate features of an example embodiment, like reference numerals are used to identify like parts throughout the figures.

Referring to <FIG>, depicted is a flowchart of a process to treat milk in accordance with an embodiment of the present invention. Instead of pasteurization, the process uses a high pressure to remove bacteria and other pathogens from milk. Using high pressures to treat milk allows the process to occur at lower temperatures than a typical pasteurization process, which may thereby avoid degradation of certain proteins and enzymes associated by high temperature processing of milk. The described process may also produce milk with a longer stable shelf life than pasteurized milk. The described process may also avoid certain organoleptic changes to milk which may otherwise occur due to pasteurization, particularly high temperature pasteurization used to produce UHT milk. The process of <FIG> includes the steps of homogenizing the milk <NUM>, cooling the milk to an initial loading temperature <NUM>, transferring the milk to sealed containers <NUM>, subjecting the milk in the sealed containers to a high pressure processing step <NUM> and cooling the milk <NUM>. However, certain optional steps may also be used by the process for treating milk as herein described.

In the example embodiment, raw milk is typically obtained by milking animals on a farm and may be reduced in temperature to between about <NUM> and about <NUM> as soon as practicable after milking. The chilled milk may then be transported to a processing site where the milk may be stored in vats at a temperature of between about <NUM> and about <NUM> in anticipation of processing.

The stored milk may then be passed through a clarifier in order to remove certain foreign materials and to help minimize any sedimentation effects that may otherwise occur when the milk is subsequently homogenized.

Milk may then undergo a preheating step where the milk may be preheated to between about <NUM> and about <NUM>, and in a preferred range of between about <NUM> and <NUM>. Once milk has been preheated, the milk may then undergo a homogenization step <NUM> where the milk is homogenized whilst the temperature of the milk is maintained between about <NUM> and <NUM>, and in a preferred range of between about <NUM> and <NUM>. Homogenizing the milk at temperatures below about <NUM> may induce deleterious effects in milk, such as premature rancidity and sedimentation of leucocytes and epithelial cells. If milk is heated to temperatures exceeding about <NUM> or about <NUM>, denaturing of phosphatase enzymes as well as casein and whey proteins may begin to occur, thereby reducing the nutritional qualities of milk. It was found that maintaining the temperature of milk within the range of about <NUM> to <NUM> during homogenization will allow for a buffer between the deleterious effects experienced by the milk outside of the approximate <NUM> to <NUM> range.

Homogenization of the milk will reduce the size of the fat globules within the milk, and disperse the reduced globules uniformly through the milk. In this step the milk is forced under pressure through small holes to reduce the size of the fat globules, allowing them to disperse uniformly through the rest of the milk. The homogenization step <NUM> may be carried out when the milk is at a temperature above about <NUM> (i.e. above ambient temperature) and below about <NUM>. In certain preferred embodiments the homogenization step may be carried out with milk at a temperature of between about <NUM> to about <NUM>.

Following homogenization, milk may be delivered to a temperature controlled balance tank <NUM>. The balance tank is configured to reduce the temperature of milk below the <NUM> to <NUM> range or below the preferred range of about <NUM> to about <NUM>. The balance tank is also configured to maintain the temperature of the milk above the initial loading temperature of the downstream high pressure processing step. After the milk has been temperature controlled by the balance tank <NUM>, the milk may then be transferred to a filling head. In certain embodiments, the balance tank may be located at a higher elevation than the filling head such that the milk may flow to the transfer head under the influence of gravity.

The filling head distributes the milk into individual packages <NUM> which may be subsequently sealed. The packages may be PET bottles, glass bottles, pouches or any other suitable package.

The packaged milk may then undergo a high pressure processing step <NUM>. In the high pressure processing step, the packaged milk is immersed in a fluid, such as for example water, within a high pressure processing chamber and exposed to elevated pressures. As the pressure inside the high pressure processing chamber is increased, the fluid evenly exerts a hydrostatic pressure to the packaged milk. It was found that subjecting the packaged milk to the elevated pressures for a defined period of time may deactivate certain pathogens in the milk, thereby producing milk with pathogen levels substantially safe for human consumption. High pressure processing of the milk was also found to lead to milk with a longer stable shelf life than pasteurized milk, allowing the milk to be transported to markets that are too distant for pasteurized milk to access before the shelf life expires.

The elevated pressured applied to milk in the high pressure processing step may be in the order of about 350MPa to about 1500MPa, though other pressures may also be used. Higher pressures may require that milk is exposed to elevated pressures for a shorter period of time than lower pressures, leading to a higher throughput of milk through the process step. However, higher pressures may require more expensive equipment and involve a higher associated operating cost than lower pressures. Similarly, lower pressures may require that the milk is exposed to elevated pressures for a longer amount of time which in some circumstances may effect the commercial viability of the process. In one example embodiment, the high pressure processing step exposed the packaged milk to an elevated pressure of about 600MPa for approximately <NUM> minutes in order to cause the inactivation of certain pathogens within the milk. Performing the high pressure processing step may be beneficial in avoiding higher pressure that may complicate and add to the expense of the process. It was also found that this pressure produced a milk with pathogen levels substantially safe for human consumption in a time frame of about <NUM> minutes. The time frame of about <NUM> minutes is beneficial as longer time frames may reduce the commercial feasibility of the batch operated high pressure processing step compared with other sterilization methods, although in some embodiments treatment times of <NUM> minutes or about <NUM> minutes may be acceptable. However, it is to be understood that the exact time required to reduce pathogen levels in the high pressure processing step may be a function of the properties of the milk undergoing treatment. For example, milk with a higher loading of pathogens may require a longer treatment time with high pressure processing to adequately reduce the pathogen levels. Similarly, milk with a relatively lower loading to pathogens may require a shorter treatment time with high pressure processing to achieve adequate pathogen mortality, such that high pressure processing at a pressure of less than 600MPa may be used to achieve an adequate pathogen mortality within about <NUM> minutes or less. In certain non-limiting embodiments, it has been found that an elevated pressure of about 500MPa to about 750MPa in the high pressure processing step has been found to produce acceptable results in an acceptable time frame, although it is to be understood that certain parameters such as the initial pathogen loading of the milk and the types of pathogens present in the milk may effect the parameters at which the high pressure processing step is operated. In some embodiments, the milk may be subjected to elevated pressures for a short time frame of about <NUM> minutes or less or about <NUM> minute or less or less than about <NUM> seconds.

The initial loading temperature of the fluid in the high pressure processing step may be chosen to increase the mortality of certain pathogens in the milk to make the milk safer for human consumption. The loading temperature may also take into consideration the temperature rise in the high pressure processing chamber which may occur due to the elevated pressures. Without wishing to be bound by theory, a temperature rise of approximately <NUM> to <NUM> may be expected for about every 100MPa increase in the chamber. Therefore a loading temperature of about <NUM> to about <NUM> may be selected as the temperature within the chamber for high pressure processing at about 600MPa such that the temperature may rise from <NUM> to <NUM> to about <NUM> to <NUM> as the chamber is pressurized from atmospheric to 600MPa. Maintaining the temperature of the milk at about <NUM> to <NUM> will comfortably avoid the temperature of about <NUM> or about <NUM> at which certain nutritional components of the milk may begin to denature. It may be beneficial to perform high pressure processing at a relatively high temperature such as about <NUM> to about <NUM> to help facilitate the mortality of pathogens in the milk, particularly pathogens that may display some resistance to high pressures, while keeping the temperature below about <NUM> or about <NUM> to avoid degradation of certain nutritional and/or organoleptic properties of the milk. However, it has been found that performing high pressure processing on milk at a temperature of about <NUM> or lower may provide for acceptable results, however, lower temperatures may require that the high pressure processing step is performed for a longer time period or at a higher pressure. The combination of elevated pressures and elevated temperatures below about <NUM> has been surprisingly found to produce milk with pathogen levels substantially safe for human consumption in a process that may be commercially viable compared to pasteurization. The milk produced by such a process may also have improved organoleptic and nutritional properties compared to pasteurized milk and may also have a longer shelf life.

Otherwise stated, it may be beneficial to perform the high pressure processing step on milk with a temperature raised above an approximate bottom limit of about <NUM> or about <NUM> to assist in the reduction of pathogen levels, but below an approximate upper limit of about <NUM> to avoid or minimize degradation of the milk in terms of nutritional value and/or organoleptic properties.

It has also been found that the temperature regime of the process to treat milk may assist in the germination of certain spore forming pathogens such as bacillus cereus, such that the germinated spores may be deactivated by the elevated pressures of the high pressure processing step. For example, the temperature regime of an initial loading temperature of about <NUM> to <NUM> leading to a milk temperature of about <NUM> to about <NUM> in the high pressure processing step operated at an elevated pressure of about 600MPa has been found to assist in the germination of certain spore forming pathogens such that the germinated spores may be more easily deactivated by the elevated pressures of the high pressure processing step. Furthermore, during the initial stages of the high pressure processing step, pressures are ramped up to the designated elevated pressure. These lower pressures at the initial stages of the ramp-up in pressure may further assist the germination of spore forming pathogens in conjunction with the temperature regime of the process, leading to easier pathogen kill at the elevated pressure. In this manner, the temperature and pressure regime if the high pressure processing step may lead to increase mortality of certain spore forming pathogens such as bacillus cereus.

It has been found that homogenizing milk at a temperature between about <NUM> and <NUM>, preferably between about <NUM> and <NUM>, and subsequently subjecting the homogenized milk to the high pressure processing step, that the resultant milk may display substantially reduced pathogen levels, as well as improved nutritional value, shelf life and organoleptic properties when compared to milk produced by a pasteurization process.

In certain preferred embodiment, the temperature of the fluid used to pressurize the chamber of the high pressure processing step may be pre-heated to the same or similar temperature as the initial loading temperature of the milk in the high pressure processing step. By preheating the fluid, the effect of the elevated pressure will increase the temperature of the fluid to about the same degree as the elevated pressure will increase the temperature of the packaged milk. In this manner, heat transfer between the fluid and the packed milk will be minimized, thereby simplifying the process in controlling the temperature of the packed milk to between about <NUM> to about <NUM>, or between about <NUM> to about <NUM> for the reasons noted above.

Following high pressure processing of the milk, the packaged milk is at a relatively high temperature, for example about <NUM> to <NUM>, such that cooling <NUM> may be required for subsequent storage and shipping. Cooling may be achieved by any suitable cooling method step such as for example by spraying chilled water over and around the packaged milk in order to reduce the temperature of the milk to below <NUM>. An alternative cooling method step may be a flash cooling step wherein the packaged milk is subjected to a reduced pressure environment which thereby reduces the temperature of the packaged milk. Cooling the milk by these methods may cause rapid temperature reduction, limiting the time that the milk is exposed to high temperatures, which may lead to an extension in the shelf life of the milk. Once the internal temperature of the milk has been brought below about <NUM>, the milk may be transferred to a cold room for storage at below <NUM> until the milk is subsequently distributed to the market.

Milk treated by the high pressure processing step for a sufficient amount of time may display substantially reduced pathogen levels. The pathogen levels may be at levels safe for human consumption or at levels approaching safe for human consumption. The pathogen levels may be the same or similar to the pathogen levels of milk treated by a pasteurization process.

In some cases, depending on the pathogen loading initially present in the milk, as well as the type of pathogens present in the milk, further treatment in addition to the high pressure processing step may be required to reduce the pathogen levels in the milk. In some embodiments, UV treatment or ozone treatment of the milk may be performed to further reduce the pathogen levels of the milk if required. In some embodiments, a bactofugation step may also be performed to reduce the pathogen loading of milk before the high pressure processing step in some embodiments. For example, when treating milk with a particularly high initial loading of pathogens it may be advantageous to use one of these additional processing steps before the high pressure processing step.

The process as herein described may be used to treat milk that has been standardized to produce a treated milk with various fat and SNF levels, for example skim milk.

As used herein, milk refers to the liquid produced by the mammary glands of mammals. Milk is an emulsion or colloid of butterfat globules within a water-based fluid that contains dissolved carbohydrates and protein aggregates with minerals. The process as herein described may be used to treat milk from any animal, including: bovine, ovine, caprine, bubaline and camelus animals. It is preferred that the milk treatment process herein described is completed within <NUM> hours or preferably <NUM> hours from the time of obtaining the milk from these animals. Milk treated in such a time frame may display improved organoleptic properties and may further display increased shelf life.

Claim 1:
A process for treating milk including the steps of:
a homogenization step wherein the milk is maintained at a temperature of below about <NUM>; and,
a high pressure processing step, wherein the milk is subjected to an elevated pressure above about <NUM> MPa wherein the elevated pressure of the high pressure processing step does not induce an increase in the temperature of the milk in excess of a limiting temperature of about <NUM> during the high pressure processing step characterized in that the elevated pressure of the high pressure processing step induces a temperature increase in the milk such that the temperature of the milk is increased to at least about <NUM> during the high pressure processing step.