PATENT ABSTRACT
A lubrication fluid including cyclic hydrocarbons in combination with dimethylsilicone fluids and/or di-alkyl or di-cycloalkyl or alkyl-cycloalkyl, or mixtures thereof, and di-end-capped polypropylene oxides or highly branched esters to produce very high traction elastohydrodynamic (EHD) traction fluids and to modify the low temperature viscometric properties of the mixed fluids without adversely affecting the very high elastohydrodynamic shear strength or traction coefficients of the very high shear strength cyclic hydrocarbon fluid in the resulting mixed fluids with improved low temperature viscosity.

PATENT DESCRIPTION
FIELD OF THE INVENTION 
       [0001]    The present invention involves the use of dimethylsilicone fluids of moderate viscosity and/or di-alkyl or di-cycloalkyl or alkyl-cycloalkyl, or mixtures thereof, of di-end-capped polypropylene oxides or of ester compounds in combination with cyclic hydrocarbons to produce very high shear strength elastohydrodynamic (EHD) traction fluids and to modify the low temperature viscometric properties of the mixed fluids without adversely affecting the very high elastohydrodynamic shear strength or traction coefficients of the very high shear strength cyclic hydrocarbon fluid in the resulting mixed fluids with improved low temperature viscosity. 
       BACKGROUND OF THE INVENTION 
       [0002]    Elastohydrodynamic traction drives are power transmission devices that operate by transmitting torque through a thin elastohydrodynamic film of fluid between nominally-smooth, rolling-sliding, highly-loaded contacts. The efficient transfer of torque relies upon the high-stress shear strength of the fluid used to lubricate the surfaces in these high-stress elastically-deformed contacts. Fluids with very high elastohydrodynamic shear strength, or high traction coefficients, enable the most efficient transfer of torque through these contacts from one surface to the other. Thus, the shear strength properties of the fluid under the EHD contact operational conditions effectively dictate the sizing of the device for a given power or torque transfer requirement. Or, in any given size of an EHD traction transmission, determines the loading of the contact, the contact stress, required to produce a required torque through the device and thus has a large impact on the durability of the traction drive components. Prior art fluids are described in U.S. Pat. No. 7,645,395 and references therein. 
       SUMMARY OF THE INVENTION 
       [0003]    The present disclosure provides for, in one embodiment, a lubrication fluid including a dimethylsiloxane fluid having a viscosity of 20 cS at 77° F. or greater in combination with a polycyclic hydrocarbon fluid. The dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups so to modify the low temperature properties of polycyclic hydrocarbons fluids. In one embodiment, the dimethylsiloxane fluid has a viscosity of 20 cS but not greater than 50 cS at 77° F. 
         [0004]    The present disclosure provides for, in another embodiment, a lubrication fluid including dimethylsiloxane fluid having a viscosity of 20 cS at 77° F. or greater in combination with oil-soluble di-end-capped polypropyleneoxide compounds and a polycyclic hydrocarbon fluid. The dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups so to modify the low temperature properties of polycyclic hydrocarbons fluids. In one embodiment, the dimethylsiloxane fluid has a viscosity of 20 cS but not greater than 50 cS at 77° F. 
         [0005]    The present disclosure provides for, in yet another embodiment, the lubrication fluid including a dimethylsiloxane compound having a viscosity range of 20 cSt at 77° F. or greater in combination with a polycyclic hydrocarbon fluid and an ester compound independently selected from: a branched alkyl ester, a cycloester, a cycloalkyl ester and combinations thereof. The dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups. 
     
    
     DETAILED DESCRIPTION OF THE EMBODIMENTS 
       [0006]    The present invention provides for formulations for lubricants of high elastohydrodynamic shear strength or traction coefficients and good low temperature rheology. This combination of properties is generally known in the art to be very difficult to achieve. Historically, achieving fluid formulations with good low temperature rheological properties has always compromised elastohydrodynamic shear strength to some degree. The various formulation embodiments described herein eliminate these losses and in some cases the formulation scheme actually is found to improve elastohydrodynamic shear strength under certain operational conditions in elastohydrodynamic traction contacts while achieving good low temperature rheological properties suitable for all-weather operations. 
         [0007]    In one embodiment, the lubrication fluid comprises a dimethylsiloxane fluid having a viscosity of 20 cS at 77° F. or greater in combination with a polycyclic hydrocarbon fluid wherein the dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups so to modify the low temperature properties of polycyclic hydrocarbons fluids. In one embodiment, the dimethylsiloxane fluid has a viscosity of 20 cS but not greater than 50 cS at 77° F. 
         [0008]    In another embodiment, the lubrication fluid consists essentially of dimethylsiloxane fluid having a viscosity of 20 cS at 77° F. or greater in combination with a polycyclic hydrocarbon fluid, wherein the dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups so to modify the low temperature properties of polycyclic hydrocarbons fluids. In one embodiment, the dimethylsiloxane fluid has a viscosity of 20 cS but not greater than 50 cS at 77° F. 
         [0009]    In yet another embodiment, the lubrication fluid comprises dimethylsiloxane fluid having a viscosity of 20 cS at 77° F. or greater in combination with oil-soluble di-end-capped polypropyleneoxide compounds and a polycyclic hydrocarbon fluid, wherein the dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups so to modify the low temperature properties of polycyclic hydrocarbons fluids. In one embodiment, the dimethylsiloxane fluid has a viscosity of 20 cS but not greater than 50 cS at 77° F. 
         [0010]    In still yet another embodiment, the lubrication fluid consists essentially of dimethylsiloxane fluid having a viscosity of 20 cS at 77° F. or greater in combination in combination with oil-soluble di-end-capped polypropyleneoxide compounds and a polycyclic hydrocarbon fluid, wherein the dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups so to modify the low temperature properties of polycyclic hydrocarbons fluids. In one embodiment, the dimethylsiloxane fluid has a viscosity of 20 cS but not greater than 50 cS at 77° F. 
         [0011]    In yet another embodiment, the lubrication fluid comprises a dimethylsiloxane compound having a viscosity range of 20 cSt at 77° F. or greater in combination with a polycyclic hydrocarbon fluid and an ester compound independently selected from: a branched alkyl ester, a cycloester, a cycloalkyl ester and combinations thereof. The dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups. 
         [0012]    In still yet another embodiment, the lubrication fluid consists essentially of a dimethylsiloxane compound having a viscosity range of 20 cSt at 77° F. or greater in combination with a polycyclic hydrocarbon fluid and an ester compound independently selected from: a branched alkyl ester, a cycloester, a cycloalkyl ester and combinations thereof. The dimethylsiloxane fluid does not contain more than 10 wt. % of functional groups other than methyl functional groups. 
         [0013]    For the purposes of this disclosure, consists essentially of excludes the inclusion of any component that materially changes the low temperature properties of polycyclic hydrocarbons fluids. 
         [0014]    It was unexpectedly found that addition of dimethylsiloxane fluids to polycyclic hydrocarbons fluid with or without oil-soluble di-end-capped polypropylene oxide compounds results in a lubrication fluid having improved low temperature properties without degrading the desired elastohydrodynamic shear strength properties or traction coefficients of the binary or ternary lubrication fluid relative to the polycyclic hydrocarbons fluid alone. 
         [0015]    It was further was unexpectedly found that addition of dimethylsiloxane fluids to polycyclic hydrocarbons fluid with branched ester, cycloester or cycloalkyl ester compounds results in a lubrication fluid having improved low temperature properties without degrading the desired elastohydrodynamic shear strength properties or traction coefficients of the binary or ternary lubrication fluid relative to the polycyclic hydrocarbons fluid alone. 
         [0016]    Base Oils 
         [0017]    The present invention provides for a lubrication fluid based on a polycyclic hydrocarbon fluid which exhibits good shear strength but poor low temperature properties. In some embodiments, the polycyclic hydrocarbon fluid is a perhydro dimer of alpha-methylstyrene. In some another embodiments, the polycyclic hydrocarbon fluid is a perhydro linear dimer of alpha-methylstyrene. 
         [0018]    In one embodiment, the polycyclic hydrocarbon fluid may be combined with a dimethylsiloxane fluid having a viscosity of at least 20 cS at 77° F. or greater wherein the dimethylsiloxane fluid contains no more than 10 wt. % of functional groups other than methyl functional groups. The dimethylsiloxane fluid may be used at an amount ranging from 0.1 wt. to 25 wt. %. 
         [0019]    In another embodiment, the polycyclic hydrocarbon fluid may be combined with a dimethylsiloxane fluid having a viscosity of at least 20 cS at 77° F. or greater and oil-soluble di-end-capped polypropylene oxide compounds wherein the dimethylsiloxane fluid contains no more than 10 wt. % of functional groups other than methyl functional groups. The dimethylsiloxane fluid may be used at an amount ranging from 0.1 wt. to 25 wt. %. The oil-soluble di-end-capped polypropylene oxide compound may be used at an amount ranging from 0.1 wt. to 25 wt. %. In one such embodiment, the di-end-capped polypropylene oxide compounds may contain alkyl groups, cycloaliphatic rings, aromatic rings or combinations of these organic groups as the end-capping organic groups. In one embodiment, the end-capping organic groups have one to ten carbon atoms. 
         [0020]    In another embodiment, the polycyclic hydrocarbon fluid may be combined with a dimethylsiloxane fluid having a viscosity of at least 20 cS at 77° F. or greater and branched ester, cycloester or cycloalkyl ester compounds wherein the dimethylsiloxane fluid contains no more than 10 wt. % of functional groups other than methyl functional groups. The dimethylsiloxane fluid may be used at an amount ranging from 0.1 wt. to 25 wt. %. The branched ester, cycloester, cycloalkyl ester compounds and combinations thereof may be used at an amount ranging from 0.1 wt. to 25 wt. %. 
         [0021]    In one embodiment, the ester compound is a branched alkyl ester having 6 to 12 carbon atoms in the branched alkyl group and 3 to 4 ester groups. In one embodiment, the branched alkyl ester has at least two methyl groups distributed along the backbone of the branched alkyl ester. In another embodiment, the branched alkyl ester has at least one branching methyl or branching alkyl group per two carbon atoms located along the backbone of the branched alkyl ester. In one embodiment, the branched alkyl ester is trimethylhexane trimethoxypropane ester. In another embodiment, the branched alkyl ester is trimethylhexane pentaerithritol ester. 
         [0022]    In one embodiment, the ester compound is a cycloester or cycloalkyl ester compound selected from cyclohexyl group or alkyl cyclohexyl group having 6 to 10 carbon atoms and 3 to 4 ester groups. In one embodiment, the cycloester compound independently includes tri-(cyclohexyl)trimethoxypropane and tri-(cyclohexyl)pentaerithritol. In another embodiment, the cycloalkyl ester compound independently includes (alkyl branched-cyclohexyl)trimethoxypropane and tri-(alkyl branched-cyclohexyl)pentaerithritol. Examples include (methyl branched-cyclohexyl)trimethoxypropane and tri-(methylcyclohexyl)pentaerithritol. In some such embodiments, the number of methyl groups attached to the cyclohexyl group ranges from 1 to 3. 
         [0023]    In one embodiment, the dimethylsiloxane fluid may have other functional groups including, but are not limited to, higher alkyl groups, cycloaliphatic rings, aromatic rings or a combination of these non-methyl organic groups. In yet another embodiment, the dimethylsiloxane fluids may be produced as purely dimethyl-derivatives. 
         [0024]    The viscosity grades of such dimethylsiloxane fluids have the added advantage of being relatively non-volatile at typical lubricant or transmission operation temperatures in a EHD traction drive or traction drive transmission of at least 20 cS at 77° F. and higher. For example, typically 10 cSt (at 77° F.) dimethylsiloxane has a volatility of 50 wt % at 150° C. relative to 20 cSt dimethylsiloxane which typically has only a 5% volatility at 150° C. 
         [0025]    In one embodiment, the dimethylsiloxane fluid has a viscosity greater than 20 cSt at 77° F. but not greater than 50 cS at 77° F. and may be used at an amount ranging from 0.1 wt. to 25 wt. %. In one embodiment, the dimethylsiloxane fluid has a viscosity greater than 25 cSt at 77° F. but not greater than 50 cS at 77° F. and may be used at an amount ranging from 0.1 wt. to 25 wt. %. In one embodiment, the dimethylsiloxane fluid has a viscosity greater than 30 cSt at 77° F. but not greater than 50 cS at 77° F. and may be used at an amount ranging from 0.1 wt. to 25 wt. %. In yet another embodiment, the dimethylsiloxane fluid has a viscosity of greater than 40 cSt at 77° F. but not greater than 50 cS at 77° F. and may be used at an amount ranging from 0.1 wt. to 25 wt. %. The higher viscosity versions are contemplated to be appropriate when higher viscosity grade elastohydrodynamic traction fluid lubricants are desired whereby higher formulation concentrations are needed to significantly modify the low temperature rheology of the finished fluids which results in finished fluids with kinematic viscosities of about 4.0 cSt or above, measured at 100° C. 
         [0026]    The lubrication fluids described herein can serve as base fluids for the formulation of high elastohydrodynamic shear strength fluids for use in elastohydrodynamic continuously or infinitely variable transmission or in elastohydrodynamic traction drives in general. To these combination base fluids appropriate lubricant performance additives may be added to complete the formulation of the transmission or traction drive fluid. These additives may include antioxidants, antiwear agents, anti-corrosion agents, anti-foamants, anti-rust agents, detergents, dispersants, extreme-pressure agents, friction modifiers, seal swell agents and/or viscosity modifier additives. 
         [0027]    The various embodiments of the lubrication fluids described herein allow for production of useful fully-formulated EHD traction fluids having kinematic viscosities of from about 3.7 to 4.5 cS at 100° C. and low temperature dynamic viscosities ranging from 28,000 cP down to about 5,000 cP which do not compromise EHD shear strength properties to any appreciable degree. 
         [0028]    The following examples describe various embodiments of the invention. Other embodiments within the scope of the claims herein will be apparent to one skilled in the art from consideration of the specification or practice of the invention as disclosed herein. It is intended that the specification, together with the examples, be considered exemplary only, with the scope and spirit of the invention being indicated by the claims which follow the examples. In the examples, all percentages are given on a weight basis unless otherwise indicated. 
         [0029]    In the below examples, the following abbreviations are used: Sep=Separation; No Sep=Separation; SCL-Slightly Cloudy; and Cl-Cloudy 
       Comparative Example 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer 
       [0030]      
         [0000]    
       
         
               
               
               
             
           
               
                   
                   
               
             
             
               
                   
                 Component 
                 wt. % 
               
               
                   
                   
               
               
                   
                 Perhydro-alpha-Methylstyrene Dimer 
                 96.8 
               
               
                   
                 Poly-Propylene Oxide Fluid 
               
               
                   
                 Dimethylsiloxane, 20 cSt @ 77 F. 
               
               
                   
                 Dimethylsiloxane, 30 cSt @ 77 F. 
               
               
                   
                 Performance Additive Package 
                 3.0 
               
               
                   
                 Anti-Foamant Package 
                 0.2 
               
               
                   
                   
                 100.00 
               
               
                   
                   
               
               
                   
                 Test 
                 Units 
               
               
                   
                   
               
               
                   
                 CS 40 C., cS 
                 20.15 
               
               
                   
                 CS 100 C., cS 
                 3.66 
               
               
                   
                 VI 
                 31 
               
               
                   
                 Anton Paar SVM, −20 C., cP 
                 4813 
               
               
                   
                 Anton Paar SVM, −30 C., cP 
                 31182 
               
               
                   
                 Appearance (24 hrs @ temperature) 
               
               
                   
                 70 F. 
                 C 
               
               
                   
                 35 F. 
                 C 
               
               
                   
                  0 F. 
                 No Sep 
               
               
                   
                   
               
             
          
         
       
     
       Example 1 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer and Poly-Propylene Oxide 
       [0031]      
         [0000]    
       
         
               
               
               
               
             
               
               
               
               
             
               
               
             
               
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha-Methylstyrene Dimer 
                 91.80 
                 86.80 
                 81.80 
               
               
                 Poly-Propylene Oxide Fluid 
                 5.00 
                 10.00 
                 15.00 
               
               
                 Dimethylsiloxane, 20 cSt @ 77 F. 
               
               
                 Performance Additive Package 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
             
          
           
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 18.63 
                 20.09 
                 19.69 
               
               
                 CS 100 C., cS 
                 3.66 
                 3.89 
                 3.96 
               
               
                 VI 
                 63 
                 74 
                 92 
               
               
                 Anton Paar SVM, −20 C., cP 
                 4440 
                 3258 
                 3333 
               
               
                 Anton Paar SVM, −30 C., cP 
                 27609 
                 20094 
                 23088 
               
               
                 Brookfield, −30 C., cP 
               
             
          
           
               
                 Appearance, 24 hrs @ temp 
                   
               
             
          
           
               
                 70-75 F. 
                 C 
                 C 
                 C 
               
               
                 35-40 F. 
                 C 
                 C 
                 C 
               
               
                  0-5 F. 
                 No Sep 
                 No Sep 
                 No Sep 
               
               
                   
               
             
          
         
       
     
       Example 2 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer, Poly-Propylene Oxide and Dimethylsiloxane, 20 cSt @ 77° F. 
       [0032]      
         [0000]    
       
         
               
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha-Methylstyrene Dimer 
                 86.80 
                 81.80 
                 76.80 
                 71.80 
                 66.80 
                 81.80 
                 76.80 
               
               
                 Poly-Propylene Oxide Fluid 
                 5.00 
                 5.00 
                 5.00 
                 5.00 
                 5.00 
                 10.00 
                 10.00 
               
               
                 Dimethylsiloxane, 20 cSt @ 77 F. 
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
                 5.00 
                 10.00 
               
               
                 Performance Additive Package 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 18.80 
                 18.65 
                 17.32 
                 16.46 
                 14.69 
                 19.50 
                 18.55 
               
               
                 CS 100 C., cS 
                 3.77 
                 3.92 
                 4.04 
                 4.10 
                 3.98 
                 4.05 
                 4.08 
               
               
                 VI 
                 79 
                 103 
                 136 
                 150 
                 183 
                 105 
                 121 
               
               
                 Anton Paar SVM, −20 C., cP 
                 2547 
                 1672 
                 1166 
                 774 
                 641 
                 2149 
                 1541 
               
               
                 Anton Paar SVM, −30 C., cP 
                 13818 
                 8689 
                 6026 
                 3759 
                 3153 
                 11471 
                 7886 
               
               
                 Brookfield, −30 C., cP 
                   
                 9118 
                   
                   
                   
                   
                 7728 
               
               
                 Appearance, 24 hrs @ temp 
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 35-40 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 0-5 F. 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
               
               
                   
               
             
          
           
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha-Methylstyrene Dimer 
                 71.80 
                 66.80 
                 61.80 
                 76.80 
                 71.80 
                 66.80 
                 61.80 
                 56.80 
               
               
                 Poly-Propylene Oxide Fluid 
                 10.00 
                 10.00 
                 10.00 
                 15.00 
                 15.00 
                 15.00 
                 15.00 
                 15.00 
               
               
                 Dimethylsiloxane, 20 cSt @ 77 F. 
                 15.00 
                 20.00 
                 25.00 
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
               
               
                 Performance Additive Package 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 17.59 
                 16.48 
                 14.92 
                 18.47 
                 17.22 
                 17.20 
                 17.14 
                 16.77 
               
               
                 CS 100 C., cS 
                 4.15 
                 4.15 
                 4.13 
                 4.00 
                 4.03 
                 4.22 
                 4.37 
                 4.49 
               
               
                 VI 
                 143 
                 163 
                 197 
                 114 
                 137 
                 158 
                 177 
                 198 
               
               
                 Anton Paar SVM, −20 C., cP 
                 914 
                 706 
                 624 
                 2165 
                 1398 
                 953 
                 811 
                 689 
               
               
                 Anton Paar SVM, −30 C., cP 
                 4384 
                 3272 
                 2859 
                 12378 
                 7440 
                 4667 
                 3646 
                 2804 
               
               
                 Brookfield, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance, 24 hrs @ temp 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 35-40 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 0-5 F. 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
               
               
                   
               
             
          
         
       
     
       Example 3 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer, Poly-Propylene Oxide and Dimethylsiloxane, 30 cSt @ 77° F. 
       [0033]      
         [0000]    
       
         
               
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 86.80 
                 81.80 
                 76.80 
                 71.80 
                 66.80 
                 81.80 
                 76.80 
               
               
                 Methylstyrene Dimer 
                   
                   
                   
                   
                   
                   
                   
               
               
                 Poly-Propylene Oxide Fluid 
                 5.00 
                 5.00 
                 5.00 
                 5.00 
                 5.00 
                 10.00 
                 10.00 
               
               
                 Shin Etsu DC200, 30 cSt 
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
                 5.00 
                 10.00 
               
               
                 Performance Additive 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 19.42 
                 18.36 
                 18.05 
                 17.26 
                 17.35 
                 18.94 
                 19.56 
               
               
                 CS 100 C., cS 
                 3.81 
                 4.03 
                 4.20 
                 4.32 
                 4.54 
                 4.00 
                 4.32 
               
               
                 VI 
                 73 
                 118 
                 141 
                 168 
                 192 
                 107 
                 131 
               
               
                 Anton Paar SVM, −20 C., cP 
                 3225 
                 2078 
                 1778 
                   
                   
                 2270 
                 1818 
               
               
                 Anton Paar SVM, −30 C., cP 
                 19186 
                 11296 
                 9398 
                   
                   
                 12944 
                 9756 
               
               
                 Appearance, 24 hrs @ temp 
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 35-40 F. 
                 C 
                 SCL 
                 SCL 
                 Sep 
                 Sep 
                 C 
                 SCL 
               
               
                 0-5 F. 
                 No Sep 
                 No Sep 
                 No Sep 
                   
                   
                 No Sep 
                 No Sep 
               
               
                   
               
             
          
           
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 71.80 
                 66.80 
                 61.80 
                 76.80 
                 71.80 
                 66.80 
                 61.80 
                 56.80 
               
               
                 Methylstyrene Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Poly-Propylene Oxide Fluid 
                 10.00 
                 10.00 
                 10.00 
                 15.00 
                 15.00 
                 15.00 
                 15.00 
                 15.00 
               
               
                 Shin Etsu DC200, 30 cSt 
                 15.00 
                 20.00 
                 25.00 
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
               
               
                 Performance Additive 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 19.22 
                   
                   
                 20.44 
                 20.16 
                 19.74 
                 19.57 
                 19.03 
               
               
                 CS 100 C., cS 
                 4.50 
                   
                   
                 4.38 
                 4.52 
                 4.67 
                 4.82 
                 5.00 
               
               
                 VI 
                 155 
                   
                   
                 126 
                 143 
                 163 
                 181 
                 209 
               
               
                 Anton Paar SVM, −20 C., cP 
                   
                   
                   
                 2338 
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −30 C., cP 
                   
                   
                   
                 14450 
                   
                   
                   
                   
               
               
                 Appearance, 24 hrs @ temp 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 35-40 F. 
                 Sep 
                 Sep 
                 Sep 
                 C 
                 CL 
                 CL 
                 CL 
                 Sep 
               
               
                 0-5 F. 
                   
                   
                   
                 No Sep 
               
               
                   
               
             
          
         
       
     
       Example 4 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer, Poly-Propylene Oxide and Dimethylsiloxane, 50 cSt @ 77° F. 
       [0034]      
         [0000]    
       
         
               
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
             
               
               
             
               
               
               
               
               
               
               
               
               
             
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha-Methylstyrene Dimer 
                 86.80 
                 81.80 
                 76.80 
                 71.80 
                 66.80 
                 81.80 
                 76.80 
               
               
                 Poly-Propylene Oxide Fluid 
                 5.00 
                 5.00 
                 5.00 
                 5.00 
                 5.00 
                 10.00 
                 10.00 
               
               
                 Dimethylsiloxane, 50 cSt @ 77 F. 
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
                 5.00 
                 10.00 
               
               
                 Performance Additive Package 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
               
               
                   
               
               
                 CS 40 C., cS 
                   
                   
                   
                   
                   
                   
                   
               
               
                 CS 100 C., cS 
                   
                   
                   
                   
                   
                   
                   
               
               
                 VI 
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance, 24 hrs @ temp 
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 SCl 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
                 SCl 
                 Sep 
               
               
                 35-40 F. 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
               
               
                 0-5 F. 
               
               
                   
               
             
          
           
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha-Methylstyrene Dimer 
                 71.80 
                 66.80 
                 61.80 
                 76.80 
                 71.80 
                 66.80 
                 61.80 
                 56.80 
               
               
                 Poly-Propylene Oxide Fluid 
                 10.00 
                 10.00 
                 10.00 
                 15.00 
                 15.00 
                 15.00 
                 15.00 
                 15.00 
               
               
                 Dimethylsiloxane, 50 cSt @ 77 F. 
                 15.00 
                 20.00 
                 25.00 
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
               
               
                 Performance Additive Package 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
             
          
           
               
                 Test 
                 Unit 
               
               
                   
               
             
          
           
               
                 CS 40 C., cS 
                   
                   
                   
                 21.000 
                   
                   
                   
                   
               
               
                 CS 100 C., cS 
                   
                   
                   
                 4.42 
                   
                   
                   
                   
               
               
                 VI 
                   
                   
                   
                 122 
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −20 C., cP 
                   
                   
                   
                 2713 
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −30 C., cP 
                   
                   
                   
                 17492 
                   
                   
                   
                   
               
               
                 Appearance, 24 hrs @ temp 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 Sep 
                 Sep 
                 Sep 
                 C 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
               
               
                 35-40 F. 
                 Sep 
                 Sep 
                 Sep 
                 C 
                 Sep 
                 Sep 
                 Sep 
                 Sep 
               
             
          
           
               
                 0-5 F. 
                 No Sep 
                   
               
               
                   
               
             
          
         
       
     
       Example 5 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer with or without Poly-Propylene Oxide and with or without Dimethylsiloxane, 20 cSt @ 77° F. or 30 cSt @ 77° F. 
       [0035]      
         [0000]    
       
         
               
               
               
               
               
               
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 71.8 
                 91.8 
                 86.8 
                 81.8 
               
               
                 Methylstyrene Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Poly-Propylene Oxide Fluid 
                 5.0 
                 10.0 
                 15.0 
                 20.0 
                 25.0 
                   
                   
                   
               
               
                 Dimethylsiloxane, 20 cSt 
                   
                   
                   
                   
                   
                 5.0 
                 10.0 
                 15.0 
               
               
                 @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethylsiloxane, 30 cSt 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
               
               
                 Additive Package 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant Package 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 20.36 
                 20.78 
                 21.12 
                 21.43 
                 21.96 
                 18.92 
                 17.67 
                 16.94 
               
               
                 CS 100 C., cS 
                 3.76 
                 3.92 
                 4.00 
                 4.15 
                 4.41 
                 3.72 
                 3.76 
                 3.88 
               
               
                 VI 
                 46 
                 66 
                 73 
                 90 
                 110 
                 68 
                 100 
                 124 
               
               
                 Anton Paar SVM, −20 C., cP 
                 4248 
                 3798 
                 3788 
                 3857 
                 3916 
                 2907 
                 1967 
                 1447 
               
               
                 Anton Paar SVM, −30 C., cP 
                 26364 
                 25216 
                 25883 
                 26634 
                 27137 
                 16999 
                 11244 
                 8057 
               
               
                 Appearance (24 hrs 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 @ temperature) 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 35 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 0 F. 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 76.8 
                 71.8 
                 96.8 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 71.8 
               
               
                 Methylstyrene Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Poly-Propylene Oxide Fluid 
                 20.0 
                 25.0 
                   
                   
                   
                   
                   
                   
               
               
                 Dimethylsiloxane, 20 cSt 
                   
                   
                   
                 5.0 
                 10.0 
                 15.0 
                 20.0 
                 25.0 
               
               
                 @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethylsiloxane, 30 cSt 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
                 3.0 
               
               
                 Additive Package 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant Package 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 16.08 
                 15.58 
                 20.32 
                 19.31 
                 18.59 
                 17.93 
                 17.48 
                 15.72 
               
               
                 CS 100 C., cS 
                 3.90 
                 4.03 
                 3.67 
                 3.80 
                 3.94 
                 4.07 
                 4.22 
                 4.08 
               
               
                 VI 
                 141 
                 167 
                 31 
                 74 
                 106 
                 129 
                 153 
                 171 
               
               
                 Anton Paar SVM, −20 C., cP 
                 1186 
                 938 
                 5161 
                 3149 
                 2388 
                 1985 
                 1534 
                 956 
               
               
                 Anton Paar SVM, −30 C., cP 
                 6473 
                 5207 
                 33580 
                 19169 
                 13640 
                 11172 
                 7600 
                 5352 
               
               
                 Appearance (24 hrs 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 @ temperature) 
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 35 F. 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
                 C 
               
               
                 0 F. 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 No Sep 
                 Sep 
                 Sep 
               
               
                   
               
             
          
         
       
     
       Example 6 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer and Dimethylsiloxane, 50 cSt @ 77° F. 
       [0036]      
         [0000]    
       
         
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
             
           
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                 Perhydro-alpha-Methylstyrene Dimer 
                 96.8 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 71.8 
               
               
                 Poly-Propylene Oxide Fluid 
                   
                   
                   
                   
                   
                   
               
               
                 Dimethylsiloxane, 50 cSt @ 77 F. 
                   
                 5.00 
                 10.00 
                 15.00 
                 20.00 
                 25.00 
               
               
                 Performance Additive Package 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
                 3.00 
               
               
                 Anti-Foamant Package 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
                 0.20 
               
               
                   
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
                 100.00 
               
               
                   
               
               
                 Test 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
                 Unit 
               
               
                   
               
               
                 CS 40 C., cS 
                 20.32 
                 19.80 
                 20.20 
                 19.80 
                 19.50 
                   
               
               
                 CS 100 C., cS 
                 3.67 
                 3.87 
                 4.23 
                 4.08 
                 4.34 
                   
               
               
                 VI 
                 31 
                 76 
                 114 
                 105 
                 134 
                   
               
               
                 Anton Paar SVM, −20 C., cP 
                 5161 
                 3370 
                 2785 
                   
                   
                   
               
               
                 Anton Paar SVM, −30 C., cP 
                 33580 
                 22050 
                 16010 
                   
                   
                   
               
               
                 Appearance (24 hrs @ temperature) 
                   
                   
                   
                   
                   
                   
               
               
                 70 F. 
                 C 
                 C 
                 C 
                   
                   
                 Sep 
               
               
                 35 F. 
                 C 
                 CL 
                 CL 
                   
                   
                   
               
               
                 0 F. 
                 No Sep 
                 No Sep 
                 No Sep 
                 Sep 
                 Sep 
                 Sep 
               
               
                   
               
             
          
         
       
     
       Example 7 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer, Tri-Iso-C 9  Trimethoxylpropane Ester with or without Dimethylsiloxane, 20 cSt @ 77° F. 
       [0037]      
         [0000]    
       
         
               
               
               
               
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro- 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 86.8 
                 81.8 
               
               
                 alpha- 
                   
                   
                   
                   
                   
                   
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
               
               
                 Tri-i-C9 TMP 
                 5 
                 5 
                 5 
                 5 
                 10 
                 10 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                   
                 5 
                 10 
                 15 
                   
                 5 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 20.27 
                 19.22 
                 18.16 
                 17.29 
                 20.96 
                 19.50 
               
               
                 CS 100 C., cS 
                 3.680 
                 3.788 
                 3.857 
                 3.940 
                 3.800 
                 3.856 
               
               
                 VI 
                 33.2 
                 73.9 
                 103.5 
                 125.2 
                 42.2 
                 79.5 
               
               
                 Anton Paar 
                 3696.2 
                 2678.3 
                 1711.6 
                 1209.4 
                 4352.4 
                 2540.1 
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                 22538 
                 14748 
                 8956 
                 6366 
                 26690 
                 13574 
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 35-40 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 0-5 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro- 
                 76.8 
                 71.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
               
               
                 alpha- 
                   
                   
                   
                   
                   
                   
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
               
               
                 Tri-i-C9 TMP 
                 10 
                 10 
                 15 
                 15 
                 15 
                 15 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                 10 
                 15 
                   
                 5 
                 10 
                 15 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 18.62 
                 17.73 
                 21.49 
                 20.17 
                 19.06 
                 18.26 
               
               
                 CS 100 C., cS 
                 3.934 
                 4.023 
                 3.886 
                 3.956 
                 4.017 
                 4.123 
               
               
                 VI 
                 105.4 
                 127.2 
                 47.5 
                 82.8 
                 107.9 
                 129.8 
               
               
                 Anton Paar 
                 1701.7 
                 1115.8 
                 4223 
                 2578.3 
                 1652.2 
                 1094.1 
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                 8369 
                 5487 
                 25637 
                 13683 
                 7833 
                 4770 
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 35-40 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 0-5 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 86.8 
                 81.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
               
               
                 Tri-i-C9 TMP ester 
                 5 
                 5 
                 5 
                 5 
                 10 
                 10 
               
               
                 Dimethacone, 30 cSt 
                   
                 5 
                 10 
                 15 
                   
                 5 
               
               
                 @ 77 F. 
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive Package 
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 20.27 
                 19.74 
                 19.14 
                 18.72 
                 20.96 
                 20.16 
               
               
                 CS 100 C., cS 
                 3.680 
                 3.875 
                 4.029 
                 4.171 
                 3.800 
                 3.956 
               
               
                 VI 
                 33.2 
                 78.1 
                 108.0 
                 128.1 
                 42.2 
                 83.2 
               
               
                 Anton Paar SVM, −20 C., 
                 3696.2 
                 — 
                 — 
                 — 
                 4352.4 
                 — 
               
               
                 cP 
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −30 C., 
                 22538 
                 — 
                 — 
                 — 
                 26690 
                 — 
               
               
                 cP 
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 35-40 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 0-5 F. 
                 Clear, NS 
                 Cldy, NS 
                 Cldy, NS 
                 Cldy, NS 
                 Clear, NS 
                 Cldy, NS 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 76.8 
                 71.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
               
               
                 Tri-i-C9 TMP ester 
                 10 
                 10 
                 15 
                 15 
                 15 
                 15 
               
               
                 Dimethacone, 30 cSt 
                 10 
                 15 
                   
                 5 
                 10 
                 15 
               
               
                 @ 77 F. 
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive Package 
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 19.6 
                 19.19 
                 21.49 
                 20.66 
                 20.21 
                 19.81 
               
               
                 CS 100 C., cS 
                 4.123 
                 4.311 
                 3.886 
                 4.069 
                 4.238 
                 4.454 
               
               
                 VI 
                 11.3 
                 135.4 
                 47.5 
                 91.1 
                 114.9 
                 140.9 
               
               
                 Anton Paar SVM, −20 C., 
                 — 
                 — 
                 4223 
                 2656 
                 — 
                 — 
               
               
                 cP 
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar SVM, −30 C., 
                 — 
                 — 
                 25637 
                 14165 
                 — 
                 — 
               
               
                 cP 
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 35-40 F. 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
                 Clear, NS 
               
               
                 0-5 F. 
                 Cldy, NS 
                 Cldy, NS 
                 Clear, NS 
                 Clear, NS 
                 Cldy, NS 
                 Cldy, NS 
               
               
                   
               
             
          
         
       
     
       Example 8 
     Lubrication Fluid Containing Perhydro-Alpha-Methylstyrene Dimer, Tri-Iso-C 9  Tpentaerithritol Ester with or without Dimethylsiloxane, 20 cSt @ 77° F. 
       [0038]      
         [0000]    
       
         
               
               
               
               
               
               
               
               
               
               
             
           
               
                   
               
             
             
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
                 86.8 
                 81.8 
                 76.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Tetra-i-C9 PE 
                 5 
                 5 
                 5 
                 5 
                 5 
                 5 
                 10 
                 10 
                 10 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                   
                 5 
                 10 
                 15 
                 20 
                 25 
                   
                 5 
                 10 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 12.65 
                 19.31 
                   
                   
                   
                   
                 21.53 
                 20.15 
                   
               
               
                 CS 100 C., cS 
                 3.95 
                 3.85 
                   
                   
                   
                   
                 3.92 
                 3.98 
                   
               
               
                 VI 
                 56 
                 81.7 
                   
                   
                   
                   
                 51.7 
                 86.6 
                   
               
               
                 Anton Paar 
                 4601 
                 2702.8 
                   
                   
                   
                   
                 3734.9 
                 2280.1 
                   
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                 27745 
                 14793 
                   
                   
                   
                   
                 21392 
                 11614 
                   
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
               
               
                 35-40 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
               
               
                 0-5 F. 
                 clear NS 
                 clear NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 clear NS 
                 cldy NS 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 71.8 
                 66.8 
                 61.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
                 61.8 
                 56.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Tetra-i-C9 PE 
                 10 
                 10 
                 10 
                 15 
                 15 
                 15 
                 15 
                 15 
                 15 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                 15 
                 20 
                 25 
                   
                 5 
                 10 
                 15 
                 20 
                 25 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                   
                   
                   
                 22.07 
                 20.68 
                   
                   
                   
                   
               
               
                 CS 100 C., cS 
                   
                   
                   
                 4.04 
                 4.1 
                   
                   
                   
                   
               
               
                 VI 
                   
                   
                   
                 62.3 
                 95.2 
                   
                   
                   
                   
               
               
                 Anton Paar 
                   
                   
                   
                 3191.2 
                 2048 
                   
                   
                   
                   
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                   
                   
                   
                 17219 
                 9830 
                   
                   
                   
                   
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
               
               
                 35-40 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
               
               
                 0-5 F. 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 clear NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
                 86.8 
                 81.8 
                 76.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Tetra-i-C9 PE 
                 5 
                 5 
                 5 
                 5 
                 5 
                 5 
                 10 
                 10 
                 10 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                   
                 5 
                 10 
                 15 
                 20 
                 25 
                   
                 5 
                 10 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 20.63 
                   
                   
                   
                   
                   
                 21.57 
                   
                   
               
               
                 CS 100 C., cS 
                 3.78 
                   
                   
                   
                   
                   
                 3.92 
                   
                   
               
               
                 VI 
                 44.1 
                   
                   
                   
                   
                   
                 51.7 
                   
                   
               
               
                 Anton Paar 
                 4324 
                   
                   
                   
                   
                   
                 2902 
                   
                   
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                 25671 
                   
                   
                   
                   
                   
                 16225 
                   
                   
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
               
               
                 35-40 F. 
                 clear NS 
                 cldy NS 
                 cldy NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 clear NS 
                 cldy NS 
               
               
                 0-5 F. 
                 clear NS 
                 cldy NS 
                 cldy NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 cldy NS 
                 cldy NS 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 71.8 
                 66.8 
                 61.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
                 61.8 
                 56.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Tetra-i-C9 PE 
                 10 
                 10 
                 10 
                 15 
                 15 
                 15 
                 15 
                 15 
                 15 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                 15 
                 20 
                 25 
                   
                 5 
                 10 
                 15 
                 20 
                 25 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                   
                   
                   
                 21.48 
                   
                   
                   
                   
                   
               
               
                 CS 100 C., cS 
                   
                   
                   
                 3.98 
                   
                   
                   
                   
                   
               
               
                 VI 
                   
                   
                   
                 63.1 
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                   
                   
                   
                 3122 
                   
                   
                   
                   
                   
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                   
                   
                   
                 16896 
                   
                   
                   
                   
                   
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
               
               
                 35-40 F. 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 cldy NS 
                 cldy NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
               
               
                 0-5 F. 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 91.8 
                 86.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
                 86.8 
                 81.8 
                 76.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Tetra-i-C9 PE 
                 5 
                 5 
                 5 
                 5 
                 5 
                 5 
                 10 
                 10 
                 10 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                   
                 5 
                 10 
                 15 
                 20 
                 25 
                   
                 5 
                 10 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                 20.5 
                   
                   
                   
                   
                   
                 20.93 
                   
                   
               
               
                 CS 100 C., cS 
                 3.74 
                   
                   
                   
                   
                   
                 3.85 
                   
                   
               
               
                 VI 
                 40.8 
                   
                   
                   
                   
                   
                 52.2 
                   
                   
               
               
                 Anton Paar 
                 4027 
                   
                   
                   
                   
                   
                 3540 
                   
                   
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                 24316 
                   
                   
                   
                   
                   
                 20279 
                   
                   
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 clear NS 
                 cldy NS 
                 clear NS 
                 cldy NS 
                 cldy SEP 
               
               
                 35-40 F. 
                 clear NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 cldy NS 
                 cldy SEP 
               
               
                 0-5 F. 
                 clear NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 cldy SEP 
                 cldy SEP 
               
               
                   
               
               
                 Component 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
                 Wt. % 
               
               
                   
               
               
                 Perhydro-alpha- 
                 71.8 
                 66.8 
                 61.8 
                 81.8 
                 76.8 
                 71.8 
                 66.8 
                 61.8 
                 56.8 
               
               
                 Methylstyrene 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimer 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Tetra-i-C9 PE 
                 10 
                 10 
                 10 
                 15 
                 15 
                 15 
                 15 
                 15 
                 15 
               
               
                 ester 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Dimethacone, 
                 15 
                 20 
                 25 
                   
                 5 
                 10 
                 15 
                 20 
                 25 
               
               
                 20 cSt @ 77 F. 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Performance 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
                 3 
               
               
                 Additive 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anti-Foamant 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
                 0.2 
               
               
                 Package 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                   
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
                 100 
               
               
                 CS 40 C., cS 
                   
                   
                   
                 21.46 
                   
                   
                   
                   
                   
               
               
                 CS 100 C., cS 
                   
                   
                   
                 3.98 
                   
                   
                   
                   
                   
               
               
                 VI 
                   
                   
                   
                 63.1 
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                   
                   
                   
                 3150 
                   
                   
                   
                   
                   
               
               
                 SVM, −20 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Anton Paar 
                   
                   
                   
                 17197 
                   
                   
                   
                   
                   
               
               
                 SVM, −30 C., cP 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 Appearance 
                   
                   
                   
                   
                   
                   
                   
                   
                   
               
               
                 70-75 F. 
                 cldy SEP 
                 cldy SEP 
                 cldy NS 
                 clear NS 
                 cldy NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy NS 
               
               
                 35-40 F. 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
               
               
                 0-5 F. 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 clear NS 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
                 cldy SEP 
               
               
                   
               
             
          
         
       
     
         [0039]    It will be appreciated by those skilled in the art that changes could be made to the exemplary embodiments shown and described above without departing from the broad inventive concept thereof. It is understood, therefore, that this invention is not limited to the exemplary embodiments shown and described, but it is intended to cover modifications within the spirit and scope of the present invention as defined by the claims. For example, specific features of the exemplary embodiments may or may not be part of the claimed invention and features of the disclosed embodiments may be combined. Accordingly, reference should be made to the appended claims, rather than the foregoing specification, as indicating the scope of the disclosure. Unless specifically set forth herein, the terms “a”, “an” and “the” are not limited to one element but instead should be read as meaning “at least one”.