Patent Publication Number: US-2023142194-A1

Title: Use of arrays of quartz particles during single crystal silicon ingot production

Description:
CROSS-REFERENCE TO RELATED APPLICATION 
     This application claims the benefit of U.S. Provisional Patent Application No. 63/276,969, filed Nov. 8, 2021, which is incorporated herein by reference in its entirety. 
    
    
     FIELD OF THE DISCLOSURE 
     The field of the disclosure relates to methods for producing single crystal silicon ingots by Continuous Czochralski (CCz) and, in particular, methods in which an array of quartz particles are added to the crucible assembly before ingot growth. 
     BACKGROUND 
     Continuous Czochralski (CCz) is well suited to form 300 mm or 200 mm diameter single crystal silicon ingots such as ingots that are relative heavily doped with arsenic or phosphorous. Continuous Czochralski methods involve forming a single crystal silicon ingot from a melt of silicon while continuously or intermittently adding solid polycrystalline silicon to the melt to replenish the melt while the ingot is grown. The methods may involve forming multiple ingots from the same melt while the hot zone remains at temperature (i.e., with a melt continuously being present in the crucible assembly while the plurality of ingots is grown). 
     Customers increasingly expect that wafers grown by continuous Czochralski have the same relatively low void count as wafers grown by standard batch Czochralski. Continuous Czochralski methods may involve a crucible assembly that includes at least two and often three melt zones that are separated by physical barriers—an outer melt zone into which solid polycrystalline silicon is fed, a middle melt zone in which the melt stabilizes, and an inner melt zone from which the silicon ingot is pulled. Addition of solid polycrystalline silicon to the melt causes inert gas bubbles (e.g., argon bubbles) to form in the melt which impacts the void count. 
     A need exists for methods for forming silicon ingots which reduce the defect count in silicon wafers sliced from the ingot and/or which promote dissipation of the inert gas bubbles. 
     This section is intended to introduce the reader to various aspects of art that may be related to various aspects of the disclosure, which are described and/or claimed below. This discussion is believed to be helpful in providing the reader with background information to facilitate a better understanding of the various aspects of the present disclosure. Accordingly, it should be understood that these statements are to be read in this light, and not as admissions of prior art. 
     SUMMARY 
     One aspect of the present disclosure is directed to a method for forming a single crystal silicon ingot. Solid-phase polycrystalline silicon is added to a crucible assembly. An array of quartz particles is added to the crucible assembly. The array includes a plurality of quartz particles and a plurality of linking members that interconnect the quartz particles. The polycrystalline silicon is heated to form a silicon melt. The silicon melt is contacted with a seed crystal. The seed crystal is withdrawn from the silicon melt to form a silicon ingot. 
     Various refinements exist of the features noted in relation to the above-mentioned aspects of the present disclosure. Further features may also be incorporated in the above-mentioned aspects of the present disclosure as well. These refinements and additional features may exist individually or in any combination. For instance, various features discussed below in relation to any of the illustrated embodiments of the present disclosure may be incorporated into any of the above-described aspects of the present disclosure, alone or in any combination. 
    
    
     
       BRIEF DESCRIPTION OF THE DRAWINGS 
         FIG.  1    is a cross-section view of an example ingot puller apparatus having a solid polycrystalline silicon charge disposed therein; 
         FIG.  2    is a cross-section view of the ingot puller apparatus having an array of quartz particles disposed on the surface of the polycrystalline silicon charge; 
         FIG.  3    is a cross-section view of the ingot puller apparatus having a melt disposed within the crucible assembly with the array being disposed within the melt; 
         FIG.  4    is a cross-section view of the ingot puller apparatus showing a silicon ingot being pulled from the silicon melt; 
         FIG.  5    is a top view of the crucible assembly of the ingot puller apparatus with an array of quartz particles disposed in the outer melt zone; 
         FIG.  6    is a schematic of a process for forming an array of quartz particles; 
         FIG.  7    is a schematic of a quartz structure that may be incorporated into an array; 
         FIG.  8    is an embodiment of a quartz particle of the array; 
         FIG.  9    is another embodiment of quartz particles of the array; 
         FIG.  10    is another embodiment of a quartz particle of the array; 
         FIG.  11    is a schematic of quartz cullets in a silicon melt; 
         FIG.  12    is a schematic of the quartz cullets after partial dissolution thereof; 
         FIG.  13    is a schematic of the quartz cullets after coalescence; 
         FIG.  14    is a graph of the relative concentration of SiO dissolved in the silicon melt for the cullet spacing shown in each of  FIGS.  11 - 13   ; and 
         FIG.  15    is a graph showing the incremental moles of SiO (g) generated as a function of immersion time in a silicon melt for four cases of different lengths and diameters of quartz rods. 
     
    
    
     Corresponding reference characters indicate corresponding parts throughout the drawings. 
     DETAILED DESCRIPTION 
     Provisions of the present disclosure relate to methods for growing a single crystal silicon ingot in a continuous Czochralski (CCz) process. An array of quartz particles is added to the crucible assembly. The array may be made of quartz particles that are connected in the array by linking members. The array may be placed in the crucible assembly with solid polycrystalline silicon prior to melt-down. 
     An example ingot puller apparatus  5  for producing an ingot  60  by a continuous Czochralski process is shown in  FIG.  4   . The ingot puller apparatus  5  includes a crucible assembly  10  that contains a melt  6  of semiconductor or solar grade silicon material. A susceptor  13  supports the crucible assembly  10 . The crucible assembly  10  has a sidewall  40  and one or more fluid barriers  20 ,  30  or “weirs” that separate the melt into different melt zones. In the illustrated embodiment, the crucible assembly  10  includes a first weir  20 . The first weir  20  and sidewall  40  define an outer melt zone  42  of the silicon melt  6  and crucible assembly  10 . The crucible assembly  10  includes a second weir  30  radially inward to the first weir  20  which defines an inner melt zone  22  of the silicon melt and crucible assembly  10 . The inner melt zone  22  is the growth region from which the single crystal silicon ingot  60  is grown. The first weir  20  and a second weir  30  define a middle melt zone  32  of the crucible assembly  10  and silicon melt in which the melt  6  may stabilize as it moves toward the inner melt zone  22 . The first and second weirs  20 ,  30  each have at least one opening defined therein to permit molten silicon to flow radially inward towards the growth region of the inner melt zone  22 . 
     In the illustrated embodiment, the first weir  20 , second weir  30 , and sidewall  40  each have a generally annular shape. The first weir  20 , second weir  30 , and sidewall  40  may be part of three nested crucibles which are joined at the bottom or floor  45  of the crucible assembly  10  (i.e., the first and second weirs  20 ,  30  are the sidewalls of two crucibles nested within a larger crucible). The crucible assembly configuration depicted in  FIGS.  1 - 4    is exemplary. In other embodiments, the crucible assembly  10  has a single layer floor (i.e., does not have nested crucibles) with the weirs extending upward from the floor  45 . Optionally, the floor  45  may be flat rather than curved and/or the weirs  20 ,  30  and/or sidewall  40  may be straight-sided. Further, while the illustrated crucible assembly  10  is shown with two weirs, in other embodiments the crucible assembly may have a single weir or even no weirs. 
     A feeding tube  46  feeds polycrystalline silicon which may be, for example, granular, chunk, chip, or a combination of thereof, into the outer melt zone  42  at a rate sufficient to maintain a substantially constant melt elevation level and volume during growth of the ingot  60 . 
     Generally, the melt  6  from which the ingot  60  is drawn is formed by loading polycrystalline silicon into a crucible to form an initial silicon charge  27  ( FIG.  1   ). In general, an initial charge is between about 10 kilograms and about 200 kilograms of polycrystalline silicon, which may be granular, chunk, chip, or a combination thereof. The mass of the initial charge depends on the desired crystal diameter and hot zone design. Initial charge does not reflect the length of the ingot crystal, because polycrystalline silicon is continuously fed during crystal growth. 
     A variety of sources of polycrystalline silicon may be used including, for example, granular polycrystalline silicon produced by thermal decomposition of silane or a halosilane in a fluidized bed reactor or polycrystalline silicon produced in a Siemens reactor. As described below, an array of quartz particles (i.e., which may be referred to herein as quartz or glass particles and is meant to include fused quartz particles) may be added to the initial charge  27  of solid-phase polycrystalline silicon in the outer melt zone  42  or the inner melt zone  32  of the crucible assembly  10  prior to melting the initial charge  27  of polycrystalline silicon (or later if a smaller array is added such as in a system capable of feeding larger chunks of silicon). 
     Once polycrystalline silicon (and the array of quartz particles) is added to the crucible assembly  10  to form a charge  27 , the charge  27  is heated to a temperature above about the melting temperature of silicon (e.g., about 1412° C.) to melt the charge, and thereby form a silicon melt  6  ( FIG.  3   ) comprising molten silicon. The silicon melt  6  has an initial volume of molten silicon and has an initial melt elevation level, and these parameters are determined by the size of the initial charge  27 . In some embodiments, the crucible assembly  10  comprising the silicon melt  6  is heated to a temperature of at least about 1425° C., at least about 1450° C. or even at least about 1500° C. 
     The ingot puller apparatus  5  includes a pulling mechanism  114  ( FIG.  4   ) for growing and pulling the ingot  60  from the melt within the inner melt zone  22 . The pulling mechanism  114  includes a pulling cable  118 , a seed holder or chuck  120  coupled to one end of the pulling cable  118 , and a seed crystal  122  coupled to the seed holder or chuck  120  for initiating crystal growth. One end of the pulling cable  118  is connected to a lifting mechanism (e.g., driven pulley or drum, or any other suitable type of lifting mechanism) and the other end is connected to the chuck  120  that holds the seed crystal  122 . In operation, the seed crystal  122  is lowered to contact the melt  6  in the inner melt zone  22 . The pulling mechanism  114  is operated to cause the seed crystal  122  to rise along pull axis A. This causes a single crystal ingot  60  to be pulled from the melt  6 . 
     Once the charge  27  ( FIG.  1   ) of polycrystalline silicon is liquefied to form a silicon melt  6  ( FIG.  3   ) comprising molten silicon, the silicon seed crystal  122  ( FIG.  4   ) is lowered to contact the melt  6  within the inner melt zone  22 . The silicon seed crystal  122  is then withdrawn from the melt  6  with silicon being attached thereto to form a neck  52  thereby forming a melt-solid interface near or at the surface of the melt  6 . 
     The pulling mechanism  114  may rotate the seed crystal  122  and ingot  60  connected thereto. A crucible drive unit  44  may rotate the susceptor  13  and crucible assembly  10 . In some embodiments, the silicon seed crystal  122  and the crucible assembly  10  are rotated in opposite directions, i.e., counter-rotation. Counter-rotation achieves convection in the silicon melt  6 . Rotation of the seed crystal  122  is mainly used to provide a symmetric temperature profile, suppress angular variation of impurities and also to control crystal melt interface shape. 
     After formation of the neck  52 , an outwardly flaring seed-cone portion  54  (or “crown”) adjacent the neck  52  is grown. In general, the pull rate is decreased from the neck portion pull rate to a rate suitable for growing the outwardly flaring seed-cone portion  54 . Once the seed-cone portion reaches the target diameter, the main body  56  or “constant-diameter portion” of the ingot  60  is grown. In some embodiments, the main body  56  of the ingot  60  has a diameter of about 150 mm, at least about 150 mm, about 200 mm, at least about 200 mm, about 300 mm, at least about 300 mm, about 450 mm, or even at least about 450 mm. 
     While the ingot  60  is pulled from the melt  6 , solid polysilicon feedstock is added to the outer melt zone  42  through the tube  46  or other channel to replenish the melt  6  in the ingot growth apparatus  5 . Solid polycrystalline silicon may be added from a polycrystalline silicon feed system  66  and may be continuously or intermittently added to the ingot puller apparatus  5  to maintain the melt level. Generally, polycrystalline silicon may be metered into the ingot puller apparatus  5  by any method available to those of skill in the art. 
     In some embodiments, dopant is also added to the melt  6  during ingot growth. Dopant may be introduced from a dopant feed system  72 . Dopant may be added as a gas or solid and may be added to the outer melt zone  42 . 
     The apparatus  5  may include a heat shield  116  disposed about the ingot  60  to permit the growing ingot  60  to radiate its latent heat of solidification and thermal flux from the melt  6 . The heat shield  116  may be at least partially conical in shape and angles downwardly at an angle to create an annular opening in which the ingot  60  is disposed. A flow of an inert gas, such as argon, is typically provided along the length of the growing crystal. The ingot  60  is pulled through a growth chamber  78  that is sealed from the surrounding atmosphere. 
     A plurality of independently controlled annular bottom heaters  70  may be disposed in a radial pattern beneath the crucible assembly  10 . Annular bottom heaters  70  apply heat in a relatively controlled distribution across the entire base surface area of the crucible assembly  10 . The annular bottom heaters  70  may be planar resistive heating elements that are individually controlled. The apparatus  5  may include one or more side heaters  74  disposed radially outward to the crucible assembly  10  to control the temperature distribution through melt  6 . 
     The ingot growth apparatus  5  shown in  FIGS.  1 - 4    and described herein is exemplary and generally any system in which a crystal ingot is prepared by a continuous Czochralski method may be used unless stated otherwise. 
     In accordance with embodiments of the present disclosure, before the ingot  60  is grown, an array  31  ( FIG.  2   ) of quartz particles to the crucible assembly  10 . The array  31  may be added to the crucible assembly  10  before heating the polycrystalline silicon  27  to form the silicon melt  6 . The array  31  may be positioned on the initial charge  27  of polycrystalline silicon  27  or may be disposed within the charge  27  (e.g., with polycrystalline silicon disposed above and below the charge). 
     An example of an array  31  of quartz particles that is disposed in the outer melt zone  42  is shown in  FIG.  5   . The array  31  includes a plurality of quartz particles  33  and a plurality of linking members  37  that connect adjacent quartz particles  33 . The linking members  37  may be made of quartz. The array  31  may be made by 3D printing or by any other suitable method. In methods that involve 3D printing, the array may be built upward from the base with the structure being consolidated or fused layer by layer. In the 3D printing method, the deposition head or fusion source may be capable of translating in an x-y plane to effect consolidation to the final or “green” state of the array. Examples of suitable 3D printing methods that may be used include von Witzendorff et al., “Additive Manufacturing of Glass: CO 2 -Laser Glass Deposition Printing,” Procedia CIRP 74 (2018), 272-275 and Luo et al., “Additive Manufacturing of Glass,” Journal of Manufacturing Science and Engineering, vol. 136, 061024: 1-6 (2014), both of which are incorporated herein by reference for all relevant and consistent purposes. 
     In some embodiments, 3D printing is used to form an array which is a composite and/or incorporated doped materials. For example, the array  31  may be made of quartz that is doped with silicon to reduce surface crystallization of the fused silica. 
     Another embodiment of an array  31  is shown in  FIG.  6   . The array  31  includes linking members  37  that are built as a scaffold. The linking members  37  of the array  31  are made of unit cells  49  (e.g., parallelepiped) that may be stacked and linked to form a 3D scaffold. Each scaffold may incorporate a second structure that that has a quartz surface area (e.g., through porosity or another structure). The linking members  37  of the unit cells  49  may contain structure within the linking member (i.e., rather than solid bars). For example, the structure  41  shown in  FIG.  7    having a quartz particle  33  formed therein may be incorporated within the linking members  37 . 
     Other embodiments of the array  31  include monolithic disks that incorporate the quartz particles. The array  31  may incorporate a porous pattern such as a “basket-weave” pattern or a “bird&#39;s nest” pattern ( FIG.  5   ). 
     Generally, the quartz particles  33  which are incorporated into the array  31  may have any suitable size and shape that allows the array  31  to function as described herein. For example, the quartz particles  33  may be shaped as a rod, tube, sphere or have an irregular shape. In some embodiments, the particles have a size (i.e., largest dimension) between 10 μm 500 mm. The particles may be sized based on scaffold survivability which is dependent on erosion by the melt and the desired conditioning of the melt. 
     In some embodiments, the quartz particles  33  of the array  31  have a relatively high surface area. For example, the quartz particles may have a surface area to mass ratio of at least 0.1 cm 2  quartz/grams of quartz or at least 0.5 cm 2  quartz/grams of quartz (e.g., 0.1 cm 2  quartz/grams of quartz to 10 cm 2  quartz/grams of quartz). In some embodiments, the quartz particles  33  of the array  31  have a relatively high surface area relative to the amount of silicon in the crucible such as at least 10 cm 2  quartz/kg of silicon or at least 50 cm 2  quartz/kg of silicon (e.g., 10 cm 2  quartz/kg of silicon to 250 cm 2  quartz/kg of silicon). 
     The array  31  may be any size and shape that allows the array to function as described herein. In accordance with some embodiments of the present disclosure, the array  31  of quartz particles may have a sufficient width such that the array  31  continuously extends from the sidewall  40  of the crucible assembly  10  to the first weir  20 . In other embodiments, the array  31  has a width less than the distance between the sidewall  40  of the crucible assembly  10  to the first weir  20 . In some embodiments, the array  31  has a width between about 50 mm to about 75 mm and/or a height (i.e., depth) between 6 mm and 100 mm. 
     An embodiment of a quartz particle  33  for use in an array  31  is shown in  FIG.  7   . The quartz particle  33  is shaped as a hollow sphere having openings  51  formed therein. In the embodiment illustrated in  FIG.  8   , the quartz particles  33  include spires which extend from a core of the structure. In the embodiment illustrated in  FIG.  9   , the quartz particles include dimples which increase the surface area of the particle  33 . 
     The array  31  may be less dense then the melt  6  which allows the array  31  to float on the melt with a portion of the array  31  being disposed above the melt  6 . In other embodiments, the array  31  may have a density more similar to the melt such that the array  31  is immersed (or partially immersed) in the melt  6 . 
     In some continuous Czochralski processes, more than one ingot is grown while the hot zone (i.e., lower portion of the apparatus  5  such as the crucible assembly  10  and the susceptor  13 ) remains heated with silicon melt  6  being continuously within the crucible assembly  10 . In such methods, a first ingot is grown to a target length and growth is terminated, the ingot is removed from the ingot puller, and a seed crystal is then lowered into the melt to initiate growth of a second single crystal silicon ingot (i.e., using the same melt from which the first ingot was withdrawn). Subsequent ingots may be grown with the hot zone intact and at temperature with a continuous melt of silicon being within the crucible assembly  10  (e.g., until one or more components of the hot zone have degraded such as the crucible assembly requiring cool-down and replacement of the degraded component). For example, at least 1, 2, 3, 4, 5, 6, 10, or 20 or more ingots may be grown. The array  31  of ingot particles  33  may be present in the crucible assembly  10  during growth of one or more of the subsequently grown ingots (or all subsequently grown ingots while the hot zone is intact). 
     In some embodiments, no further quartz (e.g., a second array of quartz particles or free-floating quartz) are added to the crucible assembly  10  after the array  31  is positioned in the crucible assembly. For example, no further quartz is added during the entire period at which the hot zone is intact (e.g., during growth of subsequent ingots). In other embodiment, additional amounts of quartz are added during ingot growth (e.g., after the first ingot is grown). 
     Compared to conventional methods for forming single crystal silicon ingots, methods of the present disclosure have several advantages. Without being bound by any particular theory, it is believed that addition of polycrystalline silicon into the outer melt zone of the crucible assembly creates relatively small bubbles (e.g., less than 10 μm) of the inert gas (e.g., argon) that can be carried by the melt through the openings within each weir which allows bubbles to reach the silicon-melt interface. The array of quartz particles provides surface area and nucleation points for inert gas bubbles to aggregate, thereby increasing the size of the bubbles to allow them to become more buoyant. The array or particles provide a monolithic layer of quartz on the surface of the melt (e.g. with less gaps relative to non-arrayed quartz cullets). The array dissolves an amount after melt formation and the dissolved quartz helps remove inert gas from the melt. The array may be placed in the crucible assembly relatively easily before the hot zone is up to temperature (e.g., placed on the initial charge of polycrystalline silicon). Use of an array keeps the quartz particles dispersed and increases the surface area exposed to the melt, thereby better sweeping the melt of argon. The quartz particles may be configured to have a relatively high surface area compared to quartz cullets. Interconnected small feature sizes allow for increased SiO 2  dissolution (due to increase surface area) but with limited coalescence. 
     In embodiments in which the array is made by 3D printing, the surface area of the quartz particles may be increased and the particles may be interconnected in an array. 3D printing allows binders which are used in glass production to be eliminated. 3D printing allows the array to be tailored along its thickness such that regions of the array which dissolve faster due to proximity to the melt free surface may be optimized for structure integrity and SiO yield, while sections which are submerged in the melt may also be tailored to have a spacing and cross-section such that the dissolution by the melt does not render the structure unstable. The cross-sectional taper can be tailored so as to maintain the connectivity of the structure to provide sufficient surface to optimize silica production (e.g., thicker at the junction points and thinner on peripheral areas which keeps the array intact and retains array spacing). 3D printing allows a larger wall structure to be produced, where the actual structure of the wall can act as a SiO(g) generator and particle filter. Conversely, smaller macro-dimensions spheres can be produced thereby preserving the porosity to generate SiO(g) at a high rate. 3D printing could be used to yield fully dense materials that may be integrated with a porous structure (e.g., a fully dense outer shell with a porous inner core or, conversely, a fully dense inner shell with a porous outer shell depending on the evolution of the array during crystal growth). 
     EXAMPLES 
     The processes of the present disclosure are further illustrated by the following Examples. These Examples should not be viewed in a limiting sense. 
     Example 1: Increase in Quartz Particle Spacing in Conventional Methods 
       FIGS.  11 - 13    schematically show conventional cylindrical quartz particles after addition to a silicon melt (e.g., in the outer melt zone of the crucible assembly). In  FIG.  11   , after addition of the cullets, there is a depth of quartz which has some open porosity due to natural packing of the surfaces. As the crystal pulling growth progresses ( FIG.  12   ), cross-sections of the quartz surfaces are reduced and the distance between quartz pieces widens. As dissolution of quartz into the melt progresses ( FIG.  13   ), the cullets begin to coalesce. The coalescence results in a more open pathway for the silicon melt. 
     Because quartz (SiO 2 ) dissolves to produce dissolved SiO which in turn can nucleate a SiO bubble, an interaction volume can be defined as shown in the highlighted regions between the quartz shapes in  FIGS.  11  and  12   . The so-called interaction volume allows for sufficient production of SiO bubbles which can capture argon and which are annihilated at the melt free surface. It can be seen that as the shapes are dissolved, the cross-section is reduced, and when the shapes become sufficiently small and mobile, the shapes coalescence ( FIG.  13   ). This opens the spacing between the shapes resulting in clusters. The physical events of dissolution and coalescence result in changes to the concentration of dissolved SiO in the melt represented by the interaction volume which alters the effectiveness of argon removal by bubble nucleation. 
     A schematic of hypothesized profiles is shown in  FIG.  14   , with the 3 matching cases of  FIGS.  11 - 13    (“a”, “b” and “c”, respectively).  FIG.  14    shows the relative concentration of SiO dissolved in the silicon melt for the different spacing of quartz shapes. There is a critical concentration (“[SiO]* critical ) below which a bubble cannot nucleate, grow, collect argon gas and reduce grown in voids. As shown in  FIG.  14   , the spatial layout of the dissolving quartz shapes impacts the ability of the particles to sustain operable mechanisms for void reduction. 
     The generation of SiO proceeds by the following reaction between the quartz shapes and the silicon liquid: 
       Si(l)+SiO 2 (s)=&gt;2SiO(g) 
     The mass of the SiO 2  that dissolves into the silicon melt is proportional to the amount of SiO(g) generated. Using a literature average value of 10 μm/hr for the dissolution of SiO 2  into a silicon liquid, the incremental mole generation rate at a total elapsed time of immersion was calculated as a function of the total mass of quartz shapes added as well as the surface area of the shapes. In the simulation of  FIG.  15   , a total mass of 5 kg of quartz shapes was used, and the feature sizes for the diameter and length of a rod are shown as D and L respectively. Four cases of 2 cm, 1.2 cm, 0.6 cm and 0.3 cm for L and D are shown. An increased generation rate of SiO(g) occurs for smaller feature sizes. However, the compromising situation is the coalescence effect which allows for regions in the silicon melt which can by-pass the conditioning action of the SiO(g) to reduce large area void defects. 
     As used herein, the terms “about,” “substantially,” “essentially” and “approximately” when used in conjunction with ranges of dimensions, concentrations, temperatures or other physical or chemical properties or characteristics is meant to cover variations that may exist in the upper and/or lower limits of the ranges of the properties or characteristics, including, for example, variations resulting from rounding, measurement methodology or other statistical variation. 
     When introducing elements of the present disclosure or the embodiment(s) thereof, the articles “a”, “an”, “the” and “said” are intended to mean that there are one or more of the elements. The terms “comprising,” “including,” “containing” and “having” are intended to be inclusive and mean that there may be additional elements other than the listed elements. The use of terms indicating a particular orientation (e.g., “top”, “bottom”, “side”, etc.) is for convenience of description and does not require any particular orientation of the item described. 
     As various changes could be made in the above constructions and methods without departing from the scope of the disclosure, it is intended that all matter contained in the above description and shown in the accompanying drawing[s] shall be interpreted as illustrative and not in a limiting sense.