Document ID: chunk:federal_register_of_legislation:F2013C00288:reg:1850:p116
Version: federal_register_of_legislation:F2013C00288
Segment Type: reg
Provision Reference: reg 1850 (pt 116/117)
Character Range: 696646–700168

control, preparation and storage
4.1 Sample preparation – general principles
4.2 Sample preparation: non-volatiles and semi-volatiles
4.2.1 Separation and removal of extraneous (non-soil)
components
4.2.2 Homogenising (for non-volatile constituents)
4.2.3 Preparation of field-moist ('as received') analysis
portions
4.2.4 Preparation of dry analysis portions (non-volatiles
only)
4.2.4.1 Sample drying
4.2.4.2 Grinding of dry sample
4.2.4.3 Sieving
4.2.4.4 Partitioning of dry samples to obtain representative
analysis portions
4.2.4.5 Equipment cleaning during sample preparation
(including grinding, sieving and homogenising
procedures)
4.2.5 Sample Preparation Summary  Non-volatiles and
semi-volatiles
4.3 Volatile analytes  sample collection and preparation
4.3.1 Sample collection
4.3.2 Preliminary screening analysis
4.4 Sample storage
4.4.1 Holding Times
4.5 Documentation and reporting
4.5.1 Sample receipt report
4.5.2 Analytical report
5 Analytical methods
5.1 Method selection
6 Physicochemical analyses
6.1 Soil moisture content
6.1.1 Scope and application
6.2 Soil pH
6.2.1 Scope and application
6.2.2 Principle
6.3 Electrical conductivity
6.3.1 Scope and application
6.3.2 Principle
6.4 Cation exchange capacity and exchangeable cations
6.4.1 Scope and application
6.4.2 Principle
6.5 Water-soluble chloride
6.5.1 Scope and application
6.5.2 Principle
6.5.3 Interferences
6.6 Organic carbon
6.6.1 Scope and application
6.6.2 Interferences
7 Metals
7.1 Aqua regia digestible metals
7.1.1 Scope and application
7.1.2 Principle
7.2 Acid digestible metals in sediments, sludges and soils
7.2.1 Scope and application
7.2.2 Principle
7.2.2.1 For FAAS and ICPAES
7.2.2.2 For GFAAS and ICPMS
7.3 Metals by microwave assisted acid digestion of
sediments, sludges, soils and oils
7.3.1 Scope and application
7.3.2 Principle
7.4 Mercury
7.4.1 Scope and application
7.4.2 Principle
7.5 Hexavalent Chromium
7.5.1 Scope and application
7.5.2 Principle
8 Halides
8.1 Bromide
8.1.1 Scope and application
8.1.2 Principle
8.2 Fluoride
8.2.1 Scope and application
8.2.2 Principle
9 Non-metals (cyanide and sulfur)
9.1 Cyanide (weak acid dissociable)
9.1.1 Scope and application
9.1.2 Principle
9.2 Total sulfur
9.2.1 Scope and application
9.2.2 Principle
9.3 Sulfate
9.3.1 Scope and application
9.3.2 Principle
9.4 Sulfide
9.4.1 Scope and application
9.4.2 Principle
10 Organics
10.1 Volatile organics
10.1.1 Scope and application
10.1.2 Monocyclic aromatic hydrocarbons
10.1.2.1 Preliminary screening
10.1.2.2 Sample extraction
10.1.2.3 Sample clean-up
10.1.2.4 Sample analysis
10.1.3 Volatile halogenated compounds (VHC)
10.1.3.1 Sample extraction
10.1.3.2 Sample clean-up
10.1.3.3 Sample analysis
10.1.4 Miscellaneous volatile organic compounds
10.1.4.1 Scope
10.1.4.2 Sample extraction
10.1.4.3 Sample clean-up
10.1.4.4 Sample analysis
10.1.5 Total recoverable hydrocarbons - volatile
10.1.5.1 Scope
10.1.5.2 Sample extraction
10.1.5.3 Extract clean-up
10.1.5.4 Extract analysis
10.2 Semi-volatile organics
10.2.1 Scope and application
10.2.2 Semi-volatile chlorinated hydrocarbons
10.2.2.1 Sample extraction
10.2.2.2 Extract clean-up
10.2.2.3 Extract analysis
10.2.3 Polycyclic aromatic hydrocarbons by solvent
extraction
10.2.3.1 Scope and application
10.2.3.2 Sample extraction
10.2.3.3 Sample clean-up
10.2.3.4 Extract analysis
10.2.4 Polycyclic aromatic hydrocarbons by supercritical
fluid extraction
10.2.4.1 Sample extraction
10.2.4.2 Extract clean-up
10.2.4.3 Extract analysis
10.2.5 Organochlorine pesticides