Patent Publication Number: US-2023140437-A1

Title: Heavy load vortex internal apparatus for handling plastic granular material and method related thereto

Description:
CROSS REFERENCE TO RELATED APPLICATIONS 
     This application is a continuation under 35 U.S.C. § 120 of International Application PCT/EP2020/068176, filed Jun. 28, 2020, the contents of which are incorporated by reference herein. 
    
    
     FIELD OF THE INVENTION 
     The invention relates to a swirling trough device for treating plastic granules. 
     BACKGROUND 
     Certain plastic granules are subjected after the actual granulation to an in particular thermal post-treatment in order to change the structure of the granules. For example, polylactide granules (PLA granules) polytetrafluoroethylene granules (PET granules) are first obtained from the granulation process in an amorphous state. The amorphous granules are converted into an at least partially crystalline state in a post-treatment step, also referred to as crystallization. This results in an increased alignment among the molecular chains. 
     The temperature control plays an important role for the crystallization. On the one hand, the amorphous granules must be brought to a corresponding reaction temperature or held at it. On the other hand, however, some granules, such as PLA granules, PET granules, and PU granules, tend to stick together in a transition phase. 
     PLA granules usually exit the granulator at a temperature in the range of 80 to 120° C. The individual PLA granule particles initially have a very sticky surface. Due to the glass transition temperature of about 60 to 80° C. and the crystallization temperature of about 90° C., which are very close to each other, drying and crystallizing PLA is made difficult because the granule particles must be prevented from sticking to each other during crystallization. 
     PET granules, also, are already sticky under the reaction temperature required for the crystallization, which is about 80° C. to 170° C. In order to avoid agglomeration of the granule particles, they must therefore be moved during the crystallization. The tendency to stick together decreases as the degree of crystallization increases. 
     Many technical solutions for crystallizing such granules are known from the prior art. 
     More recent approaches are based upon the consideration of subjecting the pre-dried, warm granules from the granulation to a vibration excitation during an immediately downstream crystallization process. The vibration excitation prevents adhesion of the granule particles. At the same time, the process heat stored in the granule particles can be utilized for the crystallization, so that no additional heat is required. In contrast to this, granules which are temporarily stored in a silo, for example, must, in order to prevent the adhesion, first be cooled down, and subsequently heated again for the crystallization. 
     EP 1 924 414 B1 discloses the post-treatment of the granules in the range of their reaction temperature for the crystallization, using what is known as a swirling trough device. Such a device comprises a vibrating trough for receiving the granules and at least one vibration exciter for vibration excitation of the vibrating trough. The vibration excitation takes place with a distinct transverse component perpendicular to a plane which is spanned by the longitudinal direction of the vibrating trough and the vertical direction. 
     This special type of vibration excitation causes a helical movement of the granules in the longitudinal direction of the vibrating trough, which is characteristic of swirling trough devices. Due to the vibration excitation in the transverse direction, the granule particles move upwards on the side wall of the vibrating trough and then slide back into the trough, over the subsequently rising granule particles, upon reaching vertical wall portions. This results in an uninterrupted, continuous granule flow with high interaction of the granule particles with one another, such that these can exchange process heat with one another. In this way, not only a very narrow residence time spectrum of the granule particles in the crystallization stage is achieved, but at the same time also a very homogeneous temperature profile, which has an advantageous effect on the product quality. Using conventional vibrating conveyors, screen machines, or screw conveyors, such an effect cannot be achieved, since a helical movement of the granules with high interaction of the granule particles is not possible there. 
     The swirling trough device proposed in EP 1924414 B1, which can be attributed to the applicant of the present application, is suitable only for relatively small product throughput rates due to the design. Due to the transverse component required for generating the helical movement of the product, high mass forces transverse to the vertical direction and longitudinal direction of the vibrating trough occur as the product quantity increases. 
     SUMMARY 
     An object of the present invention is that of achieving higher product throughput rates using a swirling trough device during the crystallization of plastic granules. 
     Such an object may be achieved by a heavy-duty swirling trough device according to claim  1 . Said device comprises a vibrating trough for receiving plastic granules, which has a trough base and two opposite side walls, wherein the length of the vibrating trough in the longitudinal direction is greater than the maximum height and width of a trough cross-section perpendicular to the longitudinal direction; at least two vibration exciters for generating a vibration excitation which has a transverse component perpendicular to a plane formed by the longitudinal direction and the vertical direction; and at least two trough supports, which are spaced apart from one another in the longitudinal direction of the vibrating trough, each support the trough base and the side walls from the outside, and also bridge the vibrating trough on the side opposite the trough base; wherein one vibration exciter is fastened to at least two of the trough supports in each case. 
     Such a configuration makes it possible for the first time to treat product quantities having a mass of 3 to 10 t without losses in the product quality. In this case, accelerations of 30 to 60 kgm/s 2  can be achieved. 
     Due to the special design of the trough supports, the high mass forces in the transverse direction can be managed well. 
     Advantageous embodiments of the invention form the subject matter of further claims. 
     Thus, for a particularly stable design, the trough supports can each form a closed ring which radially surrounds the vibrating trough. 
     Preferably, the vibrating trough passes substantially perpendicularly through the trough supports, so that the longitudinal direction of the vibrating trough and the main extension plane of the respective trough support enclose a smallest angle in the range from 75° to 88°. The trough supports thus brace the vibrating trough substantially in the plane of its cross-section. 
     In one variant, the main extension plane of the trough support is a vertical plane which extends substantially transversely to the longitudinal direction of the vibrating trough. Several trough supports can be placed parallel to one another in the longitudinal direction of the vibrating troughs. 
     In a further variant, the trough support has a one-piece support plate with a constant wall thickness, in which a passage opening for the vibrating trough is formed. Such a plate can be produced with little effort. If necessary, it can additionally be stiffened at its edge by flange plates. 
     Furthermore, the trough base of the vibrating trough can be inclined downwards in the longitudinal direction from a feed end to an outlet end. This promotes the transport of granules in the longitudinal direction through the vibrating trough. Preferably, the product transport is brought about solely by the new feed at the feed end, but can optionally also be assisted vibrationally. However, the skin vibration excitation component remains aligned in the transverse direction. High accelerations of granule particles in the longitudinal direction are avoided. 
     In a preferred variant, the trough base of the vibrating trough is inclined in the longitudinal direction at an angle in the range of 2° to 15° to the horizontal plane. 
     According to a further variant, the trough cross-section between a feed end and an outlet end of the vibrating trough is free of barriers. This promotes the mixing in the product stream and is advantageous for homogeneous product quality. 
     The trough supports can be included in a cage-like housing structure which, on the one hand, has a high stiffness, but on the other requires a small amount of material and is thus relatively lightweight. For this purpose, according to a further variant, adjacent trough supports are connected to one another by at least three longitudinal members in the longitudinal direction of the vibrating trough. 
     It has also been shown that the direction of force action of the vibration excitation plays an important role precisely in the case of high product masses in the vibrating trough. Preferably, also with regard to the overall height and support of the device, the vibration exciters, above the vibrating trough, and, there, preferably in a region above or laterally outside next to one of the side walls, are arranged in such a way that the force action line of the vibration excitation of the respective vibration exciter extends at a distance of at most 20%, and preferably at most 10%, of the width of the vibrating trough between the side walls to the upper edge of the side wall on the side of the vibration exciter. The above arrangement of the vibration exciters also enables a simple thermal insulation of the vibrating trough from below. 
     Preferably, the force action line of the vibration excitation of the respective vibration exciter is aligned and matched to the width of the vibrating trough such that it intersects this upstream of the center of the trough base in the transverse direction of the vibrating trough. 
     In a further variant, the force action line of the vibration excitation of the vibration excitation of the respective vibration exciter in a vertical plane including the transverse direction preferably encloses an angle in the range of 25° to 50° with the trough base. Angles that are too flat and too steep prevent the desired rise of the granule particles on the side wall and the formation of a pronounced helical movement or a vortex in the vibrating trough. 
     In order to promote the helical movement of granules in the vibrating trough, the trough base has a straight portion in the plane of the trough cross-section which is inclined downwards away from the vibration exciter to a horizontal in the plane of the trough cross-section, and in particular can be inclined to the horizontal at an angle of 2° to 15°. 
     In the case of larger trough widths, the straight portion can be divided into two or more straight segments by one or more beads extending in the longitudinal direction of the vibrating trough. In this case, the average total inclination preferably remains in the aforementioned framework of 2° to 15°. 
     In this connection, it is further advantageous if the side walls of the vibrating trough each merge into the trough base via a curved portion, wherein the radius of curvature of the curved portion on the side of the vibration exciter is greater than the radius of curvature of the curved portion on the opposite side. Due to the reduced radius of curvature on the side facing away from the vibration exciter, the usable capacity of the vibrating trough is also increased. 
     Preferably, the ratio of the radius of curvature of the curved portion on the side of the vibration exciter to the radius of curvature of the curved portion on the opposite side is greater than 2, and more preferably greater than 5. 
     Furthermore, the ratio of the radius of curvature of the curved portion on the side of the vibration exciter to the width of the vibrating trough between the side walls should as far as possible be selected so as to be less than 0.3 and greater than 0.1. 
     As already mentioned, the radius of curvature of the curved portion on the side of the vibration exciter is to be greater, and in particular significantly greater, than the radius of curvature of the curved portion on the opposite side. In a further variant, this larger radius of curvature is selected such that it is at least a quarter of the greatest trough depth of the vibrating trough, i.e., the height of the vibrating trough measured on the inside thereof. 
     The target filling of the vibrating trough is greater than 50% of the trough cross-section. 
     The heavy-duty swirling trough device explained above is suitable in particular for carrying out a method for crystallizing plastic granules having a tendency to stick together. Said method includes loading the vibrating trough according to one of the aforementioned claims with plastic granules which, when fed in, have a temperature above the glass transition temperature thereof in the range of the reaction temperature thereof for crystallization, and exciting the vibrating trough by means of the vibration exciter in such a way that the plastic granules in the vibrating trough are subjected to a helical movement, wherein the residence time of the plastic granules in the vibrating trough is 20 to 60 minutes, and the vibrating trough is filled with plastic granules over at least 50% of its cross-section. In this case, the feed of granules is preferably carried out continuously. However, a batch operation is also possible. 
    
    
     
       BRIEF DESCRIPTION OF THE DRAWING 
       The invention will be explained in more detail below with reference to an embodiment shown in the drawings, in which: 
         FIG.  1    is a three-dimensional view of a heavy-duty swirling trough device according to one embodiment of the invention, 
         FIG.  2    is a further three-dimensional view of the heavy-duty swirling trough device according to  FIG.  1   , 
         FIG.  3    is a sectional view of the heavy-duty swirling trough device according to  FIG.  1   , and 
         FIG.  4    is a detail view of the trough base of a variant having a beaded straight portion. 
     
    
    
     DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS 
     The embodiment in  FIGS.  1  through  3    shows a device which is suitable and configured for crystallizing plastic granules in the form of a heavy-duty swirling trough device  1 . The technical principle of a swirling trough, upon which the present invention is based, is explained in EP 1924414 B1, the content of which in this respect is explicitly incorporated into the present disclosure. 
     In the figures and in the following explanations, reference is made to a Cartesian coordinate system xyz, in which x represents a horizontal axis, y represents a horizontal axis orthogonal to x, and z represents a vertical axis orthogonal to x and y. The vertical axis z coincides with the direction of gravity. Consequently, the x- and y-axes span a horizontal plane xy perpendicular to the direction of gravity. 
     For the heavy-duty swirling trough device, reference is further made to a further Cartesian location coordinate system abc, in which a defines a longitudinal axis of the device, b defines a transverse direction of the device orthogonal thereto, and c defines a horizontal orthogonal to a and b. The transverse direction b coincides with the y-axis. If reference is made in the following to a transverse direction, this is to be understood as defined above. The longitudinal axis a can coincide with the x-axis, and the vertical direction c with the z-axis. As a rule, the longitudinal axis a and the vertical direction z are, however, slightly inclined towards the corresponding axes x and z, as will be explained in more detail further below. 
     The heavy-duty swirling trough device  1  initially comprises a vibrating trough  10  for receiving plastic granules. The vibrating trough  10  is designed in the manner of an elongate trough having a substantially U-shaped cross-sectional profile. Accordingly, it has a trough base  11  and two opposite side walls  12   a  and  12   a , which are connected to one another by the trough base  11 . 
     Preferably, the cross-sectional profile is constant over the length of the vibrating trough  10 . In addition, this is free of barriers, between its ends, in the longitudinal direction a. 
     The side walls  12   a  and  12   b  can be oriented substantially parallel to one another and have a constant distance from one another in the longitudinal direction, which is preferably in a range of 1,000 to 3,000 mm, and further preferably of 1,500 to 2,500 mm. They extend in the longitudinal and vertical directions a and c of the vibrating trough. 
     The side walls  12   a  and  12   b  each merge into the trough base  11  via a curved portion  13   a  or  13   b.    
     The trough base  11  can in principle be designed as a substantially planar surface in the horizontal plane xy. However, it is preferably slightly inclined in the longitudinal direction a and/or in the transverse direction b of the vibrating trough  10 . 
     Thus, the trough base  11  of the vibrating trough  10  can be inclined downwards in the longitudinal direction a from a feed end  14  to an outlet end  15  of the vibrating trough  10  in order to promote the passage of granules from the feed end  14  to the outlet end  15 . This is the case in particular if the feed of granules in the vibrating trough  10  is to be accomplished solely and exclusively by the feed of granules into the vibrating trough  10 , i.e., without conveying vibrational support. In a modification thereof, a feed of granules in the longitudinal direction a can, however, also be generated vibrationally. The latter also includes the possibility of reversing the feed direction of the granules in the vibrating trough  10 . 
     The inclination in the longitudinal direction a preferably takes place at an angle α in the range of 2° to 15° to the horizontal plane xy. In relation to the coordinate systems defined above, this means that the longitudinal axis a is set to the x-axis and the mentioned angle α. 
     The inclination of the trough base  11  in the transverse direction b is indicated in  FIG.  3   . The trough base  11  has a straight portion in the plane of the trough cross-section, i.e., a plane bc, which is inclined downwards to a horizontal b in the plane bc of the trough cross-section, from the first side wall  12   a  to the second side wall  12   b . The straight portion of the trough base  11  is preferably inclined at an angle β of 2° to 15° in particular to the horizontal b. The trough base  11  thus represents an inclined plane in the transverse direction b of the vibrating trough  10 . 
     In a modification of the embodiment, the straight portion of the trough base  11  is divided by one or more beads  11   a , extending in the longitudinal direction a of the vibrating trough  10 , into two or more straight segments  11   b ,  11   c , which are angled relative to one another.  FIG.  4    shows, by way of example, the cross-section of a beaded trough base  11  having two straight segments  11   b  and  11   c . In this case, the average total inclination ( 3 , which is measured between the merging of the trough base  11  into the curved portions  13   a  and  13   b , preferably remains in the range of 2° to 15°. The beads of the trough base  11  achieve a stiffening effect. 
     As already mentioned, the side walls  12   a  and  12   b  of the vibrating trough  10  each merge into the trough base  11  via a curved portion  13   a  and  13   b . In this case, as also indicated in  FIG.  3   , the radius of curvature r a  of the curved portion  13   a  on one side is greater than the radius of curvature r b  of the curved portion  13   b  on the opposite side. In the region of the curved portion  13   a  of the first-mentioned side, the vortex formation takes place in the granules. The smaller radius of curvature r b  on the opposite side is advantageous for a large filling volume of the vibrating trough  10 , as a result of which a high product throughput can be achieved. 
     The larger radius of curvature r a  is selected such that it is at least a quarter of the greatest trough depth t of the vibrating trough  10 , i.e., the height of the vibrating trough  10  measured on the inside thereof. 
     The ratio of the radius of curvature r a  of the curved portion  13   a  on the first-mentioned side to the radius of curvature r b  of the curved portion  13   b  on the opposite side is greater than 2, and more preferably greater than 5. 
     Particularly expedient radii of curvature r a  for the curved portion  13   a  on the first-mentioned side lie in the range of 180 to 450 mm at a trough width of 1,800 mm. 
     With respect to the clear width w of the vibrating trough  10  between the side walls  12   a  and  12   b , i.e., the extension thereof in the transverse direction b or y, the ratio of the radius of curvature r a  of the curved portion  13   a  on the first-mentioned side to the width of the vibrating trough  10  is preferably less than 0.25 and/or greater than 0.1. 
     Usually, the clear width w is selected so as to be greater than the trough depth t. 
     The device  1  further comprises at least two vibration exciters  20  for generating vibration excitation on the vibrating trough  10 , wherein the vibration excitation has a component in the transverse direction b or y. This transverse component of the vibration excitation is decisive, in conjunction with the formation of the cross-sectional profile of the vibrating trough  10 , for the formation of a vortex or helical movement of the granules about an axis, parallel to the longitudinal direction a, in the vibrating trough  10 . In addition, the vibration excitation can contain a component in the vertical direction z or height direction c. In contrast, the proportion in the longitudinal direction a or in the direction of the x-axis is negligible. 
     The vibration exciters  20  can be designed, for example, as directed exciters, which are coupled to one another so that the excitation by all vibration exciters  20  takes place synchronously. However, other types of exciters are also possible. 
     The vibration exciter  20  is not attached directly to the vibrating trough  10 , but, rather, to a cage-like housing structure  30 , which is explained in more detail below and which carries the vibrating trough  10 . 
     The housing structure  30  is based upon two or more trough supports  31 , which are preferably arranged in parallel, i.e., in the longitudinal direction a of the vibrating trough  10 , in succession. In this case, the trough supports  31  are each spaced apart from one another, as can be clearly seen in  FIGS.  1  and  2   . The trough supports  31  can be produced as initially separate components. In the present case, three trough supports  31  are shown by way of example. However, the number thereof can also be selected to be smaller or larger, depending upon the length of the vibrating trough  10 . 
     The housing structure  30  also has longitudinal members  32  by which adjacent trough supports  31  are rigidly connected to one another. In the present case, three longitudinal members  32  are provided, which extend laterally to the vibrating trough  10 , and preferably in the x-direction, in order to connect at least two adjacent trough supports  31  or, optionally, also all the trough supports  31 . The longitudinal members  32  can be rod-shaped or bar-shaped. In one variant, these have a constant cross-sectional profile. In particular, the longitudinal members  32  can also be designed as hollow profiles. 
     The housing structure  30  is supported against a substrate via springs  40 . The springs  40  are preferably arranged on at least some of the trough supports  31 . 
     The vibration exciters  20  preferably sit above the vibrating trough  10  on the trough supports  31 , and preferably above the side wall  12   a  of the first-mentioned side, or somewhat laterally to the outside thereof. 
     With regard to the simultaneous processing of large masses of granules on the order of magnitude of 3 to 10 t in the vibrating trough  10 , the trough supports  31  are designed in a special manner. 
     The cross-section of a trough support  31  can be clearly seen in  FIG.  3   . The trough support  31  is rigidly connected to the vibrating trough  10 . In particular, the trough support  31  has two vertical struts  31   a  and  31   b , which extend vertically upwards from a lower base portion  31   c . The vertical struts  31   a  and  31   b  are connected to one another by a bracket portion  31   d , so that a passage opening  33  for the vibrating trough  10  is formed between said portions  31   a  through  31   d . The trough support  31  has its main extension in the direction of the y- and z-axes, i.e., its extension in the x-direction is comparatively small relative thereto, such that it can be referred to as disk-shaped or plate-shaped. 
     As can be seen in  FIGS.  1  through  3   , the trough support  31  supports the trough base  11  and the side walls  12   a  and  12   b  of the vibrating trough  10  from the outside. Thus, the vertical struts  31   a  and  31   b  rest against the side walls  12   a  and  12   b  of the vibrating trough, on the outside. Likewise, the trough base  11  rests on the lower base portion  31   c.    
     Furthermore, the trough support  31  bridges the vibrating trough  10  on the side opposite the trough base  11 . The bracket portion  31   d , which connects the vertical struts  31   a  and  31   b  to one another, accordingly extends above the vibrating trough  10  in the transverse direction b or y. 
     In the present case, the trough supports  31  each form a closed ring, which radially surrounds the vibrating trough  10 . 
     In this case, the vibrating trough  10  passes approximately perpendicularly through the trough supports  31 , i.e., the longitudinal direction a of the vibrating trough  10  encloses a smallest angle with the main extension plane xy of the respective trough support  31  in the range of 75° to 90°. 
     As a result, a very stable mounting of the vibrating trough  10  on the housing structure  30  is achieved, which in turn can be designed so as to be relatively lightweight. In particular, any widening or breathing of the vibrating trough  10  in the transverse direction b is counteracted. 
     In one variant, the trough supports  31  each have a one-piece support plate  34  with a constant wall thickness, in which the passage opening  33  for the vibrating trough  10  is formed. Additional stiffening can be achieved very easily by flange plates  35  welded to the outer edges of the support plate  34 . 
     Instead of a one-piece support plate  34 , the ring structure of a trough support  31  directly supporting the vibrating trough  10  can also be assembled, and in particular welded, from several individual parts. 
     Furthermore, it is possible to produce a trough support  31  as a casting. 
     The vibration exciters  20  are arranged on the trough supports  31  above the vibrating trough  10  in a region above or laterally outside next to one of the side walls  12   a  in such a way that the force action line k of the vibration excitation of the respective vibration exciter  20  extends at a distance of at most 20%, and more preferably at most 10%, of the width w of the vibrating trough  10  between the side walls  12   a  and  12   b  to the upper edge  12   c  of the side wall  12   a  on the side of the vibration exciter. 
     The force action line k of the vibration excitation of the respective vibration exciter  20  preferably intersects the trough base  11  upstream of the center of the trough base  11  in the transverse direction b or y of the vibrating trough  10 . This promotes the vortex formation in the region of the more gently curved curved portion  13   a , on the side of the vibration exciter, of the vibrating trough  10  and ensures a large number of collisions between the granule particles to be treated. 
     Furthermore, the force action line k of the vibration excitation of the respective vibration exciter  20  in a vertical plane yz that includes the transverse direction b or y encloses an angle γ in the range of 25° to 50° with the trough base  11 . 
     By means of the above heavy-duty swirling trough device  1 , granule masses of 3 to 10 t can be treated simultaneously without losses in the product quality, wherein acceleration values in the range from 30 to 60 kgm/s 2  are possible, which ensure that the granule particles do not stick together. 
     In this case, the target filling of the vibrating trough  10  can be greater than 50% of the trough cross-section, i.e., good utilization of the treatment space for the granules is achieved. 
     Due to the radial encompassing of the trough-shaped vibrating trough  10 , the trough supports  31  are particularly suitable for absorbing forces introduced in the direction of the y-axis, transverse to the product flow direction. These forces are very high in the case of a large product filling and can also be additionally amplified in their effect by the dynamic excitation of the product, and in particular clump formation in the product, which cannot be excluded. 
     Achievable widths of the vibrating trough  10  are approximately 1,000 to 3,000 mm. In this case, construction lengths of 5,000 to 10,000 mm are possible. 
     This takes account of the fact that, in the case of certain plastics, increasingly higher performance, i.e., product volumes at an approximately constant residence time, is desired, but the number of vibrating troughs to be used in series is to remain limited, as far as possible, to a maximum of three swirling trough devices, for reasons of installation and cost. 
     The design of the housing structure  30  carrying the vibrating trough  10 , consisting of several, preferably disk-shaped, trough supports  31 , each of which radially encompasses the trough-shaped vibrating trough  10  and at the same time absorbs the forces introduced by the vibration exciter  20 , remains comparatively lightweight and expedient to produce, despite the ability to support the high transverse forces. 
     The heavy-duty swirling trough device  1  explained above is suitable in particular for carrying out a method for crystallizing plastic granules having a tendency to stick together, such as PLA, PET, or PU. For this purpose, the vibrating trough  10  of the heavy-duty swirling trough device  1  is loaded with plastic granules which have already been heated when fed in, i.e., in particular have a temperature above the glass transition temperature thereof in the range of the reaction temperature thereof for crystallization. 
     In particular, the raw granules can be directly taken over from a granulating device, with a view to saving energy, without said granules having to be cooled beforehand. However, this means that, in the case of limited space conditions, sufficient space must be present for the subsequent swirling trough or swirling troughs, which is why a compact design which enables large throughputs is of great importance. 
     The vibrating trough  10  is excited by means of the vibration exciter  20 , which is, spatially, advantageously attached to the trough supports  31 , in such a way that the plastic granules are subjected to a helical or vortex-like movement in the vibrating trough  10 , so that good mixing of the granules results. This in turn results in the temperature profile for all granule particles remaining very uniform, i.e., all granule particles are treated as far as possible under the same conditions, so that a very homogeneous product quality is established. 
     The residence time of the plastic granules in the vibrating trough  10  under vibration excitation is usually 20 to 60 min when the vibrating trough is filled with approximately 50% of its cross-section or more. At the end of the residence time, the crystallization has progressed to such an extent that the granule particles are no longer sticky, such that they are either completely filled or can be crystallized in further devices to higher degrees of crystallization. 
     The invention has been explained in detail above with reference to one possible embodiment and further modifications. The embodiment and the modifications serve to prove the feasibility of the invention. Technical individual features which were explained above in the context of further individual features can also be implemented independently of said further individual features and in combination with other individual features, even if this is not expressly described, as long as this is technically possible. The invention is therefore expressly not limited to the embodiment specifically described, but includes all embodiments defined by the claims.