PATENT ABSTRACT
The present invention provides a phthalic acid diamide derivative represented by the general formula (I)  
                         
 
     (wherein R 1 , R 2  and R 3  are each H, C 3 -C 6  cycloalkyl group, group of the formula —A 1 —Q l  or the like; X may be the same or different and are each halogen atom, nitro group, phenyl group, group of the formula —A 2 —R 7  or the like; n is 1 to 4; Y may be same or different and are each halogen atom, cyano group, phenyl group, group of the formula —A 2 —R 7  or the like; m is 1 to 5; Z 1  and Z 2  are each O or S), fluorine-containing aniline compound represented by the general formula (ST-I) as starting material for said phthalic acid diamide derivative  
                         
 
     (wherein R a  is halogen atom, C 1 -C 6  alkyl group or the like and R b , R c  and R d  is H or C 2 -C 6  perfluoroalkyl group), and an agricultural and horticultural insecticide containing said phthaldiamide derivative, as well as to provide a method for use of said insecticide. The agricultural and horticultural insecticides of the present invention show excellent activities for controlling injurious insects.

PATENT DESCRIPTION
CROSS-REFERENCE TO RELATED APPLICATION  
       [0001]    This application is a continuation-in-part application of earlier U.S. application Ser. No. 09/198,391 filed Nov. 24, 1998 of which contents are all incorporated herein by reference. 
     
    
     
       BACKGROUND OF THE INVENTION  
         [0002]    1. Field of the Invention  
           [0003]    The present invention relates to phthalic acid diamide derivatives, fluorine-containing aniline compounds as starting material for said derivative, agricultural and horticultural insecticides containing said derivative as an active ingredient, and a method for application of the insecticides.  
           [0004]    2. Related Art  
           [0005]    Japanese Patent Application Nos. 59-163353 and 61-180753 and J. C. S. Perkin I, 1338-1350, (1978), etc. disclose some of the phthalic acid diamide derivatives of the present invention but neither describe nor suggest their usefulness as agricultural and horticultural insecticides. JP-A-63-99046 and JP-A-6-184065 describe the fact that anilines similar to the fluorine-containing aniline compound of the present invention are useful as intermediates of benzoylurea type insecticides.  
         SUMMARY OF THE INVENTION  
         [0006]    The present inventors earnestly studied in order to develop a novel agricultural and horticultural insecticide, and consequently found that the phthalic acid diamide derivatives represented by the general formula (I) of the present invention are novel compounds not known as agricultural and horticultural insecticides in any literature and that said derivatives including the compounds disclosed in the above references can be used for a new purpose as agricultural and horticultural insecticides. Further, the present inventors found that the fluorine-containing aniline compounds represented by the general formula (ST-I) of the present invention are novel compounds which have not been known in any literature and is useful as an intermediate of a medicine, agrochemical, chemical product etc. In particular, they found that the fluorine-containing aniline compound of the general formula (ST-I) is useful as a starting material for the agricultural and horticultural insecticide containing the phthalic acid diamide derivative of the general formula (I) as an active ingredient. Thus, the present invention has been accomplished.  
         DETAILED DESCRIPTION OF THE INVENTION  
         [0007]    The present invention relates to phthalic acid diamide derivatives of the general formula (I),  
                         
 
           [0008]    wherein R 1 , R 2  and R 3  may be the same or different, and are each a hydrogen atom, a cyano group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 3 -C 6  cycloalkenyl group, a halo-C 3 -C 6  cycloalkenyl group or a group of the formula —A 1 —Q l  (wherein A 1  is —O—, —S—, —SO 2 —, —C(═O)—, a group of the formula —N(R 4 )— (wherein R 4  is a C 1 -C 6  alkylcarbonyl group, a halo-C 1 -C 6  alkylcarbonyl group, a C 1 -C 6  alkoxycarbonyl group, a phenylcarbonyl group, or a substituted phenylcarbonyl group having at least one substituent which may be the same or different, and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different), a C 1 -C 8  alkylene group, a C 3 -C 6  alkenylene group or a C 3 -C 6  alkynylene group;  
           [0009]    (1) when A 1  is —O— or a group of the formula —N(R 4 )— (wherein R 4  is the same as defined above), then Q is a hydrogen atom, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a halo-C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkyl sulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl-C 1 -C 4  alkyl group or a substituted phenyl-C 1 -C 4  alkyl group having at least one substituent, in the phenyl ring, which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different;  
           [0010]    (2) when A 1  is —S—, —SO 2 — or —C(═O)—, then Q is a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a halo-C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a mono-C 1 -C 6  alkylamino group, a di-C 1 -C 6  alkylamino group which may be the same or different, a C 1 -C 6  alkoxycarbonylamino group, a C 1 -C 6  alkoxycarbonyl-C 1 -C 6  alkylamino group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a phenylamino group, a substituted phenylamino group having at least one substituent, in the phenyl ring, which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which means pyridyl group, pyridine-N-oxide group, pyrimidinyl group, furyl group, tetrahydrofuryl group, thienyl group, tetrahydrothienyl group, tetrahydropyranyl group, tetrahydrothiopyranyl group, oxazolyl group, isoxazolyl group, oxadiazolyl group, thiazolyl group, isothiazolyl group, thiadiazolyl group, imidazolyl group, triazolyl group or a pyrazolyl group), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different,  
           [0011]    (3) when A 1  is a C 1 -C 8  alkylene group, a C 3 -C 6  alkenylene group or a C 3 -C 6  alkynylene group, then Q is a hydrogen atom, a halogen atom, a cyano group, a nitro group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 1 -C 6  alkoxycarbonyl group, a di-C 1 -C 6  alkoxyphosphoryl group which may be the same or different, a di-C 1 -C 6  alkoxythiophosphoryl group which may be the same or different, a diphenylphosphino group, a diphenylphosphono group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —Z 3 —R 5  (wherein Z 3  is —O—, —S—, —SO—, —SO 2 — or a group of the formula —N(R 6 )— (wherein R 6  is a hydrogen atom, a C 1 -C 6  alkylcarbonyl group, a halo-C 1 -C 6  alkylcarbonyl group, a C 1 -C 6  alkoxycarbonyl group, a phenylcarbonyl group, a substituted phenylcarbonyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl C 1 -C 4  alkoxycarbonyl group, or a substituted phenyl C 1 -C 4  alkoxycarbonyl group having at least one substituent, in the phenyl ring, which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different); and  
           [0012]    R 5  is a hydrogen atom, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a halo-C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a halo-C 3 -C 6  alkynyl group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 1 -C 6  alkylcarbonyl group, a halo C 1 -C 6  alkylcarbonyl group, a C 1 -C 6  alkoxycarbonyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl C 1 -C 4  alkyl group, a substituted phenyl C 1 -C 4  alkyl group having at least one substituent, in the phenyl ring, which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different);  
           [0013]    l is an integer of 1 to 4); further,  
           [0014]    R 1  and R 2  may form a 4 to 7 membered ring by combining to each other, in which the ring may contain the same or different 1 to 3 hetero atoms selected from the group consisting of oxygen atom, sulfur atom and nitrogen atom;  
           [0015]    X may be the same or different, and is a hydrogen atom, a halogen atom, a cyano group, a nitro group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a phenyl group, a substituted phenyl group having at least one substituents which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined the above), a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —A 2 —R 7  (wherein A 2  is —O—, —S—, —SO—, —SO 2 —, —C(═O)—, —C(═NOR 8 )— (wherein R 8  is a hydrogen atom, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a halo-C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a C 3 -C 6  cycloalkyl group, a phenyl-C 1 -C 4  alkyl group, or a substituted phenyl-C 1 -C 4  alkyl group having at least one substituent, in the phenyl ring, which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different), a C 1 -C 6  alkylene group, a halo-C 1 -C 6  alkylene group, a C 2 -C 6  alkenylene group, a halo-C 2 -C 6  alkenylene group, a C 2 -C 6  alkynylene group or a halo-C 3 -C 6  alkynylene group; (1) when A 2  is —O—, —S—, —SO— or —SO 2 —, then R 7  is a hydrogen atom, a C 1 -C 6  alkyl group, a halo C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a halo-C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a halo-C 3 -C 6  alkynyl group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 3 -C 6  cycloalkenyl group, a halo-C 3 -C 6  cycloalkenyl group, a di-C 1 -C 6  alkoxyphosphoryl group which may be the same or different, a di-C 1 -C 6  alkoxythiophosphoryl group which may be the same or different, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituents which may be the same or different and are selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —A 3 —R 9  (wherein A 3  is —C(═O)—, —SO 2 —, a C 1 -C 6  alkylene group, a halo-C 1 -C 6  alkylene group, a C 2 -C 6  alkenylene group, a halo-C 2 -C 6  alkenylene group, a C 3 -C 6  alkynylene group or a halo-C 3 -C 6  alkynylene group,  
           [0016]    (i) when A 3  is —C(═O)— or —SO 2 —, then R 9  is a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 1 -C 6  alkoxy group, a mono-C 1 -C 6  alkylamino group, a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined the above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  . alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, (ii) when A 3  is a C 1 -C 6  alkylene group, a halo-C 1 -C 6  alkylene group, a C 2 -C 6  alkenylene group, a halo-C 2 -C 6  alkenylene group, a C 3 -C 6  alkynylene group or a halo-C 3 -C 6  alkynylene group, then R 9  is a hydrogen atom, a halogen atom, a cyano group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 1 -C 6  alkoxycarbonyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —A 4 —R 10  (wherein A 4  is —O—, —S—, —SO—, —SO 2 —, —C(═O)—, or a group of the formula —N(R 11 )— (wherein R 11  is a hydrogen atom, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a C 3 -C 6  cycloalkyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a -halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different); and  
           [0017]    R 10  is a hydrogen atom, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 3 -C 6  alkenyl group, a halo-C 3 -C 6  alkenyl group, a C 3 -C 6  alkynyl group, a halo-C 3 -C 6  alkynyl group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 3 -C 6  cycloalkenyl group, a halo-C 3 -C 6  cycloalkenyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined the above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined the above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different)); (2) when A 2  is —C(═O)— or a group of the formula —C(═NOR 8 )— (wherein R 8  is the same as defined above), then R 7  is a C 1 -C 6  alkyl group, a halo C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a mono-C 1 -C 6  alkylamino group, a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a phenylamino group, a substituted phenylamino group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having one or more substituents which may be the same or different and are selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, (3) when A 2  is a C 1 -C 6  alkylene group, a halo-C 1 -C 6  alkylene group, C 2 -C 6  alkenylene group, a halo-C 2 -C 6  alkenylene group, a C 2 -C 6  alkynylene group or a halo-C 3 -C 6  alkynylene group, then R 7  is a hydrogen atom, a halogen atom, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 1 -C 6  alkoxycarbonyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —A 5 —R 12  (wherein A 5  is —O—, —S—, —SO—, —SO 2 — or a group of the formula —N(R 13 )— (wherein R 13  is a hydrogen atom, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a C 3 -C 6  cycloalkyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituents which may be the same or different and are selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different); and R 12  is a hydrogen atom, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituents which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —A 6 —R 14  (wherein A 6  is —C(═O)—, —SO 2 —, a C 1 -C 6  alkylene group, a halo-C,-C 6  alkylene group, a C 2 -C 6  alkenylene group, a halo-C 2 -C 6  alkenylene group, a C 2 -C 6  alkynylene group or a halo-C 3 -C 6  alkynylene group;  
           [0018]    (i) when A 6  is —C(═O)— or —SO 2 —, then R 14  is a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined the above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different;  
           [0019]    (ii) when A 6  is a C 1 -C 6  alkylene group, a halo-C 1 -C 6  alkylene group, a C 2 -C 6  alkenylene group, a halo-C 2 -C 6  alkenylene group, a C 2 -C 6  alkynylene group or a halo-C 3 -C 6  alkynylene group, then R 14  is a hydrogen atom, a halogen atom, a cyano group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a C 1 -C 6  alkylcarbonyl group, a halo-C 1 -C 6  alkylcarbonyl group, a C 1 -C 6  alkoxycarbonyl group, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and are selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-Ca-C 6  alkylamino group and a di-Co-C 6  alkylamino group which may be the same or different, a phenoxy group, a substituted phenoxy group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a phenylthio group, a substituted phenylthio group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6 -alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), or a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  z z.2 alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different)));  
           [0020]    n is an integer of 1 to 4;  
           [0021]    further, x may form a condensed ring (which means naphthalene, tetrahydronaphthalene, indene, indane, quinoline, quinazoline, chroman, isochroman, indole, indoline, benzodioxane, benzodioxole, benzofuran, dihydrobenzofuran, benzothiophene, dihydrobenzothiophene, benzoxazole, benzothiazole, benzimidazole or indazole), by combining together with the adjacent carbon atoms in the phenyl ring, and said condensed ring may have at least one substituents, which may be the same or different, and selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 6 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group, a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), and a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different;  
           [0022]    Y is the same or different, and is a hydrogen atom, a halogen atom, a cyano group, a nitro group, a C 3 -C 6  cycloalkyl group, a halo-C 3 -C 6  cycloalkyl group, a di-C 1 -C 6  alkoxyphosphoryl group which may be the same or different, a di-C 1 -C 6  alkoxythiophosphoryl group which may be the same or different, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C—C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C l-C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined the above), a substituted heterocyclic group (wherein the heterocyclic group is the same as defined above) having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, or a group of the formula —A 2 —R 7  (wherein A 2  and R 7  are the same as defined above);  
           [0023]    m is an integer of 1 to 5;  
           [0024]    further, Y may form a condensed ring (the condensed ring is the same as defined above), by combining together with the adjacent carbon atoms in the phenyl ring, said condensed ring may have at least one substituents, which may be the same or different, and selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group, a di-C 1 -C 6  alkylamino group which may be the same or different, a phenyl group, a substituted phenyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a naphthyl group, a substituted naphthyl group having at least one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different, a heterocyclic group (which is the same as defined above), and a substituted heterocyclic group (wherein said heterocyclic group is the same as defined above) having at lease one substituent which may be the same or different and is selected from the group consisting of a halogen atom, a cyano group, a nitro group, a C 1 -C 6  alkyl group, a halo-C 1 -C 6  alkyl group, a C 2 -C 6  alkenyl group, a halo-C 2 -C 6  alkenyl group, a C 2 -C 6  alkynyl group, a halo-C 2 -C 6  alkynyl group, a C 1 -C 6  alkoxy group, a halo-C 1 -C 6  alkoxy group, a C 1 -C 6  alkylthio group, a halo-C 1 -C 6  alkylthio group, a C 1 -C 6  alkylsulfinyl group, a halo-C 1 -C 6  alkylsulfinyl group, a C 1 -C 6  alkylsulfonyl group, a halo-C 1 -C 6  alkylsulfonyl group, a mono-C 1 -C 6  alkylamino group and a di-C 1 -C 6  alkylamino group which may be the same or different;  
           [0025]    Z 1  and Z 2  are each represents an oxygen atom or a sulfur atom; provided that,  
           [0026]    (1) when X, R 1  and R 3  are hydrogen atoms at the same time; m is an integer of 2; Y at 2-position is a fluorine atom and Y at 3-position is a chlorine atom; then R 2  is not ethyl group, isopropyl group, cyclohexyl group, 2-propenyl group, methylthiopropyl group and a-methylbenzyl group,  
           [0027]    (2) when X and R 3  are hydrogen atoms at the same time; m is an integer of 2; Y at 2-position is a fluorine atom and Y at 3-position is a chlorine atom; then the 4 to 7 membered ring by combining R 1  and R 2  to each other, in which the ring may contain the same or different 1 to 3 hetero atoms selected from the group consisting of oxygen atom, sulfur atom and nitrogen atom is not morpholino group,  
           [0028]    (3) when X, R 1  and R 3  are hydrogen atoms at the same time; and R 2  is 1,2,2-trimethylpropyl group; then Y is not a hydrogen atom,  
           [0029]    (4) when X, R 1  and R 3  are hydrogen atoms at the same time; R 2  is 2,2-dimethylpropyl group; and m is an integer of 1; then Y is not 2-ethoxy group, and  
           [0030]    (5) when X, R 1  and R 3  are hydrogen atoms at the same time; and R 2  is tert-butyl group group; and m is an integer of 1; then Y is not 4-chlorine atom, 2-nitro group, 4-nitro group, 3-methoxy group, 4-methoxy group and 2,6-dimethyl groups;  
           [0031]    fluorine-containing aniline compounds represented by the general formula (ST-I) as starting material for the phthalic acid diamide derivatives:  
                         
 
           [0032]    (wherein R a  is a halogen atom, a C 1 -C 6  alkyl group, a C 1 -C 6  alkoxy group or a trifluoromethyl group, and each of R b , R c  and R d  is a hydrogen atom or a C 2 -C 6  perfluoroalkyl group, provided that at least one of R b , R c  and R d  is not a hydrogen atom and that R c  is neither a pentafluoroethyl group nor a n-heptafluoropropyl group when R a  is a fluorine atom and each of R b  and R d  is a hydrogen atom); agricultural and horticultural insecticides containing as an active ingredient any of the phthalic acid diamide derivatives of the general formula (I) including known compounds; and a method for application of the insecticides.  
           [0033]    In the definition of the general formula (I) representing the phthalic acid diamide derivative of the present invention, the halogen atom includes chlorine atom, bromine atom, iodine atom and fluorine atom. The term “C 1 -C 6  alkyl”, means a linear or branched alkyl group of 1 to 6 carbon atoms, such as methyl, ethyl, n-propyl, i-propyl, n-butyl, i-butyl, s-butyl, t-butyl, n-pentyl, n-hexyl, or the like. The term “C 1 -C 8  alkylene” means a linear or branched alkylene group of 1 to 8 carbon atoms, such as methylene, ethylene, propylene, trimethylene, dimethylmethylene, tetramethylene, i-butylene, dimethylethylene, pentamethylene, hexamethylene, heptamethylene, octamethylene or the like. The term “halo-C 1 -C 6  alkyl” means a substituted and linear or branched alkyl group of 1 to 6 carbon atoms having as the substituent(s) one or more halogen atoms which may be the same or different.  
           [0034]    As the ring which R 1  and R 2  form by combining to each other, i.e., the 4- to 7-membered ring by combining to each other, in which the ring may contain the same or different 1 to 3 hetero atoms selected from the group consisting of oxygen atom, sulfur atom and nitrogen atom, there can be exemplified azetidine ring, pyrrolidine ring, pyrroline ring, piperidine ring, imidazolidine ring, imidazoline ring, oxazolidine ring, thiazolidine ring, isoxazolidine ring, isothiazolidine ring, tetrahydropyridine ring, piperazine ring, morpholine ring, thiomorpholine ring, dioxazine ring, dithiazine ring, etc.  
           [0035]    The phthalic acid diamide derivative of the general formula (I) of the present invention contains an asymmetric carbon atom or some asymmetric center in the structural formula in some cases or has two optical isomers in some cases. The present invention includes these optical isomers and all mixtures containing the optical isomers in arbitrary proportions.  
           [0036]    Preferable examples of each substituent of the phthalic acid diamide derivative of the general formula (I) of the present invention are as follows. Preferable examples of each of R 1  and R 2  which may be the same or different are hydrogen atom, C 1 -C 6  alkyl groups such as methyl, ethyl, i-propyl, etc. Preferable examples of R 3  are hydrogen atom, and C 1 -C 6  alkyl groups such as methyl, ethyl, n-propyl, i-propyl, n-butyl, etc. Preferable examples of X are halogen atoms, nitro group, halo-C 1 -C 6  alkyl groups, halo-C 1 -C 6  alkoxy groups, halo-C 1 -C 6  alkylthio groups, etc. Preferable examples of Y are halo-C 1 -C 6  alkyl groups, halo-C 1 -C 6  alkoxy groups, halo-C 1 -C 6  alkylthio groups, etc.  
           [0037]    The phthalic acid diamide derivative of the general formula (I) of the present invention can be produced, for example, by any of the processes illustrated below.  
                         
 
           [0038]    wherein R 1 , R 2 , X, n, Y and m are as defined above.  
           [0039]    A phthalic anhydride derivative of the general formula (V) is reacted with an aniline of the general formula (IV) in the presence of an inert solvent to obtain a phthalimide derivative of the general formula (III). The phthalimide derivative (III) is reacted with an amine of the general formula (II) after or without being isolated, whereby a phthalic acid diamide derivative of the general formula (I-1) can be produced.  
           [0040]    (1) General Formula (V)→General Formula (III)  
           [0041]    As the inert solvent used in this reaction, any solvent may be used so long as it does not markedly inhibit the progress of the reaction. There can be exemplified aromatic hydrocarbons such as benzene, toluene, xylene, etc.; halogenated hydrocarbons such as dichloromethane, chloroform, carbon tetrachloride, etc., chlorinated aromatic hydrocarbons such as chlorobenzene, dichlorobenzene, etc.; a cyclic or cyclic ethers such as diethyl ether, dioxane, tetrahydrofuran, etc., esters such as ethyl acetate, etc.; amides such as dimethylformamide, dimethylacetamide, etc.; acids such as acetic acid, etc.; dimethyl sulfoxide; and 1,3-dimethyl-2-imidazolidinone. These inert solvents may be used alone or as a mixture thereof.  
           [0042]    Since the reaction is an equimolar reaction, it is sufficient that the reactants are used in equimolar amounts, though either of them may be used in excess. If necessary, the reaction may be carried out under dehydrating conditions.  
           [0043]    As to the reaction temperature, the reaction can be carried out in a temperature range of room temperature to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0044]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. The desired compound can be subjected to the subsequent reaction without isolation from the reaction solution.  
           [0045]    The phthalic anhydride derivative of the general formula (V) can be produced by the process described in J. Org. Chem., 52, 129 (1987), J. Am. Chem. Soc., 51, 1865 (1929), J. Am. Chem. Soc., 63, 1542 (1941), etc. The aniline of the general formula (IV) can be produced by the process described in J. Org. Chem., 29, 1 (1964), Angew. Chem. Int. Ed. Engl., 24, 871 (1985), Synthesis, 1984, 667, Bulletin of the Chemical Society of Japan, 1973, 2351, DE-2606982, JP-A-1-90163, etc.  
           [0046]    (2) General Formula (III)→General Formula (I-1)  
           [0047]    In this reaction, there can be used the inert solvents exemplified above as the inert solvent used in the reaction (1).  
           [0048]    Since the reaction is an equimolar reaction, it is sufficient that the reactants are used in equimolar amounts, though the amine of the general formula (II) may be used in excess.  
           [0049]    As to the reaction temperature, the reaction can be carried out in a temperature range of room temperature to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0050]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. Production process 2.  
                         
 
           [0051]    wherein R 1 , R 2 , n, X, Y and m are as defined above, and X′ is a halogen atom or a nitro group, provided that X is other than a hydrogen atom or a nitro group.  
           [0052]    A phthalimide derivative of the general formula (III-1) is reacted with a reactant corresponding to X in the presence of an inert solvent to obtain a phthalimide derivative of the general formula (III). The phthalimide, derivative (III) is reacted with an amine of the general formula (II) after or without being isolated, whereby a phthalic acid diamide derivative of the general formula (I-1) can be produced.  
           [0053]    (1) General Formula (III-1)→General Formula (III)  
           [0054]    This reaction can be carried out according to the methods described in J. Org. Chem., 42, 3415 (1977), Tetrahedron, 25, 5921 (1969), Synthesis, 1984, 667, Chem. Lett., 1973, 471, J. Org. Chem., 39, 3318 (1974), J. Org. Chem., 39, 3327 (1974), etc.  
           [0055]    (2) General Formula (III)→General Formula (I-1)  
           [0056]    This reaction can be carried out according to production process 1-(2).  
                         
 
           [0057]    wherein R 1 , R 2 , X, Y, m and n are as defined above.  
           [0058]    A phthalic anhydride of the general formula (V-1) is reacted with an aniline of the general formula (IV) in the presence of an inert solvent to obtain a phthalimide derivative of the general formula (III-2). The phthalimide derivative (III-2) is subjected to catalytic reduction with hydrogen after or without isolation to obtain a phthalimide derivative of the general formula (III-3). The phthalimide derivative (III-3) is converted to a phthalimide derivative of the general formula (III) by adding a diazotizing agent and then a metal salt after or without isolation of the phthalimide derivative (III-3). The phthalimide derivative (III) is reacted with an amine of the general formula (II) after or without being isolated, whereby a phthalic acid diamide derivative of the general formula (I-1) can be produced.  
           [0059]    (1) General Formula (V-1)→General Formula (III-2)  
           [0060]    The desired compound can be produced by this reaction in the same manner as in production process 1-(1).  
           [0061]    (2) General Formula (III-2)→General Formula (III-3)  
           [0062]    Any solvent may be used in this reaction so long as it does not markedly inhibit the progress of the reaction. There can be exemplified alcohols such as methanol, ethanol, propanol, etc.; acyclic or cyclic ethers such as diethyl ether, dioxane, tetrahydrofuran, etc., and acids such as acetic acid, etc. These inert solvents may be used alone or as a mixture thereof.  
           [0063]    As the catalyst for catalytic reduction used in this reaction, there can be exemplified palladium carbon, Raney nickel, palladium black, platinum black, etc. The amount of the catalyst used may be properly chosen in a range of 0.1 to 10% by weight based on the weight of the phthalimide derivative of the general formula (III-2). This reaction is carried out under a hydrogen atmosphere and the hydrogen pressure may be properly chosen in a range of 1 to 10 atmospheric pressure.  
           [0064]    As to the reaction temperature, the reaction can be carried out in a temperature range of room temperature to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0065]    After completion of the reaction, the desired compound is isolated from the reaction mixture containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. The desired compound can be subjected to the subsequent reaction without isolation from the reaction mixture.  
           [0066]    (3) General Formula (III-3)→General Formula (III)  
           [0067]    In this reaction, an acidic solvent can be used as an inert solvent. The acidic solvent includes, for example, an aqueous hydrochloric acid solution, an aqueous hydrobromic acid solution, an aqueous hydroiodic acid solution, an aqueous sulfuric acid solution, acetic acid and trifluoroacetic acid. These acidic solvents may be used alone or as a mixture thereof. In addition, these acidic solvents may be used in admixture with ethers such as tetrahydrofuran, dioxane, etc.  
           [0068]    The diazotizing agent includes, for example, sodium nitrite, nitrosyl hydrogensulfate and alkyl nitrites. The amount of the diazotizing agent used may be properly chosen in a range of equal amount to excess amount relative to the amount of the phthalimide derivative of the general formula (III-3).  
           [0069]    As to the reaction temperature, the reaction can be carried out in a temperature range of −50° C. to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0070]    As the metal salt added after the production of a diazonium salt, there can be used, for example, cuprous chloride, cuprous bromide, potassium iodide, copper cyanide, potassium xanthate and sodium thiorate. The amount of the metal salt used may be properly chosen in a range of 1 equivalent to excess equivalents per equivalent of the phthalimide derivative of the general formula (III-3).  
           [0071]    After completion of the reaction, the desired compound is isolated from the reaction mixture containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. The desired compound can be subjected to the subsequent reaction without isolation from the reaction mixture.  
           [0072]    The reaction can be carried out according to the method described in Org. Synth., IV, 160 (1963), Org. Synth., III, 809 (1959), J. Am. Chem. Soc., 92, 3520 (1970), etc.  
           [0073]    (4) General Formula (III)→General Formula (I-1)  
           [0074]    The desired compound can be produced by this reaction in the same manner as in production process 1-(2).  
                         
 
           [0075]    wherein R 1 , R 2 , X, Y, m and n are as defined above.  
           [0076]    A phthalimide derivative of the general formula (III-2) is reacted with an amine of the general formula (II) in the presence of an inert solvent to obtain a phthalic acid diamide derivative of the general formula (I-3). The phthalic acid diamide derivative (I-3) is subjected to catalytic reduction with hydrogen after or without isolation to obtain a phthalic acid diamide derivative of the general formula (I-2). A phthalic acid diamide derivative of the general formula (I-1) can be produced from the phthalic acid diamide derivative (I-2) by adding a diazotizing agent and then a metal salt after or without isolating the phthalic acid diamide derivative (I-2).  
           [0077]    (1) General Formula (III-2)→General Formula (I-3)  
           [0078]    The desired compound can be produced by this reaction in the same manner as in production process 1-(2).  
           [0079]    (2) General Formula (I-3)→General Formula (I-2)  
           [0080]    The desired compound can be produced by this reaction in the same manner as in production process 3-(2).  
           [0081]    (3) General Formula (I-2)→General Formula (I-1)  
           [0082]    The desired compound can be produced by this reaction in the same manner as in production process 3-(3).  
                         
 
           [0083]    wherein R 1 , R 2  R 3 , X, n, Y and m are as defined above.  
           [0084]    A phthalic anhydride derivative of the general formula (V) is reacted with an amine of the general formula (II) in the presence of an inert solvent to obtain a phthalamide of the general formula (III-4). The phthalamide (III-4) is treated as follows after or without isolation. When R 2  of the phthalamide (III-4) is a hydrogen atom, the phthalamide (III-4) is condensed into a compound of the general formula (VI) in the presence of a condensing agent, and the compound (VI) is reacted with an aniline of the general formula (IV) in the presence of an inert solvent after or without being isolated. When R 2  of the phthalamide (III-4) is other than a hydrogen atom, the phthalamide (III-4) is condensed with an aniline of the general formula (IV) in the presence of a condensing agent. Thus, a phthalic acid diamide derivative of the general formula (I) can be produced.  
           [0085]    Alternatively, a phthalic anhydride derivative of the general formula (V) is reacted with an aniline of the general formula (IV) in the presence of an inert solvent to obtain a phthalanilide of the general formula (III-5). The phthalanilide (III-5) is treated as follows after or without isolation. When R 3  of the phthalanilide (III-5) is a hydrogen atom, the phthalanilide (III-5) is condensed into a compound of the general formula (VI-1) in the presence of a condensing agent, and the compound (VI-1) is reacted with an amine of the general formula (II) in the presence of an inert solvent after or without being isolated. When R 3  of the phthalanilide (III-5) is other than a hydrogen atom, the phthalanilide (III-5) is condensed with an amine of the general formula (II) in the presence of a condensing agent. Thus, a phthalic acid diamide derivative of the general formula (I) can be produced.  
           [0086]    (1) General formula (V) or general formula (VI-1)→general formula (III-4) or general formula (I), respectively  
           [0087]    The desired compound can be produced by this reaction in the same manner as in production process 1-(2).  
           [0088]    (2) General formula (III-4) or general formula (III-5)→general formula (VI) or general formula (VI-1), respectively  
           [0089]    The desired compound can be produced by this reaction according to the method described in J. Med. Chem., 10, 982 (1967).  
           [0090]    (3) General formula (VI) or general formula (V)→general formula (I) or general formula (III-5), respectively  
           [0091]    The desired compound can be produced by this reaction in the same manner as in production process 1-(2).  
           [0092]    (4) General formula (III-4) or general formula (III-5)→general formula (I)  
           [0093]    The desired compound can be produced by reacting the phthalamide derivative of the general formula (III-4) or the general formula (III-5) with the aniline of the general formula (IV) or the amine of the general formula (II), respectively, in the presence of a condensing agent and an inert solvent. If necessary, the reaction can be carried out in the presence of a base.  
           [0094]    The inert solvent used in the reaction includes, for example, tetrahydrofuran, diethyl ether, dioxane, chloroform and dichloromethane. As the condensing agent used in the reaction, any condensing agent may be used so long as it is used in usual amide synthesis. The condensing agent includes, for example, Mukaiyama reagent (e.g. 2-chloro-N-methylpyridinium iodide), 1,3-dicyclohexylcarbodiimide (DCC), carbonyldiimidazole (CDI) and diethyl phosphorocyanidate (DEPC). The amount of the condensing agent used may be properly chosen in a range of 1 mole to excess moles per mole of the phthalamide derivative of the general formula (III-4) or the general formula (III-5).  
           [0095]    As the base usable in the reaction, there can be exemplified organic bases such as triethylamine, pyridine, etc. and inorganic bases such as potassium carbonate, etc. The amount of the base used may be properly chosen in a range of 1 mole to excess moles per mole of the phthalamide derivative of the general formula (III-4) or the general formula (III-5).  
           [0096]    As to the reaction temperature, the reaction can be carried out in a temperature range of 0° C. to the boiling point of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it ranges from several minutes to 48 hours.  
           [0097]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced.  
                         
 
           [0098]    wherein R 1 , R 2 , X, n, Y and m are as defined above, Hal is a halogen atom, and R 15  is a (C 1 -C 3 )alkyl group.  
           [0099]    A phthalic acid ester derivative of the general formula (VII) is halogenated into a phthaloyl halide of the general formula (VII-1) in the presence or absence of an inert solvent. The phthaloyl halide (VII-1) is reacted with an aniline of the general formula (IV) in the presence -4 of an inert solvent and a base after or without being isolated, to obtain a phthalanilide of the general formula (III-6). The phthalanilide (III-6) is hydrolyzed into a phthalanilide of the general formula (III-5) in the presence or absence of an inert solvent after or without being isolated. The phthalanilide (III-5) is condensed into a phthalic anhydride derivative of the general formula (VI-1)-after or without being isolated. The phthalic anhydride derivative (VI-1) is reacted with an amine of the general formula (II), whereby a phthalic acid diamide derivative of the general formula (I-1) can be produced.  
           [0100]    (1) General Formula (VII)→General Formula (VII-1)  
           [0101]    As the inert solvent usable in this reaction, any solvent may be used so long as it does not markedly inhibit the progress of the reaction. There can be exemplified aromatic hydrocarbons such as benzene, toluene, xylene, etc.; halogenated hydrocarbons such as dichloromethane, chloroform, carbon tetrachloride, etc., chlorinated aromatic hydrocarbons such as chlorobenzene, dichlorobenzene, etc.; acyclic or cyclic ethers such as diethyl ether, dioxane, tetrahydrofuran, etc., and esters such as ethyl acetate, etc. These inert solvents may be used alone or as a mixture thereof.  
           [0102]    As the halogenating agents, there can be used, for example, thionyl chloride, phosphoryl chloride, and phosphorus trichloride. The amount of the halogenating agent used may be properly chosen in a range of 1 to 10 equivalents per equivalent of the phthalic acid ester of the general formula (VII).  
           [0103]    As to the reaction temperature, the reaction can be carried out in a temperature range of 0° C. to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0104]    After completion of the reaction, the desired compound-is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. The desired compound can be subjected to the subsequent reaction without isolation from the reaction solution.  
           [0105]    The phthalic acid ester of the general formula (VII) can be produced, for example, by the process described in J. Med. Chem., 31, 1466 (1988).  
           [0106]    (2) General Formula (VII-1)→General Formula (III-6)  
           [0107]    As the inert solvent used in this reaction, there may be used, for example, the inert solvents exemplified in production process 1-(1).  
           [0108]    As the base, an inorganic base or an organic base may be used. As the inorganic base, there may be used, for example, hydroxides of alkali metals, such as sodium hydroxide, potassium hydroxide, etc. As the organic base, there may be used triethylamine, pyridine, etc. The amount of the base used may be properly chosen in a range of 0.5 to 3 equivalents per equivalent of the phthaloyl halide of the general formula (VII-1).  
           [0109]    Since the reaction is an equimolar reaction, it is sufficient that the reactants are used in equimolar amounts, though the amount of the aniline of the general formula (IV) used may be properly chosen in a range of 0.5 to 2 equivalents per equivalent of the phthaloyl halide of the general formula (VII-1).  
           [0110]    As to the reaction temperature, the reaction can be carried out in a temperature range of 0° C. to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0111]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. The desired compound can be subjected to the subsequent reaction without isolation from the reaction solution.  
           [0112]    (3) General Formula (III-6)→General Formula (III-5)  
           [0113]    As the inert solvent usable in this reaction, there may be used water, alcohols (e.g. methanol, ethanol and propanol) as water-soluble solvents, and mixed solvents of water and a water-soluble solvent.  
           [0114]    As the base used for the hydrolysis, there may be used, for example, hydroxides of alkali metals, such as sodium hydroxide, potassium hydroxide, etc. The amount of the base used may be properly chosen in a range of 1 to 10 equivalents per equivalent of the phthalanilide of the general formula (III-6).  
           [0115]    As to the reaction temperature, the reaction can be carried out in a temperature range of 0° C. to the reflux temperature of the inert solvent used. Although the reaction time is varied depending on the scale of reaction, the reaction temperature, etc., it may be properly chosen in a range of several minutes to 48 hours.  
           [0116]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be produced. The desired compound can be subjected to the subsequent reaction without isolation from the reaction solution.  
           [0117]    (4) General Formula (III-5)→General Formula (VI-1)  
           [0118]    The desired compound can be produced by this reaction according to production process 5-(2).  
           [0119]    (5) General Formula (VI-1)→General Formula (I-1)  
           [0120]    The desired compound can be produced by this reaction according to production process 1-(2).  
                         
 
           [0121]    wherein R 1 , R 2 , R 3 , X, Y, m, n, Z and Z are as defined above.  
           [0122]    A benzamide derivative of the general formula (VIII-1) or the general formula (VIII-2) or a thiobenzamide derivative of the general formula (VIII-3) or the general formula (VIII-4) obtained by thiocarbonylation of the benzamide derivative of the general formula (VIII-1) or the general formula (VIII-2), respectively, is subjected to ortho-metallation by using a metal reagent such as butyllithium. The compound thus obtained is directly reacted with an isocyanate or isothiocyanate derivative of the general formula (IX-1) or (IX-2), or the compound is reacted with carbon dioxide to obtain a phthalamide derivative of the general formula (III-4′) or the general formula (III-5′), which is treated in the same manner as in production processes 5-(1) to 5-(4). Thus, a phthalic acid diamide derivative of the general formula (I) can be produced.  
           [0123]    (1) General formula (VIII-1) or general formula (VIII-2)→general formula (VIII-3) or general formula (VIII-4), respectively  
           [0124]    The desired compound can be produced by this reaction according to the method described in J. Org. Chem., 46, 3558 (1981).  
           [0125]    (2) General formula (VIII-1), general formula (VIII-2), general formula (VIII-3) or general formula (VIII-4)→general formula (I)  
           [0126]    In this step, the benzamide derivative of the general formula (VIII-1) or the general formula (VIII-2) or the thiobenzamide derivative of the general formula (VIII-3) or the general formula (VIII-4) obtained by thiocarbonylation of the benzamide derivative of the general formula (VIII-1) or the general formula (VIII-2), respectively, is subjected to ortho-lithiation according to the method described in J. Org. Chem., 29, 853 (1964). The compound thus obtained is reacted with the isocyanate or isothiocyanate derivative of the general formula (IX-1) or (IX-2) at −80° C. to room temperature, whereby the desired compound can be produced.  
           [0127]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be obtained.  
           [0128]    (3) General formula (VIII-1), general formula (VIII-2), general formula (VIII-3) or general formula (VIII-4)→general formula (III-4′) or the general formula (III-5′)  
           [0129]    In this step, the desired compound can be produced by carrying out the same ortho-lithiation as in the above step (2) and introducing carbon dioxide into the ortho-lithiation product at −80° C. to room temperature.  
           [0130]    After completion of the reaction, the desired compound is isolated from the reaction solution containing the desired compound by a conventional method, and if necessary, purified by recrystallization, column chromatography, etc., whereby the desired compound can be obtained.  
           [0131]    (4) General formula (III-4′) or general formula (III-5′)→general formula (I)  
           [0132]    In this step, the desired compound can be produced in the same manner as in production process 1-(2) or 5-(4).  
           [0133]    Tables 1 and 2 show typical examples of the phthalic acid diamide derivative of the general formula (I) used as the active ingredient of the agricultural and horticultural insecticide of the present invention, but the examples are not intended in any way to limit the scope of the present invention.  
           [0134]    General Formula (I):  
                                                                                                                                                                                                                                                                                                                                                                                                                               TABLE 1                               (I)                                                                              Physical                               Properties                               (melting       No   R 1     R 2     R 3     Xn   ym   point: ° C.                    1   H   H   H   3-NO 2     2-CH 3 -5-Cl   173-175       2   CH 3     H   H   H   4-CF 3     129-131       3   CH 3     H   H   3-NO 2     2-CH 3 -5-Cl   169-171       4   CH 3     H   H   3-NO 2     2-CH 2 4-CHF 2     167-169       5   CH 3     CH 3     H   6-NO 2     2-CH 3 -5-Cl   171-173       6   CH 3     CH 3     H   6-NO 2     2-CH 3 -4-OCHF 2     167-169       7   C 2 H 5     H   H   H   4-CF 3     134-136       8   C 2 H 5     H   H   3-Cl   2-CH 3 -4-OCHF 2     179-180       9   C 2 H 5     H   H   6-Cl   2-CH 3 -4-OCHF 2     189-190       10   C 2 H 5     H   H   3-NO 2     2-CH 3 -5-Cl   175-177       11   C 2 H 5     H   H   3-NO 2     2-CH 3 -4-OCHF 2     207-208       12   C 2 H 5     C 2 H 5     H   H   4-CF 3     148-150       13   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -5-Cl   175-177       14   n-C 3 H 7     H   H   H   4-CF 3     138-140       15   n-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCHF 2     171-173       16   n-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCHF 2     189-191       17   n-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCHF 2     184-186       18   n-C 3 H 7     H   H   3-NO 2     2-CH 3 -5-Cl   187-189       19   n-C 3 H 7     H   H   5-CF 3     2,6-(C 2 H 5 ) 2     230-232       20   i-C 3 H 7     H   H   H   H   192-194       21   i-C 3 H 7     H   H   H   2-NO 2     198-200       22   i-C 3 H 7     H   H   H   4-NO 2     139-141       23   i-C 3 H 7     H   H   H   4-F   199-201       24   i-C 3 H 7     H   H   H   2-CH 3     191-193       25   i-C 3 H 7     H   H   H   4-CF 3     198-200       26   i-C 3 H 7     H   H   H   3-CF 3     174-176       27   i-C 3 H 7     H   H   H   4-CF 2 CF 2 CF 3     237-238       28   i-C 3 H 7     H   H   H   4-(CF 2 ) 3 CF 3     137-139       29   i-C 3 H 7     H   H   H   4-OCF 3     155-157       30   i-C 3 H 7     H   H   H   4-OCF 2 CHFOC 3 F 7 -n   220-222       31   i-C 3 H 7     H   H   H   3-SCF 3     176-178       32   i-C 3 H 7     H   H   H   4-SCHF 2     169-170       33   i-C 3 H 7     H   H   H   4-SCH 2 CF 3     166-167       34   i-C 3 H 7     H   H   H   4-SCF 2 CHF 2     169-170       35   i-C 3 H 7     H   H   H   4-S(CF 2 ) 3 CF 3     159-161       36   i-C 3 H 7     H   H   H   4-SCF(CF 3 ) 2     145-147       37   i-C 3 H 7     H   H   H   4-SCF 2 CBrF 2     158-160       38   i-C 3 H 7     H   H   H   4-SOCF 2 CBrF 2     180-182       39   i-C 3 H 7     H   H   H   4-SO(CF 2 ) 3 CF 3     192-193       40   i-C 3 H 7     H   H   H   4-SO 2 CH 2 CF 3     169-170       41   i-C 3 H 7     H   H   H   2,3-Cl 2     151-153       42   i-C 3 H 7     H   H   H   2,4-Cl 2     162-164       43   i-C 3 H 7     H   H   H   3,4-F 2     172-174       44   i-C 3 H 7     H   H   H   2,4-(CH 3 ) 2     162-163       45   i-C 3 H 7     H   H   H   2-Cl-4-CF 3     197-199       46   i-C 3 H 7     H   H   H   2-Cl-4-CF(CF 3 ) 2     201-202       47   i-C 3 H 7     H   H   H   2-Cl-4-OCF 3     151-153       48   i-C 3 H 7     H   H   H   2-Br-4-OCF 3     146-147       49   i-C 3 H 7     H   H   H   2-CH 3 -3-Cl   196-198       50   i-C 3 H 7     H   H   H   2-CH 3 -4-Cl   180-182       51   i-C 3 H 7     H   H   H   2-CH 3 -5-Cl   161-162       52   i-C 3 H 7     H   H   H   2-CH 3 -4-Br   159-261       53   i-C 3 H 7     H   H   H   2-CH 3 -5-F   168-170       54   i-C 3 H 7     H   H   H   2-CH 3 -5-C 4 H 9 -t   203-204       55   i-C 3 H 7     H   H   H   2-CH 3 -4-CF 2 CF 3     157-159       56   i-C 3 H 7     H   H   H   2-CH 3 -4-CF 2 CF 2 CF 3     177-178       57   i-C 3 H 7     H   H   H   2-CH 3 -4-CF(CF 3 ) 2     230-231       58   i-C 3 H 7     H   H   H   2-CH 3 -4-OCHF 2     135-137       59   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 3     172-173       60   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CHF 2     145-146       61   i-C 3 H 7     H   H   H   2-CH 3 -3-OCF 2 CHClF   172-174       62   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CHClF   142-144       63   i-C 3 H 7     H   H   H   2-CH 3 -4-CF 2 CBrF 2     164-166       64   i-C 3 H 7     H   H   H   2-CH 3 -4-CF 2 CCl 2 F   172-173       65   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CHFCF 3     151-152       66   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CBrFCF 3     163-164       67   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CHFOCF 3     146-148       68   i-C 3 H 7     H   H   H   2-CH 3 -4-SC 3 H 7 -i   178-180       69   i-C 3 H 7     H   H   H   2-CH 3 -4-OCH 2 OCH 3     165-166       70   i-C 3 H 7     H   H   H   2-CH 2 -4-OCH 2 SCH 3     160-162       71   i-C 3 H 7     H   H   H   2-CH 3 -4-COOCH 3     163-165       72   i-C 3 H 7     H   H   H   2-CH 3 -4-OCH 2 COOCH 3     121-122       73   i-C 3 H 7     H   H   H   2-CH 3 -4-(F5-PhO)   185-187       74   i-C 3 H 7     H   H   H   2-CH 3 -4-(3-CF 3 -PhO)   150-152       75   i-C 3 H 7     H   H   H   2-CH 3 -4-(2-Cl-4-CF 3 -PhO)   183-185       76   i-C 3 H 7     H   H   H   2-CH 3 -4-(4-Cl-Ph-CH 2 O)   188-189       77   i-C 3 H 7     H   H   H   2-CH 3 -4-(4-Cl-PhS)   181-182       78   i-C 3 H 7     H   H   H   2-CH 3 -4-(5-CF 3 -2-Pyi-O)   165-167       79   i-C 3 H 7     H   H   H   2-CH 3 -4-(3-Cl-   184-185                           5-CF 3 -2-Pyi-O)       80   i-C 3 H 7     H   H   H   4-(3-Cl-5-CF 3 -2-Pyi-S)   173-175       81   i-C 3 H 7     H   H   H   2-CH 2 -4-P═O(OC 2 H 5 ) 2     134-136       82   i-C 3 H 7     H   H   H   2-CH 3 -4-OP═S(OCH 3 ) 2     132-134       83   i-C 3 H 7     H   H   H   2-CF 3 -4-OCHF 2     147-149       84   i-C 3 H 7     H   H   H   3,5-Cl 2 -4-OCHF 2     183-185       85   i-C 3 H 7     H   H   H   3-N═C(CF 3 )-NH-4   217-218       86   i-C 3 H 7     H   H   H   3-N═C(CF 3 )-N(CH 3 )-4   171-173       87   i-C 3 H 7     H   H   3-Cl   4-C 4 H 9 -n   169-171       88   i-C 3 H 7     H   H   3-Cl   4-C 4 H 9 -t   224-226       89   i-C 3 H 7     H   H   3-Cl   4-CF(CF 3 ) 2     198-200       90   i-C 3 H 7     H   H   3-Cl   4-CF 2 CF 2 CFS   203-204       91   i-C 3 H 7     H   H   3-Cl   4-(CF 2 ) 3 CF 3     176-178       92   i-C 3 H 7     H   H   3-Cl   4-OCHF 2     205-207       93   i-C 3 H 7     H   H   3-Cl   4-OCF 2 CHFOC 3 F 7 -n   169-171       94   i-C 3 H 7     H   H   3-Cl   4-SCH 3     231-232       95   i-C 3 H 7     H   H   6-Cl   4-SCH 3     193-195       96   i-C 3 H 7     H   H   3-Cl   4-SOCH 3     178-182       97   i-C 3 H 7     H   H   3-Cl   4-SO 2 CH 3     208-210       98   i-C 3 H 7     H   H   3-Cl   4-SCHF 2     220-222       99   i-C 3 H 7     H   H   3-Cl   3-SCF 3     189-191       100   i-C 3 H 7     H   H   3-Cl   3-SOCF 3     183-187       101   i-C 3 H 7     H   H   3-Cl   4-SCH 2 CF 3     191-193       102   i-C 3 H 7     H   H   3-Cl   4-SCF 2 CHF 2     198-200       103   i-C 3 H 7     H   H   3-Cl   4-SCF 2 CBrF 2     201-203       104   i-C 3 H 7     H   H   3-Cl   4-SCF(CF 3 ) 2     221-223       105   i-C 3 H 7     H   H   3-Cl   4-S(CF 2 ) 3 CF 3     199-200       106   i-C 3 H 7     H   H   3-Cl   4-SOCF(CF 3 ) 2     204-206       107   i-C 3 H 7     H   H   3-Cl   4-SO 2 CH 2 CF 3     202-204       108   i-C 3 H 7     H   H   3-Cl   4-SO 2 CF 2 CHF 2     227-230       109   i-C 3 H 7     H   H   3-Cl   4-COCH 3     217-219       110   i-C 3 H 7     H   H   3-Cl   4-Ph   215-217       111   i-C 3 H 7     H   H   3-Cl   2,3-Cl 2     168-169       112   i-C 3 H 7     H   H   3-Cl   2,4-Cl 2     190-192       113   i-C 3 H 7     H   H   3-Cl   2,4-F 2     188-190       114   i-C 3 H 7     H   H   3-Cl   2-Cl-4-F   172-173       115   i-C 3 H 7     H   H   3-Cl   2-F-4-Cl   181-182       116   i-C 3 H 7     H   H   3-Cl   2,3,4-F3   174-176       117   i-C 3 H 7     H   H   3-Cl   2,3-(CH 3 ) 2     187-189       118   i-C 3 H 7     H   H   3-Cl   2-CH 3 -3-Cl   200-202       119   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-Cl   213-215       120   i-C 3 H 7     H   H   3-Cl   2-CH 3 -5-Cl   183-185       121   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-Br   210-212       122   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-I   206-208       123   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCH 3     191-192       124   i-C 3 H 7     H   H   3-Cl   2,3-(CH 3 ) 2 -4-OCH 3     208-210       125   i-C 3 H 7     H   H   3-Cl   2-Cl-4-CF 3     156-157       126   i-C 3 H 7     H   H   3-Cl   2-Cl-4-CF(CF 3 ) 2     204-206       127   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CF 3     219-220       128   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     199-200       129   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CCl3   169-171       130   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CF 2 CF 2 CF 3     214-215       131   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CF(CF 3 ) 2     220-222       132   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-(CF 2 ) 3 CF 3     188-189       133   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-(CF 2 )5CF 3     161-163       134   i-C 3 H 7     H   H   3-Cl   3-Cl-4-OCHF 2     197-199       135   i-C 3 H 7     H   H   3-Cl   2-Cl-4-OCF 3     158-159       136   i-C 3 H 7     H   H   3-Cl   2-Br-4-OCF 3     169-170       137   i-C 3 H 7     H   H   3-Cl   3-F-4-OCHF 2     211-212       138   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCHF 2     193-195       139   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 3     199-201       140   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCBrF 2     181-182       141   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CHF 2     202-204       142   i-C 3 H 7     H   H   3-Cl   2-CH 3 -3-OCF 2 CHClF   169-171       143   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CHClF   194-196       144   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CBrF 2     193-194       145   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CCl 2 F   202-203       146   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CHFCF 3     186-187       147   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCH 2 CF 2 CHF 2     207-208       148   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CBrFCFS   205-206       149   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CHFOCF 3     179-181       150   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCHF 2 -5-Cl   191-192       151   i-C 3 H 7     H   H   3-Cl   3,5-Cl 2 -4-OCHF 2     205-207       152   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CHF 2 -5-Cl   211-212       153   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SC 3 H 7 -i   189-191       154   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SCHF 2     189-191       155   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SOCHF 2     173-176       156   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SO 2 CHF 2     168-170       157   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-F5-PhO)   224-226       158   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-(5-CF 3 -2-Pyi-O)   189-191       159   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-(3-Cl-   204-205                           5-CF 3 -2-Pyi-O)       160   i-C 3 H 7     H   H   3-Cl   4-(3-Cl-5-CF 3 -2-Pyi-S)   213-215       161   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-P═O(OC 2 H 5 ) 2     71-73       162   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OP═S(OCH 3 ) 2     168-170       163   i-C 3 H 7     H   H   3-Cl   2-CF 3 -4-OCHF 2     194-196       164   i-C 3 H 7     H   H   3-Cl   3-CF 3 -4-OCHF 2     208-209       165   i-C 3 H 7     H   H   3-Cl   3-N═C(CF 3 )-O-4   248-250       166   i-C 3 H 7     H   H   3-Cl   3-N═C(CF 3 )-NH-4   194-196       167   i-C 3 H 7     H   H   3-Cl   3-N═C(CF 3 )-N(CH 3 )-4   225-227       168   i-C 3 H 7     H   H   4-Cl   H   190-192       169   i-C 3 H 7     H   H   4-Cl   4-F   213-215       170   i-C 3 H 7     H   H   4-Cl   2-CH 3     208-210       171   i-C 3 H 7     H   H   4-Cl   3-CF 3     196-198       172   i-C 3 H 7     H   H   4-Cl   4-OCF 3     192-194       173   i-C 3 H 7     H   H   4-Cl   2,4-Cl 2     174-176       174   i-C 3 H 7     H   H   4-Cl   3,4-F 2     231-233       175   i-C 3 H 7     H   H   4-Cl   2,3-Cl 2     186-188       176   i-C 3 H 7     H   H   4-Cl   2-CH 3 -3-Cl   203-205       177   i-C 3 H 7     H   H   4-Cl   2-CH 3 -4-Cl   206-208       178   i-C 3 H 7     H   H   4-Cl   2-CH 3 -5-Cl   207-208       179   i-C 3 H 7     H   H   4-Cl   2-CH 3 -5-F   229-231       180   i-C 3 H 7     H   H   4-Cl   2-CH 3 -4-OCHF 2     223-224       181   i-C 3 H 7     H   H   5-Cl   H   186-188       182   i-C 3 H 7     H   H   5-Cl   4-F   209-211       183   i-C 3 H 7     H   H   5-Cl   2-CH 3     187-189       184   i-C 3 H 7     H   H   5-Cl   3-CF 3     198-200       185   i-C 3 H 7     H   H   5-Cl   4-OCF 3     180-182       186   i-C 3 H 7     H   H   5-Cl   2,3-Cl 2     167-169       187   i-C 3 H 7     H   H   5-Cl   2,4-Cl 2     165-167       188   i-C 3 H 7     H   H   5-Cl   3,4-F 2     207-209       189   i-C 3 H 7     H   H   5-Cl   2-CH 3 -3-Cl   204-206       190   i-C 3 H 7     H   H   5-Cl   2-CH 3 -4-Cl   202-204       191   i-C 3 H 7     H   H   5-Cl   2-CH 3 -5-Cl   209-210       192   i-C 3 H 7     H   H   5-Cl   2-CH 3 -5-F   192-194       193   i-C 3 H 7     H   H   5-Cl   2-CH 3 -4-OCHF 2     188-189       194   i-C 3 H 7     H   H   5-Cl   2,3,4-F3   224-226       195   i-C 3 H 7     H   H   6-Cl   4-C 4 H 9 -n   194-196       196   i-C 3 H 7     H   H   6-Cl   4-C 4 H 9 -t   235-237       197   i-C 3 H 7     H   H   6-Cl   4-CF 2 CF 2 CF 3     216-217       198   i-C 3 H 7     H   H   6-Cl   4-CF(CF 3 ) 2     209-211       199   i-C 3 H 7     H   H   6-Cl   4-(CF 2 ) 3 CF 3     196-198       200   i-C 3 H 7     H   H   6-Cl   4-OCHF 2     223-225       201   i-C 3 H 7     H   H   6-Cl   4-OCF 2 CHFOC 3 F 7 -n   205-207       202   i-C 3 H 7     H   H   6-Cl   4-SCH 2 CF 3     189-190       203   i-C 3 H 7     H   H   6-Cl   4-SCF 2 CHF 2     211-213       204   i-C 3 H 7     H   H   6-Cl   4-SCF(CF 3 ) 3     250-252       205   i-C 3 H 7     H   H   6-Cl   4-S(CF 2 ) 3 CF 3     210-212       206   i-C 3 H 7     H   H   6-Cl   3-SOCF 3     212-215       207   i-C 3 H 7     H   H   6-Cl   4-COCH 3     230-232       208   i-C 3 H 7     H   H   6-Cl   2,3-Cl 2     179-180       209   i-C 3 H 7     H   H   6-Cl   2,4-Cl 2     199-200       210   i-C 3 H 7     H   H   6-Cl   2,4-F 2     196-198       211   i-C 3 H 7     H   H   6-Cl   2-Cl-4-F   196-197       212   i-C 3 H 7     H   H   6-Cl   2-F-4-Cl   184-186       213   i-C 3 H 7     H   H   6-Cl   2,3-(CH 3 ) 2     214-216       214   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-Cl   238-235       215   i-C 3 H 7     H   H   6-Cl   2-CH 3 -5-Cl   204-206       216   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-Br   242-244       217   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-I   236-238       218   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCH 3     195-197       219   i-C 3 H 7     H   H   6-Cl   2,3-(CH 3 ) 2 -4-OCH 3     242-244       220   i-C 3 H 7     H   H   6-Cl   2-Cl-4-CF 3     171-172       221   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-CF 3     234-236       222   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CCl 3     169-171       223   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-CF 2 CF 3     215-217       224   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-CF(CF 3 ) 2     238-240       225   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-(CF 2 ) 3 CF 3     177-178       226   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-(CF 2 ) 3 CF 3     167-169       227   i-C 3 H 7     H   H   6-Cl   3,5-Cl 2 -4-OCHF 2     196-198       228   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CCl 2 F   218-220       229   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CBrF 2     214-215       230   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCH 2 CF 2 CHF 2     212-213       231   i-C 3 H 7     H   H   6-Cl   2-Cl-4-CF(CF 2 ) 3     212-214       232   i-C 3 H 7     H   H   6-Cl   3-Cl-4-OCHF 2     204-206       233   i-C 3 H 7     H   H   6-Cl   3-F-4-OCHF 2     225-227       234   i-C 3 H 7     H   H   6-Cl   2-Cl-4-OCF 3     161-162       235   i-C 3 H 7     H   H   6-Cl   2-Br-4-OCF 3     188-189       236   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCHF 2     213-215       237   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 3     212-214       238   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCBrF 2     195-196       239   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CHF 2     199-201       240   i-C 3 H 7     H   H   6-Cl   2-CH 2 -3-OCF 2 CHClF   195-197       241   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CHClF   204-213       242   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CHFCF 3     199-200       243   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CBrFCF 3     226-227       244   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CHFOCF 3     210-212       245   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCHF 2 -5-Cl   234-235       246   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OCF 2 CHF 2 -5-Cl   230-232       247   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-SCHF 2     199-201       248   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-(F5-PhO)   243-245       249   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-(5-CF 3 -2-Pyi-O)   116-120       250   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-(3-Cl-   219-221                           5-CF 3 -2-Pyi-O)       251   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-P═O(OC 2 H 5 ) 2     146-147       252   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OP═S(OCH 3 ) 2     183-185       253   i-C 3 H 7     H   H   6-Cl   2-CF 3 -4-OCHF 2     234-236       254   i-C 3 H 7     H   H   6-Cl   3-CF 3 -4-OCHF 2     204-205       255   i-C 3 H 7     H   H   6-Cl   3-N═C(CF 3 )-O-4   270-272       256   i-C 3 H 7     H   H   6-Cl   3-N═C(CF 3 )-NH-4   213-215       257   i-C 3 H 7     H   H   6-Cl   3-N═C(CF 3 )-N(CH 3 )-4   239-241       258   i-C 3 H 7     H   H   3,6-Cl 2     2-CH 3 -4-OCHF 2     221-222       259   i-C 3 H 7     H   H   3,6-Cl 2     2-CH 3 -4-Cl   234-235       260   i-C 3 H 7     H   H   3,4,5,6-Cl 4     2-CH 3 -4-Cl   265-266       261   i-C 3 H 7     H   H   3-Br   4-CF 3     221-223       262   i-C 3 H 7     H   H   3-Br   4-OCF 3     208-210       263   i-C 3 H 7     H   H   3-Br   2,3-(CH 3 ) 2     248-250       264   i-C 3 H 7     H   H   3-Br   2,4-(CH 3 ) 2     223-224       265   i-C 3 H 7     H   H   3-Br   2,4,6-(CH 3 ) 3     254-255       266   i-C 3 H 7     H   H   3-Br   2-CH 3 -3-Cl   215-217       267   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-Cl   176-178       268   i-C 3 H 7     H   H   3-Br   2-CH 3 -5-Cl   196-198       269   i-C 3 H 7     H   H   3-Br   2,3-(CH 3 ) 2 -4-Cl   222-224       270   i-C 3 H 7     H   H   3-Br   2,4-(CH 3 ) 2 -3-Cl   236-238       271   i-C 3 H 7     H   H   3-Br   2-C 2 H 5 -4-Cl   205-207       272   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-Br   220-222       273   i-C 3 H 7     H   H   3-Br   2,3-(CH 3 ) 2 -4-Br   200-202       274   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-I   203-205       275   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-F   223-224       276   i-C 3 H 7     H   H   3-Br   2-Cl-4-CF 3     156-157       277   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-CF 3     227-228       278   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-CF 2 CF 3     201-202       279   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-CF 2 CF 2 CF 3     199-200       280   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-CF(CF 3 ) 2     222-224       281   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-(CF 2 ) 3 CF 3     190-191       282   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCH 3     199-200       283   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCH 2 CF 2 CHF 2     206-207       284   i-C 3 H 7     H   H   3-Br   2,4-(CH 3 ) 2 -3-OCHF 2     187-189       285   i-C 3 H 7     H   H   3-Br   2,3-(CH 3 ) 2 -4-OCH 3     206-208       286   i-C 3 H 7     H   H   3-Br   2-Cl-4-OCF 3     165-167       287   i-C 3 H 7     H   H   3-Br   2-Br-4-OCF 3     179-180       288   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCHF 2     205-207       289   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCF 3     211-213       290   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCBrF 2     178-180       291   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCF 2 CHFCF 3     196-197       292   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCF 2 CHClF   194-195       293   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCF 2 CHF 2     205-207       294   i-C 3 H 7     H   H   3-Br   2-CH 3 -3-Cl-4-OCHF 2     229-230       295   i-C 3 H 7     H   H   3-Br   2,3-(CH 3 ) 2 -4-OCHF 2     219-220       296   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-SCH 3     215-217       297   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-(3-CF 3 -PhO)   156-158       298   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-(3-Cl-   206-208                           5-CF 3 -2-Pyi-O)       299   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-(5-CF 3 -   182-184                           2-Pyi-O)       300   i-C 3 H 7     H   H   3-Br   -3-OCH 2 O-4-   195-198       301   i-C 3 H 7     H   H   6-Br   4-CF 3     190-192       302   i-C 3 H 7     H   H   6-Br   4-OCF 3     210-212       303   i-C 3 H 7     H   H   6-Br   2,3-(CH 3 ) 2     250-252       304   i-C 3 H 7     H   H   6-Br   2,4,6-(CH 3 ) 3     272-274       305   i-C 3 H 7     H   H   6-Br   2-CH 3 -3-Cl   214-216       306   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-Cl   198-200       307   i-C 3 H 7     H   H   6-Br   2-CH 3 -5-Cl   194-196       308   i-C 3 H 7     H   H   6-Br   2,3-(CH 3 ) 2 -4-Cl   227-229       309   i-C 3 H 7     H   H   6-Br   2,4-(CH 3 ) 2 -3-Cl   249-251       310   i-C 3 H 7     H   H   6-Br   2-C 2 H 5 -4-Cl   243-245       311   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-Br   227-228       312   i-C 3 H 7     H   H   6-Br   2,3-(CH 3 ) 2 -4-Br   209-211       313   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-I   227-229       314   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-F   231-232       315   i-C 3 H 7     H   H   6-Br   2-Cl-4-CF 3     169-170       316   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-CF 3     232-234       317   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-CF(CF 3 ) 2     236-238       318   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-(CF 2 ) 3 CF 3     208-210       319   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCH 2 CF 2 CHF 2     209-211       320   i-C 3 H 7     H   H   6-Br   2,4-(CH 3 ) 2 -3-OCHF 2     247-249       321   i-C 3 H 7     H   H   6-Br   2,3-(CH 3 ) 2 -4-OCH 3     250-252       322   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCH 3     220-222       323   i-C 3 H 7     H   H   6-Br   2-Cl-4-OCF 3     182-183       324   i-C 3 H 7     H   H   6-Br   2-Br-4-OCF 3     195-196       325   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCHF 2     225-226       326   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCF 3     223-225       327   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCBrF 2     194-196       328   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCF 2 CHFCF 3     212-213       329   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCF 2 CHClF   211-213       330   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-OCF 2 CHF 2     214-215       331   i-C 3 H 7     H   H   6-Br   2,3-(CH 3 ) 2 -4-OCHF 2     228-229       332   i-C 3 H 7     H   H   6-Br   2-CH 3 -3-Cl-4-OCHF 2     224-225       333   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-SCH 3     215-217       334   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-(3-CF 3 -PhO)   194-195       335   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-(5-CF 3 -   201-203                           2-Pyi-O)       336   i-C 3 H 7     H   H   6-Br   2-CH 3 -4-(3-Cl-5-   234-236                           CF 3 -2-Pyi-O)       337   i-C 3 H 7     H   H   6-Br   -3-OCH 2 O-4-   205-207       338   i-C 3 H 7     H   H   3,4-Br 2     2-CH 3 -4-OCHF 2     196-197       339   i-C 3 H 7     H   H   3,4-Br 2     2-CH 3 -4-Cl   199-201       340   i-C 3 H 7     H   H   3,6-Br   2-CH 3 -4-OCHF 2     233-234       341   i-C 3 H 7     H   H   3,6-Br 2     2-CH 3 -4-Cl   245-247       342   i-C 3 H 7     H   H   5,6-Br 2     2-CH 3 -4-OCHF 2     208-210       343   i-C 3 H 7     H   H   5,6-Br 2     2-CH 3 -4-Cl   259-261       344   i-C 3 H 7     H   H   3,4,5,6-Br 4     2-CH 3 -4-Cl   270-272       345   i-C 3 H 7     H   H   3-I   4-Cl   230-232       346   i-C 3 H 7     H   H   3-I   4-Br   251-253       347   i-C 3 H 7     H   H   3-I   4-I   231-233       348   i-C 3 H 7     H   H   3-I   3-CF 3     194-197       349   i-C 3 H 7     H   H   3-I   4-CF 3     223-224       350   i-C 3 H 7     H   H   3-I   4-CF 2 CF 2 CF 3     217-219       351   i-C 3 H 7     H   H   3-I   4-CF(CF 3 ) 2     209-211       352   i-C 3 H 7     H   H   3-I   4-OCF 3     222-223       353   i-C 3 H 7     H   H   3-I   4-OCF 2 CHFOCF 3     192-194       354   i-C 3 H 7     H   H   3-I   4-SCHF 2     204-206       355   i-C 3 H 7     H   H   3-I   4-SCH 2 CF 3     195-197       356   i-C 3 H 7     H   H   3-I   4-SCF 2 CHF 2     196-198       357   i-C 3 H 7     H   H   3-I   4-SCF 2 CBrF 2     203-205       358   i-C 3 H 7     H   H   3-I   4-SCF(CF 3 ) 2     170-172       359   i-C 3 H 7     H   H   3-I   4-S(CF 2 ) 3 CF 3     185-187       360   i-C 3 H 7     H   H   3-I   3,4-F 2     227-229       361   i-C 3 H 7     H   H   3-I   2-CH 3 -3-Cl   222-224       362   i-C 3 H 7     H   H   3-I   2-CH 3 -4-Cl   215-217       363   i-C 3 H 7     H   H   3-I   2-CH 3 -5-Cl   210-212       364   i-C 3 H 7     H   H   3-I   2,4-(CH 3 ) 2 -3-Cl   226-228       365   i-C 3 H 7     H   H   3-I   2,3-(CHa) 2 -4-Cl   235-237       366   i-C 3 H 7     H   H   3-I   2-CH 3 -4-Br   227-229       367   i-C 3 H 7     H   H   3-I   2-CH 3 -4-I   201-203       368   i-C 3 H 7     H   H   3-I   2-CH 3 -4-F   227-228       369   i-C 3 H 7     H   H   3-I   2-Cl-4-CF 3     170-171       370   i-C 3 H 7     H   H   3-I   2-CH 3 -3-CF 3     179-181       371   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF 3     202-203       372   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF 2 CF 3     195-196       373   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF 2 CF 2 CF 3     193-195       374   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF(CF 3 ) 2     211-213       375   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(CF 2 ) 3 CF 3     203-204       376   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCH 3     204-206       377   i-C 3 H 7     H   H   3-I   2-CH 3 -4-O-C 3 H 7 -i   209-211       378   i-C 3 H 7     H   H   3-I   2,3-(CH 3 ) 2 -4-OCH 3     220-222       379   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCH 2 CF 3     223-224       380   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CBrF 2     228-230       381   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CCl 2 F   230-231       382   i-C 3 H 7     H   H   3-I   3-F-4-OCHF 2     208-210       383   i-C 3 H 7     H   H   3-I   3,5-Cl 2 -4-OCHF 2     234-236       384   i-C 3 H 7     H   H   3-I   3-OCH 3 -4-OCHF 2     196-198       385   i-C 3 H 7     H   H   3-I   3,4-(OCHF 2 ) 2     171-172       386   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 3     214-216       387   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCHF 2     207-209       388   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCH 2 CF 2 CHF 2     229-231       389   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCBrF 2     181-182       390   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CHF 2     197-199       391   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CHF 2 -5-Cl   198-200       392   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CHClF   200-201       393   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CHFCF 3     213-214       394   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CBrFCF 3     233-234       395   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CHFOCF 3     213-215       396   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCHF 2 -5-Cl   230-232       397   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(F 5 -PhO)   245-247       398   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(3-CF 3 -PhO)   168-170       399   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(5-CF 3 -2-   186-188                           Pyi-O)       400   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(3-Cl-5-CF 3 -   212-214                           2-Pyi-O)       401   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SO 2 CH 3     172-175       402   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SC 3 H 7 -i   190-192       403   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SCF 2 CF 2 CF 3     227-228       404   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(4-Cl-PhS)   191-192       405   i-C 3 H 7     H   H   3-I   4-(3-Cl-5-CF 3 -2-Pyi-S)   198-200       406   i-C 3 H 7     H   H   3-I   2-Br-4-OCF 3     196-198       407   i-C 3 H 7     H   H   3-I   2-Cl-4-CF 2 CF 2 CF 3     162-164       408   i-C 3 H 7     H   H   3-I   2-Cl-4-OCF 3     173-175       409   i-C 3 H 7     H   H   3-I   2-CF 3 -4-OCHF 2     219-220       410   i-C 3 H 7     H   H   3-I   3-CF 3 -4-OCHF 2     128-130       411   i-C 3 H 7     H   H   6-I   4-Cl   251-253       412   i-C 3 H 7     H   H   6-I   4-Br   270-272       413   i-C 3 H 7     H   H   6-I   4-I   242-244       414   i-C 3 H 7     H   H   6-I   3-CF 3     210-212       415   i-C 3 H 7     H   H   6-I   4-CF 3     201-202       416   i-C 3 H 7     H   H   6-I   4-CF(CF 3 ) 2     238-240       417   i-C 3 H 7     H   H   6-I   4-CF 2 CF 2 CF 3     -   238-240       418   i-C 3 H 7     H   H   6-I   4-OCF 3     193-194       419   i-C 3 H 7     H   H   6-I   4-OCF 2 CHFOC 3 F 7 -n   213-214       420   i-C 3 H 7     H   H   6-I   4-SCH 2 CF 3     217-219       421   i-C 3 H 7     H   H   6-I   4-SCHF 2     224-226       422   i-C 3 H 7     H   H   6-I   4-SCF 2 CHF 2     213-215       423   i-C 3 H 7     H   H   6-I   4-SCF 2 CBrF 2     220-222       424   i-C 3 H 7     H   H   6-I   4-SCF 2 CF 2 CF 3     196-197       425   i-C 3 H 7     H   H   6-I   4-SCF(CF 3 ) 2     216-218       426   i-C 3 H 7     H   H   6-I   4-S(CF 2 ) 3 CF 3     201-203       427   i-C 3 H 7     H   H   6-I   2-CH 3 -3-Cl   252-254       428   i-C 3 H 7     H   H   6-I   2-CH 3 -4-Cl   244-246       429   i-C 3 H 7     H   H   6-I   2,4-(CH 3 ) 2 -3-Cl   260-262       430   i-C 3 H 7     H   H   6-I   2-CH 3 -4-Br   241-243       431   i-C 3 H 7     H   H   6-I   2-CH 3 -4-I   213-215       432   i-C 3 H 7     H   H   6-I   2-CH 3 -4-F   251-252       433   i-C 3 H 7     H   H   6-I   2-Cl-4-CF 3     195-196       434   i-C 3 H 7     H   H   6-I   2,3-(CH 3 ) 2 -4-Cl   253-255       435   i-C 3 H 7     H   H   6-I   2-CH 3 -3-CF 3     245-251       436   i-C 3 H 7     H   H   6-I   2-CH 3 -4-CF 3     220-221       437   i-C 3 H 7     H   H   6-I   2-CH 3 -4-CF 2 CF 3     203-206       438   i-C 3 H 7     H   H   6-I   2-CH 3 -4-CF 2 CF 2 CF 3     154-156       439   i-C 3 H 7     H   H   6-I   2-CH 3 -4-CF(CF 3 ) 2     237-239       440   i-C 3 H 7     H   H   6-I   2-CH 3 -4-(CF 2 ) 3 CF 3     168-170       441   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCH 3     215-217       442   i-C 3 H 7     H   H   6-I   2-CH 3 -4-O-C 3 H 7 -i   212-214       443   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCH 2 CF 3     233-234       444   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CBrF 2     242-244       445   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CCl 2 F   251-253       446   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CBrFCF 3     251-253       447   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCH 2 CF 2 CHF 2     235-237       448   i-C 3 H 7     H   H   6-I   3-F-4-OCHF 2     214-216       449   i-C 3 H 7     H   H   6-I   3,5-Cl 2 -4-OCHF 2     211-213       450   i-C 3 H 7     H   H   6-I   3-OCH 3 -4-OCHF 2     215-217       451   i-C 3 H 7     H   H   6-I   2,3-(CH 3 ) 2 -4-OCH 3     253-254       452   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCBrF 2     192-194       453   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CHF 2     216-218       454   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CHF 2 -5-Cl   230-232       455   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CHClF   205-207       456   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CHFCF 3     222-223       457   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 CHFOCF 3     258-260       458   i-C 3 H 7     H   H   6-I   2-CH 3 -4-(3-CF 3 -PhO)   198-199       459   i-C 3 H 7     H   H   6-I   2-CH 3 -4-(F5PhO)   262-264       460   i-C 3 H 7     H   H   6-I   2-CH 3 -4-(5-CF 3 -2-Pyi-O)   245-246       461   i-C 3 H 7     H   H   6-I   2-CH 3 -4-(3-Cl-   231-232                           5-CF 3 -2-Pyi-O)       462   i-C 3 H 7     H   H   6-I   2-CH 3 -4-SC 3 H 7 -i   197-199       463   i-C 3 H 7     H   H   6-I   2-CH 3 -4-(4-Cl-PhS)   211-213       464   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 3     230-232       465   i-C 3 H 7     H   H   6-I   2-Cl-4-OCHF 2     238-239       466   i-C 3 H 7     H   H   6-I   2-Br-4-OCFs   215-217       467   i-C 3 H 7     H   H   6-I   2-Cl-4-OCF 3     186-188       468   i-C 3 H 7     H   H   6-I   2-Cl-4-CF 2 CF 2 CF 3     199-200       469   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCHF 2     226-228       470   i-C 3 H 7     H   H   6-I   2-CH 3 -4-OCHF 2 -5-Cl   239-240       471   i-C 3 H 7     H   H   6-I   3-CF 3 -4-OCHF 2     238-239       472   i-C 3 H 7     H   H   3-F   4-(CF 2 ) 3 CF 3     187-188       473   i-C 3 H 7     H   H   3-F   4-CF 2 CF 2 CF 3     182-183       474   i-C 3 H 7     H   H   3-F   4-CF(CF 3 ) 2     206-208       475   i-C 3 H 7     H   H   3-F   4-OCF 3     197-199       476   i-C 3 H 7     H   H   3-F   4-OCF 2 CHFOC 3 F 7 -n   142-144       477   i-C 3 H 7     H   H   3-F   4-SCHF 2     190-192       478   i-C 3 H 7     H   H   3-F   4-SCH 2 CF 3     157-158       479   i-C 3 H 7     H   H   3-F   4-SCF 2 CHF 2     177-178       480   i-C 3 H 7     H   H   3-F   4-SCF 2 CBrF 2     197-199       481   i-C 3 H 7     H   H   3-F   4-SCF(CF 3 ) 2     206-208       482   i-C 3 H 7     H   H   3-F   4-S(CF 2 ) 3 CF 3     173-174       483   i-C 3 H 7     H   H   3-F   4-SOCH 2 CF 3     115-119       484   i-C 3 H 7     H   H   3-F   4-SOCF 2 CBrF 2     181-182       485   i-C 3 H 7     H   H   3-F   4-SOCF(CF 3 ) 2     195-197       486   i-C 3 H 7     H   H   3-F   4-SO(CF 2 ) 3 CF 3     175-176       487   i-C 3 H 7     H   H   3-F   4-SO 2 CH 2 CF 3     199-202       488   i-C 3 H 7     H   H   3-F   2,3-Cl 2     175-177       489   i-C 3 H 7     H   H   3-F   2-CH 3 -3-Cl   193-194       490   i-C 3 H 7     H   H   3-F   2-CH 3 -4-Cl   192-194       491   i-C 3 H 7     H   H   3-F   2-CH 3 -5-Cl   191-193       492   i-C 3 H 7     H   H   3-F   2-CH 3 -4-I   192-194       493   i-C 3 H 7     H   H   3-F   2-CH 3 -5-F   175-177       494   i-C 3 H 7     H   H   3-F   2-CH 3 -3-F   187-189       495   i-C 3 H 7     H   H   3-F   2-CH 3 -4-CF 2 CF 3     213-214       496   i-C 3 H 7     H   H   3-F   2-CH 3 -4-CF 2 CF 2 CF 3     191-192       497   i-C 3 H 7     H   H   3-F   2-CH 3 -4-CF(CF 3 ) 2     241-243       498   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(CF 2 ) 3 CF 3     138-139       499   i-C 3 H 7     H   H   3-F   2-CH 3 -3-OCHF 2     172-174       500   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCHF 2     160-162       501   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CCl3   162-163       502   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CCl 2 F   207-208       503   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CBrF 2     196-197       504   i-C 3 H 7     H   H   3-F   2-Cl-4-CF 3     169-170       505   i-C 3 H 7     H   H   3-F   2-Cl-4-CF 2 CF 2 CF 3     169-170       506   i-C 3 H 7     H   H   3-F   3,5-Cl 2 -4-OCHF 2     201-202       507   i-C 3 H 7     H   H   3-F   2-Cl-4-CF(CF 3 ) 2     223-225       508   i-C 3 H 7     H   H   3-F   2-Cl-4-OCF 3     169-170       509   i-C 3 H 7     H   H   3-F   2-Br-4-OCF 3     164-165       510   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 3     183-184       511   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCBrF 2     177-178       512   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CHF 2     172-173       513   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CHClF   168-169       514   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CHFCF 3     160-162       515   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CHFOCF 3     148-150       516   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CBrFCF 3     148-150       517   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCHF 2 -5-Cl   187-188       518   i-C 3 H 7     H   H   3-F   2-CH 3 -4-SC 3 H 7 -i   165-167       519   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(3-CF 3 -PhO)   135-136       520   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(F5-PhO)   206-207       521   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(2-Cl-4-   215-217                           CF 3 -PhO)       522   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(4-Cl-PhS)   176-178       523   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(5-CF 3 -2-Pyi-O)   175-176       524   i-C 3 H 7     H   H   3-F   2-CH 3 -4-(3-Cl-   188-190                           5-CF 3 -2-Pyi-O)       525   i-C 3 H 7     H   H   3-F   4-(3-Cl-5-CF 3 -2-Pyi-S)   213-215       526   i-C 3 H 7     H   H   3-F   2-CHS-4-OP═S(OCH 3 ) 2     175-177       527   i-C 3 H 7     H   H   3-F   2-CF 3 -4-OCHF 2     180-182       528   i-C 3 H 7     H   H   3-F   -3-OCH 2 O-4-   197-199       529   i-C 3 H 7     H   H   4-F   2-CH 3 -4-Cl   217-218       530   i-C2H7   H   H   4-F   2-CH 3 -5-Cl   202-203       531   i-C 3 H 7     H   H   4-F   2-CH 3 -4-OCHF 2     191-193       532   i-C 3 H 7     H   H   5-F   2-CH 3 -4-Cl   197-198       533   i-C 3 H 7     H   H   5-F   2-CH 3 -4-CF 2 CF 2 CF 3     213-215       534   i-C 3 H 7     H   H   5-F   2-CH 3 -4-OCHF 2     181-182       535   i-C 3 H 7     H   H   6-F   4-CF 2 CF 2 CF 3     201-202       536   i-C 3 H 7     H   H   6-F   4-(CF 2 ) 3 CF 3     156-158       537   i-C 3 H 7     H   H   6-F   4-OCF 3     212-214       538   i-C 3 H 7     H   H   6-F   4-OCF 2 CHFOC 3 F 7 -n   178-180       539   i-C 3 H 7     H   H   6-F   4-SCH 2 CF 3     176-178       540   i-C 3 H 7     H   H   6-F   4-SCF 2 CHF 2     230-232       541   i-C 3 H 7     H   H   6-F   4-SCF(CF 3 ) 2     218-220       542   i-C 3 H 7     H   H   6-F   4-S(CF 2 ) 3 CF 3     178-181       543   i-C 3 H 7     H   H   6-F   2,3-Cl 2     158-160       544   i-C 3 H 7     H   H   6-F   2-CH 3 -3-Cl   182-184       545   i-C 3 H 7     H   H   6-F   2-CH 3 -4-Cl   204-206       546   i-C 3 H 7     H   H   6-F   2-CH 3 -5-Cl   196-199       547   i-C 3 H 7     H   H   6-F   2-CH 3 -4-I   213-215       548   i-C 3 H 7     H   H   6-F   2-CH 3 -3-F   165-167       549   i-C 3 H 7     H   H   6-F   2-CH 3 -5-F   181-183       550   i-C 3 H 7     H   H   6-F   2-Cl-4-CF 3     190-191       551   i-C 3 H 7     H   H   6-F   2-CH 3 -4-CF 2 CF 3     222-223       552   i-C 3 H 7     H   H   6-F   2-CH 2 -4-OCF 2 CCl3   184-185       553   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CCl 2 F   214-215       554   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CBrF 2     208-210       555   i-C 3 H 7     H   H   6-F   2-CH 3 -4-CF 2 CF 2 CF 3     168-170       556   i-C 3 H 7     H   H   6-F   2-CH 3 -4-CF(CF 3 ) 2     255-257       557   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(CF 2 ) 3 CF 3     157-159       558   i-C 3 H 7     H   H   6-F   2-CH 3 -3-OCHF 2     177-179       559   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCHF 2     176-178       560   i-C 3 H 7     H   H   6-F   3,5-Cl 2 -4-OCHF 2     198-200       561   i-C 3 H 7     H   H   6-F   2-Cl-4-CF(CF 3 ) 2     241-243       562   i-C 3 H 7     H   H   6-F   2-Cl-4-OCF 3     171-172       563   i-C 3 H 7     H   H   6-F   2-Br-4-OCF 3     181-182       564   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 3     193-195       565   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCBrF 2     181-183       566   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CHF 2     185-187       567   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CHClF   175-176       568   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CHFCF 3     176-178       569   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CBrFCF 3     217-219       570   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCF 2 CHFOCF 3     183-185       571   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OCHF 2 -5-Cl   209-211       572   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(3-CF 3 -PhO)   184-185       573   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(F 5 -PhO)   227-228       574   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(2-Cl-4-CF 3 -PhO)   220-222       575   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(4-Cl-PhS)   190-193       576   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(5-CF 3 -2-Pyi-O)   206-207       577   i-C 3 H 7     H   H   6-F   2-CH 3 -4-(3-Cl-   177-179                           5-CF 3 -2-Pyi-O)       578   i-C 3 H 7     H   H   6-F   2-CH 3 -4-OP═S(OCH 3 ) 2     188-190       579   i-C 3 H 7     H   H   6-F   2-CF 3 -4-OCHF 2 -   223-225       580   i-C 3 H 7     H   H   6-F   3-OCH 2 O-4-   201-203       581   i-C 3 H 7     H   H   3,6-F 2     2-CH 3 -4-OCHF 2     203-204       582   i-C 3 H 7     H   H   3,6-F 2     2-CH 3 -4-Cl   221-222       583   i-C 3 H 7     H   H   3,4,5,6-F 4     2-CH 3 -5-Cl   189-191       584   i-C 3 H 7     H   H   3-NO 2     2,3-Cl 2     201-203       585   i-C 3 H 7     H   H   3-NO 2     H   236-238       586   i-C 3 H 7     H   H   3-NO 2     2-Cl   190-192       587   i-C 3 H 7     H   H   3-NO 2     3-Cl   227-229       588   i-C 3 H 7     H   H   3-NO 2     4-Cl   238-240       589   i-C 3 H 7     H   H   3-NO 2     2-Br   170-172       590   i-C 3 H 7     H   H   3-NO 2     3-Br   196-198       591   i-C 3 H 7     H   H   3-NO 2     4-Br   205-207       592   i-C 3 H 7     H   H   3-NO 2     2-F   199-201       593   i-C 3 H 7     H   H   3-NO 2     3-F   228-230       594   i-C 3 H 7     H   H   3-NO 2     4-F   250-252       595   i-C 3 H 7     H   H   3-NO 2     4-I   187-189       596   i-C 3 H 7     H   H   3-NO 2     4-NO 2     201-203       597   i-C 3 H 7     H   H   3-NO 2     3-CN   220-222       598   i-C 3 H 7     H   H   3-NO 2     4-CN   226-228       599   i-C 3 H 7     H   H   3-NO 2     2-CH 3     227-228       600   i-C 3 H 7     H   H   3-NO 2     3-CH 3     195-197       601   i-C 3 H 7     H   H   3-NO 2     4-CH 3     196-198       602   i-C 3 H 7     H   H   3-NO 2     2-C 2 H 5     189-191       603   i-C 3 H 7     H   H   3-NO 2     2-C 3 H 7 -i   190-192       604   i-C 3 H 7     H   H   3-NO 2     4-C 3 H 7 -i   221-223       605   i-C 3 H 7     H   H   3-NO 2     4-C 4 H 9 -n   193-195       606   i-C 3 H 7     H   H   3-NO 2     4-CF 3     192-194       607   i-C 3 H 7     H   H   3-NO 2     3-CF 3     220-222       608   i-C 3 H 7     H   H   3-NO 2     2-CF 3     215-217       609   i-C 3 H 7     H   H   3-NO 2     4-CF 2 CF 2 CF 3     184-185       610   i-C 3 H 7     H   H   3-NO 2     4-CF(CF 3 ) 2     243-244       611   i-C 3 H 7     H   H   3-NO 2     4-(CF 2 ) 3 CF 3     220-221       612   i-C 3 H 7     H   H   3-NO 2     2-OCH 3     172-174       613   i-C 3 H 7     H   H   3-NO 2     3-OCH 3     201-203       614   i-C 3 H 7     H   H   3-NO 2     4-OCH 3     221-223       615   i-C 3 H 7     H   H   3-NO 2     3-O-C 3 H 7 -i   198-200       616   i-C 3 H 7     H   H   3-NO 2     3-OCHF 2     188-190       617   i-C 3 H 7     H   H   3-NO 2     4-OCHF 2     222-224       618   i-C 3 H 7     H   H   3-NO 2     4-OCF 2     234-236       619   i-C 3 H 7     H   H   3-NO 2     4-OCF 2 CHFOC 3 F 7 -n   138-140       620   i-C 3 H 7     H   H   3-NO 2     4-COOCH 3     192-194       621   i-C 3 H 7     H   H   3-NO 2     3-SCH 3     205-207       622   i-C 3 H 7     H   H   3-NO 2     2-SCH 3     201-203       623   i-C 3 H 7     H   H   3-NO 2     3-SCF 3     203-205       624   i-C 3 H 7     H   H   3-NO 2     4-SCH 2 CF 3     155-156       625   i-C 3 H 7     H   H   3-NO 2     4-SCHF 2     183-185       626   i-C 3 H 7     H   H   3-NO 2     4-SCF 2 CHF 2     235-237       627   i-C 3 H 7     H   H   3-NO 2     4-SCF 2 CF 3     190-192       628   i-C 3 H 7     H   H   3-NO 2     4-SCF 2 CBrF 2     228-230       629   i-C 3 H 7     H   H   3-NO 2     4-SCF(CF 3 ) 2     242-243       630   i-C 3 H 7     H   H   3-NO 2     4-S(CF 2 ) 3 CF 3     229-230       631   i-C 3 H 7     H   H   3-NO 2     4-SO(CF 2 ) 3 CF 3     190-193       632   i-C 3 H 7     H   H   3-NO 2     4-O-Ph   228-230       633   i-C 3 H 7     H   H   3-NO 2     2,4-Cl 2     202-204       634   i-C 3 H 7     H   H   3-NO 2     2,5-Cl 2     230-232       635   i-C 3 H 7     H   H   3-NO 2     2,6-Cl 2     210-212       636   i-C 3 H 7     H   H   3-NO 2     3,4-Cl 2     227-229       637   i-C 3 H 7     H   H   3-NO 2     3,5-Cl 2     194-196       638   i-C 3 H 7     H   H   3-NO 2     2,3-F 2     184-186       639   i-C 3 H 7     H   H   3-NO 2     2,4-F 2     210-212       640   i-C 3 H 7     H   H   3-NO 2     2,5-F 2     191-193       641   i-C 3 H 7     H   H   3-NO 2     2,6-F 2     173-175       642   i-C 3 H 7     H   H   3-NO 2     3,4-F 2     241-243       643   i-C 3 H 7     H   H   3-NO 2     3-Cl-4-F   203-205       644   i-C 3 H 7     H   H   3-NO 2     2,3,4-Cl 3     203-205       645   i-C 3 H 7     H   H   3-NO 2     2,3,4-F 3     202-204       646   i-C 3 H 7     H   H   3-NO 2     2,3,4,5,6-F 5     192-194       647   i-C 3 H 7     H   H   3-NO 2     2,3-(CH 3 ) 2     200-202       648   i-C 3 H 7     H   H   3-NO 2     2,4-(CH 3 ) 2     201-203       649   i-C 3 H 7     H   H   3-NO 2     2,5-(CH 3 ) 2     221-223       650   i-C 3 H 7     H   H   3-NO 2     2,6-(CH 3 ) 2     234-236       651   i-C 3 H 7     H   H   3-NO 2     3,4-(CH 3 ) 2     195-197       652   i-C 3 H 7     H   H   3-NO 2     2,4,6-(CH 3 ) 3     229-231       653   i-C 3 H 7     H   H   3-NO 2     2,6-(C 2 H 5 ) 2     258-260       654   i-C 3 H 7     H   H   3-NO 2     3,5-(CF 3 ) 2     225-227       655   i-C 3 H 7     H   H   3-NO 2     3-Cl-4-CH 3     208-210       656   i-C 3 H 7     H   H   3-NO 2     2-Cl-4-CH 3     195-197       657   i-C 3 H 7     H   H   3-NO 2     2-F-4-Cl-5-CH 3     193-195       658   i-C 3 H 7     H   H   3-NO 2     3-Cl-4-OCHF 2     222-224       659   i-C 3 H 7     H   H   3-NO 2     3,5-Cl 2 -4-OCHF 2     218-220       660   i-C 3 H 7     H   H   3-NO 2     2-Cl-4-CF 3     217-219       661   i-C 3 H 7     H   H   3-NO 2     2-Cl-5-CF 3     193-195       662   i-C 3 H 7     H   H   3-NO 2     2,6-Cl 2 -4-CF 3     226-228       663   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-Cl   198-200       664   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-Cl   235-237       665   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -5-Cl   218-219       666   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -6-Cl   248-250       667   i-C 3 H 7     H   H   3-NO 2     2-C 2 H 5 -4-Cl   235-237       668   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4,5-Cl 2     196-198       669   i-C 3 H 7     H   H   3-NO 2     2,3-(CH 3 ) 2 -4-Cl   226-228       670   i-C 3 H 7     H   H   3-NO 2     2,4-(CH 3 ) 2 -3-Cl   203-205       671   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-Br   214-216       672   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -5-Br   191-193       673   i-C 3 H 7     H   H   3-O2   2-CH 3 -4-I   227-227       674   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-F   199-201       675   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-F   226-228       676   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -5-F   213-215       677   i-C 3 H 7     H   H   3-NO 2     2-C 2 H 5 -5-F   191-193       678   i-C 3 H 7     H   H   3-NO 2     3-CF 3 -4-Cl   215-217       679   i-C 3 H 7     H   H   3-NO 2     2-CF 3 -4-Cl   208-210       680   i-C 3 H 7     H   H   3-NO 2     3-CH 3 -4-Br   199-201       681   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-CF 3     221-222       682   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-CF 3     236-237       683   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-CF 2 CF 3     218-219       684   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-CF 2 CF 2 CF 3     188-189       685   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-CF(CF 3 ) 2     248-250       686   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(CF 2 ) 2 CFs   225-226       687   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-OCH 3     198-200       688   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCH 3     208-210       689   i-C 3 H 7     H   H   3-NO 2     2,3-(CH 3 ) 2 -4-OCH 3     253-255       690   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-O-C 3 H 7 -i   233-234       691   i-C 3 H 7     H   H   3-NO 2     3-CF 2 -5-OCH 3     214-216       692   i-C 3 H 7     H   H   3-NO 2     2-CF 3 -4-OCHF 2     201-203       693   i-C 3 H 7     H   H   3-NO 2     3-CF 3 -4-OCHF 2     231-232       694   i-C 3 H 7     H   H   3-NO 2     2,4-(CH 3 ) 2 -3-OCH 3     201-203       695   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-OCHF 2     200-202       696   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCHF 2     186-188       697   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCH 2 CF 3     241-243       698   i-C3Hr   H   H   3-NO 2     2-CH 3 -4-OCF 2 CBrF 2     229-230       699   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCH 2 CF 2 CHF 2     199-200       700   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CBrFCF 3     224-226       701   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCH 2 CHFOCF 3     208-210       702   i-C 3 H 7     H   H   3-NO 2     3-OCH 3 -4-OCHF 2     242-243       703   i-C 3 H 7     H   H   3-NO 2     2-Cl-4-CF(CF 3 ) 2     198-200       704   i-C 3 H 7     H   H   3-NO 2     2-Cl-4-OCF 3     188-190       705   i-C 3 H 7     H   H   3-NO 2     2-Br-4-OCF 3     202-203       706   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-NO 2     201-203       707   i-C 3 H 7     H   H   3-NO 2     2-Cl-5-NO 2     193-195       708   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -5-NO 2     197-199       709   i-C 3 H 7     H   H   3-NO 2     2,3-(CH 3 ) 2 -4-NO 2     207-209       710   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 3     184-186       711   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCBrF 2     217-218       712   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CHF 2     205-207       713   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-OCF 2 CHClF   164-166       714   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CHClF   192-193       715   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CCl 2 F   212-213       716   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CHFCF 3     198-199       717   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -3-Cl-4-OCHF 2     236-238       718   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CHF 2 -5-Cl   233-234       719   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-SCH 3     214-216       720   i-C 3 H 7     H   H   3-NO 2     2,3-(CH 3 ) 2 -4-SCH 3     254-256       721   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-SC 3 H 7 -i   209-211       722   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-SCHF 2     225-227       723   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-N(CH 3 ) 2     215-217       724   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(3-CF 3 -PhO)   174-175       725   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(F-5-PhO)   242-244       726   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(2-Cl-   191-192                           4-CF 3 -PhO)       727   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(4-Cl-PhS)   165-167       728   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(5-CF 3 -   216-218                           2-Pyi-O)       729   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-(3-Cl-   236-238                           5-CF 3 -2-Pyi-O)       730   i-C 3 H 7     H   H   3-NO 2     4-(3-Cl-5-CF 3 -   190-192                           2-Pyi-S)       731   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-P═O(OC 2 H 5 ) 2     128-130       732   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-P═S(OCH 3 ) 2     128-130       733   i-C 3 H 7     H   H   3-NO 2     3-OCH 2 O-4-   229-231       734   i-C 3 H 7     H   H   3-NO 2     3-CH 2 CH 2 CH 2 -4   209-211       735   i-C 3 H 7     H   H   3-NO 2     2-CH 2 CH 2 CH 2 -3   226-228       736   i-C 3 H 7     H   H   3-NO 2     3-N═C(CF 3 )-NH-4   162-164       737   i-C 3 H 7     H   H   3-NO 2     3-N═C(CF 3 )-N(CH 3 )-4   186-188       738   i-C 3 H 7     H   H   5-NO 2     2-CH 3 -5-Cl   226-228       739   i-C 3 H 7     H   H   6-NO 2     2-CH 3 -5-Cl   247-249       740   i-C 3 H 7     H   H   6-NO 2     2-Cl-4-CF 3     Crystals       741   i-C 3 H 7     H   H   6-NO 2     2-Cl-4-CF 2 CF 2 CF 3     192-193       742   i-C 3 H 7     H   H   6-NO 2     2-CH 3 -4-CF 3     239-240       743   i-C 3 H 7     H   H   6-NO 2     2-CH 3 -4-OCF 2 CHFCF 2     252-253       744   i-C 3 H 7     H   H   3-CN   2-CH 3 -4-Cl   162-164       745   i-C 3 H 7     H   H   6-CN   2-CH 3 -4-Cl   Crystals       749   i-C 3 H 7     H   H   3-CH 3     4-OCF 3     180-182       750   i-C 3 H 7     H   H   3-CH 3     2-CH 3 -4-Cl   169-171       751   i-C 3 H 7     H   H   3-OH3   2-CH 3 -4-OCHF 2     192-193       752   i-C 3 H 7     H   H   5-CH 3     2-CH 3 -5-Cl   193-195       753   i-C 3 H 7     H   H   6-C 2 H 5     2-CH 3 -4-Cl   180-182       754   i-C 3 H 7     H   H   3-CF 3     H   202-204       755   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -5-Cl   196-198       756   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -3-Cl   216-218       757   i-C 3 H 7     H   H   3-CF 3     2,6-(C 2 H 5 ) 2     238-239       758   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-Cl   207-209       759   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-OCHF 2     212-213       760   i-C 3 H 7     H   H   5-CF 3     2,6-(C 2 H 5 ) 2     240-241       761   i-C 3 H 7     H   H   5-CF 3     2-CH 3 -4-Cl   203-205       762   i-C 3 H 7     H   H   5-CF 3     3-CF 3 -5-OCH 3     209-210       763   i-C 3 H 7     H   H   5-CF 3     2-CH 3 -4-OCHF 2     196-197       764   i-C 3 H 7     H   H   6-CF 3     H   152-154       765   i-C 3 H 7     H   H   6-CF 3     2-CH 3 -3-Cl   158-160       766   i-C 3 H 7     H   H   6-CF 3     2-CH 3 -5-Cl   273-275       767   i-C 3 H 7     H   H   3-OCH 3     4-OCF 3     178-180       768   i-C 3 H 7     H   H   3-OCH 3     2-CH 3 -4-Br   214-215       769   i-C 3 H 7     H   H   6-OCH 3     4-OCF 3     189-190       770   i-C 3 H 7     H   H   6-OCH 3     2-CH 3 -5-Cl   155-157       771   i-C 3 H 7     H   H   6-OCH 3     2-CH 2 -4-Br   195-197       772   i-C 3 H 7     H   H   3-OCHF 2     2-CH 3 -4-Cl   212-213       773   i-C 3 H 7     H   H   3-OCHF 2     2-CH 3 -5-Cl   198-200       774   i-C 3 H 7     H   H   3-OCHF 2     2-CH 3 -4-OCHF 2     174-175       775   i-C 3 H 7     H   H   4-OCHF 2     2-CH 3 -5-Cl   215-217       776   i-C 3 H 7     H   H   5-OCHF 2     2-CH 3 -5-Cl   173-175       777   i-C 3 H 7     H   H   6-OCHF 2     2-CH 3 -4-Cl   224-226       778   i-C 3 H 7     H   H   6-OCHF 2     2-CH 3 -5-Cl   191-193       779   i-C 3 H 7     H   H   6-OCHF 2     2-CH 3 -4-OCHF 2     199-200       780   i-C 3 H 7     H   H   3-SCH 3     2-CH 3 -3-Cl   191-193       781   i-C 3 H 7     H   H   3-SCH 3     2-CH 3 -4-Cl   188-190       782   i-C 3 H 7     H   H   3-SCH 3     2-CH 3 -4-Br   185-187       783   i-C 3 H 7     H   H   3-SCH 3     2-CH 3 -4-OCHF 2     159-161       784   i-C 3 H 7     H   H   6-SCH 3     2-CH 3 -4-Br   201-202       785   i-C 3 H 7     H   H   6-SCH 3     2-CH 3 -3-Cl   207-209       786   i-C 3 H 7     H   H   6-SCH 3     2-CH 3 -4-Cl   204-206       787   i-C 3 H 7     H   H   6-SCH 3     2-CH 3 -4-OCHF 2     212-214       788   i-C 3 H 7     H   H   3-SC 3 H 7 -i   2-CH 3 -4-Cl   183-184       789   i-C 3 H 7     H   H   6-SC 3 H 7 -i   2-CH 3 -4-Cl   228-229       790   i-C 3 H 7     H   H   3-SOCH 3     2-CH 3 -4-Br   125-130       791   i-C 3 H 7     H   H   3-SOCH 3     2-CH 3 -4-OCHF 2     215-217       792   i-C 3 H 7     H   H   6-SOCH 3     2-CH 3 -4-Br   203-208       793   i-C 3 H 7     H   H   3-SOC 3 H 7 -i   2-CH 3 -4-Cl   157-160       794   i-C 3 H 7     H   H   6-SOC 3 H 7 -i   2-CH 3 -4-Cl   170-173       795   i-C 3 H 7     H   H   3-SO 2 CH 3     2-CH 3 -4-OCHF 2     211-213       796   i-C 3 H 7     H   H   3-SO 2 C 3 H 7 -i   2-CH 3 -4-Cl   240-242       797   i-C 3 H 7     H   H   3-SCH 2 CF 3     2-CH 3 -4-OCHF 2     184-186       798   i-C 3 H 7     H   H   6-SCH 2 CF 3     2-CH 3 -4-OCHF 2     239-241       799   i-C 3 H 7     H   H   3-SOCH 2 CF 3     2-CH 3 -4-OCHF 2     198-200       800   i-C 3 H 7     H   H   6-SOCH 2 CF 3     2-CH 3 -4-OCHF 2     238-240       801   i-C 3 H 7     H   H   6-C≡CH   2-CH 3 -4-Cl   253-255       802   i-C 3 H 7     H   H   6-COOCH 3     2-CH 3 -4-Cl   149-151       803   i-C 3 H 7     H   H   3-CONHC 3 H 7 -i   2-CH 3 -4-Cl   187-189       804   i-C 3 H 7     H   H   6-CONHC 3 H 7 -i   2-CH 3 -4-Cl   191-193       807   i-C 3 H 7     H   H   3-Ph   2-CH 3 -4-Cl   228-229       808   i-C 3 H 7     H   H   6-Ph   4-OCF 3     213-214       809   i-C 3 H 7     H   H   6-Ph   2-CH 3 -4-Cl   254-256       810   i-C 3 H 7     H   H   3-O-Ph   2-CH 3 -4-OCHF 2     175-177       811   i-C 3 H 7     H   H   6-O-Ph   2-CH 3 -4-OCHF 2     194-196       812   i-C 3 H 7     H   H   3-(4-Cl-PhO)   2-CH 3 -4-Br   204-206       813   i-C 3 H 7     H   H   3-S—Ph   2-CH 3 -4-Cl   204-206       814   i-C 3 H 7     H   H   3-S—Ph   2-CH 3 -4-Br   193-194       815   i-C 3 H 7     H   H   6-S—Ph   2-CH 3 -4-Cl   211-213       816   i-C 3 H 7     H   H   6-S—Ph   2-CH 3 -4-Br   193-194       817   i-C 3 H 7     H   H   3-SO—Ph   2-CH 3 -4-Cl   201-203       818   i-C 3 H 7     H   H   3-SO 2 —Ph   2-CH 3 -4-Cl   189-191       819   i-C 3 H 7     H   H   3-CH═CH—CH═CH-4   2-CH 3 -4-OCHF 2     158-160       820   i-C 3 H 7     H   H   5-CH═CH—CH═CH-6   2-CH 3 -4-OCHF 2     154-155       821   i-C 3 H 7     H   H   3-CH═CH—CH═CH-4   2-CH 3 -5-Cl   156-158       822   i-C 3 H 7     H   H   4-CH═CH—CH═CH-5   2-CH 3 -5-Cl   229-231       823   i-C 3 H 7     H   H   5-CH═CH—CH═CH-6   2-CH 3 -5-Cl   232-234       824   i-C 3 H 7     CH 3     H   H   4-CF 3     178-180       825   i-C 3 H 7     CH 3     H   3-NO 2     2-CH 3 -4-OCHF 2     148-149       826   i-C 3 H 7     CH 3     H   H   2-CH 3 -4-Cl   82-83       827   i-C 3 H 7     H   CH 3     H   2-CH 3 -4-Cl   165-166       828   i-C 3 H 7     CH 2 OCH 3     H   H   2-CH 3 -4-Cl   Oil       829   n-C 4 H 9     H   H   H   4-CF 3     171-173       830   n-C 4 H 9     H   H   3-NO 2     2-CH 3 -5-Cl   172-174       831   i-C 4 H 9     H   H   3-NO 2     2-CH 3 -5-Cl   186-188       832   i-C 4 H 9     H   H   3-NO 2     2-CH 3 -4-OCHF 2     192-193       833   i-C 4 H 9     H   H   H   4-CF 3     149-151       834   i-C 4 H 9     CH 3     H   6-NO 2     2-CH 3 -4-OCHF 2     135-137       835   s-C 4 H 9     H   H   H   4-CF 3     194-195       836   s-C 4 H 9     H   H   3-Cl   2-CH 3 -4-OCHF 2     203-205       837   s-C 4 H 9     H   H   6-Cl   2-CH 3 -4-OCHF 2     213-215       838   s-C 4 H 9     H   H   3-NO 2     2-CH 3 -5-Cl   205-207       839   s-C 4 H 9     H   H   3-NO 2     2-CH 3 -4-OCHF 2     228-229       840   t-C 4 H 9     H   H   H   H   237-239       841   t-C 4 H 9     H   H   H   2-CH 3 -5-Cl   200-202       842   t-C 4 H 9     H   H   3-NO 2     2-CH 3 -5-Cl   256-258       843   t-C 4 H 9     H   H   3-NO 2     2-CH 3 -4-OCHF 2     172-173       844   CH 2 C(CH 3 ) 3     H   H   3-NO 2     2-CH 3 -4-OCHF 2     226-227       845   CH(C 2 H 5 ) 2     H   H   3-NO 2     2-CH 3 -4-OCHF 2     245-246       846   CH(CH 3 )CH(CH 3 ) 2     H   H   3-NO 2     2-CH 3 -4-OCHF 2     245-247       847   n-C 8 H 17     H   H   3-NO 2     2-CH 3 -5-Cl   164-166       848   c-C 3 H 5     H   H   H   4-CF 3     195-197       849   c-C 3 H 5     H   H   3-Cl   2-CH 3 -4-OCHF 2     156-158       850   c-C 3 H 5     H   H   6-Cl   2-CH 3 -4-OCHF 2     179-181       851   c-C 3 H 5     H   H   3-NO 2     2-CH 3 -5-Cl   194-196       852   c-C 3 H 5     H   H   3-NO 2     2-CH 3 -4-OCHF   219-192       853   c-C 4 H 7     H   H   H   2-CH 3 -5-Cl   205-207       854   c-C 4 H 7     H   H   3-NO 2     2-CH 3 -5-Cl   206-208       855   c-C 4 H 7     H   H   3-NO 2     2-CH 3 -5-F   199-201       856   c-C 5 H 9     H   H   3-NO 2     2-CH 3 -4-OCHF 2     219-220       857   c-C 5 H 9     H   H   H   4-CF 3     208-210                       858   c-C 5 H 9     H   H   3-NO 2     2-CH 3 -5-Cl   200-202       859   c-C 6 H 11     H   H   3-NO 2     2-CH 3 -5-Cl   225-227       860   CH 2 —C 3 H 5 -c   H   H   3-NO 2     2-CH 3 -5-F   190-192       861   CH 2 CH 2 Cl   H   H   3-NO 2     2-CH 3 -5-F   179-181       862   CH 2 CH 2 F   H   H   3-NO 2     2-CH 3 -5-F   179-181       863   CH 2 CH 2 F   H   H   3-NO 2     2-CH 3 -4-OCHF 2     190-191       864   CH 2 CF 3     H   H   H   2-CH 3 -5-Cl   187-189       865   CH 2 CH═CH 2     H   H   H   4-CF 3     161-163       866   CH 2 CH═CH 2     H   H   3-NO 2     2-CH 3 -5-Cl   175-177       867   CH 2 CH═CH 2     H   H   3-NO 2     2-CH 3 -4-OCHF 2     194-195       868   CH 2 C≡CH   H   H   H   4-CF 3     185-188       869   CH 2 C≡CH   H   H   3-NO 2     2-CH 3 -5-Cl   191-193       870   CH 2 C≡CH   H   H   3-NO 2     2-CH 3 -4-OCHF 2     190-191       871   CH 2 CH 2 OCH 3     H   H   3-NO 2     2-CH 3 -5-Cl   165-167       872   CH 2 CH 2 OCH 3     H   H   3-NO 2     2-CH 3 -4-OCHF 2     165-167       873   CH(CH 3 )CH 2 OCH 3     H   H   H   4-CF 3     252-253       874   CH(CH 3 )CH 2 OCH 3     H   H   3-NO 2     2-CH 3 -4-OCHF 2     153-155       875   CH 2 CH(OC 2 H 5 ) 2     H   H   3-NO 2     2-CH 3 -4-OCHF 2     149-151       876   CH 2 -Ph   H   H   H   4-CF 3     148-150       877   CH 2 -Ph   H   H   3-NO 2     2-CH 3 -5-Cl   196-198       878   CH(CH 3 )-Ph   H   H   3-NO 2     2-CH 3 -5-Cl   168-170       879   CH(CH 3 )-Ph   H   H   3-NO 2     2-CH 3 -4-OCHF 2     187-189               880   CH 2 CH 2 O-(2,4-   H   H   3-NO 2     2-CH 3 -5-Cl   126-128           (CH 3 ) 2 )-Ph            881   —CH 2 CH 2 CH 2 CH 2 —   H   H   4-CF 3     170-171       882   —CH 2 CH 2 CH 2 CH 2 —   H   6-NO 2     2-CH 3 -5-Cl   157-159       883   —CH 2 CH 2 CH 2 CH 2 —   H   6-NO 2     2-CH 3 -4-OCHF 2     163-165       884   —CH 2 CH 2 OCH 2 CH 2 —   H   H   4-CF 3     167-168       885   —CH 2 CH 2 OCH 2 CH 2 —   H   6-NO 2     2-CH 3 -5-Cl   192-194       886   —CH 2 CH 2 OCH 2 CH 2 —   H   6-NO 2     2-CH 3 -4-OCHF 2     186-188       887   —CH 2 CH(CH 3 )—OCH(CH 3 )CH 2 —   H   6-NO 2     3-CF 3 -5-OCH 3     164-165            888   CH 2 -3-Pyi   H   H   3-NO 2     2-CH 3 -4-Br   180-182       889   i-C 3 H 7     H   H   H   4-CF 2 CF 3     155-157       890   i-C 3 H 7     H   H   3-NO 2     4-CF 2 CF 3     223-225       891   i-C 3 H 7     H   H   3-F   4-CF 2 CF 3     199-201       892   i-C 3 H 7     H   H   6-F   4-CF 2 CF 3     213-215       893   i-C 3 H 7     H   H   3-Cl   4-CF 2 CF 3     214-216       894   i-C 3 H 7     H   H   6-Cl   4-CF 2 CF 3     225-227       895   i-C 3 H 7     H   H   3-I   4-CF 2 CF 3     208-210       896   i-C 3 H 7     H   H   6-I   4-CF 2 CF 3     224-226       897   i-C 3 H 7     H   H   H   2-CH 3 -4-OSO 2 -   135-137           (4-CH 2 —Ph)       898   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OSO 2 -   208-210                           (4-CH 3 —Ph)       899   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OSO 2 -   187-189                           (4-CH 3 —Ph)       900   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-OSO 2 -   218-220                           (4-CH 3 —Ph)       901   i-C 3 H 7     H   H   3-F   2-F-4-O-(4-CF 3 -2-   137-139                           Cl—Ph)       902   i-C 3 H 7     H   H   6-F   2-F-4-O-(4-CF 3 -2-   155-157                           Cl—Ph)       903   i-C 3 H 7     H   H   3-Cl   2-F-4-O-(4-CF 3 -2-   119-121                           Cl—Ph)       904   i-C 3 H 7     H   H   6-Cl   2-F-4-O-(4-CF 3 -2-   154-156                           Cl—Ph)       905   i-C 3 H 7     H   H   3-F   2-CH 3 -4-SCF 2 CF 3     140-142       906   i-C 3 H 7     H   H   6-F   2-CH 3 -4-SCF 2 CF 3     162-164       907   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SCF 2 CF 3     172-173       908   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-SCF 2 CF 3     193-195       909   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SCF 2 CF 3     207-209       910   i-C 3 H 7     H   H   6-I   2-CH 3 -4-SCF 2 CF 3     196-198       911   i-C 3 H 7     H   H   3-Cl   4-CH═C(Cl)CF 3     196.3-208.2       912   i-C 3 H 7     H   H   6-Cl   4-CH═C(Cl)CF 3     202.8-209.4       913   i-C 3 H 7     H   H   3-Cl   4-CH═CBr 2     209.8-214.8       914   i-C 3 H 7     H   H   6-Cl   4-CH═CBr 2     207.7-213.9       915   i-C 3 H 7     H   H   3-Cl   4-CH═CCl 2     120.1       916   i-C 3 H 7     H   H   6-Cl   4-CH═CCl 2     199.7       917   i-C 3 H 7     H   H   3-I   4-CH═C(Cl)CF 3     196.6       918   i-C 3 H 7     H   H   6-I   4-CH═C(Cl)CF 3     203.3       919   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -4-I   195.5       920   i-C 3 H 7     H   H   6-I   2-C 2 H 5 -4-I   242.3       921   C 2 H 5     H   H   H   2-C 2 H 5 -3-Cl-6-C 2 H 5     171-173       922   i-C 3 H 7     H   H   H   2-C 2 H 5 -3-Cl-6-C 2 H 5     185-186       923   t-C 4 H 9     H   H   H   2-C 2 H 5 -3-Cl-6-C 2 H 5     166-167       924   i-C 3 H 7     H   H   3-Cl   2-C 2 H 5 -3-Cl-6-C 2 H 5     260-261       925   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -3-Cl-6-C 2 H 5     269-271       926   t-C 4 H 9     H   H   3-Cl   2-C 2 H 5 -3-Cl-6-C 2 H 5     221-222       927   t-C 4 H 9     H   H   H   2-CH 3 -4-Cl   216-218       928   t-C 4 H 9     H   H   H   4-CF 3     220-221       929   t-C 4 H 9     H   H   H   4-OCF 3     178-179       930   t-C 4 H 9     H   H   H   2-CH 3 -4-OCF 3     184-185       931   t-C 4 H 9     H   H   H   2-CH 3 -4-CF 2 CF 3     223-224       932   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     219-220       933   t-C 4 H 9     H   CH 3     H   4-OCF 3     155-158       934   t-C 4 H 9     H   H   3-Cl   4-CF 3     228-229       935   t-C 4 H 9     H   H   6-Cl   4-CF 3     253-255       936   t-C 4 H 9     H   H   3-Cl   4-OCF 3     268-270       937   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-Cl   242-244       938   t-C 4 H 9     H   H   6-Cl   2-CH 3 -4-Cl   262-264       939   t-C 4 H 9     H   H   3-I   4CF 3     268-269       940   t-C 4 H 9     H   H   3-I   4-OCF 3     263-265       941   t-C 4 H 9     H   H   3-I   2-CH 3 -4-Cl   218-220       942   t-C 4 H 9     H   H   3-I   2-CH 3 -4-CF 2 CF 3     205-207       943   t-C 4 H 9     H   H   6-I   2-CH 3 -4-CF 2 CF 3     216-217       944   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-OCF 3     260-262       945   n-C 4 H 9     H   H   3-I   2-CH 3 -4-CF 2 CF 3     173.1-178.5       946   n-C 4 H 9     H   H   6-I   2-CH 3 -4-CF 2 CF 3     181.8-187.7       947   n-C 5 H 11     H   H   3-I   2-CH 3 -4-CF 2 CF 3     140.2-151.4       948   n-C 5 H 11     H   H   6-I   2-CH 3 -4-CF 2 CF 3     168.7-171.3       949   n-C 6 H 13     H   H   3-I   2-CH 3 -4-CF 2 CF 3     135.5-143.9       950   n-C 6 H 13     H   H   6-I   2-CH 3 -4-CF 2 CF 3     167.1-169.9       951   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -4-I   254.8-273.8       952   i-C 3 H 7     H   H   3-I   2-n-C 3 H 7 -4-I   179.7       953   i-C 3 H 7     H   H   3-CH 3     2-CH 3 -4-CF 2 CF 3     184-186       954   i-C 3 H 7     H   H   6-CH 3     2-CH 3 -4-CF 2 CF 3     177-179       955   t-C 4 H 9     H   H   3-CH 3     2-CH 3 -4-CF 2 CF 3     198-200       956   t-C 4 H 9     H   H   6-CH 3     2-CH 3 -4-CF 2 CF 3     236-237       957   t-C 4 H 9     H   H   3-I   2-CH 3 -4-OCF 3     208-210       958   t-C 4 H 9     H   H   6-I   2-CH 3 -4-OCF 3     253-255       959   n-C 3 H 7     H   H   3-I   2-CH 3 -3Cl   190-192       960   n-C 3 H 7     H   H   6-I   2-CH 3 -3-Cl   159-161       961   n-C 3 H 7     H   H   6-I   2-C 2 H 5 -3-Cl-6-C 2 H 5     225-228       962   i-C 3 H 7     H   H   3-NO 2     4-OCOCF 3     185-187       963   i-C 3 H 7     H   H   3-Cl   4-OCOCF 3     Paste       964   i-C 3 H 7     H   H   3-I   4-OCOCF 3     Paste       965   i-C 3 H 7     H   H   3-I   2-i-C 3 H 7 -4-I   132.5       966   i-C 3 H 7     H   H   3-I   2-n-C 4 H 9 -4-I   194.2-198.3       967   i-C 3 H 7     H   H   3-I   2-CH 3 -4-Br-6-CH 3     119.1       968   i-C 3 H 7     H   H   3-Cl   4-CO2CH(CF 3 ) 2     168-170       969   i-C 3 H 7     H   H   3-I   4-CO2CH(CF 3 ) 2     193-195       970   i-C 3 H 7     H   H   3-NO 2     4-CO2CH(CF 3 ) 2     215-217       971   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-C≡C-   123-125                           (2,4-Cl 2 —Ph)       972   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C≡C-   138-140                           (2,4-Cl 2 —Ph)       973   i-C 3 H 7     H   H   3-Cl   3-OCF 2 CF 2 -4   125-128       974   i-C 3 H 7     H   H   3-I   3-OCF 2 CF 2 -4   123-126       975   i-C 3 H 7     H   H   H   3-OCF 2 CF 2 O-4   152-154       976   i-C 3 H 7     H   H   3-NO 2     3-OCF 2 CF 2 O-4   247-248       977   i-C 3 H 7     H   H   3-Cl   3-OCF 2 CF 2 O-4   224-226       978   i-C 3 H 7     H   H   H   4-C(CF 3 ) 2 OH   87-89       979   i-C 3 H 7     H   H   3-NO 2     4-C(CF 3 ) 2 OH   205-207       980   i-C 3 H 7     H   H   3-Cl   4-C(CF 3 ) 2 OH   187-189       981   CH 2 CH 2 OCH 3     H   H   3-I   2-CH 3 -4-CF 2 CF 3     145.3-151.7       982   CH 2 CH 2 OCH 3     H   H   6-I   2-CH 3 -4-CF 2 CF 3     166.7-169.4       983   CH 2 CH 2 OC 2 H 5     H   H   3-I   2-CH 3 -4-CF 2 CF 3     146.5-150.3       984   CH 2 CH 2 OC 2 H 5     H   H   6-I   2-CH 3 -4-CF 2 CF 3     157.3-160.4       985   (CH 2 ) 3 OCH 3     H   H   3-I   2-CH 3 -4-CF 2 CF 3     151.9-155.8       986   (CH 2 ) 3 OCH 3     H   H   6-I   2-CH 3 -4-CF 2 CF 3     156.5-158.8       987   CH 2 CH═CH 2     H   H   3-I   2-CH 3 -4-CF 2 CF 3     157.5       988   CH 2 CH═CH 2     H   H   6-I   2-CH 3 -4-CF 2 CF 3     164.6-171.3       989   CH 2 C≡CH   H   H   3-I   2-CH 3 -4-CF 2 CF 3     153.6-158.4       990   CH 2 C≡CH   H   H   6-I   2-CH 3 -4-CF 2 CF 3     171.5-178.1       991   c-C 5 H 9     H   H   3-I   2-CH 3 -4-CF 2 CF 3     212.9       992   c-C 5 H 9     H   H   6-I   2-CH 3 -4-CF 2 CF 3     205.2       993   c-C 6 H 11     H   H   3-I   2-CH 3 -4-CF 2 CF 3     219.7-224.3       994   c-C 6 H 11     H   H   6-I   2-CH 3 -4-CF 2 CF 3     239.0-244.4       995   i-C 3 H 7     H   H   H   4-SCF 3     182-184       996   i-C 3 H 7     H   H   3-NO 2     4-SCF 3     228-229       997   i-C 3 H 7     H   H   3-Cl   4-SCF 3     229-231       998   i-C 3 H 7     H   H   3-I   4-SCF 3     226-227       999   i-C 3 H 7     H   H   H   4-SOCF 3     175-178       1000   i-C 3 H 7     H   H   3-NO 2     4-SOCF 3     202-205       1001   i-C 3 H 7     H   H   3-Cl   4-SOCF 3     242-244       1002   i-C 3 H 7     H   H   3-I   4-SOCF 3     229-231       1003   i-C 3 H 7     H   H   3-I   3-OCF 2 CF 2 O-4   163-165       1004   i-C 3 H 7     H   H   3-I   4-C(CF 3 ) 2 OH   227-229       1005   i-C 4 H 9     H   H   3-I   2-CH 3 -4-CF 2 CF 3     200.4-206.8       1006   i-C 4 H 9     H   H   6-I   2-CH 3 -4-CF 2 CF 3     179.2-181.8       1007   s-C 4 H 9     H   H   3-I   2-CH 3 -4-CF 2 CF 3     226.0-230.9       1008   s-C 4 H 9     H   H   6-I   2-CH 3 -4-CF 2 CF 3     216.1-218.0       1009   s-C5H11   H   H   3-I   2-CH 2 -4-CF 2 CF 2     215.3-218.2       1010   s-C5H11   H   H   6-I   2-CH 2 -4-CF 2 CF 3     191.4-210.5       1011   CH(C 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-CF 2 CF 3     234.8-236.9       1012   CH(C 2 H 5 ) 2     H   H   6-I   2-CH 3 -4-CF 2 CF 3     253.7-255.7       1013   CH(C 2 H 5 )CH 2 O—CH 3     H   H   3-I   2--CH 3 -4-CF 2 CF 3     177       1014   CH(C 2 H 5 )CH 2 O—CH 3     H   H   6-I   2-CH 3 -4-CF 2 CF 3     198.3-201.0       1015   i-C 5 H 11     H   H   3-I   2-CH 3 -4-CF 2 CF 3     190.0-192.5       1016   i-C 5 H 11     H   H   6-I   2-CH 3 -4-CF 2 CF 3     187.8       1017   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -4-CF 2 CF 2     232.5-235.8       1018   t-C 4 H 9     H   H   H   2-CH 3 -4-OCHF 2     138-140       1019   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-OCHF 2     206-208       1020   t-C 4 H 9     H   H   3-I   2-CH 3 -4-OCHF 2     204-206       1021   t-C 4 H 9     H   H   H   2-Cl-4-OCF 3     162-164       1022   t-C 4 H 9     H   H   3-Cl   2-Cl-4-OCF 3     189-191       1023   t-C 4 H 9     H   H   3-I   2-Cl-4-OCF 3     188-190       1024   c-C 3 H 5     H   H   3-I   2-CH 3 -4-CF 2 CF 3     156.0-165.0       1025   c-C 3 H 5     H   H   6-I   2-CH 3 -4-CF 2 CF 3     173.2-176.4       1026   CH 2 CH(CH 3 )—C 2 H 5     H   H   3-I   2-CH 3 -4-CF 2 CF 3     148.6       1027   CH 2 CH(CH 3 )—C 2 H 5     H   H   6-I   2-CH 3 -4-CF 2 CF 3     157.8       1028   CH 2 -c-C 6 H 11     H   H   3-I   2-CH 3 -4-CF 2 CF 3     186.8-188.7       1029   CH 2 (4-t-C 4 H 9 -   H   H   3-I   2-CH 3 -4-CF 2 CF 3     226.0-231.2           c-C6H11)       1030   CH 2 (4-t-C 4 H 9 -   H   H   6-I   2-CH 3 -4-CF 2 CF 3     215.4           c-C6H11)       1031   CH(CH 3 )CH 2 O—CH 3     H   H   3-I   2-CH 3 -4-CF 2 CF 3     187.2-189.9       1032   CH(CH 3 )CH 2 O—CH 3     H   H   6-I   2-CH 3 -4-CF 2 CF 3     169.7-176.1       1033   CH(CH 3 )CH—(CH 3 ) 2     H   H   3-I   2-CH 3 -4-CF 2 CF 3     208.3-212.7       1034   CH(CH 3 )CH—(CH 3 ) 2     H   H   6-I   2-CH 3 -4-CF 2 CF 3     219.3-223.0       1035   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-CF 2 CF 3     131.3       1036   C 2 H 5     C 2 H 5     H   6-I   2-CH 3 -4-CF 2 CF 3     137         1037   t-C 4 H 9     H   H   H   2-CH 3 -4-CF(CF 3 ) 2     172-175       1038   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-CF(CF 3 ) 2     241-243       1039   t-C 4 H 9     H   H   3-I   2-CH 3 -4-CF(CF 3 ) 2     238-240       1040   CH 2 CF 3     H   H   3-I   2-CH 3 -4-CF 2 CF 3     166.1-175.5       1041   CH 2 CF 3     H   H   6-I   2-CH 3 -4-CF 2 CF 3     184.7-202.5       1042   i-C 3 H 7     CH 3     H   3-I   2-CH 3 -4-CF 2 CF 3     201.4       1043   i-C 4 H 9     CH 3     H   3-I   2-CH 3 -4-CF 2 CF 3     183.5-189.0       1044   n-C 3 H 7     n-C 3 H 7     H   3-I   2-CH 3 -4-CF 2 CF 3     142.6-145.4       1045   CH 2 CH═CH 2     CH 2 CH═CH 2     H   3-I   2-CH 3 -4-CF 2 CF 3     100.2-105.6       1046   CH 2 CH 2 O—C 2 H 5     CH 2 CH 2 O—C 2 H 5     H   3-I   2-CH 3 -4-CF 2 CF 3     84.0-87.3            1047   CH 2 CH 2 CH 2 CH 2     H   3-I   2-CH 3 -4-CF 2 CF 3     172.7-177.3            1048   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-CF 2 CF 3     119.1       1049   t-C 4 H 9     H   H   H   2-CH 3 -4-OCBrF 2     195-197       1050   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-OCBrF 2     198-200       1051   t-C 4 H 9     H   H   3-I   2-CH 3 -4-OCBrF 2     196-198       1052   t-C 4 H 9     H   H   H   4-C(CF 3 ) 2 OH   123-125       1053   t-C 4 H 9     H   H   3-Cl   4-C(CF 3 ) 2 OH   185-187       1054   t-C 4 H 9     H   H   3-I   4-C(CF 3 ) 2 OH   203-205       1055   i-C 3 H 7     H   H   3-I   2,4-F 2     236-237       1056   C 2 H 5     H   H   3-I   2-CH 3 -4-OCF 2 —CHF 2     176-178       1057   C 2 H 5     H   H   6-I   2-CH 3 -4-OCF 2 —CHF 2     207-209       1058   n-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 —CHF 2     185-187       1059   n-C 3 H 7     H   H   6-I   2-CH 3 -4-OCF 2 —CHF 2     215-217       1060   t-C 4 H 9     H   H   H   2-CH 3 -4-OCF 2 —CHF 2     197-198       1061   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-OCF 2 —CHF 2     192-194       1062   t-C 4 H 9     H   H   3-I   2-CH 3 -4-OCF 2 —CHF 2     217-218       1063   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-O-(3,5-   186-188                           (CH 3 O) 2 -2-Pym)       1064   i-C 3 H 7     H   H   3-I   2-CH 3 -4-O-(3,5-   201-202                           (CH 3 O) 2 -2-Pym)       1065   t-C 4 H 9     H   H   H   3-OCF 2 CF 2 O-4   156-158       1066   t-C 4 H 9     H   H   3-Cl   3-OCF 2 CF 2 O-4   240-241       1067   t-C 4 H 9     H   H   3-I   3-OCF 2 CF 2 O-4   252-253       1068   CH 3     CH 3     H   3-I   2-CH 3 -4-CF 2 CF 3     148.7       1069   n-C 3 H 7     CH 3     H   3-I   2-CH 3 -4-CF 2 CF 3     129.3            1070   CH 2 CH 2 OCH 2 CH 2     H   3-I   2-CH 3 -4-CF 2 CF 3     164.7            1071   i-C 3 H 7     i-C 3 H 7     H   H   2-CH 3 -4-CF 2 CF 3     169.1       1072   i-C 3 H 7     i-C 3 H 7     H   6-I   2-CH 3 -4-CF 2 CF 3     201.2       1073   C 2 H 5     H   H   3-I   2-CH 3 -4-CF(CF 3 ) 2     194-195       1074   C 2 H 5     H   H   6-I   2-CH 3 -4-CF(CFS) 2     218-220       1075   n-C 3 H 7     H   H   3-I   2-CH 3 -4-CF(CF 3 ) 2     188-190       1076   n-C 3 H 7     H   H   6-I   2-CH 3 -4-CF(CF 3 ) 2     201-203       1077   i-C 3 H 7     H   H   H   4-SO 2 CF 3     184-186       1078   i-C 3 H 7     H   H   3-Cl   4-SO 2 CF 3     239-241       1079   i-C 3 H 7     H   H   3-I   4-SO 2 CF 3     225-227       1080   t-C 4 H 9     H   H   3-I   4-SO 2 CF 3     230-232       1081   i-C 3 H 7     i-C 3 H 7     H   3-I   2-CH 3 -4-CF 2 CF 3     Paste            1082   CH 2 CH 2 CH 2 CH 2 CH 2     H   3-I   2-CH 3 -4-CF 2 CF 3     140.0-146.8       1083   CH 2 CH 2 CH(CH 3 )CH 2     H   3-I   2-CH 3 -4-CF 2 CF 3     171.4           —CH 2 —            1086   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CF 2 —Ph   138-140       1087   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 CF 2 —Ph   160-162       1088   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CF 2 —Ph   209-211       1089   i-C 3 H 7     H   H   3-   2-CH 3 -4-OCF 2 CF 2 —Ph   190-192                   NO 2         1090   i-C 3 H 7     H   H   H   2-CH 3 -4-SCH 2 CH 2 —CF═CF 2     190-192       1091   i-C 3 H 7     H   H   H   2-CH 3 -4-SOCH 2 CH 2 —CF═CF 3     149-153       1092   i-C 3 H 7     H   H   H   2-CH 3 -4-SO 2 CH 2 —CF═CF 2     183-185       1093   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SCH 2 CH 2 —CF═CF 2     168-170       1094   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-SOCH 2 CH 2 —CF═CF 2     164-167       1096   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SCH 2 CH 2 —CF═CF 2     193-195       1097   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SOCH 2 CH 2 —CF═CF 2     182-186       1098   i-C 3 H 7     H   H   3-I   2-CH 2 -4-SO 2 CH 2 —CH 2 CF═CF 2     208-210       1099   i-C 3 H 7     H   H   H   3-OCF 2 O-4   216-218       1100   i-C 3 H 7     H   H   3-   3-OCF 2 O-4   227-229                       NO 2         1101   i-C 3 H 7     H   H   3-Cl   3-OCF 2 O-4   243-245       1102   i-C 3 H 7     H   H   3-I   3-OCF 2 O-4   229-231       1103   t-C 4 H 9     H   H   H   3-OCF 2 O-4   209-211       1104   t-C 4 H 9     H   H   3-Cl   3-OCF 2 O-4   206-208       1105   t-C 4 H 9     H   H   3-I   3-OCF 2 O-4   228-230       1106   i-C2H7   H   H   H   4-SCBrF 2     175-177       1107   i-C 3 H 7     H   H   H   4-SOCBrF 2     158-161       1108   i-C 3 H 7     H   H   3-NO 2     4-SCBrF 2     180-182       1109   i-C 3 H 7     H   H   3-NO 2     4-SOCBrF 2     195-198       1110   i-C 3 H 7     H   H   3-Cl   4-SCBrF 2     156-158       1111   i-C 3 H 7     H   H   3-Cl   4-SOCBrF 2     218-220       1112   i-C 3 H 7     H   H   3-I   4-SCBrF 2     206-208       1113   i-C 3 H 7     H   H   3-I   4-SOCBrF 2     158-160       1114   t-C 4 H 9     H   H   3-Cl   4-SCBrF 2     210-212       1115   t-C 4 H 9     H   H   3-I   4-SCBrF 2     219-220       1116   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-CF 2 CF 3     179.8-183.7            1117   CH 2 CH 2 CH 2     H   3-I   2-CH 3 -4-CF 2 CF 3     170.7           CH 2 CH 2 CH 2                  1118   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -4-OCF 3     161.9       1119   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -4-CF(CF 3 ) 2     169.1       1120   CH 3     CH 3     CH 3     3-I   2-CH 2 -4-CF 2 CF 3     141.9-146.6       1121   i-C 3 H 7     CH 3     CH 3     3-I   2-CH 3 -4-CF 2 CF 3     Paste       1122   C 2 H 5     C 2 H 5     CH 3     3-I   2-CH 3 -4-CF 2 CF 3     Paste       1123   i-C 3 H 7     H   H   H   4-SCF 3     135-137       1124   i-C 3 H 7     H   H   3-NO 2     4-SCF 3     187-189       1125   i-C 3 H 7     H   H   3-Cl   4-SCF 3     192-194       1126   i-C 3 H 7     H   H   3-I   4-SCF 3     194-196       1127   t-C 4 H 9     H   H   3-I   4-SCF 3     195-197       1128   C 2 H 5     C 2 H 5     H   3-I   4-SCF 3     173-175       1129   C 2 H 5     C 2 H 5     H   3-I   3-OCF 2 O-4   128-130       1130   C 2 H 5     C 2 H 5     H   3-I   4-C(CF 3 ) 2 OH   152-154       1131   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -4-OCF 3     178.7-182.6       1132   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -4-OCF 2 CHF 2     160.8-165.0       1133   C 2 H 5     C 2 H 5     H   3-NO 2     2-Cl-4-CF 2 CF 2     91.9-95.2       1134   C 2 H 5     C 2 H 5     H   3-NO 2     2-F-4-CF 2 CF 2     162.6-166.8       1135   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -4-Cl   188.8-190.8       1136   C 2 H 5     C 2 H 5     H   3-NO 2     4-OCF 3     185.7-187.9       1137   C 2 H 5     C 2 H 5     H   6-NO 2     2-CH 3 -4-OCF 2 CHF 2     111.2       1138   C 2 H 5     C 2 H 5     H   6-NO 2     2-CH 3 -4-Cl   149.7       1139   C 2 H 5     C 2 H 5     H   6-NO 2     4-OCF 3     173.4            1140   CH 2 CH(CH 3 )CH 2     H   6-I   2-CH 3 -4-CF 2 CF 3     166.4           CH(CH 3 )CH 2              1141   t-C 4 H 9     H   H   3-I   2-CH 3 -4-CF 3     197-198       1142   i-C 3 H 7     H   H   3-I   3-N═C(CF 2 CF 3 )O-4   214-216       1143   t-C 4 H 9     H   H   3-I   3-N═C(CF 2 CF)O-4   253-254       1144   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-CF 3     160-161       1145   i-C 3 H 7     H   H   H   3-OCHFCF 2 O-4   102-104       1146   i-C 3 H 7     H   H   3-NO 2     3-OCHFCF 2 O-4   190-192       1147   i-C 3 H 7     H   H   3-Cl   3-OCHFCF 2 O-4   123-125       1148   i-C 3 H 7     H   H   3-I   3-OCHFCF 2 O-4   218-220       1149   t-C 4 H 9     H   H   H   3-OCHFCF 2 O-4   165-167       1150   t-C 4 H 9     H   H   3-I   3-OCHFCF 2 O-4   240-241       1151   C 2 H 5     C 2 H 5     H   3-I   3-OCHFCF 2 O-4   193-195       1152   t-C 5H   11     H   H   3-F   2-CH 3 -CF 2 CF 3     223.3       1153   t-C 5H   11     H   H   3-F   2-CH 3 -4-   222                           CF(CF 3 ) 2         1154   t-C 5 H 11     H   H   3-F   2-CH 3 -4-OCF 3     193.6-195.8       1155   t-C 5 H 11     H   H   3-F   2-CH 3 -4-OCHF 2     165.5-174.0       1156   n-C 3 H 7     n-C 3 H 7     H   3-I   2-CH 3 -4-OCF 2     132.2-135.0       1157   n-C 3 H 7     n-C 3 H 7     H   3-I   2-CH 3 -4-OCHF 2     81.4-87.8       1158   n-C 3 H 7     n-C 3 H 7     H   3-I   2-CH 3 -4-   116.3                           OCF 2 CHF 2         1159   i-C 3 H 7     C 2 H 5     H   3-I   2-CH 3 -4-CF 2 CF 3     124.4       1160   i-C 3 H 7     C 2 H 5     H   3-I   4-OCF 3     137.3-144.1       1161   i-C 3 H 7     H   H   3-I   3-OCF 2 CHFO-4   161-163       1162   i-C 3 H 7     H   H   3-NO 2     3-OCF 2 CHFO-4   238-240       1163   i-C 3 H 7     H   H   3-Cl   3-OCF 2 CHFO-4   243-245       1164   i-C 3 H 7     H   H   3-I   3-OCF 2 CHFO-4   192-194       1165   t-C 4 H 9     H   H   H   3-OCF 2 CHFO-4   205-207       1166   t-C 4 H 9     H   H   3-I   3-OCF 2 CHFO-4   238-240       1167   C 2 H 5     C 2 H 5     H   3-I   3-OCF 2 CHFO-4   195-197       1168   i-C 3 H 7     H   H   3-I   2-CH 3 -4-SOCF 3     148-152       1169   t-C 4 H 9     H   H   3-I   2-CH 3 -4-SOCF 3     165-168       1173   i-C 3 H 7     H   H   3-I   3-N═C(4-CF 3 —Ph)—O-4   253-255       1174   t-C 4 H 9     H   H   3-I   3-N═C(4-CF 3 —Ph)—O-4   251-253       1175   C 2 H 5     C 2 H 5     H   3-I   3-N═C(4-CF 3 —Ph)—O-4   231-233       1176   i-C 3 H 7     H   H   3-I   3-O-C(2-CF 3 —Ph)═N-4   242-244       1177   t-C 4 H 9     H   H   3-I   3-O-C(2-CF 3 —Ph)═N-4   229-231       1178   C 2 H 5     C 2 H 5     H   3-I   3-O-C(2-CF 3 —Ph)═N-4   203-205       1179   C 2 H 5     C 2 H 5     C 2 H 5     3-I   2-CH 3 -4-CF 2 CF 3     Paste       1180   i-C 3 H 7     H   H   3-I   3-O-C(CF 2 CF 3 )═N-4   130-132       1181   t-C 4 H 9     H   H   3-I   3-O-C(CF 2 CF 3 )═N-4   205-207       1182   C 2 H 5     C 2 H 5     H   3-I   3-O-C(CF 2 CF 3 )═N-4   188-190       1183   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-OCF 3     222-224       1184   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-CF 2 CF 3     219-221       1185   C 2 H 5     C 2 H 5     H   3-CF 3     2-CH 3 -4-OCF 3     192-194       1186   C 2 H 5     C 2 H 5     H   3-CF 3     2-CH 3 -4-CF 2 CF 3     218-220       1187   i-C 3 H 7     H   H   3-Cl   2-F-4-OCF 3     126-128       1188   i-C 3 H 7     H   H   3-I   2-F-4-OCF 3     220-222       1189   t-C 4 H 9     H   H   3-I   2-F-4-OCF 3     198-200       119O   C 2 H 5     C 2 H 5     H   3-I   2-F-4-OCF 3     129-131       1191   i-C 3 H 7     H   H   3-OCF 3     2-CH 3 -4-CF 2 CF 3     190-192       1192   t-C 4 H 9     H   H   3-OCF 3     2-CH 3 -4-CF 2 CF 3     205-207       1193   C 2 H 5     C 2 H 5     H   3-OCF 3     2-CH 3 -4-CF 2 CF 3     146-148       1202   i-C 3 H 7     H   H   4-I   2-CH 3 -4-CF 2 CF 3     197-199       1203   i-C 3 H 7     H   H   5-I   2-CH 3 -4-CF 2 CF 3     201-203       1204   i-C 3 H 7     H   H   4-I   2-CH 3 -4-OCHF 2     241-243       1205   i-C 3 H 7     H   H   5-I   2-CH 3 -4-OCHF 2     214-216       1206   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-OCF 2 CHF 2     195-197       1207   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-CF(CF 3 ) 2     227-229       1208   i-C 3 H 7     H   H   H   2-C 2 H 5 -4-OCF 3     160-162       1209   i-C 3 H 7     H   H   3-Cl   2-C 2 H 5 -4-OCF 3     205-207       1210   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -4-OCF 3     241-243       1211   t-C 4 H 9     H   H   3-I   2-C 2 H 5 -4-OCF 3     224-225       1212   C 2 H 5     C 2 H 5     H   3-I   2-C 2 H 5 -4-OCF 3     141-143       1221   i-C 3 H 7     H   H   3,4-Cl 2     2-CH 3 -4-OCF 3     199-200       1222   i-C 3 H 7     H   H   3,4-Cl 2     2-CH 3 -4-CF 2 CF 3     208-209       1223   i-C 3 H 7     H   H   3,4-Cl 2     2-CH 3 -4-CF(CF 3 ) 2     228-229       1224   i-C 3 H 7     H   H   3,5-Cl 2     2-CH 3 -4-OCF 3     228-230       1225   i-C 3 H 7     H   H   3,5-Cl 2     2-CH 3 -4-CF 2 CF 3     219-220       1226   i-C 3 H 7     H   H   3,5-Cl 2     2-CH 3 -4-CF(CF 3 ) 2     211-212       1227   i-C 3 H 7     H   H   3-Cl-4-F   2-CH 3 -4-OCF 3     184-186       1228   i-C 3 H 7     H   H   3-Cl-4-F   2-CH 3 -4-CF 2 CF 3     178-180       1229   i-C 3 H 7     H   H   3-Cl-4-F   2-CH 3 -4-CF(CF 3 ) 2     200-201       1230   t-C 4 H 9     H   H   3-CF 3     2-CH 3 -4-OCF 3     209-210       1231   t-C 4 H 9     H   H   3-CF 3     2-CH 3 -4-CF 2 CF 3     210-211       1232   t-C 4 H 9     H   H   3-CF 3     2-CH 3 -4-CF(CF 3 ) 2     242-243       1233   i-C 3 H 7     H   H   3-OCF 3     2-CH 3 -4-OCF 3     219-220       1234   t-C 4 H 9     H   H   3-OCF 3     2-CH 3 -4-OCF 3     222-223       1235   C 2 H 5     C 2 H 5     H   3-OCF 3     2-CH 3 -4-OCF 3     125-126       1236   i-C 3 H 7     H   H   3-OCF 3     2-CH 3 -4-OF(CF 3 ) 2     235-236       1237   t-C 4 H 9     H   H   3-OCF 3     2-CH 3 -4-CF(CF 3 ) 2     220-222       1238   C 2 H 5     C 2 H 5     H   3-OCF 3     2-CH 3 -4-CF(CF 3 ) 2     156-157       1245   i-C 3 H 7     H   H   3-CN   2-CH 3 -4-CF 2 CF 3     168-170       1246   i-C 3 H 7     H   H   4-I   2-CH 3 -4-OCF 3     238-240       1247   i-C 3 H 7     H   H   5-I   2-CH 3 -4-OCF 3     205-206       1248   i-C 3 H 7     H   H   4-I   2-CH 3 -4-OCF 2 CHF 2     222-223       1249   i-C 3 H 7     H   H   5-I   2-CH 3 -4-OCF 2 CHF 2     203-204       1250   i-C 3 H 7     H   H   4-I   2-CH 3 -4-CF(CF 3 ) 2     215-216       1251   i-C 3 H 7     H   H   5-I   2-CH 3 -4-CF(CF 3 ) 2     216-217       1256   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     235-236                       -4-F       1257   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     225-226                       -4-F       1258   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-CF 2 CF 3     155-156                       -4-F       1259   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 3     229-231                       -4-F       1260   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-OCF 3     237-238                       -4-F       1261   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-OCF 3     140-141                       -4-F       1262   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-   264-265                       -4-F   CF(CF 3 ) 2         1263   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-   253-154                       -4-F   CF(CF 3 ) 2         1264   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-   158-159                       -4-F   CF(CF 3 ) 2         1266   i-C 3 H 7     H   H   3,4-   2-CH 3 -4-   162-164                       Br 2     CF 2 CF 3         1277   i-C 3 H 7     H   H   4-Cl   2-CH 3 -4-   185-186                           CF 2 CF 3         1278   t-C 4 H 9     H   H   4-Cl   2-CH 3 -4-   206-207                           CF 2 CF 3         1280   C 2 H 5     C 2 H 5     H   4-Cl   2-CH 3 -4-   163-164                           CF 2 CF 3         1281   C 2 H 5     C 2 H 5     H   4-Cl-   2-CH 3 -4-   193-194                       6-I   CF 2 CF 3         1283   i-C 3 H 7     H   H   3,4-F 2     2-CH 3 -4-OCF 3     194-195       1284   t-C 4 H 9     H   H   3,4-F 2     2-CH 3 -4-OCF 3     216-217       1285   C 2 H 5     C 2 H 5     H   3,4-F 2     2-CH 3 -4-OCF 3     156-157       1287   i-C 3 H 7     H   H   4,5-F 2     2-CH 3 -4-OCF 3     195-196       1288   t-C 4 H 9     H   H   4,5-F 2     2-CH 3 -4-OCF 3     223-224       1290   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OC—(CF 2 CF 3 )═C—(CF 3 ) 2     226-227       1291   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OC—(CF 2 CFs)═C—(CF 3 ) 2     204-205       1292   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OC—(OCH 3 )═C—(CF 3 ) 2     198-199       1293   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OC—(OCH 3 )═C—(CF 3 ) 2     179-180       1294   CH(CH 3 )CH 2 OH   H   H   H   2-CH 3 -4-C 2 F 5     73-74       1295   i-C 3 H 7     H   H   6-Cl   2-OCH 3 -5-Ph   120       1296   i-C 3 H 7     H   H   3-Cl   2-OCH 3 -5-Ph   195       1297   n-C 3 H 7     H   H   6-Cl   2-OCH 3 -5-Ph   200       1298   CH(CH 3 )CH 2 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     195       1299   CH(C 2 H 5 )CH 2 OH   H   H   H   2-CH 3 -4-C 2 F 5      78       1300   CH(CH 3 )CH 2 OH   H   H   3-I   2-CH 3 -4-C 2 F 5     98-99       1301   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-C≡C—C 4 H 9 -t   210       1302   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-C≡C—C 4 H 9 -t   205       1303   n-C 3 H 7     H   H   3-I   2-CH 3 -4-C 2 F 5     200       1304   n-C 3 H 7     H   H   6-I   2-CH 3 -4-C 2 F 5     195       1305   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C≡C—C 4 H 9 -t   205       1306   i-C 3 H 7     H   H   6-I   2-CH 3 -4-C≡C—C 4 H 9 -t   170       1307   CH 2 —Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     175       1308   CH 2 —Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     175       1309   CH 2 -(2-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     170       1310   CH 2 -(2-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     210       1311   CH 2     H   H   3-I   2-CH 3 -4-C 2 F 5     190       1312   CH 3     H   H   6-I   2-CH 3 -4-C 2 F 5     200       1313   C 2 H 5     H   H   3-I   2-CH 3 -4-C 2 F 5     182       1314   C 2 H 5     H   H   6-I   2-CH 3 -4-C 2 F 5     205       1315   CH 2 CH(OH)CH 3     H   H   3-Cl   2-CH 3 -4-C 2 F 5     187       1316   CH(C 2 H 5 )CH 2 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     208       1317   C(CH 3 ) 2 CH 2 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     181-182       1318   CH 2 CH(OH)C 2 H 5     H   H   3-Cl   2-CH 3 -4-C 2 F 5     171-172       1319   CH 2 CH 2 —Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     150       1320   CH 2 CH 2 —Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     190       1321   CH(CH 3 )-Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     160       1322   CH(CH 3 )-Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     190       1323   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-   220                           CH 2 CH 2 C(CH 3 ) 3         1324   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-   205                           CH 2 CH 2 C(CH 3 ) 3         1325   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-C≡C-Ph   215       1326   i-C 3 H 7     H   H   6-Cl   2-CH 3 -4-C≡C-Ph   230       1327   O-n-C 3 H 7     H   H   3-Cl   2-CH 3 -4-C 2 F 5     165       1328   O-n-C 3 H 7     H   H   6-Cl   2-CH 3 -4-C 2 F 5     150       1329   O-CH 2 CH═CHCl   H   H   3-Cl   2-CH 3 -4-C 2 F 5     150           (E)       1330   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CN   230       1331   (CH 2 ) 3 -Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     112       1332   (CH 2 ) 3 -Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     105       1333   CH 2 (4-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     198       1334   CH 2 (4-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     156       1335   CH 2 (3-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     168       1336   CH 2 (3-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     177       1337   CH 2 (2-CH 3 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     152       1338   CH 2 (2-CH 3 —Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     147       1339   CH 2 (3-CH 3 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     Crystals       1340   CH 2 (3-CH 3 —Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     173       1341   CH 2 (4-CH 3 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     175       1342   CH 2 (4-CH 3 —Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Crystals       1343   CH 2 (2-CH 3 O—Ph)   H   H   3-Cl   2-CHS-4-C 2 F 5     Crystals       1344   CH 2 (2-CH 3 O—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     176       1345   CH 2 (3-CH 3 O—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     73       1346   CH 2 (3-CH 3 O—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     86       1347   CH 2 (4-CH 3 O—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     169       1348   CH 2 (4-CH 3 O—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     168       1349   CH 2 (2,4-Cl 2 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     169       1350   CH 2 (2,4-Cl 2 —Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     205       1351   CH 2 (3,4-Cl 2 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     179       1352   CH 2 (3,4-Cl 2 —Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     192       1353   CH 2 (2,3-Cl 2 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     179       1354   CH 2 (2,3-Cl 2 —Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     208       1355   CH 2 -2-Pyi   H   H   3-Cl   2-CH 3 -4-C 2 F 5     143       1356   (CH 2 ) 2 (2-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     141       1357   (CH 2 ) 2 (2-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1358   (CH 2 ) 2 (3-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     117       1359   (CH 2 ) 2 (3-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1360   (CH 2 ) 2 (4-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     118       1361   (CH 2 ) 2 (4-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     138       1362   CH(CH 3 )(2-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     Paste       1363   CH(CH 3 )(2-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     197       1364   CH(CH 3 )(3-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     100       1365   CH(CH 3 )(3-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Crystals       1366   CH(CH 3 )(4-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     195       1367   CH(CH 3 )(4-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1368   (CH 2 ) 2 O(2-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     162       1369   (CH 2 ) 2 O(2-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     160       1370   (CH 2 ) 2 O(3-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     115       1371   (CH 2 ) 2 O(3-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     172       1372   (CH 2 ) 2 O(4-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     185       1373   (CH 2 ) 2 O(4-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     148       1374   (CH 2 ) 2 O—Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     154       1375   (CH 2 ) 2 O—Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     183       1376   (CH 2 ) 2 NH—Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     104       1377   (CH 2 ) 2 NH—Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1378   CH(CH 3 )CH 2 OH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     192       1379   CH(Ph)CH 2 OH   H   H   H   2-CH 3 -4-C 2 F 5     100-101       1380   CH(4-t-C 4 H 9 —Ph)—CH 2 O   H   H   H   2-CH 3 -4-C 2 F 5     107-108       1381   C(CH 3 ) 2 CH 2 OH   H   H   H   2-CH 3 -4-C 2 F 5     227       1382   i-C 3 H 7     H   H   3-Cl   2-F-4-C 2 F 5     190       1383   i-C 3 H 7     H   H   3-Cl   2-Cl-4-C 2 F 5     180       1384   i-C 3 H 7     H   H   3-Cl   2-CF 3 -4-C 2 F 5     235       1385   i-C 3 H 7     H   H   3-I   2-F-4-C 2 F 5     190       1386   i-C 3 H 7     H   H   3-I   2-Cl-4-C 2 F 5     200       1387   i-C 3 H 7     H   H   3-I   2-CF 3 -4-C 2 F 5     255       1388   i-C 3 H 7     H   H   3-I   2-OCH 3 -4-C 2 F 5     152       1389   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CN   215       1390   2-Fur   H   H   3-Cl   2-CH 3 -4-C 2 F 5     178       1391   2-Fur   H   H   6-Cl   2-CH 3 -4-C 2 F 5     149       1392   2-TetFur   H   H   3-Cl   2-CH 3 -4-C 2 F 5     153       1393   2-TetFur   H   H   6-Cl   2-CH 3 -4-C 2 F 5     130       1394   CH 2 -4-Pyi   H   H   3-Cl   2-CH 3 -4-C 2 F 5     88       1395   CH 2 -4-Pyi   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1396   (CH 2 ) 3 OH   H   H   H   2-CH 3 -4-C 2 F 5     83-84       1397   (CH 2 ) 2 OH   H   H   H   2-CH 3 -4-C 2 F 5     136       1398   CH 2 CH(OH)CH 2 Ph   H   H   H   2-CH 3 -4-C 2 F 5     77-78       1399   (CH 2 ) 3 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     188       1400   CH 2 —Ph   H   H   3-I   2-CH 3 -4-C 2 F 5     172       1401   CH 2 —Ph   H   H   6-I   2-CH 3 -4-C 2 F 5     212       1402   CH 2 (2-Cl—Ph)   H   H   3-I   2-CH 3 -4-C 2 F 5     136       1403   CH 2 (2-Cl—Ph)   H   H   6-I   2-CH 3 -4-C 2 F 5     214       1404   CH 2 (2-CH 3 —Ph)   H   H   3-I   2-CH 3 -4-C 2 F 5     100       1405   CH 2 (2-CH 3 —Ph)   H   H   6-I   2-CH 3 -4-C 2 F 5     185       1406   CH 2 —Ph   CH 3     H   3-Cl   2-CH 3 -4-C 2 F 5     Paste       1407   CH 2 —Ph   CH 2 —Ph   H   3-Cl   2-CH 3 -4-C 2 F 5     136       1408   CH 2 —Ph   CH 2 —Ph   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1409   i-C 3 H 7     H   H   3-I   2-C 2 F 5 -4-Br   250       1410   i-C 3 H 7     H   H   3-I   2-C 2 F 5 -4-C 2 F 5     245       1411   CH 2 C≡CH   H   H   H   2-CH 3 -4-C 2 F 5     133-135       1412   CH(4-Ph—Ph)CH 2 —OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     112       1414   C(CH 3 ) 2 C≡CH   H   H   H   2-CH 3 -4-C 2 F 5     207       1415   C(CH 3 ) 2 CH 2 OH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     231       1416   CH(4-Cl—Ph)CH 2 —   H   H   6-Cl   2-CH 3 -4-C 2 F 5     225       1417   C(CH 3 ) 2 -Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     190       1418   C(CH 3 ) 2 CH 2 -Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     192       1419   CH 2 -3-Pyi   H   H   3-Cl   2-CH 3 -4-C 2 F 5     Paste       1420   CH 2 -3-Pyi   H   H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1421   CH 2 —Ph   H   H   3-Cl   2-CH 3 -4-OCHF 2     187       1422   CH 2 —Ph   H   H   6-Cl   2-CH 3 -4-OCHF 2     198       1423   CH 2 -(2-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-OCHF 2     178       1424   CH 2 -(2-Cl—Ph)   H   H   6-Cl   2-CH 3 -4-OCHF 2     192       1425   CH 2 -(2-CH 3 —Ph)   H   H   3-Cl   2-CH 3 -4-OCHF 2     183       1426   CH 2 -(2-CH 3 —Ph)   H   H   6-Cl   2-CH 3 -4-OCHF 2     192       1427   t-C 4 H 9     H   H   3-I   2-F-4-C 2 F 5     220       1428   t-C 4 H 9     H   H   3-I   2-Cl-4-C 2 F 5     187       1429   t-C 4 H 9     H   H   3-I   2-CF 3 -4-C 2 F 5     240       1430   CH 2 —Ph   H   H   3-I   2-CH 3 -4-OCHF 2     176       1431   CH 2 —Ph   H   H   6-I   2-CH 3 -4-OCHF 2     196       1432   CH 2 -(2-Cl—Ph)   H   H   3-I   2-CH 3 -4-OCHF 2     189       1433   CH 2 -(2-Cl—Ph)   H   H   6-I   2-CH 3 -4-OCHF 2     227       1434   CH 2 -(2-CH 3 —Ph)   H   H   3-I   2-CH 3 -4-OCHF 2     215       1435   CH 2 -(2-CH 3 —Ph)   H   H   6-I   2-CH 3 -4-OCHF 2     209       1436   CH 2 —Ph   CH 3     H   6-Cl   2-CH 3 -4-C 2 F 5     Paste       1437   CH 2 —Ph   CH 3     H   3-Cl   2-CH 3 -4-OCHF 2     Paste       1438   CH 2 —Ph   CH 3     H   3-I   2-CH 3 -4-C 2 F 5     175       1439   CH 2 —Ph   CH 3     H   6-I   2-CH 3 -4-C 2 F 5     Paste       1440   CH 2 —Ph   CH 3     H   3-I   2-CH 3 -4-OCHF 2     Paste       1441   CH(C 2 H 5 )CH 2 OH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     213       1442   (R)-C*H(Ph)—CH 2 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     105-107       1443   (R)-C*H(Ph)—CH 2 OH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     145-146       1445   (S)-C*H(CH 3 )—CH 2 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     93-95       1446   (S)-C*H(CH 3 )—CH 2 OH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     93-95       1447   t-C 4 H 9     H   H   3-Cl   4-C 2 F 5     275       1448   t-C 4 H 9     H   H   3-Cl   2-F-4-C 2 F 5     225       1449   t-C 4 H 9     H   H   3-Cl   2-Cl-4-C 2 F 5     200       1450   n-C 3 H 7     H   H   3-I   2-CH 3 -4-OCHF 2     181       1451   n-C 3 H 7     H   H   6-I   2-CH 3 -4-OCHF 2     233       1452   c-C 3 H 5     H   H   3-I   2-CH 3 -4-OCHF 2     182       1453   c-C 3 H 5     H   H   6-I   2-CH 3 -4-OCHF 2     231       1454   s-C 4 H 9     H   H   3-I   2-CH 3 -4-OCHF 2     225       1455   s-C 4 H 9     H   H   6-I   2-CHS-4-OCHF 2     244       1456   CH 2 C≡CH   H   H   3-I   2-CH 3 -4-OCHF 2     196       1457   CH 2 —Ph   C 2 H 5     H   3-Cl   2-CH 3 -4-C 2 F 5     Paste       1458   (R)-C*H(CH 3 )-Ph   H   H   3-Cl   2-CH 3 -4-OCHF 2     136       1459   (S)-C*H(CH 3 )-Ph   H   H   3-Cl   2-CH 3 -4-OCHF 2     136       1460   (R)-C*H(CH 3 )-CH 3 OH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     94-95       1461   (R)-C*H(CH 3 )-CH 2 OH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     94-95       1464   C(CH 3 ) 2 CH 2 OH   H   H   3-I   2-CH 3 -4-C 2 F 5     118       1465   CH(CH 3 )CH 2 OH   H   H   6-I   2-CH 3 -4-C 2 F 5     130-131       1466   C(CH 3 ) 2 C≡CH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     210-211       1467   C(CH 3 ) 2 C≡CH   H   H   6-Cl   2-CH 3 -4-C 2 F 5     230       1468   CH 2 (2-F—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     187       1469   CH 2 (2-F—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     165       1470   CH 2 —Ph   H   H   3-F   2-CH 3 -4-C 2 F 5     158       1471   CH 2 —Ph   H   H   6-F   2-CH 3 -4-C 2 F 5     134       1472   s-C 4 H 9     H   H   3-I   2-F-4-C 2 F 5     200       1473   s-C 4 H 9     H   H   3-I   2-Cl-4-C 2 F 5     205       1474   i-C 3 H 7     H   H   3-I   2-F-4-n-C 3 F 7     165       1475   t-C 4 H 9     H   H   3-I   2-C 2 H 5 -4-C 2 F 5     235       1476   CH 2 CH(OH)Ph   H   H   3-Cl   2-CH 3 -4-C 2 F 5     108       1477   CH 2 CH(OH)Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     105       1478   C(CH 3 ) 2 C≡CH   H   H   3-Cl   2-CH 3 -4-C 2 F 5     105       1479   C(CH 2 ) 2 C≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     110           2-Thi       1480   C(CH 3 ) 2 C≡C—Ph   H   H   6-Cl   2-CH 3 -4-C 2 F 5     194       1481   (R)-C*H(CH 3 )-CH 2 O   H   H   3-I   2-CH 3 -4-C 2 F 5     103-105       1482   (S)-C*H(CH 3 )-CH 2 O   H   H   3-I   2-CH 3 -4-C 2 F 5     103-105       1483   (R)-C*H(CH 3 )-CH 2 O   H   H   6-I   2-CH 3 -4-C 2 F 5     173-174       1484   C(CH 3)   2 (4-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     218       1485   C(CH 3 ) 2 (3-Cl—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     128       1486   CH 2 —Ph   H   H   3-Cl   2-F-4-C 2 F 5     162       1487   CH 2 —Ph   H   H   3-Cl   2-Cl-4-C 2 F 5     153       1488   C 2 H 5     H   H   3-Cl   2-F-4-C 2 F 5     135       1489   C 2 H 5     H   H   3-Cl   2-Cl-4-C 2 F 5     125       1490   C 2 H 5     H   H   3-Cl   2-F-4-n-C 3 F 7     128       1491   n-C 3 H 7     H   H   3-Cl   2-F-4-C 2 F 5     153       1492   n-C 3 H 7     H   H   3-Cl   2-Cl-4-C 2 F 5     147       1493   n-C 3 H 7     H   H   3-Cl   2-F-4-n-C 3 F 7     142       1494   i-C 3 H 7     H   H   3-Cl   2-F-4-n-C 3 F 7     142       1495   i-C 3 H 7     H   H   3-Cl   2-C 2 H 5 -4-C 2 F 5     213       1496   t-C 4 H 9     H   H   3-Cl   2-F-4-n-C 3 F 7     172       1497   t-C 4 H 9     H   H   3-Cl   2-C 2 H 5 -4-C 2 F 5     194       1498   s-C 4 H 9     H   H   3-Cl   2-F-4-C 2 F 5     209       1499   s-C 4 H 9     H   H   3-Cl   2-Cl-4-C 2 F 5     194       1500   s-C 4 H 9     H   H   3-Cl   2-F-4-n-C 3 F 7     182       1501   s-C 4 H 9     H   H   3-Cl   2-C 2 H 5 -4-C 2 F 5     212       1502   C 2 H 5     H   H   3-I   2-F-4-C 2 F 5     135       1503   C 2 H 5     H   H   3-I   2-Cl-4-C 2 F 5     155       1504   t-C 4 H 9     H   H   3-I   2-F-4-n-C 3 F 7     180       1505   t-C 4 H 9     H   H   3-F   2-CH 3 -4-C 2 F 5     220       1506   t-C 4 H 9     H   H   3-F   2-CH 3 -4-OCHF 2     186       1507   t-C 4 H 9     H   H   3-F   2-F-4-C 2 F 5     214       1508   t-C 4 H 9     H   H   3-F   2-Cl-4-C 2 F 5     222       1509   t-C 4 H 9     H   H   3-F   2-F-4-n-C 3 F 7     179       1510   C 2 H 5     H   H   3-F   2-F-4-C 2 F 5     125       1511   C 2 H 5     H   H   6-F   2-F-4-C 2 F 5     155       1512   n-C 3 H 7     H   H   3-F   2-F-4-C 2 F 5     130       1513   n-C 3 H 7     H   H   6-F   2-4C 2 F 5     170       1514   i-C 3 H 7     H   H   3-F   2-F-4-C 2 F 5     190       1515   i-C 3 H 7     H   H   6-F   2-F-4-C 2 F 5     180       1516   i-C 3 H 7     H   H   3-F   2-Cl-4-C 2 F 5     210       1517   i-C 3 H 7     H   H   6-F   2-Cl-4-C 2 F 5     160       1518   (S)-C*H(CH 3 )CH 2 O   H   H   6-I   2-CH 3 -4-C 2 F 5     1731-174       1519   C(CH 3 ) 2 CH 2 OH   H   H   3-I   2-CH 3 -4-OCF 3     205       1520   C(CH 3 ) 2 CH 2 OH   H   H   6-I   2-CH 3 -4-OCF 3     248       1521   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(4-CF 3 O—Ph)   247-250       1522   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(4-CF 3 —Ph)   243-246       1523   CH 2 (2-CF 3 —Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     183       1524   n-C 3 H 7     H   H   3-I   2-F-4-n-C 3 F 7     145       1525   C 2 H 5     C 2 H 5     H   3-F   2-CH 3 -4-C 2 F 5     135       1526   C 2 H 5     C 2 H 5     H   3-F   2-CH 3 -4-i-C 3 F 7     150       1527   C 2 H 5     C 2 H 5     H   3-F   2-CH 3 -4-OCF 3     125       1528   C 2 H 5     C 2 H 5     H   3-F   2-CH 3 -4-OCHF 2     110       1529   C 2 H 5     C 2 H 5     H   3-F   2-CH 3 -4-OCF 2 CHF 2     155       1530   C 2 H 5     C 2 H 5     H   3-F   2-F-4-C 2 F 5     130       1531   C 2 H 5     C 2 H 5     H   3-F   2-Cl-4-C 2 F 5     110       1532   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-i-C 3 F 7     142       1533   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-OCFs   142       1534   C 2 H 5     C 2 H 5     H   3-I   4-OCF 3     142       1535   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-C 2 F 5     150       1536   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-OCF 3     123       1537   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-i-C 3 F 7     147       1538   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-OCHF 2     92       1539   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-OCF 2 CHF 2     135       1540   C 2 H 5     C 2 H 5     H   3-Cl   2-Cl-4-C 2 F 5     110       1541   C 2 H 5     C 2 H 5     H   3-Cl   2-F-4-C 2 F 5     113       1542   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -Cl   142       1543   C 2 H 5     C 2 H 5     H   3-Cl   2-C 2 H 5 -4-C 2 F 5     101       1544   C 2 H 5     C 2 H 5     H   3-Cl   4-OCF 3     138       1545   C 2 H 5     C 2 H 5     H   3-Cl   4-CF 3     188       1546   C 2 H 5     C 2 H 5     H   3-F   2-CH 3 -4-Cl   135       1547   C 2 H 5     C 2 H 5     H   3-F   4-CF 3     175       1548   C 2 H 5     C 2 H 5     H   3-F   4-OCF 3     155       1549   C 2 H 5     C 2 H 5     H   3-F   2-C 2 H 5 -4-C 2 F 5     80       1550   C 2 H 5     C 2 H 5     H   3-NO 2     2-CH 3 -4-C 2 F 5     185       1551   C 2 H 5     C 2 H 5     H   6-NO 2     2-CH 3 -4-C 2 F 5     145       1552   t-C 4 H 9     H   H   3-I   3-CH 3 -4-C 2 F 5     215       1553   CH 2 —Ph   CH 3     CH 3     3-Cl   2-CH 3 -4-C 2 F 5     Paste       1554   CH(CH 3 )—Ph   H   CH 3     3-Cl   2-CH 3 -4-C 2 F 5     Paste       1555   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-OCHF 2     138-139       1556   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-OCF 2 CHF 2     136       1557   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-Cl   179       1558   C 2 H 5     C 2 H 5     H   3-I   4-CF 3     187       1559   C 2 H 5     C 2 H 5     H   3-I   2-C 2 H 5 -4-C 2 F 5     106       1560   C 2 H 5     C 2 H 5     H   3-I   2-Cl-4-C 2 F 5     103-105       1561   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-C 2 F 5     115       1562   t-C 4 H 9     H   H   3-I   2-Br-4-C 2 F 5     185       1563   i-C 3 H 7     H   H   3-I   3-CH 3 -4-C 2 F 5     240       1564   i-C 3 H 7     H   H   H   4-O-(2-Pym)   246       1565   C(CH 3 ) 2 —CH 2 CH 3     H   H   3-I   2-CH 3 -4-C 2 F 5     193       1566   C(CH 3 ) 2 —CH 2 CH 3     H   H   3-I   2-CH 3 -4-OCF 3     180       1567   C(CH 3 ) 2 CH 2 CH 3     H   H   3-I       178-179       1568   C(CH 3 ) 2 CH 2 CH 3     H   H   3-I   2-CH 3 -4-OCHF 2     176-177       1569   C(CH 3 ) 2 CH═CH 2     H   H   3-Cl   2-CH 3 -4-C 2 F 5     223-224       1570   C(CH 3 ) 2 CH≡C—   H   H   3-Cl   2-CH 3 -4-C 2 F 5     92-93       1571   C(CH 3 ) 2 CH≡C—   H   H   3-Cl   2-CH 3 -4-C 2 F 5     96-97       1572   C(CH 3 ) 2 CH≡C—   H   H   3-Cl   2-CH 3 -4-C 2 F 5     88-89       1573   n-C 3 H 7     C 2 H 5     H   3-I   2-CH 3 -4-C 2 F 5     93       1574   n-C 3 H 7     C 2 H 5     H   3-I   2-CH 3 -4-OCF 3     109       1575   n-C 3 H 7     C 2 H 5     H   3-I   2-CH 2 -4-OCHF 2     102       1576   CH 2 (4-CF 3 O—Ph)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     172       1577   CH 2 (4-CF 3 O—Ph)   H   H   6-Cl   2-CH 3 -4-C 2 F 5     193       1578   CH 2 (3-Cl—Ph)   CH 3     H   3-Cl   2-CH 3 -4-C 2 F 5     Paste       1579   CH 2 (2-F—Ph)   CH 3     H   3-Cl   2-CH 3 -4-C 2 F 5     115       1580   i-C 3 H 7     H   H   3-I   2-Br-4-C 2 F 5     190       1581   n-C 3 H 7     C 2 H 5     H   3-F   2-CH 3 -4-C 2 F 5     120       1582   n-C 3 H 7     C 2 H 5     H   3-F   4-OCF 3     115       1583   n-C 3 H 7     C 2 H 5     H   3-F   4-OCHF 2     85       1584   n-C 3 H 7     C 2 H 5     H   3-F   2-Cl-4-C 2 F 5     75       1585   C(CH 3 ) 2 CH≡C—   H   H   3-Cl   2-CH 3 -4-C 2 F 5     102-103       1586   C(CH 3 ) 2 CH≡C—   H   H   3-Cl   2-CH 3 -4-C 2 F 5     115-117       1587   C(CH 3 ) 2 CH≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     169           2-Pyi       1588   C(CH 3 ) 2 CH≡CH   H   H   3-Cl   2-CH 3 -4-OCHF 2     191-192       1589   C(CH 3 ) 2 CH═CH 2     H   H   6-Cl   2-CH 3 -4-C 2 F 5     242       1590   C(CH 3 ) 2 CH≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     134-135           3-Pyi       1591   i-C 3 H 7     H   H   H   2-CH 3 -4-(2,6-   165                           (CH 3 O) 2 —Ph)       1592   i-C 3 H 7     H   H   H   2-CH 3 -4-(3,5-   150                           (CH 3 O) 2 —Ph)       1593   C 2 H 5     C 2 H 5     H   H   2-CH 3 -4-(3,5-   Paste                           (CH 3 O) 2 —Ph)       1594   i-C 3 H 7     H   H   3-Cl   2-F-4-(OCF 2 O)-5   195       1595   i-C 3 H 7     H   H   3-I   2-F-4-(OCF 2 O)-5   208       1596   t-C 4 H 9     H   H   3-I   2-F-4-(OCF 2 O)-5   202       1597   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-(OCHFCF 2 —O)-5   211       1598   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(OCHFCF 2 —O)-5   212       1599   t-C 4 H 9     H   H   3-I   2-CH 3 -4-(OCHFCF 2 —O)-5   217       1600   i-C 3 H 7     H   H   3-I   2-Cl-4-(OCHFCF 2 —O)-5   210       1601   i-C 3 H 7     H   H   3-I   2-Cl-4-(OCF 2 CHF—O)-5   214       1602   C(CH 3 ) 2 C≡CH   H   H   3-Cl   2-CH 3 -4-OCF 3     178-180       1603   C(CH 3 ) 2 CHBr—CH 2 Br   H   H   3-Cl   2-CH 3 -4-C 2 F 5     130-131       1604   C(CH 3 ) 2 CH═CH—Ph(E)   H   H   3-Cl   2-CH 3 -4-C 2 F 5     90-93       1605   C(CH 3 ) 2 CH 2 Br   H   H   3-I   2-CH 3 -4-OCF 3     139-141       1606   (S)-C*H—(CH 3 )—CH 2 Br   H   H   3-I   2-CH 3 -4-C 2 F 5     105-107       1607   (R)-C*H—(CH 3 )—CH 2 Br   H   H   3-I   2-CH 3 -4-C 2 F 5     105-107       1608   i-C 3 H 7     H   H   3-I   3-Cl-4-C 2 F 5     145       1609   t-C 4 H 9     H   H   3-I   3-Cl-4-C 2 F 5     260       1610   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C 2 F 5 -5-CH 3     210       1611   t-C 4 H 9     H   H   3-I   2-CH 3 -4-C 2 F 5 -5-CH 3     215       1612   i-C 3 H 7     H   H   3-I   2,3-(CH 3 ) 2 -4-C 2 F 5     210       1613   t-C 4 H 9     H   H   3-I   2,3-(CH 3 ) 2 -4-C 2 F 5     220       1614   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-(4-F-Ph)   130-133       1615   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-(4-Cl-Ph)   173-175       1616   i-C 3 H 7     H   H   H   2-CH 3 -4-O-(2-Thz)   149       1617   i-C 3 H 7     H   H   3-I   Mixture of 2-CH 3 -4-   235                           (4-(2-CH 3 -Thz)) and                           CH 2 -5-(4-(2-CH 3 -                           Thz)) (1:1)       1618   i-C 3 H 7     H   H   3-I   2-CH 3 -4-O-(2-Pym)   239       1619   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-(4-CF 2 -Ph) 112-115       1620   i-C 3 H 7     H   H   3-I   4-CF 2 CF 2 O-5   239       1621   i-C 3 H 7     H   H   3-Cl   4-CF 2 CF 2 O-5   243       1622   i-C 3 H 7     H   H   3-I   2-Cl-4-OCF 2 O-5   226       1623   i-C 3 H 7     H   H   3-Cl   2-Cl-4-OCF 2 O-5   223       1624   t-C 4 H 9     H   H   3-I   2-Cl-4-OCF 2 O-5   221       1625   i-C 3 H 7     H   H   3-I   2-Cl-4-OCF 2 CF 2 O   241       1626   i-C 3 H 7     H   H   3-I   2-Cl-3-OCF 2 CF 2 O-4   219       1627   C(CH 3 ) 2 CH 2 Cl   H   H   3-I   2-CH 3 -4-OCF 3     160       1628   C(CH 3 ) 2 C≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     78-80           3-Thi       1629   C(CH 3 ) 2 C≡CH   H   H   3-I   2-CH 3 -4-C 2 F 5     187-188       1630   i-C 3 H 7     H   H   3-I   2-CH 3 -4-(3,5-(CH 3 O) 2 —Ph)   199       1631   i-C 3 H 7     H   H   H   3-OCH 2 O-4   195       1632   i-C 3 H 7     H   H   H   2-F-4-Cl   177       1633   C(CH 3 ) 2 C≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     92-93           (4-CF 3 O—Ph)       1634   C(CH 3 ) 2 C≡CH   H   H   3-I   2-CH 3 -4-OCF 3     188-189       1635   C(CH 3 ) 2 C≡CH   H   H   3-I   2-CH 3 -4-OCHF 2     175-176       1636   i-C 3 H 7     H   H   3-I   4-N═(n-C 3 F 7 )C—O-5   182       1637   i-C 3 H 7     H   H   3-I   4-O—C(n-C 3 F 7 )═N-5   250       1638   i-C 3 H 7     H   H   3-Cl   4-O—C(n-C 3 F 7 )═N-5   168       1639   t-C 4 H 9     H   H   3-I   4-O—C(n-C 3 F 7 )═N-5   248       1640   i-C 3 H 7     H   H   3-I   2,3-(CH 3 ) 2 -4-C 2 F 5     195       1641   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OC(CF 3 )═N-5   229       1642   i-C 3 H 7     H   H   3-Cl   2-Cl-3-OCF 2 CF 2 O-4   188       1643   i-C 3 H 7     H   H   3-Cl   2-Cl-4-OCF 2 CF 2 O-5   203       1644   t-C 4 H 9     H   H   3-I   2-Cl-3-OCF 2 CF 2 O-4   189       1645   t-C 4 H 9     H   H   3-I   2-Cl-4-OCF 2 CF 2 O-5   234       1646   C(CH 3 ) 2 CH 2 Cl   H   H   3-I   2-CH 3 -4-C 2 F 5     168-169       1647   C(CH 3 ) 2 CH 2 Br   H   H   3-I   2-CH 3 -4-C 2 F 5     167-168       1648   C(CH 3 ) 2 C═C-   H   H   3-I   2-CH 3 -4-C 2 F 5     90           Naph       1649   C(CH 3 ) 2 C≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     105-106           (5-Br-2-Pyi)       1650   C(CH 3 ) 2 C≡C-   H   H   3-Cl   2-CH 3 -4-C 2 F 5     103-105           (2,4-F 2 -Ph)       1651   (S)-C*H(CH 3 )—CH 2 F   H   H   3-Cl   2-CH 3 -4-C 2 F 5     135       1652   (S)-C*H—(CH 3 )—CH 2 Br   H   H   3-Cl   2-CH 3 -4-C 2 F 5     193-198       1653   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C 2 F 5 -5-   210                           Cl       1654   t-C 4 H 9     H   H   3-I   2-CH 3 -4-C 2 F 5 -5-   200                           Cl       1655   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C 2 F 5 -5-   190                           CH 3         1656   t-C 4 H 9     H   H   3-I   2-CH 3 -4-C 2 F 5 -5-   195                           CH 3         1657   i-C 3 H 7     H   H   H   3-(2-CH 3 -4-Thz)   211       1658   i-C 3 H 7     H   H   3-I   3-(2-CF 3 -4-Thz)   122       1659   i-C 3 H 7     H   H   3-I   3-(2-CH 3 -4-Oxa)   102       1660   i-C 3 H 7     H   H   3-I   2-I-4-OCF 2 O-5   252       1661   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-OCF 2 O-5   218       1662   t-C 4 H 9     H   H   3-I   2-CH 3 O-4-C 2 F 5     135       1663   i-C 3 H 7     H   H   3-I   2-CH 3 -4-i-C 3 F 7 -5-F   235       1664   t-C 4 H 9     H   H   3-I   2-CH 3 -4-i-C 3 F 7 -5-F 2     30       1665   i-C 3 H 7     H   H   3-I   2-CH 2 -4-i-C 3 F 7 -5-Cl 2     10       1666   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF 2 CF 2 O-5   198       1667   i-C 3 H 7     H   H   3-I   2-CH 3 -4-i-C 3 F 7     270       1668   t-C 4 H 9     H   H   3-I   2-CH 3 -4-i-C 3 F 7     290       1669   i-C 3 H 7     H   H   3-I   2-F-4-i-C 3 F 7     205       1670   t-C 4 H 9     H   H   3-I   2-F-4-i-C 3 F 7     210       1671   i-C 3 H 7     H   H   3-I   2-SCH 3 -4-i-C 3 F 7     205       1672   t-C 4 H 9     H   H   3-I   2-SCH 3 -4-i-C 3 F 7     205       1673   i-C 3 H 7     H   H   3-I   2,4-(CH 3 ) 2 -4-i-C 3 F 7 240       1674   t-C 4 H 9     H   H   3-I   2,4-(CH 3 ) 2 -4-i-C 3 F 7 245       1675   i-C 3 H 7     H   H   3-I   4-(2-CH 3 -4-Thz)   217       1676   i-C 3 H 7     H   H   3-I   4-(2-CH 3 -4-Oxa)   212       1677   i-C 3 H 7     H   H   3-I   4-(2-i-C 3 H 7 -4-Thz) 199       1678   i-C 3 H 7     H   H   3-NO 2     4-(2-CH 3 -4-Thz)   230       1679   i-C 3 H 7     H   H   3-I   2-Cl-3-OCF 2 CHFO-4   188       1680   i-C 3 H 7     H   H   3-I   2-Cl-3-OCHFCF 2 O-4   191       1681   i-C 3 H 7     H   H   3-I   Mixture of 2-Cl-3-   199                           OCHFCF 2 O-4-5-Cl and                           2-Cl-3-OCHFCF 2 O-4-6-                           Cl (1:1)       1682   i-C 3 H 7     H   H   3-I   2-Cl-3-N═C(CF 3 )-O-4   265       1683   t-C 4 H 9     H   H   3-I   2-Cl-3-N═C(CF 3 )-O-4   259       1684   i-C 3 H 7     H   H   3-I   2-Br-4-OCF 2 CHFO-5   185       1685   i-C 3 H 7     H   H   3-I   Mixture of 2,3-Br 2 -4-   250                           CF 2 CHFO-5; 2,5-Br 2 -3-                           CHFCF 2 O-4; and 2,6-                           Br 2 -3-OCF 2 CHFO-4(1:1:1)       1686   i-C 3 H 7     H   H   3-I   Mixture of 2,3-Br 2 -4-   228                           CHFCF 2 O-5; 2,5-Br 2 -3-                           CF 2 CHFO-4; and 2,6-                           Br 2 -3-OCF 2 CHFO-4(1:1:1)       1689   i-C 3 H 7     H   H   3-I   2,3-(CH 3 ) 2 -4-i-C 3 F 7     270       1690   t-C 4 H 9     H   H   3-I   2,3-(CH 3 ) 2 -4-i-C 3 F 7     280       1691   i-C 3 H 7     H   H   3-I   2-i-C 3 H 7 -4-i-C 3 F 7     240       1692   t-C 4 H 9     H   H   3-I   2-i-C 3 H 7 -4-i-C 3 F 7     245       1693   i-C 3 H 7     H   H   3-I   2-OC 2 H 5 -4-i-C 3 F 7     195       1694   t-C 4 H 9     H   H   3-I   2-OC 2 H 5 -4-i-C 3 F 7     210       1695   i-C 3 H 7     H   H   3-I   3-F-4-i-C 3 F 7     265       1696   t-C 4 H 9     H   H   3-I   3-F-4-i-C 3 F 7     285       1697   i-C 3 H 7     H   H   3-I   3-Cl-4-i-C 3 F 7     295       1698   i-C 3 H 7     H   H   3-I   2-Br-4-i-C 3 F 7 -5-CH 3     240       1699   i-C 3 H 7     H   H   3-I   2-Br-4-i-C 3 F 7     240       1700   i-C 3 H 7     H   H   3-I   2-SCH 3 -4-C 2 F 5     200       1703   i-C 3 H 7     H   H   3-I   4-(2-c-C 3 H 5 -4-Thz)   198       1714   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -4-i-C 3 F 7     220       1715   i-C 3 H 7     H   H   3-I   2-OCH 3 -4-i-C 3 F 7     190       1716   i-C 3 H 7     H   H   3-I   2,6-(CH 3 ) 2 -4-i-C 3 F 7     275       1717   i-C 3 H 7     H   H   3-I   2,6-(CH 3 ) 2 -4-C 2 F 5     250       1722   i-C 3 H 7     H   H   3-I   2-Cl-4-i-C 3 F 7     220       1723   t-C 4 H 9     H   H   3-I   2-Cl-4-i-C 3 F 7     210       1726   i-C 3 H 7     H   H   3-I   2-(CH 2 )4-3-4-i-C 3 F 7     260       1727   t-C 4 H 9     H   H   3-I   2-(CH 2 )4-3-4-i-C 3 F 7     272       1732   i-C 3 H 7     H   H   3-I   2-Cl-3-OCF 2 CF 2 O-4   245       1733   i-C 3 H 7     H   H   3-I   2-Cl-3-OCHFCF 2 O-4   190       1737   i-C 3 H 7     H   H   3-I   4-C(CH 3 )═NOCH 3     190       1742   i-C 3 H 7     H   H   3-I   2-OCF 2 O-3   190       1743   i-C 3 H 7     H   H   3-I   2-OCF 2 O-3-6-Cl   213       1744   i-C 3 H 7     H   H   3-I   2-OCF 2 O-3-4-Cl   202       1745   i-C 3 H 7     H   H   3-I   2-OCF 2 O-3-4,6-Cl 2     228       1746   i-C 3 H 7     H   H   3-I   2-OCF 2 O-3-4-i-C 3 F 7     175       1747   t-C 4 H 9     H   H   3-I   2-OCF 2 O-3-4-Cl   235       1748   t-C 4 H 9     H   H   3-I   2-OCF 2 O-3-4,6-Cl 2     243       1749   i-C 3 H 7     H   H   3-I   4-C(CH 3 )═NOCH 2 —Ph   205       1750   i-C 3 H 7     H   H   3-I   4-C(CH 3 )═NOCH 2 —CH═CH 2     Decomp.       1751   CH 3     CH 3     H   H   2-CH 3 -4-Cl   149       1752   C 2 H 5     C 2 H 5     H   H   2-CH 3 -4-Cl   172       1753   n-C 3 H 7     n-C 3 H 7     H   H   2-CH 3 -4-Cl   126       1762   i-C 3 H 7     H   H   3-I   3-C(i-C 3 F 7 )═NN-   Paste                           (i-C 3 F 7 )-4       1763   i-C 3 H 7     H   H   3-I   4-i-C 3 H 7 -2-N═CH-S-3   200       1764   i-C 3 H 7     H   H   3-I   3-S-C(i-C 3 H 7 )═N-4   218       1765   i-C 3 H 7     H   H   3-I   4-(2-CF 3 -4-Thz)   105       1766   i-C 3 H 7     H   H   3-I   3-SCH 3 -4-i-C 3 F 7     160       1767   i-C 3 H 7     H   H   3-I   2-Ph-4-i-C 3 F 7     240       1768   i-C 3 H 7     H   H   3-I   2-OPh-4-i-C 3 F 7     180       1769   i-C 3 H 7     H   H   3-I   2-OCH 3 -4-i-C 3 F 7     265       1770   (CH 2 ) 2 -3-Pyi   H   H   3-I   2-CH 3 -4-i-C 3 F 7     Amorphous       1771   (CH 2 ) 2 -3-Pyi   H   H   6-I   2-CH 3 -4-i-C 3 F 7     Amorphous       1772   (CH 2 ) 2 -3-Pyi   H   H   3-I   2-CH 3 -4-OCF 3     169-173       1773   H(CH 3 )-2-Pyi   H   H   3-I   2-CH 3 -4-i-C 3 F 7     Amorphous       1774   H(CH 3 )-2-Pyi   H   H   6-I   2-CH 3 -4-i-C 3 F 7     Amorphous       1775   H(CH 3 )-2-Pyi   H   H   3-I   2-CH 3 -4-OCF 3     158-161       1776   H(CH 3 )-2-Pyi   H   H   6-I   2-CH 3 -4-OCF 3     213-216       1777   H(CH 3 )-2-Pyi   H   H   3-I   2-CH 3 -4-C 2 F 5     149-152       1778   H(CH 3 )-2-Pyi   H   H   6-I   2-CH 3 -4-C 2 F 5     194-196       1780   N(Ph)COCF 3     H   H   3-I   2-CH 3 -4-C 2 F 5     239-241       1799   CH(CH 3 )-2-Fur   H   H   3-I   2-CH 3 -4-i-C 3 F 7     191       1800   CH(CH 3 )-2-Thi   H   H   3-I   2-CH 3 -4-i-C 3 F 7     159       1801   i-C 3 H 7     H   H   3-CF 3     2-CH 3 -4-C 2 F 5     210-212       1802   i-C 3 H 7     H   H   3-Cl-6-   2-CH 3 -4-C 2 F 5     236-237                       CF 3 S       1803   i-C 3 H 7     H   H   3-CF 3 SO   2-CH 3 -4-C2F6   186-187       1804   i-C 3 H 7     H   H   3-CF 3 SO   2-CH 3 -4-C 2 F 5     206-208       1805   i-C 3 H 7     H   H   3-CF 3 SO   2-CH 3 -4-i-C 3 F 7     211-213       1815   i-C 3 H 7     H   H   3-I   2-CH 3 -4-s-C 4 F 9     190       1816   i-C 3 H 7     H   H   3-I   2-OH-4-i-C 3 F 7     155       1824   i-C 3 H 7     H   H   3-I   2-N═C(CF 3 )O-3   132                           4-i-C 3 F 7         1825   i-C 3 H 7     H   H   3-I   2-N═C(CF 3 )O-3   145       1826   t-C 4 H 9     H   H   3-I   2-N═C(CF 3 )O-3   110                           4-i-C 3 F 7         1827   t-C 4 H 9     H   H   3-I   2-N═C(CF 2 )O-3   120       1829   (CH 2 ) 2 NH—CO 2 C 2 H 5     H   H   3-I   2-CH 3 -4-i-C 3 F 7     155       1830   (CH 2 ) 2 NHCO 2 CH 2 Ph   H   H   3-I   2-CH 3 -4-C 2 F 5     155       1831   (CH 2 ) 2 CH═CF 2     H   H   3-I   2-CH 3 -4-C 2 F 5     180       1838   i-C 3 H 7     H   H   H   2-CH 3 -4-OCF 2 CF 3         1839   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-OCF 2 CF 2         1840   i-C 3 H 7     H   H   3-F   2-CH 3 -4-OCF 2 CF 2         1841   i-C 3 H 7     H   H   3-Cl   2-CH~-4-OCF 2 CF 2         1842   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-OCF 2 CF 2         1843   i-C 3 H 7     H   H   3-Cl-4-F   2-CH 3 -4-OCF 2 CF 3         1844   i-C 3 H 7     H   H   3,4-Cl 2     2-CH 3 -4-OCF 2 CF 3         1845   i-C 3 H 7     H   H   3-I   4-OCF 2 CF 3         1846   i-C 3 H 7     H   H   3-I   2-Cl-4-OCF 2 CF 3         1847   i-C 3 H 7     H   H   3-I   2-CH 3 -4-OCF 2 CF 3         1848   t-C 4 H 9     H   H   3-I   2-CH 3 -4-OCF 2 CF 3         1849   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-OCF 2 CF 3         1850   i-C 3 H 7     H   H   3-I   2-C 2 H 5 4-OCF 2 CF 3         1851   i-C 3 H 7     H   H   H   2-CH 3 -4-O-n-C 3 F 7         1852   i-C 3 H 7     H   H   3-NO 2     2-CH 3 -4-O-n-C 3 F 7         1853   i-C 3 H 7     H   H   3-F   2-CH 3 -4-O-n-C 3 F 7         1854   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-O-n-C 3 F 7         1855   i-C 3 H 7     H   H   3-Br   2-CH 3 -4-O-n-C 3 F 7         1856   t-C 4 H 9     H   H   3-Cl-4-F   2-CH 3 -4-O-n-C 3 F 7         1857   C 2 H 5     C 2 H 5     H   3,4-Cl 2     2-CH 3 -4-O-n-C 3 F 7         1858   i-C 3 H 7     H   H   3-I   4-O-n-C 3 F 7         1859   i-C 3 H 7     H   H   3-I   2-Cl-4-O-n-C 3 F 7         1860   i-C 3 H 7     H   H   3-I   2-CH 3 -4-O-n-C 3 F 7         1861   t-C 4 H 9     H   H   3-I   2-CH 3 -4-O-n-C 3 F 7         1862   C 2 H 5     C 2 H 5     H   3-I   2-CH 3 -4-O-n-C 3 F 7         1863   i-C 3 H 7     H   H   3-I   2-C 2 H 5 -4-OCF 2 CF 3         1864   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C≡C-t-C4F9       1865   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C≡C-CF 3         1866   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C≡C-i-C 3 F 7         1867   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF═CF 2         1868   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CF═CFCF 3         1869   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CF 3 )═CF 2         1870   i-C 3 H 7     H   H   3-I   2-CH 3 -4-COCH 3         1871   i-C 3 H 7     H   H   3-I   2-CH 3 -4-COCF 3     195       1872   i-C 3 H 7     H   H   3-I   2-CH 3 -4-COC 2 F 5         1873   i-C 3 H 7     H   H   3-I   2-CH 3 -4-COCF(CH 3 ) 2         1874   i-C 3 H 7     H   H   3-I   2-CH 3 -4-COOCH 3     217       1875   i-C 3 H 7     H   H   3-I   2-CH 3 -COOC 2 H 5         1876   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CH 3 )═NOCH 3     218       1877   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CH 3 )═NOC 2 H 5         1878   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CH 3 )═NO—CH 2 CH═CH 2         1879   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CH 3 )═NO—CH 2 C≡CH       1880   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CH 3 )═NOCH 2 —Ph       1881   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CH 2 OH       1882   i-C 3 H 7     H   H   3-I   4-CH(OH)CH 2         1883   i-C 3 H 7     H   H   3-I   2-CH 2 -4-CH(OH)CH 3         1884   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CH 2 ON═C(CH 3 ) 2         1885   i-C 3 H 7     H   H   3-I   2-CH 3 -4-CH 2 ON═C(Ph)-                           i-C 3 H 7         1886   i-C 3 H 7     H   H   3-I   2-OCH 2 O-3-4-i-C 3 F 7         1887   i-C 3 H 7     H   H   3-I   2-OCH 2 CH 2 O-3-4-i-C 3 F 7         1888   i-C 3 H 7     H   H   3-I   2-OCF 2 CF 2 O-3-4-i-C 3 F 7         1889   i-C 3 H 7     H   H   3-I   2-OCF 2 CHFO-3-4-i-C 3 F 7         1890   i-C 3 H 7     H   H   3-I   2-OCHFCF 2 O-3-4-i-C 3 F 7         1891   i-C 3 H 7     H   H   3-I   2-SCH 2 S-3-4-i-C 3 F 7         1892   i-C 3 H 7     H   H   3-I   2-SCF 2 S-3-4-i-C 3 F 7         1893   i-C 3 H 7     H   H   3-I   2-SCH 2 CH 2 S-3-4-i-C 3 F 7         1894   i-C 3 H 7     H   H   3-I   2-SCF 2 CF 2 S-3-4-i-C 3 F 7         1895   i-C 3 H 7     H   H   3-I   2-CH 2 OCH 2 -3-4-i-C 3 F 7         1896   i-C 3 H 7     H   H   3-I   2-CH 2 SCH 2 -3-4-i-C 3 F 7         1897   i-C 3 H 7     H   H   3-I   2-CF 2 OCF 2 -3-4-i-C 3 F 7         1898   i-C 3 H 7     H   H   3-I   2-CF 2 SCF 2 -3-4-i-C 3 F 7         1899   i-C2H7   H   H   3-Br   2-CH 3 -4-i-C 3 F 7         1900   i-C 3 H 7     H   H   3-Br-   2-CH 3 -4-i-C 3 F 7                         4-Cl       1901   i-C 3 H 7     H   H   3-I-4-F   2-CH 3 -4-i-C 3 F 7         1902   i-C 3 H 7     H   H   3-I-4-Cl   2-CH 3 -4-i-C 3 F 7         1903   i-C 3 H 7     H   H   3-1-4-CF 3     2-CH 3 -4-i-C 3 F 7         1904   i-C 3 H 7     H   H   3-I-4-OCH 3     2-CH 3 -4-i-C 3 F 7         1905   i-C 3 H 7     H   H   3-1-4-Br   2-CH 3 -4-i-C 3 F 7         1906   i-C 3 H 7     H   H   3-Cl-4-CF 3     2-CH 3 -4-i-C 3 F 7         1907   i-C 3 H 7     H   H   3-CF 3 -4-Cl   2-CH 3 -4-i-C 3 F 7         1908   i-C 3 H 7     H   H   3-CF 3 -4-F   2-CH 3 -4-i-C 3 F 7         1919   i-C 3 H 7     H   H   3-CF 3 -4-OCH 3     2-CH 3 -4-i-C 3 F 7         1910   i-C 3 H 7     H   H   3-N═CH—CH═CH-4   2-CH 3 -4-i-C 3 F 7         1911   i-C 3 H 7     H   H   3-OCH 2 O-4   2-CH 3 -4-i-C 3 F 7         1912   i-C 3 H 7     H   H   3-OCH 2 O-4   2-CH 3 -4-C 2 F 5         1913   i-C 3 H 7     H   H   3-OCH 2 O-4   2-CH 3 -4-OCF 3         1914   i-C 3 H 7     H   H   3-OCF 2 O-4   2-CH 3 -4-i-C 3 F 7         1915   i-C 3 H 7     H   H   3-OCF 2 O-4   2-CH 3 -4-C 2 F 5         1916   i-C 3 H 7     H   H   3-OCF 2 O-4   2-CH 3 -4-OCF 3         1917   i-C 3 H 7     H   H   3-OCH 2 CH 2 O-4   2-CH 3 -4-i-C 3 F 7         1918   i-C 3 H 7     H   H   3-OCF 2 CF 2 O-4   2-CH 3 -4-i-C 3 F 7         1919   i-C 3 H 7     H   H   3-OCHFCF 2 O-4   2-CH 3 -4-i-C 3 F 7         1920   i-C 3 H 7     H   H   3-OCF 2 CHFO-4   2-CH 3 -4-i-C 3 F 7         1921   i-C 3 H 7     H   H   3-OCH 2 CH 2 -4   2-CH 3 -4-i-C 3 F 7         1922   i-C 3 H 7     H   H   3-CH 2 CH 2 O-4   2-CH 3 -4-i-C 3 F 7         1923   i-C 3 H 7     H   H   3-OCF 2 CF 2 -4   2-CH 3 -4-i-C 3 F 7         1924   i-C 3 H 7     H   H   3-CF 2 CF 2 O-4   2-CH 3 -4-i-C 3 F 7         1925   i-C 3 H 7     H   H   3-SOCH 3     2-CH 3 -4-i-C 3 F 7         1926   i-C 3 H 7     H   H   3-SO 2 CH 3     2-CH 3 -4-i-C 3 F 7         1927   i-C 3 H 7     H   H   3-CF 3 S   2-CH 3 -4-i-C 3 F 7     222-223       1928   i-C 3 H 7     H   H   6-CF 3 S   2-CH 3 -4-i-C 3 F 7     219-221       1929   t-C 4 H 9     H   H   3-CF 3 S   2-CH 3 -4-i-C 3 F 7     231       1930   t-C 4 H 9     H   H   6-CF 3 S   2-CH 3 -4-i-C 3 F 7     245-247       1931   t-C 4 H 9     H   H   3-CF 3 SO 2     2-CH 3 -4-i-C 3 F 7         1932   t-C 4 H 9     H   H   3-CF 3 SO 2     2-CH 3 -4-C 2 F 5         1933   t-C 4 H 9     H   H   3-CF 3 SO 2     2-CH 3 -4-OCF 3         1934   C 2 H 5     C 2 H 5     H   3-CF 3 SO 2     2-CH 3 -4-i-C 3 F 7         1935   C 2 H 5     C 2 H 5     H   3-CONHCH 3     2-CH 3 -4-i-C 3 F 7         1936   C 2 H 5     C 2 H 5     H   3-CON(CH 3 ) 2     2-CH 3 -4-i-C 3 F 7         1937   C 2 H 5     C 2 H 5     H   3-COCH 3     2-CH 3 -4-i-C 3 F 7         1938   C 2 H 5     C 2 H 5     H   3-COC 2 H 5     2-CH 3 -4-i-C 3 F 7         1939   C 2 H 5     C 2 H 5     H   3-C(CH 3 )═NOCH 3     2-CH 3 -4-i-C 3 F 7         1940   C 2 H 5     C 2 H 5     H   3-C(CH 3 )═NO—C 2 H 5     2-CH 3 -4-i-C 3 F 7         1941   i-C 3 H 7     H   H   3-C≡CH   2-CH 3 -4-C 2 F 5         1942   i-C 3 H 7     H   H   3-C≡CH   2-CH 2 -4-i-C 3 F 7         1943   i-C 3 H 7     H   H   3-C≡C-t-C 4 H 9     2-CH 3 -4-C 2 F 5     195-202       1944   i-C 3 H 7     H   H   3-C≡C-t-C 4 H 9     2-CH 3 -4-i-C 3 F 7         1945   i-C 3 H 7     H   H   3-C≡C—Ph   2-CH 3 -4-C 2 F 5     179-183       1946   i-C 3 H 7     H   H   3-C≡C—Ph   2-CH 3 -4-i-C 3 F 7         1947   i-C 3 H 7     H   H   3-C≡C—CF 3     2-CH 3 -4-C 2 F 5         1948   i-C 3 H 7     H   H   3-C≡C—CF 3     2-CH 3 -4-i-C 3 F 7         1949   i-C 3 H 7     H   H   3-C 2 F 5     2-CH 3 -4-C 2 F 5         1950   t-C 4 H 9     H   H   3-C 2 F 5     2-CH 3 -4-C 2 F 5         1951   C 2 H 5     C 2 H 5     H   3-C 2 F 5     2-CH 3 -4-C 2 F 5         1952   i-C 3 H 7     H   H   3-C 2 F 5     2-CH 3 -4-i-C 3 F 7         1953   t-C 4 H 9     H   H   3-C 2 F 5     2-CH 3 -4-i-C 3 F 7         1954   C 2 H 5     C 2 H 5     H   3-C 2 F 5     2-CH 3 -4-i-C 3 F 7         1955   i-C 3 H 7     SN-   H   3-I   2-CH 3 -4-i-C 3 F 7                 (n-C 4 H 9 ) 2         1956   i-C 3 H 7     SO 2 CH 3     H   3-I   2-CH 3 -4-i-C 3 F 7         1957   i-C 3 H 7     CN   H   3-I   2-CH 3 -4-i-C 3 F 7         1958   i-C 3 H 7     COOCH 3     H   3-I   2-CH 3 -4-i-C 3 F 7         1959   i-C 3 H 7     COOC 2 H 5     H   3-I   2-CH 3 -4-i-C 3 F 7         1960   i-C 3 H 7     COCH 3     H   3-I   2-CH 3 -4-i-C 3 F 7         1961   i-C 3 H 7     COC 2 H 5     H   3-I   2-CH 3 -4-i-C 3 F 7         1962   i-C 3 H 7     CO—Ph   H   3-I   2-CH 3 -4-i-C 3 F 7         1963   i-C 3 H 7     NHCOCH 3     H   3-I   2-CH 3 -4-i-C 3 F 7         1964   C 2 H 5     C 2 H 5     SN(n-   3-I   2-CH 3 -4-i-C 3 F 7                     C 4 H 9 ) 2         1965   C 2 H 5     C 2 H 5     SO 2 CH 3     3-I   2-CH 3 -4-i-C 3 F 7         1966   C 2 H 5     C 2 H 5     ON   3-I   2-CH 3 -4-i-C 3 F 7         1967   C 2 H 5     C 2 H 5     COOCH 3     3-I   2-CH 3 -4-i-C 3 F 7         1968   C 2 H 5     C 2 H 5     COOC 2 H 5     3-I   2-CH 3 -4-i-C 3 F 7         1969   C 2 H 5     C 2 H 5     COOH3   3-I   2-CH 3 -4-i-C 3 F 7         1970   C 2 H 5     C 2 H 5     COC 2 H 5     3-I   2-CH 3 -4-i-C 3 F 7     Amorphous       1971   C 2 H 5     C 2 H 5     COPh   3-I   2-CH 3 -4-i-C 3 F 7         1972   C 2 H 5     C 2 H 5     NHCOCH 3     3-I   2-CH 3 -4-i-C 3 F 7         1973   (CH 2 ) 2 COO—CH 3     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1974   (CH 2 ) 2 COO—CH 3     H   H   3-I   2-CH 3 -4-C 2 F 5         1975   (CH 2 ) 2 COO—C 2 H 5     H   H   3-I   2-CH 3 -4-i-C 3 F 7     133.2       1976   (CH 2 ) 2 COO—C 2 H 5     H   H   3-I   2-CH 3 -4-C 2 F 5         1977   (CH 2 ) 2 COO—C 2 H 5     H   H   6-I   2-CH 3 -4-C 2 F 5     163.5       1978   CH(CH 3 )CH 2 —COOCH 3     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1979   CH(CH 3 )CH 2 COOC 2 H 5     H   H   3-I   2-CH 3 -4-i-C 3 H 7         1980   CH(CH 3 )CH 2 COO-i-   H   H   3-I   2-CH 3 -4-i-C 3 F 7             C 3 H 7         1981   (CH 2 ) 2 CONHCH 3     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1982   (CH 2 ) 2 CONHC 2 H 5     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1983   CH(CH 3 )CH 2 CONHCH 3     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1984   CH(CH 3 )CH 2 CONHC 2 H 5 H   H   3-I   2-CH 3 -4-i-C 3 F 7         1985   CH(CH 3 )CH 2 CONH-i-   H   H   3-I   2-CH 3 -4-i-C 3 F 7             C 3 H 7         1986   CH(CH 3 )CH 2 CON   H   H   3-I   2-CH 3 -4-i-C 3 F 7         1987   CH(CH 3 )CH 2 CON—(C 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1988   (CH 2 ) 2 NHCOOCH 3     H   H   3-I   2-CH 3 -4-C 2 F 5         1989   (CH 2 ) 2 NHCOOCH 3     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1990   (CH 2 ) 2 NHCOOC 2 H 5 H   H   3-I   2-CH 3 -4-C 2 F 5     145       1991   (CH 2 ) 2 NHCOOC 2 H 5     H   H   3-I   2-CH 3 -4-OCF 3     210       1992   CH(CH 3 )CH 2 NHCOOCH 3     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1993   CH(CH 3 )CH 2 NHCOO—C 2 H 5     H   H 3-I   2-CH 3 -4-i-C 3 F 7         1994   (CH 2 ) 2 P(CH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1995   CH(CH 3 )P(C 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1996   (CH 2 ) 2 P(Ph) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1997   CH(CH 3 )CH 2 P(CH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1998   CH(CH 3 )CH 2 P(C 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         1999   CH(CH 3 )CH 2 P(Ph) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2000   CH(CH 3 )(CH 2 ) 2 P—(CH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2001   CH(CH 2 )(CH 2 ) 3 P—(CH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2002   (CH 2 ) 2 PO(CH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2003   (CH 2 ) 2 PO(OC 2 H 5 ) 2     H   H   3-1   2-CH 3 -i-C2F7   Amorphous       2004   CH(CH 3 )CH 2 PO(OCH 3 ) 2     H   H   3-I   2-CH 3 -i-C 3 F 7         2005   (CH 2 ) 2 OPO(OCH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2006   CH(CH 3 )CH 2 PS(OCH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2007   CH(CH 3 )CH 2 PS—(OC 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2008   (CH 2 ) 2 OPO(OC 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2009   CH(CH 3 )CH 2 OPO—(OCH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2010   CH(CH 3 )CH 2 OPO—(OC 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2011   (CH 2 ) 2 OPS(OCH 3 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2012   (CH 2 ) 2 OPS(OC 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2013   CH(CH 3 )CH 2 OPS   H   H   3-I   2-CH 3 -4-i-C 3 F 7         2014   CH(CH 3 )CH 2 OPS—(OC 2 H 5 ) 2     H   H   3-I   2-CH 3 -4-i-C 3 F 7         2015   CH(CH 3 )-2-Pyi-N-Oxide   H   H   3-I   2-CH 3 -4-C 2 F 5     198-205       2016   CH(CH 3 )-2-Pyi-N-Oxide   H   H   3-I   2-CH 3 -4-i-C 3 F 7     208-210       2017   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CF 3 )═NOCH 3         2018   i-C 3 H 7     H   H   3-I   2-CH 3 -4-C(CF 3 )═NOCH 2 P       2019   i-C 3 H 7     H   H   3-I   2-NCHCHCHCH-3   180                           4-i-C 3 F 7         2020   i-C 3 H 7     H   H   3-I   2-n-C 3 H 7 -4-i-   225                           C 3 F 7         2021   i-C 3 H 7     H   H   3-I   2-O-(2-Pyi)-4-   158.3-159.8                           i-C 3 F 7                    
 
           [0135]    The abbreviations in Table 1 stand for the following substituents:  
           [0136]    Ph: phenyl group,  
           [0137]    c-: alicyclic hydrocarbon group,  
           [0138]    Pyi: pyridyl group,  
           [0139]    Pym: pyrimidinyl group,  
           [0140]    Fur: furyl group,  
           [0141]    TetFur: tetrahydrofuryl group,  
           [0142]    Thi: thienyl group,  
           [0143]    Thz: thiazolyl group,  
           [0144]    Naph: naphthyl group,  
           [0145]    Oxa: oxazolyl group,  
           [0146]    C*: asymmetric carbon atom  
                                               TABLE 2                                                       Physical                                       Properties                                       (melting                                       point:       No   R 1     R 2     R 3     Xn   Ym   Z 1     Z 2     ° C.                   S-1   i-C 3 H 7     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     S   0   162-164       S-2   t-C 4 H 9     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     S   0   141-143       S-3   c-C 3 H 5     H   H   3-Cl   2-CH 3 -4-CF 2 CF 3     S   0   138-139       S-4   C 2 H 5     C 2 H 5     H   3-Cl   2-CH 3 -4-CF 2 CF 3     S   0   184-186       S-5   i-C 3 H 7     H   H   H   2-CH 3 -4-Cl   S   0   168-170       S-6   i-C 3 H 7     H   H   H   2-CH 3 -4-Cl   0   S       S-7   i-C 3 H 7     H   H   3-I   2-CH 3 -4-i-C 3 H 7     0   S       S-8   i-C 3 H 7     H   H   H   2-CH 3 -4-i-C 3 H 7     S   S       S-9   i-C 3 H 7     H   H   3-I   2-CH 3 -4-i-C 3 H 7     S   S                  
 
           [0147]    The  1 H-NMR data of the compounds obtained as paste (physical properties) are given in Table 3 below.  
                   TABLE 3                       No.     1 H—NMR[CDCl 3 /TMS δ values (ppm)]                   1122   1.2-1.4(m.6H), 2.4-2.5(m.3H), 3.1-3.9(m.7H), 6.6-7.9(m.6H)       1218   1.3(d.3H), 2.3(s.3H), 2.9-3.2(m.2H), 4.4(m.1H), 6.2(d.1H),           7.1-7.5(m.3H), 7.8(d.1H), 8.0(d.1H), 8.4(d.1H),8.5(s.1H).                  
 
           [0148]    The fluorine-containing aniline compound of the general formula (ST-I) of the present invention is useful as an intermediate of a medicine, agrochemical, chemical product etc., particularly, is useful as a starting material of the phthalic acid diamide derivative of the general formula (I) of the present invention. That is, the fluorine-containing aniline compound of the general formula (ST-I) is useful as an aniline of the general formula (IV) in the Production processes 1, 3, 5 and 6 as illustrated above. The fluorine-containing aniline compound of the general formula (ST-I) of the present invention can be produced, for example, by any of the following production processes.  
                         
 
           [0149]    wherein each of X a , X b  and X c  is a hydrogen atom, an iodine atom or a bromine atom, provided that at least one of X a , X b  and X c  is not a hydrogen atom, and R a , R b , R c  and R d  are as defined above.  
           [0150]    A fluorine-containing aniline compound of the general formula (ST-I) can be produced by reacting an aniline derivative of the general formula (ST-II) with a perfluoroalkyl iodide of the general formula (ST-III), general formula (ST-IV) or general formula (ST-V) in the presence of activated copper powder and an inert solvent.  
           [0151]    Usually, the amount of each of the perfluoroalkyl iodide of the general formula (ST-III), (ST-IV) or (ST-V) and the activated copper powder used may be properly chosen in the range of 1 to 5 times the amount of the aniline derivative of the general formula (ST-II).  
           [0152]    As the inert solvent used in the reaction, any solvent may be used so long as it does not remarkably inhibit the progress of the reaction. There can be used, for example, aprotic polar solvents such as N,N-dimethylformamide (DMF), dimethyl sulfoxide (DMSO), etc. The reaction temperature may be properly chosen in the range of room temperature to 200° C.  
           [0153]    After completion of the reaction, the desired compound is isolated from the reaction mixture containing the desired compound by a conventional method and can, if necessary, be purified by silica gel chromatography, distillation, recrystallization, etc.  
           [0154]    The reaction can be carried out by the method described in Bull. Chem. Soc. Jpn., 65, 2141-2144 (1992).  
                         
 
           [0155]    wherein R a , R b , R c , R d , X a , X b  and X c  are as defined above, and Re is a protecting group such as an acyl group.  
           [0156]    A fluorine-containing aniline compound of the general formula (ST-I) can be produced by reacting an acylaniline derivative of the general formula (ST-VI) with a perfluoroalkyl iodide of the general formula (ST-III), general formula (ST-IV) or general formula (ST-V) in the presence of activated copper powder and an inert solvent to obtain an acylaniline derivative of the general formula (ST-VII), and deacylating the acylaniline derivative (ST-VII) after or without isolation.  
           [0157]    {circle over (1)} General Formula (ST-VI)→General Formula (ST-VII)  
           [0158]    This reaction can be carried out according to production process 8.  
           [0159]    {circle over (2)} General Formula (ST-VII)→General Formula (ST-I)  
           [0160]    This reaction is usually carried out under acidic conditions. In the reaction, for example, an aqueous mineral acid solution such as a 5 to 35% aqueous hydrochloric acid solution is used as an acid. If necessary, there may be used together therewith alcohols such as methanol, ethanol, etc., and inert solvents such as tetrahydrofuran (THF), acetonitrile, etc. The reaction temperature may be chosen in the range of room temperature to the boiling point of the solvent used. The desired compound can be produced by carrying out the similar workup as in production process 8.  
                         
 
           [0161]    wherein R a , R b , R c , R d , X a , X b  and X c  are as defined above.  
           [0162]    A fluorine-containing aniline compound of the general formula (ST-I) can be produced by reacting a nitrobenzene derivative of the general formula (ST-VIII) with a perfluoroalkyl iodide of the general formula (ST-III), general formula (ST-IV) or general formula (ST-V) in the presence of activated copper powder and an inert solvent to obtain a nitrobenzene derivative of the general formula (ST-IX), and reducing the nitrobenzene derivative (ST-IX) after or without isolation.  
           [0163]    {circle over (1)} General Formula (ST-VIII)→General Formula (ST-IX)  
           [0164]    This reaction can be carried out according to production process 8.  
           [0165]    {circle over (2)} General Formula (ST-IX)→General Formula (ST-I)  
           [0166]    Usually, the desired compound can be produced by subjecting the nitrobenzene derivative (ST-IX) to catalytic hydrogenation in an alcohol solvent in the presence of a catalyst such as 5% palladium carbon (proportion: 1 to 5% by weight), or reducing the nitro-benzene derivative (ST-IX) with an aqueous hydrochloric acid solution containing stannous chloride, in a solvent such as ethanol.  
           [0167]    The reaction {circle over (2)} can be carried out according to the method described in Journal of Chemical Society of Japan, 1973, 2351.  
           [0168]    Typical examples of the fluorine-containing aniline compound of the general formula (ST-I) of the present invention are given in Table 4 but they are not intended in any way to limit the scope of the present invention.  
           [0169]    General Formula (ST-I):  
                                             TABLE 4                               (ST-I)                                                                          Physical property or       No.   R a     R b     R c     R d       1 H-NMR (δ, ppm)               ST-1   CH 3     H   H   C 2 F 5     2.21(s, 3H), 3.84(br,                           2H), 6.86(s, 1H),                           6.91(d, 1H), 7.15(d,                           1H).       ST-2   CH 3     H   H   i-C 3 F 7         ST-3   CH 3     H   C 2 F 5     H   b.p. 95-105° C./                           l0 mmHg       ST-4   CH 3     H   i-C 3 F 7     H   b.p. 100-110° C./                           l0 mmHg       ST-5   CH 3     H   n-C 3 F 7     H   2.20(s, 3H), 3.9(br,                           2H), 6.70(d, 1H),                           7.22-7.27(m, 2H).       ST-6   CH 3     H   n-C 4 F 9     H   2.19(s, 3H), 4.2(br,                           2H), 6.70(d, 1H),                           7.20-7.26(m, 2H).       ST-7   CH 3     H   CF(CF 3 )   H                   —C 2 F 5         ST-8   CH 3     C 2 F 5     H   H   2.22(s, 3H), 3.83(br,                           2H), 6.86(d, 1H),                           6.99(d, 1H), 7.12(t,                           1H).       ST-9   CH 3     i-C 3 F 7     H   H       ST-10   F   H   i-C 3 F 7     H       ST-11   Cl   H   C 2 F 5     H   4.4(br, 2H), 6.8(d,                           lH), 7.27(dd, lH),                           7.47(d, 1H).       ST-12   Cl   H   i-C 3 F 7     H   4.5(br, 2H), 7.41(s,                           1H), 7.81(d, 1H),                           8.05(d, 1H).       ST-13   Cl   H   n-C 3 F 7     H   4.1(br, 2H), 6.83(d,                           1H), 7.24(d, 1H),                           7.43(s, 1H).       ST-14   Br   H   C 2 F 5     H       ST-15   OCH 3     H   C 2 F 5     H   3.85(br, 2H), 3.93(s,                           3H), 6.72(d, 1H),                           6.92(s, 1H), 7.03(d,                           1H).       ST-16   OCH 3     H   i-C 3 F 7     H       ST-17   OC 2 H 5     H   i-C 3 F 7     H       ST-18   C 2 H 5     H   C 2 F 5     H   l.29(t, 3H), 2.52(q,                           2H), 3.95(br, 2H),                           6.8(d, lH), 7.2-                           7.26(m, 2H).       ST-19   C 2 H 5     H   i-C 3 F 7     H       ST-20   i-C 3 F 7     H   i-C 3 F 7     H       ST-21   n-C 4 H 9     H   C 2 F 5     H   0.9(t, 3H), 1.4(q,                           2H), 1.6(q, 2H),                           2.5(t, 2H), 3.95(br,                           2H), 6.69(d, 2H),                           7.19-7.21(m, 2H).       ST-22   CF 3     H   C 2 F 5     H   4.52(br, 2H), 6.81(d,                           1H), 7.48(d, 1H),                           7.63(br, 1H).       ST-23   CF 3     H   i-C 3 F 7     H                  
 
           [0170]    Agricultural and horticultural insecticides containing the phthalic acid diamide derivative of the general formula (I) of the present invention as an active ingredient are suitable for controlling various insect pests such as agricultural insect pests, forest insect pests, horticultural insect pests, stored grain insect pests, sanitary insect pests, nematodes, etc., which are injurious to paddy rice, fruit trees, vegetables, other crops, flowers and ornamental plants, etc. They have a marked insecticidal effect, for example, on LEPIDOPTERA including summer fruit tortrix ( Adoxophyes orana fasciata ), smaller tea tortrix (Adoxophyes sD.), Manchurian fruit moth ( Grapholita inopinata ), oriental fruit moth ( Grapholita molesta ), soybean pod border ( Leguminivora glycinivorella ), mulberry leafroller ( Olethreutes mori ), tea leafroller ( Caloptilia thevivora ), Caloptilia sp. ( Calopilia zachrysa ), apple leafminer ( Phyllonorycter ringoniella ), pear barkminer ( Spulerrina astaurota ), common white ( Piers rapae crucivora ), tabacco budworm (Heliothis sD.), codling moth ( Laspey resia pomonella ), diamondback moth ( Plutella xylostella ), apple fruit moth ( Argyresthia conjugella ), peach fruit moth ( Carposina niponensis ), rice stem borer ( Chilo suppressalis ), rice leafroller ( Cnaphalocrocis medinalis ), tabacco moth ( Ephestia elutella ), mulberry pyralid ( Glyphodes pyloalis ), yellow rice borer ( Scirpophaga incertulas ), rice skipper ( Parnara guttata ), rice armyworm ( Pseudaletia separata ), pink borer ( Sesamia inferens ), common cutworm ( Spodoptera litura ), beet armyworm ( Spodoptera exigua ), etc.; HEMIPTERA including aster leafhopper ( Macrosteles fascifrons ), green rice leafhopper ( Nephotettix cincticeps ), brown rice planthopper ( Nilaparvata lugens ), whitebacked rice planthopper ( Sogatella furcifera ), citrus psylla ( Diaphorina citri ), grape whitefly ( Aleurolobus taonabae ), sweetpotato whitefly ( Bemisia tabaci ), greenhouse whitefly ( Trialeurodes vaporariorum ), turnip aphid ( Lipaphis erysimi ), green peach aphid ( Myzus persicae ), Indian wax scale ( Ceroplastes ceriferus ), cottony citrus scale ( Pulvinaria aurantii ), camphor scale ( Pseudaonidia duplex ), San Jose scale ( Comstockaspis perniciosa ), arrowhead scale ( Unaspis yanonensis ), etc.; COLEOPTERA including soybean beetle ( Anomala rufocuprea ), Japanese beetle ( Popillia iaponica ), tabacco beetle ( Lasioderma serricorne ), powderpost beetle ( Lyctus brunneus ), twenty-eight-spotted ladybird ( Epilachna vigintiotopunctata ), adzuki bean weevile ( Callosobruchus chinensis ), vegetable weevil ( Listroderes costirostris ), maize weevil ( Sitophilus zeamais ), boll weevil ( Anthonomus gradis gradis ), rice water weevil ( Lissorhoptrus oryzophilus ), cucurbit leaf beetle ( Aulacophora femoralis ), rice leaf beetle ( Oulema oryzae ), striped flea beetle ( Phyllotreta striolata ), pine shoot beetle ( Tomicus piniperda ), Colorado potato beetle ( Leptinotarsa decemlineata ), Mexican bean beetle ( Epilachna varivestis ), corn rootworm (Diabrotica sp.), etc.; DIPTERA including melon fly ( Dacus ( Zeugodacus )  cucurbitae ), oriental fruit fly ( Dacus ( Bactrocera )  dorsalis ), rice leafminer ( Agnomyza oryzae ), onion maggot ( Delia antiqua ), seedcorn maggot ( Delia platura ), soybean pod gall midge (Asphondylia sp.), muscid fly ( Musca domestica ), house mosquito ( Culex pipiens pipiens ), etc.; and TYLENCHIDA including root-lesion nematode (Pratylenchus sp.), coffer root-lesion nematode ( Pratylenchus coffeae ), potato cyst nematode ( Globodera rostochiensis ), root-knot nematode (Meloidogyne sp.), citrus nematode ( Tylenchulus semipenetrans ), Aphelenchus sp. ( Aphelenchus avenae ), chrysanthemum foliar ( Aphelenchoides ritzemabosi ), etc.  
           [0171]    The agricultural and horticultural insecticide containing the phthalic acid diamide derivative of the general formula (I) of the present invention as an active ingredient has a marked insecticidal effect on the above-exemplified insect pests, sanitary insect pests, and/or nematodes, which are injurious to paddy field crops, upland crops, fruit trees, vegetables, other crops, flowers and ornament plants, and the like. Therefore, the desired effect of the agricultural and horticultural insecticide of the present invention can be obtained by applying the insecticide to the paddy field water, stalks and leaves of fruit trees, vegetables, other crops, flowers and ornament plants, soil, etc. at a season at which the insect pests, sanitary pests or nematodes are expected to appear, before their appearance or at the time when their appearance is confirmed.  
           [0172]    In general, the agricultural and horticultural insecticide of the present invention is used after being prepared into conveniently usable forms according to an ordinary manner for preparation of agrochemicals.  
           [0173]    That is, the phthalic acid diamide derivative of the general formula (I) and, optionally, an adjuvant are blended with a suitable inert carrier in a proper proportion and prepared into a suitable preparation form such as a suspension, emulsifiable concentrate, soluble concentrate, wettable powder, granules, dust or tablets through dissolution, dispersion, suspension, mixing, impregnation, adsorption or sticking.  
           [0174]    The inert carrier used in this invention may be either solid or liquid. As the solid carrier, there can be exemplified soybean flour, cereal flour, wood flour, bark flour, saw dust, powdered tobacco stalks, powdered walnut shells, bran, powdered cellulose, extraction residues of vegetables, powdered synthetic polymers or resins, clays (e.g. kaolin, bentonite, and acid clay), talcs (e.g. talc and pyrophyllite), silica powders or flakes (e.g. diatomaceous earth, silica sand, mica and white carbon, i.e. synthetic, high-dispersion silicic acid, also called finely divided hydrated silica or hydrated silicic acid, some of commercially available products contain calcium silicate as the major component), activated carbon, powdered sulfur, powdered pumice, calcined diatomaceous earth, ground brick, fly ash, sand, calcium carbonate powder, calcium phosphate powder and other inorganic or mineral powders, chemical fertilizers (e.g. ammonium sulfate, ammonium phosphate, ammonium nitrate, urea and ammonium chloride), and compost. These carriers may be used alone or as a mixture thereof.  
           [0175]    The liquid carrier is that which itself has solubility or which is without such solubility but is capable of dispersing an active ingredient with the aid of an adjuvant. The following are typical examples of the liquid carrier and can be used alone or as a mixture thereof. Water; alcohols such as methanol, ethanol, isopropanol, butanol and ethylene glycol; ketones such as acetone, methyl ethyl ketone, methyl isobutyl ketone, diisobutyl ketone and cyclohexanone; ethers such as ethyl ether, dioxane, Cellosolve, dipropyl ether and tetrahydrofuran; aliphatic hydrocarbons such as kerosene and mineral oils; aromatic hydrocarbons such as benzene, toluene, xylene, solvent naphtha and alkylnaphthalenes; halogenated hydrocarbons such as dichloroethane, chloroform, carbon tetrachloride and chlorobenzene; esters such as ethyl acetate, diisopropyl phthalate, dibutyl phthalate and dioctyl phthalate; amides such as dimethylformamide, diethylformamide and dimethylacetamide; nitrites such as acetonitrile; and dimethyl sulfoxide.  
           [0176]    The following are typical examples of the adjuvant, which are used depending upon purposes and used alone or in combination in some cases, or need not to be used at all.  
           [0177]    To emulsify, disperse, dissolve and/or wet an active ingredient, a surfactant is used. As the surfactant, there can be exemplified polyoxyethylene alkyl ethers, polyoxyethylene alkylaryl ethers, polyoxyethylene higher fatty acid esters, polyoxyethylene resinates, polyoxyethylene sorbitan mono-laurate, polyoxyethylene sorbitan monooleate, alkylarylsulfonates, naphthalenesulfonic acid condensation products, ligninsulfonates and higher alcohol sulfate esters.  
           [0178]    Further, to stabilize the dispersion of an active ingredient, tackify it and/or bind it, there may be used adjuvants such as casein, gelatin, starch, methyl cellulose, carboxymethyl cellulose, gum arabic, polyvinyl alcohols, turpentine, bran oil, bentonite and ligninsulfonates.  
           [0179]    To improve the flowability of a solid product, there may be used adjuvants such as waxes, stearates and alkyl phosphates.  
           [0180]    Adjuvants such as naphthalenesulfonic acid condensation products and polycondensates of phosphates may be used as a peptizer for dispersible products.  
           [0181]    Adjuvants such as silicon oils may also be used as a defoaming agent.  
           [0182]    The content of the active ingredient may be varied as required. In dusts or granules, the suitable content thereof is from 0.01 to 50% by weight. In emulsifiable concentrates or flowable wettable powders, it is also from 0.01 to 50% by weight.  
           [0183]    The agricultural and horticultural insecticide of the present invention is used to control a variety of insect pests in the following manner. That is, it is applied to a crop on which the insect pests are expected to appear or a site where the appearance of the insect pests is undesirable, as it is or after being properly diluted with or suspended in water or the like, in an amount effective for control of the insect pests.  
           [0184]    The applying dosage of the agricultural and horticultural insecticide of the present invention is varied depending upon various factors such as a purpose, insect pests to be controlled, a growth state of a plant, tendency of insect pests appearance, weather, environmental conditions, a preparation form, an application method, an application site and an application time. It may be properly chosen in a range of 0.1 g to 10 kg (in terms of the active ingredient) per 10 ares depending upon purposes.  
           [0185]    The agricultural and horticultural insecticide of the present invention may be used in admixture with other agricultural and horticultural disease or pest controllers in order to expand both spectrum of controllable diseases and insect pest species and the period of time when effective applications are possible or to reduce the dosage.  
           [0186]    Typical examples of the present invention are described below, but they should not be construed as limiting the scope of the invention. 
       
    
    
     EXAMPLES  
     Example 1  
       [0187]    (1-1) Production of 3-chloro-N-[4-(1,1,2,2-tetrafluoroethoxy)-2-methylphenyl]phthalimide  
         [0188]    In 10 ml of acetic acid were dissolved 0.55 g of 3-chlorophthalic anhydride and 0.67 g of 4-(1,1,2,2-tetrafluoroethoxy)-2-methylaniline, and the reaction was carried out with heating under reflux for 3 hours. After completion of the reaction, the solvent was distilled off under reduced pressure and the resulting residue was washed with an ether-hexane mixed solvent to obtain 1.1 g of the desired compound.  
         [0189]    Physical property: m.p. 121-122° C.  
         [0190]    Yield: 95%.  
         [0191]    (1-2) Production of 3-chloro-N 1 -[4-(1,1,2,2-tetrafluoroethoxy)-2-methylphenyl]-N 2 -isopropylphthalic acid diamide (compound No. 141) and 6-chloro-N 2 -[4-(1,1,2,2-tetrafluoroethoxy)-2-methylphenyl]-N 2 -isopropylphthalic acid diamide (compound No. 239)  
         [0192]    In 10 ml of dioxane was dissolved 1.1 g of 3-chloro-N-[4-(1,1,2,2-tetrafluoroethoxy)-2-methylphenyl]-phthalimide, followed by adding thereto 0.5 g of isopropylamine, and the reaction was carried out at 80° C. for 3 hours. After completion of the reaction, the solvent was distilled off under reduced pressure and the resulting residue was purified by a silica gel column chromatography using a hexane/ethyl acetate (2/1) mixed solvent as an eluent, to obtain 0.4 g of the desired compound (compound No. 141) having an Rf value of 0.5 to 0.7 and 0.5 g of the other desired compound (compound No. 239) having an Rf value of 0.2 to 0.4.  
         [0193]    Compound No. 141:  
         [0194]    Physical property: m.p. 202-204° C.  
         [0195]    Yield: 31%.  
         [0196]    Compound No. 239:  
         [0197]    Physical property: m.p. 199-201° C.  
         [0198]    Yield: 39%.  
       Example 2  
       [0199]    (2-1) Production of N-(4-trifluoromethoxyphenyl)-3-nitrophthalimide  
         [0200]    In 50 ml of acetic acid were dissolved 5.97 g of 3-nitrophthalic anhydride and 5.31 g of 4-trifluoromethoxyaniline, and the reaction was carried out with heating under reflux for 3 hours. After completion of the reaction, the solvent was distilled off under reduced pressure and the resulting residue was washed with an ether-hexane mixed solvent to obtain 10.2 g of the desired compound.  
         [0201]    Physical property: m.p. 149-150° C.  
         [0202]    Yield: 97%.  
         [0203]    (2-2) Production of 3-amino-N-(4-trifluoromethoxyphenyl)phthalimide  
         [0204]    In a pressure vessel were placed 10.0 g of N-(4-trifluoromethoxyphenyl)-3-nitrophthalimide, 100 ml of acetic acid and 0.5 g of 5% palladium carbon, and catalytic reduction with hydrogen was carried out at a hydrogen pressure of 5 kg/cm 2 . After completion of the reaction, the catalyst was filtered off and the filtrate was concentrated under reduced pressure. The resulting residue was washed with an ether-hexane mixed solvent to obtain 9.0 g of the desired compound.  
         [0205]    Physical property: m.p. 161-162° C.  
         [0206]    Yield: 98%.  
         [0207]    (2-3) Production of 3-bromo-N-(4-trifluoromethoxyphenyl)phthalimide  
         [0208]    In 20 ml of acetic acid was dissolved 1.6 g of 3-amino-N-(4-trifluoromethoxyphenyl)phthalimide, and a solution of 0.35 g of sodium nitrite in 5 ml of concentrated sulfuric acid was added dropwise while maintaining the temperature at 15° C. or lower. The resulting mixture was stirred at 15° C. or lower for another 20 minutes to obtain a diazonium salt. The diazonium salt was slowly added to a mixture of a solution of 0.86 g of cuprous bromide in 50 ml of hydrobromic acid and 10 ml of toluene which was maintained at 80° C. The resulting mixture was stirred until foaming ceased. After completion of the reaction, the organic layer was washed with an aqueous sodium thiosulfate solution and an aqueous sodium chloride solution, dried over anhydrous magnesium sulfate, and then distilled under reduced pressure to remove the solvent, and the resulting residue was purified by a silica gel chromatography to obtain 1.3 g of the desired compound.  
         [0209]    Physical property: m.p. 117-118° C.  
         [0210]    Yield: 67%.  
         [0211]    (2-4) Production of 3-bromo-N 1 -(4-trifluoromethoxyphenyl)-N 2 -isopropylphthalic acid diamide (compound No. 262) and 6-bromo-N 1 -(4-trifluoromethoxyphenyl)-N 2 -isopropylphthalic acid diamide (compound No. 302)  
         [0212]    From 1.3 g of 3-bromo-N-(4-trifluoromethoxyphenyl)phthalimide, 0.5 g of the desired compound (compound No. 262) and 0.7 g of the other desired compound (compound No. 302) were obtained in the same manner as in Example 1-2.  
         [0213]    Compound No. 262:  
         [0214]    Physical property: m.p. 208-210° C.  
         [0215]    Yield: 33%.  
         [0216]    Compound No. 302:  
         [0217]    Physical property: m.p. 210-212° C.  
         [0218]    Yield: 47%.  
       Example 3  
       [0219]    (3-1) Production of N-(4-difluoromethoxy-2-methylphenyl)-3-nitrophthalimide  
         [0220]    In 100 ml of acetic acid were dissolved 5.8 g of 3-nitrophthalic anhydride and 5.2 g of 4-difluoromethoxy-2-methylaniline, and the reaction was carried out with heating under reflux for 3 hours. After completion of the reaction, the solvent was distilled off under reduced pressure and the resulting residue was washed with an ether-hexane mixed solvent to obtain 10.2 g of the desired compound.  
         [0221]    Physical property: m.p. 163-164° C.  
         [0222]    Yield: 98%.  
         [0223]    (3-2) Production of N 1 -(4-difluoromethoxy-2-methylphenyl)-N 2 -isopropyl-3-nitrophthalic acid diamide (compound No. 696)  
         [0224]    In 100 ml of dioxane was dissolved 10 g of N-(4-difluoromethoxy-2-methylphenyl)-3-nitrophthalimide, followed by adding thereto 2.5 g of isopropylamine, and the reaction was carried out for 3 hours. After completion of the reaction, the solvent was distilled off under reduced pressure and the resulting residue was washed with ether to obtain 4.0 g of the desired compound.  
         [0225]    Physical property: m.p. 148-149° C.  
         [0226]    Yield: 86%.  
         [0227]    (3-3) Production of 3-amino-N 1 -(4-difluoromethoxy-2-methylphenyl)-N 2 -isopropylphthalic acid diamide  
         [0228]    In a pressure vessel were placed 5 g of N 1 -(4-difluoromethoxy-2-methylphenyl)-N 2 -isopropyl-3-nitrophthalic acid diamide, 50 ml of acetic acid and 0.25 g of 5% palladium carbon, and catalytic reduction with hydrogen was carried out at a hydrogen pressure of 5 kg/cm. After completion of the reaction, the catalyst was filtered off and the filtrate was concentrated under reduced pressure. The resulting residue was washed with an ether-hexane mixed solvent to obtain 4.0 g of the desired compound.  
         [0229]    Physical property: m.p. 148-149° C.  
         [0230]    Yield: 86%.  
         [0231]    (3-4) Production of N 1 -(4-difluoromethoxy-2-methylphenyl)-3-iodo-N 2 -isopropylphthalic acid diamide (compound No. 387)  
         [0232]    In 20 ml of acetic acid was dissolved 1.89 g of 3-amino-N 1 -(4-difluoromethoxy-2-methylphenyl)-N 2 -isopropylphthalic acid diamide, and 1.5 g of concentrated sulfuric acid was added under ice-cooling. While maintaining the resulting solution at 15° C. or lower, a solution of 0.35 g of sodium nitrite in 0.5 ml of water was added dropwise. The resulting solution was stirred at 15° C. or lower for another 20 minutes to obtain a diazonium salt. The diazonium salt was slowly added to a mixture of 50 ml of an aqueous solution containing 1.0 g of potassium iodide and 50 ml of chloroform which was maintained at 40° C. The resulting mixture was stirred until foaming ceased. After completion of the reaction, the organic layer was washed with an aqueous sodium thiosulfate solution and an aqueous sodium chloride solution, dried over anhydrous magnesium sulfate, and then distilled under reduced pressure to remove the solvent, and the resulting residue was purified by a silica gel chromatography to obtain 0.8 g of the desired compound.  
         [0233]    Physical property: m.p. 207-209° C.  
         [0234]    Yield: 33%.  
       Example 4  
       [0235]    (4-1) Production of 3-iodo-2-N-isopropyl-phthalamic acid  
         [0236]    A solution of 0.67 g of isopropylamine in 5 ml of acetonitrile was added dropwise to a solution of 1.37 g of 3-iodophthalic anhydride in 10 ml of acetonitrile under ice-cooling, and the reaction was carried out with stirring at room temperature for another 5 hours. After completion of the reaction, the crystals formed in the reaction solution were collected by filtration and washed with a small volume of acetonitrile to obtain 1.45 g of the desired compound.  
         [0237]    Yield: 87%.  
         [0238]    [0238] 1 H-NMR [CDCl 3 /TMS, δ values (ppm)] 1.23(6H, d), 4.35(1H, m), 5.80(1H, d), 6.85(1H, broad), 7.07(1H, t), 7.93(1H, d), 7.96(1H, d).  
         [0239]    (4-2) Production of 6-iodo-N-isopropyl-phthalic acid isoimide  
         [0240]    In 10 ml of toluene was dissolved 0.45 g of 3-iodo-2-N-isopropyl-phthalamic acid, followed by adding thereto 0.85 g of trifluoroacetic anhydride, and the reaction was carried out with stirring for 30 minutes. After completion of the reaction, the solvent was distilled off under reduced pressure to obtain 0.43 g of the desired compound as a crude product. The obtained desired compound was used in the subsequent reaction without purification.  
         [0241]    Physical property: m.p. 87.5-88.5° C.  
         [0242]    (4-3) Production of 3-iodo-N 1 -(4-pentafluoroethyl-2-methylphenyl)-N 2 -isopropyl-phthalic acid diamide (compound No. 372)  
         [0243]    In 10 ml of tetrahydrofuran was dissolved 0.43 g of the 6-iodo-N-isopropyl-phthalic acid isoimide obtained in 4-2, followed by adding thereto 0.30 g of 4-pentafluoroethyl-2-methylaniline, and the reaction was carried out with stirring for 1 hour. After completion of the reaction, the solvent was removed from the reaction solution by distillation under reduced pressure, and the resulting residue was washed with ether-n-hexane to obtain 0.70 g of the desired compound.  
         [0244]    Physical property: m.p. 195-196° C.  
         [0245]    Yield: 95%.  
       Example 5  
       [0246]    (5-1) Production of ethyl 6-nitro-N-(4-chloro-2-methylphenyl)-phthalamate  
         [0247]    In 30 ml of tetrahydrofuran was dissolved 1.29 g of 3-nitro-2-ethoxycarbonylbenzoyl chloride, followed by adding thereto 0.71 g of 4-chloro-2-methylaniline and 0.56 g of triethylamine, and the reaction was carried out with stirring for 30 minutes. After completion of the reaction, the reaction solution containing the desired compound was poured into water and the desired compound was extracted with ethyl acetate. The extracted solution was dried over anhydrous magnesium sulfate and distilled under reduced pressure to remove the solvent, and the resulting residue was purified by a silica gel column chromatography to obtain 1.7 g of the desired compound.  
         [0248]    Physical property: m.p. 164-165° C.  
         [0249]    Yield: 94%.  
         [0250]    (5-2) Production of 3-nitro-N 1 -(4-chloro-2-methylphenyl)-N 2 -isopropyl-phthalic acid diamide (compound No. 664)  
         [0251]    In 20 ml of dioxane was dissolved 1.7 g of ethyl 6-nitro-N-(4-chloro-2-methylphenyl)-phthalamate, followed by adding thereto 1.5 g of isopropylamine, and the reaction was carried out with stirring at 80° C. for 1 hour. After completion of the reaction, the solvent was removed from the reaction solution containing the desired compound, by distillation under reduced pressure, and the resulting residue was purified by a silica gel column chromatography to obtain 1.5 g of the desired compound.  
         [0252]    Physical property: m.p. 202-204° C.  
         [0253]    Yield: 85%.  
       Example 6  
       [0254]    (6-1) Production of N-isopropyl-3,4-dichlorophthalamic acid  
         [0255]    In 30 ml of tetrahydrofuran was dissolved 2.32 g of N-isopropyl-3,4-dichlorobenzamide, and 21 ml of s-BuLi (0.96 M/L) was slowly added while maintaining the temperature at −70° C. The resulting mixture was stirred at −70° C. for 30 minutes, after which the cooling bath was removed. An excess of carbon dioxide was introduced into the reaction solution, and the thus treated solution was stirred at room temperature for 30 minutes to carry out the reaction.  
         [0256]    After completion of the reaction, the reaction solution was poured into water and acidified with diluted hydrochloric acid, and the desired compound was extracted with ethyl acetate. The extracted solution was dried over anhydrous magnesium sulfate and distilled under reduced pressure to remove the solvent, and the crystals thus obtained were washed with an ether-hexane mixed solvent to obtain 2.4 g of the desired compound.  
         [0257]    Physical property: m.p. 155-156° C.  
         [0258]    Yield: 86.9%.  
         [0259]    (6-2) Production of N-isopropyl-3,4-dichlorophthalic acid isoimide  
         [0260]    In 10 ml of toluene was dissolved 0.41 g of N-isopropyl-3,4-dichlorophthalamic acid, followed by adding thereto 0.42 g of trifluoroacetic anhydride, and the reaction was carried out with stirring at room temperature for 30 minutes. After completion of the reaction, the solvent was distilled off under reduced pressure to obtain 0.39 g of the desired compound as a crude product. The obtained desired compound was used in the subsequent reaction without purification.  
         [0261]    (6-3) Production of 3,4-dichloro-N 1 -(4-pentafluoroethyl-2-2 methylphenyl)-N 2 -isopropylphthalic acid diamide (compound No. 1222)  
         [0262]    In 10 ml of acetonitrile was dissolved 0.39 g of N-isopropyl-3,4-dichlorophthalic acid isoimide, followed by adding thereto 0.34 g of 4-pentafluoroethyl-2-methylaniline, and the reaction was carried out with stirring for 2 hours. After completion of the reaction, the reaction solution was maintained at 0° C. for 10 minutes and the crystals precipitated were collected by filtration and washed with hexane to obtain 0.61 g of the desired compound.  
         [0263]    Physical property: m.p. 208-209° C.  
         [0264]    Yield: 84.1%.  
       Example 7  
       [0265]    Production of 3-chloro-2-isopropylamino-thiocarbonyl-N-(pentafluoroethyl-2-methylphenyl)benzamide (compound No. S-1)  
         [0266]    In 20 ml of tetrahydrofuran was dissolved 1.06 g of N-(pentafluoroethyl-2-methylphenyl)-3-chlorobenzamide, and 7 ml of s-BuLi (0.96 M/L) was slowly added while maintaining the temperature at −70° C. The resulting mixture was stirred at −70° C. for 30 minutes, after which the cooling bath was removed. A solution of 0.33 g of isopropyl isothiocyanate in 5 ml of tetrahydrofuran was poured into the reaction solution, and the resulting solution was stirred at room temperature for 30 minutes to carry out the reaction.  
         [0267]    After completion of the reaction, the reaction solution was poured into water and acidified with diluted hydrochloric acid, and the desired compound was extracted with ethyl acetate. The extracted solution was dried over anhydrous magnesium sulfate and distilled under reduced pressure to remove the solvent, and the crystals thus obtained were washed with an ether-hexane mixed solvent to obtain 1.2 g of the desired compound.  
         [0268]    Physical property: m.p. 162-164° C.  
         [0269]    Yield: 86%.  
       Example 8  
       [0270]    Production of 2-methyl-4-pentafluoroethylaniline (compound No. ST-3)  
                         
 
         [0271]    In an autoclave were placed 11.7 g (0.05 mole) of 2-methyl-4-iodoaniline, 6.4 g of copper powder, 18.5 g of iodopentafluoroethane and 100 ml of DMSO, and the reaction was carried out with stirring for 6 hours while maintaining the internal temperature at 120° C. After completion of the reaction, the reaction mixture was cooled to room temperature, poured into 500 ml of ice water, and thoroughly stirred. Then, the insoluble materials were removed and the desired compound was extracted with 300 ml of ethyl acetate. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated, after which the residue was purified by vacuum distillation to obtain 9.8 g of the desired compound.  
         [0272]    Physical property: b.p. 95-105C/10 mmHg.  
         [0273]    Yield: 87%.  
       Example 9  
       [0274]    (9-1). Production of 2-ethyl-4-pentafluoroethylacetanilide  
                         
 
         [0275]    In an autoclave were placed 4.0 g (0.0138 mole) of 2-ethyl-4-iodoacetanilide, .1.8 g of copper powder, 5.1 g of iodopentafluoroethane and 40 ml of DMSO, and the reaction was carried out with stirring for 6 hours while maintaining the internal temperature at 120° C. After completion of the reaction, the reaction mixture was cooled to room temperature, poured into 200 ml of ice water, and thoroughly stirred. Then, the insoluble materials were removed and the desired compound was extracted with 200 ml of ethyl acetate. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated, after which the residue was purified by a silica gel column chromatography to obtain 0.7 g (yield: 18%) of the desired compound.  
         [0276]    (9-2). Production of 2-ethyl-4-pentafluoroethylaniline (compound No. ST-18)  
                         
 
         [0277]    To 10 ml of a 6N aqueous hydrochloric acid solution was added 0.6 g (2.1 mmoles) of 2-ethyl-4-pentafluoroethylacetanilide, and the reaction was carried out with heating under reflux for 2 hours. After completion of the reaction, the reaction solution was ice-cooled and then neutralized with a 10% aqueous sodium hydroxide solution, and the desired compound was extracted with ethyl acetate. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated under reduced pressure to obtain 0.4 g of the desired compound.  
         [0278]    Physical property:  
         [0279]    [0279] 1 H-NMR (δ, ppm) 1.29(t, 3H), 2.52(q, 2H), 3.95(br, 2H), 6.8(d, 1H), 7.2-7.26(m, 2H).  
         [0280]    Yield: 80%.  
       Example 10  
       [0281]    Production of 2-chloro-4-pentafluoroethylaniline (compound No. ST-11)  
                         
 
         [0282]    In an autoclave were placed 5.0 g (19.7 mmoles) of 2-chloro-4-iodoaniline, 2.8 g of copper powder, 10.0 g of iodopentafluoroethane and 50 ml of DMF, and the reaction was carried out with stirring for 20 hours while maintaining the internal temperature at 135° C. After completion of the reaction, the reaction mixture was cooled to room temperature, poured into 200 ml of ice water, and thoroughly stirred. Then, the insoluble materials were removed and the desired compound was extracted with 200 ml of ethyl acetate. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated, after which the residue was purified by a silica gel column chromatography to obtain 4.2 g of the desired compound.  
         [0283]    Physical property:  
         [0284]    [0284] 1 H-NMR (δ, ppm) 4.4(br, 2H), 6.8(d, 1H), 7.27(dd, 1H), 7.47(d, 1H).  
         [0285]    Yield: 87%.  
       Example 11  
       [0286]    Production of 2-trifluoromethyl-4-pentafluoroethylaniline (compound No. ST-22)  
                         
 
         [0287]    In an autoclave were placed 6.0 g (20.9 moles) of 2-trifluoro-4-iodoaniline, 2.8 g of copper powder, 11.1 g of iodopentafluoroethane and 40 ml of DMF, and the reaction was carried out with stirring for 7 hours while maintaining the internal temperature at 135° C. After completion of the reaction, the reaction mixture was cooled to room temperature, poured into 200 ml of ice water, and thoroughly stirred. Then, the insoluble materials were removed and the desired compound was extracted with 200 ml of ethyl acetate. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated, after which the residue was purified by a silica gel column chromatography to obtain 3.9 g of the desired compound.  
         [0288]    Physical property:  
         [0289]    [0289] 1 H-NMR (δ, ppm) 4.52(br, 2H), 6.81(d, 1H), 7.27(dd, 1H), 7.48(d, 1H), 7.63(br, 1H).  
         [0290]    Yield: 67%.  
       Example 12  
       [0291]    (12-1). Production of 2-methyl-4-(heptafluoropropan-2-yl)-nitrobenzene  
                         
 
         [0292]    In an autoclave were placed 12.0 g (0.0456 mole) of 4-iodo-2-methylnitrobenzene, 11.6 g of copper powder, 40 g of 2-iodoheptafluoropropane and 200 ml of DMF, and the reaction was carried out with stirring for 6 hours while maintaining the internal temperature at 140° C. After completion of the reaction, the reaction mixture was cooled to room temperature, poured into 600 ml of ice water, and thoroughly stirred. Then, the insoluble materials were removed and the desired compound was extracted with 300 ml of hexane. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated, after which the residue was purified by vacuum distillation to obtain 11.4 g of the desired compound.  
         [0293]    Physical property: b.p. 120-125° C./10 mmHg.  
         [0294]    Yield: 82%.  
         [0295]    (12-2). Production of 2-methyl-4-(heptafluoropropan-2-yl)-aniline (compound No. ST-4)  
                         
 
         [0296]    In 60 ml of ethanol was dissolved 11.4 g (0.0374 mole) of 2-methyl-4-(heptafluoropropan-2-yl)-nitrobenzene, and a solution of 29.5 g of SnCl 2 .2H 2 O in 40 ml of hydrochloric acid was added dropwise thereto under ice-cooling over a period of 30 minutes. After completion of the dropwise addition, the reaction was carried out at room temperature for 2 hours. After completion of the reaction, the reaction solution was poured into 200 ml of ice water and neutralized with a 40% aqueous sodium hydroxide solution under ice-cooling. Then, a 40% aqueous sodium hydroxide solution was further added thereto until a homogeneous solution was obtained, and the desired compound was extracted with 100 ml of ether. The extract solution was washed with water, dried over anhydrous sodium sulfate and then concentrated, after which the residue was purified by vacuum distillation to obtain 9.8 g of the desired compound.  
         [0297]    Physical property: b.p. 100-110° C./10 mmHg.  
         [0298]    Yield: 95%.  
       Example 13  
       [0299]    Production of 3-bromo-N 1 -(4-nonafluorobutyl-2-methylphenyl)-N 2 -isopropyl-phthalic acid diamide (Compound No. 281)  
         [0300]    In 10 ml of tetrahydrofuran was dissolved 0.54g of 6-bromo-N-isopropyl-phthalic acid isoimide, followed by adding thereto 0.30 g of 2-methyl-4-nonafluorobutylaniline, and the reaction was carried out with stirring for 1 hour. After completion of the reaction, the solvent was removed from the reaction solution by distillation under reduced pressure, and the resulting residue was washed with ether-n-hexane to obtain 1.1 g of the desired compound.  
         [0301]    Physical property: m.p. 190-191° C. Yield 94%.  
         [0302]    Typical preparation examples and test examples of the present invention are described below but they should not be construed as limiting the scope of the invention.  
         [0303]    In the preparation examples, parts are all by weight.  
       Formulation Example 1  
       [0304]    [0304]                                                       Each compound listed in Table 1   50 parts           Xylene   40 parts           Mixture of polyoxyethylene   10 parts           nonylphenyl ether and calcium           alkylbenzenesulfonate                        
         [0305]    An emulsifiable concentrate was prepared by mixing uniformly the above ingredients to effect dissolution.  
       Formulation Example 2  
       [0306]    [0306]                                                       Each compound listed in Table 1    3 parts           Clay powder   82 parts           Diatomaceous earth powder   15 parts                        
         [0307]    A dust was prepared by mixing uniformly and grinding the above ingredients.  
       Formulation Example 3  
       [0308]    [0308]                                                       Each compound listed in Table 1   5 parts           Mixed powder of bentonite and clay   90 parts            Calcium lignin sulfonate   5 parts                        
         [0309]    Granules were prepared by mixing the above ingredients uniformly, and kneading the resulting mixture together with a suitable amount of water, followed by granulation and drying.  
       Formulation Example 4  
       [0310]    [0310]                                                       Each compound listed in Table 1   20 parts           Mixture of kaolin and synthetic   75 parts           high-dispersion silicic acid           Mixture of polyoxyethylene    5 parts           nonylphenyl ether and calcium           alkylbenzenesulfonate                        
         [0311]    A wettable powder was prepared by mixing uniformly and grinding the above ingredients.  
       Test Example 1  
       [0312]    Insecticidal effect on diamondback moth ( Plutella xylostella )  
         [0313]    Adult diamondback moths were released and allowed to oviposit on a Chinese cabbage seedling. Two days after the release, the seedling having eggs deposited thereon was immersed for about 30 seconds in a liquid chemical prepared by diluting a preparation containing each compound listed in Table 1 as an active ingredient to adjust the concentration to 500 ppm. After air-drying, it was allowed to stand in a room thermostated at 25° C. Six days after the immersion, the hatched insects were counted. The mortality was calculated according to the following equation and the insecticidal effect was judged according to the criterion shown below. The test was carried out with triplicate groups of 10 insects.  
             Corrected             mortality                   (   %   )             =           [           Number                 of               hatched                 insects               in                 untreated                 group           ]     -     [           Number                 of               hatched                 insects               in                 treated                 group           ]         [           Number                 of               hatched                 insects               in                 untreated                 group           ]       ×   100                           
 
         [0314]    Criterion:  
                                                   Effect   Mortality(%)                           A   100           B   99-90           C   89-80           D   79-50                      
 
         [0315]    The results obtained are shown in Table 5.  
       Test Example 2  
       [0316]    Insecticidal effect on common cutworm ( Spodoptera Litura )  
         [0317]    A piece of cabbage leaf (cultivar; Shikidori) was immersed for about 30 seconds in a liquid chemical prepared by diluting a preparation containing each compound listed in Table 1 as an active ingredient to adjust the concentration to 500 ppm. After air-drying, it was placed in a plastic Petri dish with a diameter of 9 cm and inoculated with second-instar larvae of common cutworm, after which the dish was closed and then allowed to stand in a room thermostated at 25° C. Eight days after the inoculation, the dead and alive were counted. The mortality was calculated according to the following equation and the insecticidal effect was judged according to the criterion shown in Test Example 1. The test was carried out with triplicate groups of 10 insects.  
             Corrected             mortality                   (   %   )             =           [           Number                 of                 alive                 larvae                 in                            untreated                 group           ]     -     [           Number                 of                 alive                 larvae                 in                            treated                 group           ]         [           Number                 of                 alive                 larvae                 in                            untreated                 group           ]       ×   100                           
 
         [0318]    The results obtained are shown in Table 5.  
       Test Example 3  
       [0319]    Insecticidal effect on rice leafroller ( Cnaphalocrocis medinalis )  
         [0320]    The lamina of a rice plant at the 6 to 8 leaf stage was immersed for about 30 seconds in a liquid chemical prepared by diluting a preparation containing each compound listed in Table 1 as an active ingredient to adjust the concentration to 500 ppm. After air-drying, the lamina was placed in a plastic Petri dish with a diameter of 9 cm whose bottom had been covered with a wetted filter paper. The lamina was inoculated with third-instar larvae of rice leafroller, after which the dish was allowed to stand in a room thermostated at 25° C. and having a humidity of 70%. Four days after the inoculation, the dead and alive were counted and the insecticidal effect was judged according to the criterion shown in Test Example 1. The test was carried out with triplicate groups of 10 insects.  
         [0321]    The results obtained are shown in Table 5.  
                                                         TABLE 5                                       Test Example   Test Example   Test Example           No   1   2   3                                        1   D   D   A           2   A   C           3   C   A           4   A       D           7   A           8   A   A   A           9   A       A           10   A   D   D           11   A   C   C           12   A   D           13   D       D           14   A           15   A       A           16   A           17   A       D           18   D       A           20   A           22   A   D           23   A       D           24   A       D           25   A       A           26   A       D           27   A   A   C           28           A           29   A   B   A           30   A   A   A           31   A           32   A           33   A           34   A   C           37   A           41   A       A           42   A   D   A           43   B   D           44           A           45   A       A           46   A       B           47   A   D   A           48   A   B   A           49   A   A   A           50   A   A   A           51   A       A           52   A   A   A           53   A       A           55   A   B   A           56   A   A   A           58   A   A   A           59   A           60   A   A   A           61   A   B   A           62   A   A   A           63   A   B   A           64   A   B   A           65   A   A   A           66   A   A   B           67   A   A   A           68   A           69   A       A           70   A       A           71           D           73   A           74   A           75   A       A           76   C       B           77   A   C   A           78   A   A   A           79   A   A   D           81           A           83   A   A   A           84   A           86   B       B           87   A       A           88   A           89   A   B   A           90   A   A   B           91   A   A   A           92   A           93   A   A   A           98   A       C           99   A       A           100   A   A   A           101   A           102   A   D   A           103   A   C   A           109   A   A   C           110   A       A           111   A   C   B           112   A   A   A           113   A   B   A           114   A   A   A           115   A   C   A           116   A   D   A           117   A   A   A           118   A   A   A           119   A   A   A           120   A   D   A           121   A   A   A           122   A   A   A           123   A       A           124   A   A   A           125   A   B   A           126   A   A   A           127   A   A   A           128   A   D   A           129   A   A   A           130   A   A   A           132   A   A   A           133   A   A   A           134   A       A           135   A   A   A           136   A   A   A           137   A       A           138   A   A   A           139   A   A   A           140   A   A   A           141   A   A   A           142   A   A   B           143   A   A   A           144   A   A   A           145   A   A   A           146   A   A   A           147   A   C           148   A   A   A           149   A   A   A           150   A   A   A           151   A           152   A   A   A           153   A       D           157   A   A   A           158   A   A   A           159   A   A   A           161   A   D   A           162   A   A   B           163   A   A   A           164   A   A           165   A   B   C           167   A   A   A           168   A           169   A   D           170   A   D   B           171   A       D           172   A   A   D           173   A   D   D           174   A           175   A           176   A   D   A           177   A   A   A           178   A       A           179   A           180   A   A   A           181       A           183   A   B           185   A           186   D           187   A       D           188   D       D           189   A           190   A           191   A       A           192   A           193   A   D           194   A           195   A           196   A       D           197   A   A   A           198   A   C   A           199   A           200   A       A           201   A   B   A           202   A           203   A           206   A       A           207   A           208   A           209   A       B           210   A       D           211   A       A           212   A   D   A           213   A   A   A           214   A   A   A           215   A   D           216   A       A           217   A       A           218   A       C           219   A   D   A           220   A       A           221   A   A   A           222   A   B   A           223   A   A   A           225   A   B   A           226   A       A           227   A           228       B   A           229   A   D   A           230   A   C   A           231       B   A           232   A       A           233   A           234   A       A           235   A       A           236   A   A   A           237   A       A           238   A       A           239   A   A   A           240   A           241   A   B   A           242   A   B   A           243   A   A   B           244   A   C           245   A   D           246   A   B   B           248   A   C           249   A   D   A           250   A       D           251   A       A           252   A           253   A   A   C           254   A   A           255   A       A           256   A           257   A       B           258   A       A           259   A       D           261   A   A   D           262   A   A   D           263   A       A           264   —   D   A           265   A           266   A   A   A           267   A   A   A           268   A   A   A           269   A   A   A           270   A   A   A           271   A   A   A           272   A   A   A           273   A   D   D           274   A   A   A           275   A   D   A           276   A   A   A           277   A   A   A           278   A   A   A           279   A   A   A           281   A   A   A           282   A   A   A           283   A   A   A           284   A   A   A           285   A   D   A           286   A   A   A           287   A   A   A           288   A   A   A           289   A   A   A           290   A   A   A           291   A   A   A           292   A   A   A           293   A   A   A           294   A   A   A           295   D           296   A   A   A           297   A   A   B           298   A   A   A           299   A   A   A           300   A       A           301   A   A   D           302   A       D           303   A       D           304   A           305   A   A   A           306   A   A   A           307   A       D           308   A           309   A   A           310   A           311   A       D           312   A   A   A           313   A   A   A           314   A       A           315   A       A           316   A   A   A           318   A   B   A           319   A   B   B           320   A       D           321   A   A           322   A       B           323   A   C   A           324   A       A           325   A   A   A           326   A       A           327   A       A           328   A   A   A           329   A   A   A           330   A       A           332   A       A           333   A       D           334   A   C   C           335   A       B           336   A       D           337   A       A           338   A   B   A           339   A   B   A           340   A       A           341   A       A           342   A           343   A           345   A   B   A           346   A   C   A           347   A   B   C           348   A       A           349           A           350   A   A   A           351   A   A   A           352           A           353   A   A   A           354   A   A   A           355   A   C   A           356   A   A   A           360   A   D   A           361   A   A   A           362   A   A   A           363   A   A   A           364   A   A   D           365   A   A   A           366   A   A   A           367   A   A   A           368   A   A   A           369   A   A   A           370   A   A   A           371   A   A   A           372   A   A   A           373   A   A   A           374   A   A   A           375   A   A   A           376   A       A           377   A       A           378   A   D   A           379   A   A   A           380   A   A   A           381   A   A   A           382   A   B   A           383   A       A           384   A       C           385   A   B   A           386   A   A   A           387   A   A   A           388   A   A   B           389   A   A   A           390   A   A   A           391   A   A   A           392   A   A   A           393   A   A   A           394   A   A   A           395   A   A   A           396   A   A   A           397   A   A   A           398   A           399   A   A   A           400   A   D   A           402   A           403   A   B   A           404   A   A   A           406   A   A   A           407   A   A   A           408   A   B   A           409   A   A   A           410   A   A   A           411   A       A           412   A       C           413   A       C           414   A       A           415           A           416   A   A   A           417   A   A   A           418           A           419   A   A   A           420   A       D           421   A   B   A           422   A           424   A   A           427   A       D           428   A           429   A   D           430   A   D   D           431   A   A           432   A       A           433   A       A           434   A           435   A   B   A           436   A   B   A           437   A   C   A           438   A   B   A           439   A   A   A           440   A   C   B           441   A       B           442   A           443   A       D           444   A       A           445       B   A           446   A   A   A           447   A   B   C           448   A       A           449   A           450   A       C           451   A   A           452   A   A   A           453   A   D   A           454   A   A   A           455   A   B   A           456   A       A           457   A   A   B           458   A           459   A           460   A   B           461   A           462   A           463   A           464   A       A           465   A           466   A       A           467   A       A           468   A   A   B           469   A   A   D           470   A   C   C           471   A   A   A           472   A       B           473   A   A   A           474   A   B   A           475   A       D           476   A   A   A           477   A       C           478   A           479   A       A           480   A   B   A           488   A   A   A           489   A   A   A           490   A   A   A           491   A   A   A           492   A   A   A           493   A   A   A           494   A       A           495   A   A   A           496   A   A   A           498   A   A   A           499   A   A   A           500   A   B   A           501   A   A   A           502   A   A   A           503   A   B   A           504   A   A   A           505   A   A   A           506   A           507   A   B   A           508   A   B   A           509   A   A   A           510   A   B   A           511   A   A   A           512   A   A   A           513   A   A   A           514   A   A   A           515   A       C           516   A   A   A           517   A   A   A           518   A       B           519   A   A   A           520   A           521   A   A   A           522   A   D   A           523   A   A   A           524   A   A   A           526   A   A           527   A   A   A           528   A       A           529   A   D   A           530   A       D           531   A       A           532   A       A           533   A   A   A           534   A       A           535   A   A           536           A           537   A           538   A   A   A           539   A           540   A           543   A       A           544   A       A           545   A       A           546   A       A           547   A   A   D           548   A   A   A           549   A   A   D           550   A   C   A           551   A       A           552   A       B           553   A   C   A           554   A       A           555   A       B           557   A   C   B           558   A   A   A           559   A           560   A           561   A   C   A           562   A       A           563   A       A           564   A       B           565   A       A           566   A       B           567   A   D   D           568   A   C   A           569   A   A   A           570   A   A           571   A   C           573   A           575   A       A           576   A       C           577   A       A           579   A   A   A           580   A       A           581   A   B   A           582   A       A           584   A   D           585   A       A           586   A       D           587   A           588   A           589   A       A           590   A           591   A   D           592   A           593   A           594   A           595   A   A   A           596   D       D           597   B           598   A           599   A   D   A           600   A           601   A           602   A       A           603   B       C           604   A       D           605           C           606   A   D   A           607   A   A   A           608   A           609   A   B   A           610   A   A   C           611   A       A           612   A       D           613   A           614   A           615   A           616   A       D           617   A   A   A           618   A   A   A           619   A   A   A           621   A           622   A           623   A       A           624   A           625   A   D   D           626   A           628   A   B   A           633   A   D           634   A       D           635   A   D           636   A   D   A           637   A           638   B           639   A           640   A           641   D   D           642   A           643   A       A           644   A   A           645   A           646   A   D           647   A       B           648   A   D   A           649   A       C           650   A           652   A           653   A           654       D           656   A       A           657   D           658   A           659   A           660   A       A           661   B       D           662   A           663   A   A   D           664   A   A           665   A   A   B           666   A       D           667   A   A   A           668   A           669   A   D   A           670   A       D           671   A       D           672   A           673   A   D   D           674   A   D   A           675   A   A   A           676   A   C   A           677   A           678   A           679   A       A           680   A       D           681   A   A   A           682   A       A           683   A   A   A           684   A   A   A           686   A   A   A           687   A   D   D           688   A       A           689   A   D   A           690   A       A           691   A   D   C           692   A   D           693   A   A           694   A       A           695   A   A   A           696   A   A   A           697   A       A           698   A   B   A           699   A   A   D           700   A   A   A           701   A   A   A           703   A   A   A           704   A       A           705   A   D   A           706   A   A           708   D           709   A   A           710   A   C   A           711   A   C   A           712   A   A   A           713   A   B   D           714   A   A   A           715   A   A   A           716   A   A   A           717   A       A           718   A       A           719   A   D           720   A           721   A           722   A       A           723   D       D           724   A       B           725   A   A           727   A   B   A           728   A       A           729   A       A           732   A           733   A           735           D           737   A           738   D           740   A       A           741   A   A   A           742   A           743   D           744   C           745   D           749   A           750   A       A           751   A       A           752   A           753   A   A   D           755   A       A           758           A           759           D           765           A           766   A           767   A   C   A           768   A   B   A           769   A       D           770   A   A   A           771   A       C           772   A       A           773   A       A           774   A       A           776   B       D           777   A       D           778   A       A           780   A   A   A           781   A   A   A           782   A       A           783   A   A   A           785       A           788   C       C           790           A           791   A       A           793   A           795   A   B   A           796   A           797   A       C           798           A           799   A       A           800           C           801   A   A   D           802   D           803   A       A           808   A           819   A   B   A           821   A       A           822   D       D           824   A           825   A           826   A       A           827   A           830   C           831   D   D           832   A           833   A       D           835   A           836   A       A           837   A           838   A   C   A           839   A       C           840   A       D           841   A   D           842   A   A   D           845   A           846   A           847       D           848   A           849   A   B   A           850   A       A           851   A   D   A           852   A       D           854   A           855   A           856   A       D           858   C   A           859   D           860   A           861   A           862   A   D   D           863   A       B           864   A           865   A           866   D           867   A       C           869   A   D           870   A           871   A           872   A       C           874   A   C   A           875   A           878   C           879   A       A           880       D           881   A   D           888   D           889   A       A           890   A   A   A           891   A   A   A           892   A       A           893   A   A   A           894   A   A   A           895   A   A   A           901   A   D   A           902   A           903   A   A   A           904   A           905   A   A   A           906   A   D   A           907   A   A   A           908   A   D   A           909   A   A   A           910           A           911   A       D           912   A           913   A           914   A           915   A   A   A           916   A           917   A   A   A           918   A           919   A           920   A           924   A           925   A       A           927   A   A   A           928   A       A           929   A   A   A           930   A   A   A           931   A   A   A           932   A   A   A           933   A       A           934   A   A   A           935   A   A   A           936   A   A   A           937   A   A   A           938   A   A           939   A   A   A           940   A   A   A           941   A   A   A           942   A   A   A           943   A   C   A           944   A   A   A           945   A   A   A           946   A       A           947   A   A   A           949   A   A   A           950           C           951   A   A   A           952   A       A           953   A   A   A           954   A       A           955   A   A   A           956   A       A           957   A   A   A           958   A       A           959   A       A           965   A   C           966   A       B           971   A   A   A           972       A           973   A   A   A           974   A   A   A           975   A       A           976   A   A   A           977   A   A   A           978   A   C   A           979   A   A   A           980   A   A   A           981   A   A   A           982   A       C           983   A   A   A           984   A           985   A   A   A           986   A       A           987   A   A   A           988   A           989   A   A   A           990   A       A           991   A   A   A           992   A           993   A       A           995   A       A           996   A   A   A           997   A   A   A           998   A   A   A           999   A       A           1000   A   D   A           1001   A   A   A           1002   A   A   A           1003   A   A   A           1004   A   A   A           1005   A   A   A           1006   A           1007   A   A   A           1008   A       A           1009   A   A   A           1010   A       A           1011   A   A   A           1013   A   A   A           1014   A       A           1015   A   D   A           1016           A           1017   A   A   A           1018   A   D   A           1019   A   A   A           1020   A   A   A           1021   A       A           1022   A   A   A           1023   A   A   A           1024   A   A   A           1025   A           1026   A       A           1027           A           1028   A   A   A           1031   A   A   A           1032   A       A           1033   A   A   A           1034   A           1035   A   A   A           1036   A       A           1037   A   A   A           1038   A   A   A           1039   A   A   A           1040   A   A   A           1041   A   A   A           1042   A   A   A           1043   A       A           1044   A   A   A           1045   A   A   A           1046   A   A   A           1047   A       A           1048   A       A           1049   A   A   A           1050   A   A   A           1051   A   A   A           1052   A   A           1053   A   A   A           1054   A   A   A           1055   A   A   A           1056   A   A   A           1057   A       A           1058   A   A   A           1059   A           1060   A   A   A           1061   A   A   A           1062   A   A   A           1063           A           1064   A       A           1065   A           1066   A   C   A           1067   A   A   A           1068   A   A   A           1069   A   A   A           1070   A   A   A           1071   A   C   A           1072           A           1073   A   A   A           1074   A   A   A           1075   A   A   A           1076   A       A           1077   A       A           1078   A   A   A           1079   A   A   A           1080   A   A   A           1081   A   A   A           1082   A           1083   A           1086   A       A           1087   A   A   A           1088   A       A           1089   A       A           1099   A       A           1100   A   C   A           1101   A   C   A           1102   A   A   A           1103   A       A           1104   A   A   A           1105   A   A   A           1106   A       A           1107   A       A           1108   A       A           1109   A       A           1110   A   C   A           1111   A       A           1112   A   A   A           1113   A   A   A           1114   A   A   A           1115   A   A   A           1116   A   A   A           1117   A   A   A           1118   A   A   A           1119   A   A   A           1120   A   A   A           1121   A   A   A           1122   A   A   A           1123   A   A   A           1124   A   A   A           1125   A   A   A           1126   A   A   A           1127   A   A   A           1128   A   A   A           1129   A   A   A           1130   A   A   A           1131   A   A   A           1132   A       A           1133   A       A           1134   A       A           1135   A       A           1136   A       A           1137   A           1138           A           1139   A           1140           A           1141   A   A   A           1142   A   A   A           1143   A   C   A           1144   A   A   A           1145   A       A           1146   A   C   A           1147   A   A   A           1148   A   A   A           1149   A       A           1150   A   A   A           1151   A   A   A           1152   A   A   A           1153   A   A   A           1154   A   C   A           1155   A       A           1156   A   A   A           1157   A       A           1158   A   D   A           1159   A   A   A           1160   A   A   A           1161   A   D   A           1162   A   A   A           1163   A   A   A           1164   A   A   A           1165   A   A   A           1166   A   A   A           1167   A   A   A           1168   A   A   A           1169   A   A   A           1173   A   A   A           1174   A   A   A           1175   A           1178   A           1179   A   A           1180   A           1181   A           1182   A           1183   A   A           1184   A   A           1185   A   C           1186   A   A           1187   A   A           1188   A   A           1189   A   A           1190   A   A   A           1191   A   A   A           1192   A   A   A           1193   A   A   A           1202   A   A   A           1203   A   D   A           1204   A   A   A           1205   A       A           1206   A   A   A           1207   A   A   A           1208   A       A           1209   A   D   A           1210   A   A   A           1211   A   A   A           1212   A   A   A           1221   A   A   A           1222   A   A   A           1223   A   A   A           1224           B           1225           A           1226           A           1227   A   A   A           1228   A   A   A           1229   A   A   A           1230   A   A   A           1231   A   A   A           1232   A   A   A           1233   A   A           1234   A   A           1235   A   D           1236   A   A           1237   A   A           1238   A           1245   A   A           1246   A   A   A           1247   C           1248   A   A   A           1249   A           1250   A   A   A           1251   A   A   A           1256   A   A           1257   A   A           1258   A   A           1259   A           1260   A           1261   A   A           1262   A   A   A           1263   A   A   A           1264   A   A   A           1266   A       A           1277   A   A   A           1278   A   A   A           1280   A   A   A           1281   A       A           1283   A           1284   A       A           1285   A       A           1287   A   A   A           1288   A           1291   A           1293           A           1294   A   A   A           1295   A   A   A           1296   A   A   A           1297   A   A   A           1298   A   A   A           1299   A   A   A           1300   A   A   A           1301   A       A           1303   A   A   A           1304   A       A           1305   A   A   A           1306           A           1307   A   A   A           1308           C           1309   A   A   A           1310           B           1311   A   A   A           1312   A       A           1313   A   A   A           1314   A   A   A           1315   A   A   A           1316   A   A   A           1317   A   C   A           1318   A       A           1319   A           1321   A       A           1322   A           1323   A       A           1325   A       A           1327   A           1328   A           1330   A   A   A           1331   A       A           1332   A           1333   A       A           1335   A   C   A           1337   A       A           1338   A           1339   A       A           1340   A       A           1341   A           1342   A           1343   A       A           1345   A           1346   A           1347   A           1348   A           1349   A           1350           A           1351   A       A           1352   A       A           1353   A   A   A           1355   A   A   A           1356   A           1358   A       C           1360   A       C           1361           A           1362   A   A   A           1363   A           1364   A   A   A           1365   A           1366   A   A   A           1367   A           1368   A           1370   A       A           1372   A           1373   A           1374   A           1376   A           1379   A           1381   A       C           1382   A   A   A           1383   A   A   A           1384   A   A   A           1385   A   A   A           1386   A   A   A           1387   A   A   A           1388   A   D   A           1389   A   A   A           1390   A       A           1392   A       A           1393   A       A           1394   A       A           1395   A           1398   A           1399   A   A   A           1400   A   A   A           1401   A           1402   A   A   A           1404   A   C   A           1406   A   A   A           1409   A       A           1410   A       A           1411   A       A           1412   A           1414   A   A   A           1415   A       A           1416           A           1417   A   A   A           1418   A   A   A           1419   A       A           1420   A       A           1421   A           1423   A           1424       A   A           1427   A   A   A           1428   A   A   A           1429   A   A   A           1430   A   D   A           1431   A           1432           A           1434   A           1436   A   A   A           1438   A   A   A           1439   A       C           1440   A           1441   A       A           1442   A           1443   A           1445   A   A   A           1446   A           1447   A   A   A           1448   A   A   A           1449   A   A   A           1450   A   A   A           1451   A           1452   A   A   A           1453   A           1454   A   A   A           1456   A       A           1457   A       A           1458   A   A   A           1459   A   A           1460   A   C   A           1461   A       A           1464   A   A   A           1465   A       A           1466   A   A   A           1467   A   A   A           1468   A   C   A           1469   A           1470   A       A           1472   A   A   A           1473   A   A   A           1474   A   A   A           1475   A   A   A           1476   A           1478   A   A   A           1479   A   A   A           1480           A           1481   A   A   A           1482   A   A   A           1484   A   A   A           1485   A   A   A           1486   A   A           1487   A   A           1488   A       A           1489   A   A   A           1490   A       A           1491   A   A   A           1492   A       A           1493   A       A           1494   A   A   A           1495   A   A   A           1496   A   A   A           1497   A   A   A           1498   A   A   A           1499   A   A   A           1500   A   A   A           1501   A   A   A           1502   A   A   A           1503   A   C   A           1504   A   A   A           1505   A   A   A           1506   A   A   A           1507   A   A   A           1508   A   C   A           1509   A   C   A           1510   A       A           1511   A           1512   A   A   A           1513   A           1514   A       A           1515   A           1516   A   A   A           1517   A       A           1518   A           1519   A       A           1520           A           1521   A           1522   A   A   A           1523   A       A           1524   A   A   A           1525   A   A   A           1526   A   A   A           1527   A       A           1528   A       A           1529   A       A           1530   A       A           1531   A   A   A           1532   A   A   A           1533   A   A   A           1534   A   A   A           1535   A   A   A           1536   A   A   A           1537   A   A   A           1538   A   A   A           1539   A   A   A           1540   A   A   A           1541   A   A   A           1542   A   D   A           1543   A   A   A           1544   A   A   A           1545   A   D   A           1546   A   C   A           1547   A       A           1548   A       A           1549   A   D   A           1550   A   A   A           1551   A   D   A           1552   A   A   A           1553   A       A           1554   A   A           1555   A       A           1556   A   A   A           1557   A   A   A           1558   A   C   A           1559   A   A   A           1560   A   A   A           1561   A   A   A           1562   A   A   A           1563   A   A   A           1565   A   A   A           1566   A   A   A           1567   A   A   A           1568   A   A   A           1569   A   A   A           1570           A           1571   A   A   A           1572   A   A   A           1573   A   A   A           1574   A   A   A           1575   A       A           1576   A   D   A           1577   A           1578   A       A           1579   A           1580   A   A   A           1581   A   A   A           1582   A       A           1583   A       A           1584   A       A           1585   A   A   A           1586   A   C   A           1587   A   A   A           1588   A       A           1589   A       A           1590   A   A   A           1594   A   A           1595   A   A           1596   A   A           1597   A   A           1598   A   A           1599   A   A           1600   A   A           1601   A   A           1602   A   A   A           1603   A   A   A           1604   A   A   A           1605   A   C           1606   A   A           1607   A   A           1608   A   A           1609   A   A           1610   A   A           1611   A           1612   A   A           1613   A   A           1614   A   C   A           1615   A   A   A           1617   A       A           1618   A   C   A           1619   A   A           1620   A       A           1622   A   A   A           1623   A   C   A           1624   A   D   A           1625   A   A   A           1626   A       A           1627   A   A   A           1628   A   A   A           1629   A   A   A           1632   A       A           1633   A   A   A           1634   A   A   A           1635   A   A   A           1636   A   D   A           1637   A   A   A           1638   A   A   A           1639   A   A   A           1640   A   A   A           1641   A       A           1642   A   A   A           1643   A       A           1644   A   A   A           1645   A   A   A           1646   A   A   A           1647   A   A   A           1648   A   A   A           1649   A   A   A           1650   A   A   A           1651   A   A   A           1652   A   A   A           1653   A   A   A           1654   A   A   A           1655   A   A   A           1656   A   A   A           1658   A           1659   A       A           1660   A   A           1661   A           1662   A   A           1663   A   A           1664   A   A           1665   A   A           1666   A   A           1667   A   A           1668   A   A           1669   A   A           1670   A   A           1671   A   A           1672   A   A           1673   A           1674   A   A           1679   A   A   A           1680   A   A   A           1681   A   A   A           1682   A   A           1683   A           1684   A   A           1685   A   A           1686   A   A           1689   A   A           1690   A   A           1691   A   A           1692   A           1693   A   A           1694   A           1695   A   A           1696   A   A           1697   A   A           1698   A           1699   A   A           1700   A   D           1714   A   A   A           1715   A   A   A           1716   A   A   A           1717   A   A   A           1722   A   A   A           1723   A   A   A           1726   A       A           1727   A       A           1732   A   A   A           1733   A   A   A           1737   A   C   A           1742   A       A           1743   A       A           1747   A   C   A           1748   A       A           1750   A       A           1752   A       A           1763   A       A           1764   A   A   A           1765   A   A   A           1766   A   A   A           1767   A           1768   A       A           1770   A       A           1772   A       A           1773   A   A   A           1774   A       A           1775   A       A           1776   A       A           1777   A   A   A           1778   A       A           1799   A   A   A           1800   A   A   A           1801   A   A   A           1802   A           1803   A   A   A           1804   A           1805   A