Document ID: chunk:federal_register_of_legislation:F2013C00288:reg:1850:p117
Version: federal_register_of_legislation:F2013C00288
Segment Type: reg
Provision Reference: reg 1850 (pt 117/117)
Character Range: 699812–702362

10.2.3 Polycyclic aromatic hydrocarbons by solvent
extraction
10.2.3.1 Scope and application
10.2.3.2 Sample extraction
10.2.3.3 Sample clean-up
10.2.3.4 Extract analysis
10.2.4 Polycyclic aromatic hydrocarbons by supercritical
fluid extraction
10.2.4.1 Sample extraction
10.2.4.2 Extract clean-up
10.2.4.3 Extract analysis
10.2.5 Organochlorine pesticides and polychlorinated
biphenyls
10.2.5.1 Scope and application
10.2.5.2 Sample extraction
10.2.5.3 Extract analysis
10.2.6 Organophosphorus pesticides
10.2.6.1 Scope and application
10.2.6.2 Sample extraction
10.2.6.3 Extract clean-up
10.2.6.4 Sample Analysis
10.2.7 Total recoverable hydrocarbons
10.2.8 Total recoverable hydrocarbons by solvent extraction
10.2.8.1 Scope
10.2.8.2 Sample Extraction
10.2.8.3 Extract clean-up
10.2.8.4 Extract Analysis
10.2.9 Phenols
10.2.9.1 Scope and application
10.2.9.2 Sample extraction
10.2.9.3 Extract clean-up
10.2.10 Chlorinated herbicides
10.2.10.1 Scope and application
10.2.10.2 Sample extraction
10.2.10.3 Extract clean-up
10.2.10.4 Extract analysis
10.2.10.5 Extract analysis
10.2.11 Phthalate esters
10.2.11.1 Scope and application
10.2.11.2 Sample extraction
10.2.11.3 Extract clean-up
10.2.11.4 Extract analysis
10.2.12 Dioxins and furans
10.2.12.1 Scope and application
10.2.12.2 Sample extraction
10.2.12.3 Extract clean-up
10.2.12.4 Extract analysis
11 Leachable contaminants
11.1 Scope and application
12 Bibliography
13 Appendix 1: Determination of total
recoverable hydrocarbons (TRH) in soil
13.1 Volatile (C6 – C10) and semi-volatile (>C10C40) TRH
13.1.1 Quality control considerations
13.1.2 Method validation
13.1.2.1 Hydrocarbon product linearity
13.1.2.2 Product standard reference materials
13.1.2.3 Proficiency studies
13.2 Method A1: Determination of volatile
TRH: TRH C6 – C10
13.2.1 Scope and application
13.2.2 Limitations
13.2.3 Interferences
13.2.4 Principle
13.2.5 Method
13.2.5.1 Apparatus
13.2.5.2 Reagents and standards
13.2.5.3 Procedure
13.2.6 GC Analysis
13.2.6.1 Calibration
13.2.6.2 Measurement of test sample
13.2.7 Calculations
13.2.7.1 Integration of peaks
13.2.7.2 Calculation of vTRH (C6 – C10) content
13.3 Method A2: Determination of semi-volatile
TRH: TRH >C10 – C40
13.3.1 Scope and application
13.3.2 Limitations
13.3.3 Interferences
13.3.4 Principle
13.3.5 Method
13.3.5.1 Apparatus
13.3.5.2 Reagents and standards
13.3.5.3 Procedure
13.3.5.4 Silica gel clean-up
13.3.6 GC analysis
13.3.6.1 GC conditions
13.3.6.2 Chromatographic integration
13.3.6.3 GC calibration
13.3.7 Calculations
14 Shortened forms