Abstract:
A waterborne coating having improved chemical resistance produced from a composition containing a binder resin having post crosslinking groups, an associative thickener having post crosslinking groups and an associative dispersant having post crosslinking groups.

Description:
This application claims the benefit of Provisional application Ser. No. 60/138,086, filed Jun. 8, 1999. 
    
    
     BACKGROUND OF THE INVENTION 
     This invention relates to waterborne coatings having improved chemical resistance. Conventional latex paints are widely used because they provide low volatile organic compound emission and because they allow easier clean up than solvent borne coatings. However, when compared to solvent borne coating systems, typical latex coatings lack the chemical resistance provided by such solvent borne coatings. 
     It has now been found that latex coating compositions having superior chemical resistance can be produced by formulating a chemical coating comprising a binder resin having post crosslinking groups, an associative thickener having post crosslinking groups and an associative dispersant having post crosslinking groups. The crosslinking groups present in the polymer of the dispersant and/or the thickener can be adjusted, depending on the particular binder resin used, to optimize the desired performance properties of the coating composition. Specifically, a coating composition can be tailor made to have increased chemical resistance, corrosion resistance, humidity resistance and/or adhesion to a particular substrate by altering the levels of crosslinking on the binder, thickener and dispersant. The coating composition of the present invention may be ambient cured, oven cured or radiation cured. 
     SUMMARY OF THE INVENTION 
     The present invention is directed to an aqueous coating composition in which the binder polymer, thickener polymer and/or dispersant polymer have functional groups that further react some time after initial formation of the polymer. The aqueous coating composition contains (a) a binder polymer comprising at least one or more copolymerizable monoethylenically unsaturated monomers, wherein at least one of the monoethylenically unsaturated monomers contains latent crosslinking functionality; and (b) a second polymer comprising a monoethylenically unsaturated monomer containing latent crosslinking functionality. The second polymer may be an associative thickener or an associative dispersant. 
     The binder polymer, thickener and dispersant polymer may contain a macromonomer represented by the formula: 
                        
 
wherein R 1  is a monovalent residue of a substituted or unsubstituted hydrophobe compound; each R 2  is the same or different and is a substituted or unsubstituted divalent hydrocarbon residue; R 3  is a substituted or unsubstituted divalent hydrocarbon residue; R 4 , R 5 , R 6  are the same or different and are hydrogen or a substituted or unsubstituted monovalent hydrocarbon residue; and z is a value of 0 to 150.
 
     The binder polymer, thickener polymer and dispersant polymer may contain diacetone acrylamide as the monomer having latent crosslinking functionality. 
     The aqueous coating compositions of the present invention produce coatings having improved chemical resistance, as well as improved corrosion resistance. 
    
    
     DETAILED DESCRIPTION OF THE INVENTION 
     Binder 
     The latex polymers used as binders in accordance with the present invention (also referred to herein as “binders”) include those polymers polymerized from one or more suitable monomers. Typically, the binders are polymerized from one or more copolymerizable monoethylenically unsaturated monomers such as, for example, vinyl monomers and acrylic monomers. 
     The vinyl monomers suitable for use in accordance with the present invention include any compounds having vinyl functionality, i.e., ethylenic unsaturation, exclusive of compounds having acrylic functionality, e.g., acrylic acid, methacrylic acid, esters of such acids, acrylonitrile and acrylamides. Preferably, the vinyl monomers are selected from the group consisting of vinyl esters, vinyl aromatic hydrocarbons, vinyl aliphatic hydrocarbons, vinyl alkyl ethers and mixtures thereof. 
     Suitable vinyl monomers include vinyl esters, such as, for example, vinyl propionate, vinyl laurate, vinyl pivalate, vinyl nonanoate, vinyl decanoate, vinyl neodecanoate, vinyl butyrates, vinyl benzoates, vinyl isopropyl acetates and similar vinyl esters; vinyl aromatic hydrocarbons, such as, for example, styrene, methyl styrenes and similar lower alkyl styrenes, chlorostyrene, vinyl toluene, vinyl naphthalene and divinyl benzene; vinyl aliphatic hydrocarbon monomers, such as, for example, vinyl chloride and vinylidene chloride as well as alpha olefins such as, for example, ethylene, propylene, isobutylene, as well as conjugated dienes such as 1,3 butadiene, methyl-2-butadiene, 1,3-piperylene, 2,3-dimethyl butadiene, isoprene, cyclohexene, cyclopentadiene, and dicyclopentadiene; and vinyl alkyl ethers, such as, for example, methyl vinyl ether, isopropyl vinyl ether, n-butyl vinyl ether, and isobutyl vinyl ether. 
     The acrylic monomers suitable for use in accordance with the present invention comprise any compounds having acrylic functionality. Preferred acrylic monomers are selected from the group consisting of alkyl acrylates, alkyl methacrylates, acrylate acids and methacrylate acids as well as aromatic derivatives of acrylic and methacrylic acid, acrylamides and acrylonitrile. Typically, the alkyl acrylate and methacrylic monomers (also referred to herein as “alkyl esters of acrylic or methacrylic acid”) will have an alkyl ester portion containing from 1 to about 12, preferably about 1 to 5, carbon atoms per molecule. 
     Suitable acrylic monomers include, for example, methyl acrylate and methacrylate, ethyl acrylate and methacrylate, butyl acrylate and methacrylate, propyl acrylate and methacrylate, 2-ethyl hexyl acrylate and methacrylate, cyclohexyl acrylate and methacrylate, decyl acrylate and methacrylate, isodecyl acrylate and methacrylate, benzyl acrylate and methacrylate, isobornyl acrylate and methacrylate, neopentyl acrylate and methacrylate, 1-adamatyl methacrylate and various reaction products such as butyl, phenyl, and cresyl glycidyl ethers reacted with acrylic and methacrylic acids, hydroxyl alkyl acrylates and methacrylates such as hydroxyethyl and hydroxypropyl acrylates and methacrylates, amino acrylates, methacrylates as well as acrylic acids such as acrylic and methacrylic acid, ethacrylic acid, alpha-chloroacrylic acid, alpha-cycanoacrylic acid, crotonic acid, beta-acryloxy propionic acid, and beta-styryl acrylic acid. 
     In addition to the specific monomers described above, those skilled in the art will recognize that other monomers such as, for example, allylic monomers, or monomers which impart wet adhesion, e.g., methacrylamidoethyl ethylene urea, can be used in place of, or in addition to, the specifically described monomers in the preparation of the binders (as well as the dispersants and thickeners hereinafter described). Further details concerning such other monomers suitable for copolymerization in accordance with the present invention are known to those skilled in the art. The amount of such other monomers is dependent on the particular monomers and their intended function, which amount can be determined by those skilled in the art. 
     The binder polymer of the present invention has crosslinking functionality. At least one of the monomers used to polymerize the binder is a monoethylenically, unsaturated monomer containing “latent crosslinking” capabilities, which as used herein means a monomer which possesses the ability to further react some time after initial formation of the polymer. Activation can occur through the application of energy, e.g., through heat or radiation. Also, drying can activate the crosslinking polymer through changes in pH, oxygen content or other changes that causes a reaction to occur. The particular method of achieving crosslinking in the binder polymer is not critical to the present invention. A variety of chemistries are known in the art to produce crosslinking in latexes. 
     Examples of monomers which do not effect crosslinking until during film formation include carbonyl-containing monomers such as acrolein, methacrolein, diacetone acrylamide, diacetone methacrylamide and vinylaceto acetate. These monomers result in postcrosslinking, for example, when the aqueous polymer emulsion simultaneously contains an appropriate added amount of a polyamine compound. Particularly suitable compounds of this type are the dihydrazides and trihydrazides of aliphatic and aromatic dicarboxylic acids of 2 to 20 carbon atoms. Examples of these are oxalic dihydrazide, adipic dihydrazide and sebacic dihydrazide. Another monomer which produces postcrosslinking is, for example, 2-acetoacetoxyethyl methacrylate (alone or in combination with polyamines or polyaldehydes, such as glyoxal). 
     Other polymer building blocks which are suitable for postcrosslinking are those which contain hydrolyzable organosilicon bonds. Examples are the copolymerizable monomers methacryloyloxypropyltrimethoxysilane and vinyltrimethoxysilane. Further suitable polymer building blocks of a corresponding type are described in DE-A4341260. If the disperse polymer particles have carboxyl groups, postcrosslinking can also be effected by adding metal salts having polyvalent cations (for example Mg, Ca, Zn or Zr salts). 
     Epoxy-, hydroxyl- and/or N-alkylol-containing monomers, for example, glycidyl acrylate, N-methylolacrylamide and -methacrylamide and monoesters of dihydric alcohols with α,β-monoethylenically unsaturated carboxylic acids of 3 to 6 carbon atoms, such as hydroxyethyl, hydroxy-n-propyl or hydroxy-n-butyl acrylate and methacrylate are also suitable for postcrosslinking. 
     U.S. Pat. No. 4,144,212 describes an air-curing copolymer latex prepared by emulsion copolymerization in the presence of free radical polymerization catalysts such as inorganic or organic peroxide polymerization catalysts, with a blend (in % by weight based on the total weight of all monomers used) of (a) about 1% to about 20% of dicyclopentadienyl acrylate or dicyclopentadienyl methacrylate, (b) about 99% to about 20% of an alkyl acrylate or methacrylate, including mixtures of such monomers, and preferably a lower alkyl acrylate or methacrylate in which the alkyl groups contain from 1 to 4 carbon atoms, (c) 0% to about 5% of acrylic acid or methacrylic acid, and (d) 0% to about 85% of other monoethylenically unsaturated copolymerizable monomers, e.g., higher alkyl acrylates and methacrylates in which the alkyl groups contain from 5 to about 18 carbon atoms, acrylamide, methacrylamide, acrylonitrile or methacrylonitrile; also vinyl esters (e.g. vinyl acetate, vinyl propionate of vinyl chloride), styrene and alkyl vinyl ethers. 
     The binder resin of the present invention contains about 0.5 to 10% by weight, based on the total weight of the polymer, of at least one monomer having latent crosslinking functionality, and preferably 1 to 6% by weight, based on the total weight of the polymer, of at least one monomer having latent crosslinking functionality. 
     Typically, the particle size of the binders is from about 0.1 to 1.0 microns, preferably from about 0.2 to 0.4 microns and more preferably from about 0.25 to 0.3 microns. The Tg of the binders of the present invention is typically from about −60 to 100° C. preferably from about −30 to 70° C. and more preferably from about −15 to 60° C. As used herein, the term “Tg” means polymer glass transition temperature. Techniques for measuring the glass transition temperature of polymers are known to those skilled in the art. One such technique is, for example, differential scanning calorimetry. A particularly useful means of estimating the glass transition temperature of a polymer is that given by Fox,
 
1/ Tg   (polymer)   =x   1   /Tg   1   +x   2   /Tg   2   +x   3   /Tg   3   + . . . +x   n   /Tg   n   (1) 
 
where x 1  is the weight fraction of component i in the copolymer and Tg 1  is the homopolymer glass transition of component i. The homopolymer glass transition temperatures can be found in any publicly available source such as the Polymer Handbook. For example, the homopolymer glass transition temperatures for typical monomers are: vinyl acetate =−32° C., butyl acrylate =−54° C., and vinyl neodecanoate =−3° C. and 2-ethylhexyl acrylate =−65° C.
 
     Typically, the viscosity of the binders of the present invention is from about 20 to 3000 and preferably from about 50 to 1500 centipoise (“cP”) measured with a 40 to 60 weight percent solids composition using a Brookfield Viscometer with a number 2 spindle at 60 revolutions per minute. The molecular weight of the binders of the present invention is typically from about 104 to 10 7 , preferably from about 200,000 to 1,000,000 grams per gram mole. As used herein, the term “molecular weight” means weight average molecular weight. Techniques for altering molecular weight are well known and include, for example, utilizing multi functional monomers and chain transfer agents. Techniques for measuring the weight average molecular weight of latex polymers is known to those skilled in the art. One such technique is, for example, gel permeation chromatography. 
     The binder polymer of the present invention may contain hydrophobic groups. The monoethylenically unsaturated monomers described above can be polymerized with one or more macromonomers which are polymerizable. Such macromonomers comprise a hydrophobic portion and an alkoxylated portion which is polymerizable with the other monomers. U.S. Pat. No. 4,703,080, incorporated herein by reference, describes hydrophobic binder resins. Preferred macromonomers are urethane monomers which comprise the reaction product of a monohydric surfactant and a monoethylenically unsaturated isocyanate. These macromonomers are described in detail below with respect to the dispersant. 
     In one aspect of the present invention, the binder polymer comprises an acid functional latex. Specific acid functional monomers suitable for use in accordance with the present invention include, for example, acrylic acid, methacrylic acid, and maleic acid. 
     Preparation of latex compositions is well known in the paint and coatings art. Any of the well known free-radical emulsion polymerization techniques used to formulate latex polymers can be used in the present invention. Such procedures include, for example, single feed, core-shell, and inverted core-shell procedures which produce homogeneous or structures particles. 
     A preferred vinyl acrylate binder resin comprises 40-60% by weight of a fatty acid vinyl ester, 30-50% by weight of methylmethacrylate, 0.5 to 10% by weight of diacetone acrylamide and 0.5-5% by weight methacrylic acid, based on the total weight of the polymer. 
     A preferred acrylic binder resin comprises 20-35% by weight butyl acrylate, 40-65% by weight methyl methacrylate, 0.5-10% by weight diacetone acrylamide, 0.5-5% by weight methacrylic acid and 5-10% by weight acrylonitrile, based on the total weight of the polymer. 
     Dispersants 
     The dispersants suitable for use in accordance with the present invention comprise the reaction product of an unsaturated carboxylic acid monomer, a monoethylenically unsaturated monomer different from the carboxylic acid monomer, a macromonomer comprising a hydrophobic portion and an alkoxylated portion which is polymerizable with the other monomers, and a monomer having latent crosslinking functionality. 
     The unsaturated carboxylic acid monomers suitable for use in accordance with the present invention are typically α,β-monethylenically unsaturated carboxylic acids. Preferred carboxylic acid monomers are selected from the group consisting of acrylic acid, methacrylic acid, crotonic acid, itaconic acid, maleic acid, and mixtures thereof. Methacrylic acid is especially preferred. The concentration of the carboxylic acid monomer is typically from about 20 to 70 weight percent, preferably from about 20 to 50 weight percent and more preferably from about 35 to 45 weight percent based on the total weight of the polymer. The amount of the carboxylic acid monomer is preferably sufficient to provide a polymeric structure which will solubilize and provide viscosity enhancement when reacted with an alkali such as for example, sodium hydroxide. 
     In accordance with the present invention, the monoethylenically unsaturated monomer different from the carboxylic acid monomer preferably comprises a methyl group. More preferably, this monomer is an acrylate. Most preferably, this monomer is ethyl acrylate. Typically, the amount of the monoethylenically unsaturated monomer different from carboxylic acid is from about 5 to 70 weight percent, preferably from about 10 to 50 weight percent based on the total weight of the polymer. 
     The macromonomers suitable for manufacturing the dispersant in accordance with the present invention comprise a hydrophobic portion and an alkoxylated portion which is polymerizable with other monomer(s). As used herein, the term “macromonomer” means a polymerizable monomer which comprises the reaction product of two or more compounds. Such macromonomers include, for example, any alkoxylated, e.g., ethoxylated or propoxylated, monomers having ethylenic unsaturation and which are terminated by a hydrophobic fatty chain. Examples of unsaturated, polymerizable moieties include those selected from the group consisting of vinyl group containing moieties, methacryloyl, maleoyl, itaconoyl, crotonyl, an unsaturated urethane moiety, hemiester maleoyl, hemiester itaconoyl, CH 2 ═CHCH 2 —O—, methacrylamido and substituted methacrylamido. Examples of hydrophobic moieties include those selected from the group consisting of alkyl, alkaryl, i.e., alkylaryl or aralkyl, or aryl, linear or branched, saturated or unsaturated, and having at least 6 carbon atoms, preferably from about 6 to 30 carbon atoms per molecule. 
     Preferred macromonomers are urethane monomers which comprise the reaction product of a monohydric surfactant and a monoethylenically unsaturated isocyanate. Preferably, the urethane monomer is a nonionic, urethane monomer which is the urethane reaction product of a monohydric, nonionic surfactant with a monoethylenically unsaturated monoisocyanate, preferably one lacking ester groups, e.g., alpha, alpha-dimethyl-m-isopropenyl benzyl isocyanate. The monohydric nonionic surfactants are themselves well known and are usually alkoxylated, e.g., ethoxylated, hydrophobes containing adducted ethylene oxide to provide the hydrophilic portion of the molecule. The hydrophobes are usually aliphatic alcohols or alkyl phenols in which a carbon chain containing at least 6 carbon atoms, preferably about 6 to 30 carbon atoms, provides the hydrophobic portion of the surfactant. These surfactants are illustrated by ethylene oxide adducts of dodecyl alcohol or octyl or nonyl phenol which are available in commerce and which contain about 5 to about 150, preferably 25 to 60 moles of ethylene oxide per mole of hydrophobe. Other hydrophobic substituents, such as complex hydrophobes, disclosed for example in U.S. Pat. No. 5,488,180 issued Jan. 30, 1996, are suitable for use in accordance with the present invention. 
     The monoethylenically unsaturated isocyanates suitable for use in preparing the urethane monomers can be any isocyanates effective to form the desired urethane linkage. Preferably, the isocyanate is a monoethylenically unsaturated monoisocyanate. Any copolymerizable unsaturation may be employed, such as acrylate and methacrylate unsaturation. One may also use allylic unsaturation, as provided by allyl alcohol. These, preferably in the form of a hydroxy-functional derivative, as is obtained by reacting a C2-C4 monoepoxide, like ethylene oxide, propylene oxide or butylene oxide, with acrylic or methacrylic acid to form an hydroxy ester, are preferably reacted in equimolar proportions with an organic diisocyanate, such as toluene diisocyanate or isophorone diisocyanate. The preferred monoethylenic monoisocyanate is styryl, as in alpha, alpha-dimethyl-m-isopropenyl benzyl isocyanate, and this unsaturated monoisocyanate lacks the ester group so it forms urethanes which lack this group. The amount of the monoethylenically unsaturated isocyanate relative to the monohydric surfactant used in making the macromonomer, (on a mole ratio basis) is typically from about 0.1-2.0 to 1, preferably about 1.0 to 1.0. 
     Suitable macromonomers useful in this invention can also be represented by the formula: 
                        
 
wherein:
         R 1  is a monovalent residue of a substituted or unsubstituted hydrophobe compound;   each R 2  is the same or different and is a substituted or unsubstituted divalent hydrocarbon residue;   R 3  is a substituted or unsubstituted divalent hydrocarbon residue;   R 4 , R 5 , R 6  are the same or different and are hydrogen or a substituted or unsubstituted monovalent hydrocarbon residue;   and z is a value of 0 to 150.       

     Illustrative R 1  substituents include, for example, simple or complex hydrophobe containing from 1 to 30 carbon atoms such as alkyl, aryl, aralkyl, alkaryl and cycloakyl groups. 
     Illustrative R 3  substituents include, for example, the organic residue of ethers, esters, urethanes, amides, ureas, anhydrides and the like including mixtures thereof. The R 3  substituent can be generally described as a “linkage” between the hydrophobe bearing surfactant or alcohol and the unsaturated portion of the macromonomer compound. 
     The oxyalkylene moieties included in the macromonomer compounds may be homopolymers or block or random copolymers of straight or branched alkylene oxides. Mixtures of alkylene oxides such as ethylene oxide and propylene oxides may also be employed. 
     Further details concerning the preparation of such macromonomers are known to those skilled in the art and are disclosed, for example, in U.S. Pat. Nos. 4,514,552, 4,801,671, 5,292,828, 5,292,843 and 5,294,693, incorporated herein by reference. 
     Typically, the amount of the macromonomer is from about 0.5 to 60 weight percent, preferably from about 5 to 50 weight percent and more preferably from about 35 to 45 weight percent based on the total weight of the dispersant polymer. Typically, the molecular weight of the macromonomer ranges from about 400 to 8000 grams per gram mole. 
     Typically the viscosity of the dispersants of the present invention is from about 5 to 1500 cP in the un-neutralized form measured at 20° C. with a 20 to 50 weight percent solids composition using a Brookfield Viscometer with a number 2 spindle at 60 revolutions per minute. The molecular weight of the dispersants of the present invention is typically from about 10 3  to 10 6 , preferably from about 5,000 to 10,000 grams per gram mole. Typically, the particle size of the dispersant is from about 0.05 to 1.0 microns, preferably from about 0.1 to 0.4 microns and more preferably from about 0.1 to 0.3 microns. The Tg of the dispersants of the present invention is typically from about 0 to 90° C. preferably from about 5 to 60° C. and more preferably from about 15 to 35° C. 
     The dispersants useful in the present invention contain 0.5 to 50% by weight, preferably 20 to 35% by weight, based on the total weight of the dispersant polymer, of at least one monomer having latent crosslinking functionality. 
     Thickeners 
     Any suitable alkali soluble thickeners may be utilized in accordance with the present invention. Such alkali soluble thickeners are disclosed, for example, in U.S. Pat. Nos. 4,514,552, 4,722,962, 5,292,828 and 5,292,843, which are incorporated herein by reference. The alkali soluble thickeners typically comprise the aqueous emulsion reaction product of an unsaturated carboxylic acid monomer, e.g., methacrylic acid; a monoethylenically unsaturated monomer different from the carboxylic acid monomer, e.g. ethyl acrylate; a macromonomer comprising a hydrophobic portion and an alkoxylated portion which is polymerizable with the other monomers; and a monomer having latent crosslinking functionality. The unsaturated carboxylic acid monomer, monoethylenically unsaturated monomer different from the carboxylic acid monomer, macromonomer and latent crosslinking monomer used to polymerize the thickener can include those such as described above with reference to the binder polymer and dispersant. Often, the macromonomer is a urethane monomer which is the urethane reaction product of a monohydric surfactant and a monoethylenically unsaturated monoisocyanate. Typically, the monohydric surfactant comprises an ethyloxated or propoxylated aliphatic alcohol or alkyl phenol. 
     In a preferred aspect of the present invention, the thickeners are prepared in accordance using monomers such as those described above with respect to the preferred dispersants. Typically, the amount of the macromonomer is from about 1 to 20 weight percent, perferably from about 5 to 15 weight percent based on the total weight of the polymer. 
     Typically, the viscosity of the thickeners of the present invention is from about 5 to 1500 cP in the un-neutralized form measured at 20° C. with a 20 to 50 weight percent solids composition using a Brookfield Viscometer with a number 2 spindle at 60 revolutions per minute. The molecular weight of the thickeners of the present invention is typically from about 10 4  to 10 7 , preferably from about 20,000 to 200,000 grams per gram mole. Typically, the particle size of the thickeners is from about 0.05 to 1.0 microns, preferably from about 0.1 to 0.4 microns and more preferably from about 0.1 to 0.3 microns. The Tg of the thickeners of the present invention is typically from about 0 to 90° C., preferably from about 5 to 60° C., and more preferably from about 15 to 55° C. 
     The thickeners useful in the present invention contain 0.5 to 35% by weight, preferably 1 to 5% by weight, based on the total weight of the thickener polymer, of at least one monomer having latent crosslinking functionality. 
     The binders, dispersants and thickeners of the present invention are typically in colloidal form, i.e., aqueous dispersions, or in solution and can be prepared by emulsion polymerization in the presence of a chain transfer agent and an initiator. Specific details concerning procedures and conditions for emulsion polymerization are known to those skilled in the art. Typically, however, the polymerization is carried out in an aqueous medium at a temperature of from about 35 to 90° C. The pressure is not critical and is dependent upon the nature of the monomers employed as can be determined by one skilled in the art. 
     A chain transfer agent is preferably present during the polymerization reaction at a concentration of from about 0.01 to 5 weight percent, preferably from about 0.1 to 2 weight percent based on the total monomer content. Both water-insoluble and water-soluble chain transfer agents can be employed. Illustrative of substantially water-soluble chain transfer agents are alkyl and aryl mercaptans such as butyl mercaptan, mercaptoacetic acid, mercaptoethanol, 3-mercaptol-1,2-propanediol and 2-methyl-2-propanethiol. Illustrative of the substantially water-insoluble chain transfer agents include, for example, t-dodecyl mercaptan, phenyl mercaptan, pentaerythritol tetramercaptopropionate, octyldecyl mercaptan, tetradecyl mercaptan and 2-ethylhexyl-3-mercaptopropionate. 
     In carrying out the emulsion polymerization, an initiator (also referred to in the art as a catalyst) is preferably used at a concentration sufficient to catalyze the polymerization reaction. This will typically vary from about 0.01 to 3 weight percent based on the weight of monomers charged. However, the concentration of initiator is preferably from about 0.05 to 2 weight percent and, most preferably, from about 0.1 to 1 weight percent of the monomers charged. The particular concentration used in any instance will depend upon the specific monomer mixture undergoing reaction and the specific initiator employed, which details are known to those skilled in the art. Illustrative of suitable initiators include hydrogen peroxide, peracetic acid, t-butyl hydroperoxide, di-t-butyl hydroperoxide, dibenzoyl peroxide, benzoyl hydroperoxide, 2,4-dicholorbenzoyl peroxide, 2,5-dimethyl-2,5-bis(hydroperoxy) hexane, perbenzoic acid, t-butyl peroxypivalate, t-butyl peracetate, dilauroyl peroxide, dicapryloyl peroxide, distearoyl peroxide, dibenzoyl peroxide, diisopropyl peroxydicarbonate, didecyl peroxydicarbonate, dicicosyl peroxydicarbonate, di-t-butyl perbenzoate, 2,2′-azobis-2,4-dimethylvaleronitrile, ammonium persulfate, potassium persulfate, sodium persulfate, sodium perphosphate, azobisisobutyronitrile, as well as any of the other known initiators. Also useful are the redox catalyst systems such as sodium persulfate-sodium formaldehyde sulfoxylate, cumene hydroperoxide-sodium metabisulfite, hydrogen peroxide-ascorbic acid, and other known redox systems. Moreover, as known by those skilled in the art, traces of metal ions can be added as activators to improve the rate of polymerization, if desired. 
     The particular surfactant useful for conducting the polymerization reaction is not critical to the present invention. Typical surfactants include anionic surfactants such as sodium lauryl sulfate, sodium tridecylether sulfate, diester sulfosuccinates and sodium salts of alkyl aryl polyether sulfonates; and nonionic surfactants such as alkyl aryl polyether alcohols and ethylene oxide condensates of propylene oxide, propylene glycol adducts. 
     The reaction products of the polymerizations comprising the binders, dispersants or thickeners of the present invention typically have a solids, i.e., polymer, content of from about 15 to 65 weight percent, preferably from about 20 to 65 weight percent and more preferably from about 25 to 60 weight percent based on the weight of the latex and water. 
     EXAMPLES 
     The following examples are provided for illustrative purposes and are not intended to limit the scope of the claims which follow. 
     Example M1 
     Preparation of Macromonomer with Small Hydrophobe 
     To a one-liter glass reactor fitted with a thermometer, heating mantle, thermoregulator, stirrer, nitrogen sparge, and condenser including a Dean-Stark trap was charged 930 grams of a 40 mole ethoxylate of nonyl phenol, i.e., a small hydrophobe. The reactor contents were heated, with nitrogen sparging, to 110° C. and held for two hours while trace moisture was removed and collected in the Dean-Stark Trap (typically less than 1 g). The reactor contents were then cooled to 80° C., the Dean Stark trap was replaced with a condenser, and the nitrogen sparge was switched to an air sparge for 15 minutes. With continued air sparging, 0.02 g methoxy-hydroquinone inhibitor, 0.50 g dibutyl tin dilaurate catalyst, and 99.7 g of alpha, alpha-dimethyl-m-isopropenyl benzyl isocyanate (m-TMI, a product of CYTEC, Stamford, Conn.) were charged in order to the reactor. After a rapid initial exotherm which increased the reaction temperature about 8° C., the contents were maintained at 80° C. for an additional two hours. The product was then cooled to room temperature. The final product was a white wax in appearance with residual isocyanate content of 0.5% and with 98% of the original ethylenic unsaturation retained. 
     Example M2 
     Preparation of Macromonomer with Large Hydrophobe 
     A macromonomer was prepared substantially in accordance with Example M1, except that a 20 mole ethoxylate of bis-nonylphenoxy ethanol (large hydrophobe) was used in place of the nonylphenol (small hydrophobe) and the amounts of the reacts used were adjusted to maintain a molar ration of 1:1. 
     Example A 
     Acrylic Latex Binder Preparation 
     A monomer mixture was prepared by charging 460 g of butyl acrylate, 520 g of methyl methacrylate, 9.8 g diacetone acrylamide (DAAM), 5.4 g of methacrylic acid, 40 g of Rhodacal DS-4 (a dodecyl benzene sulfonate surfactant available from CYTEC) and 365 g of water to a two liter monomer feed cylinder. A two liter jacketed resin flask equipped with a four-bladed stainless steel mechanical stirrer, Claisen connecting tube, Friedrichs water condenser, nitrogen sparge and bubble trap, thermometer, and monomer addition inlets were used to charge 560 f of water. An initial oxidizer solution, prepared by dissolving 4 g of ammonium persulfate in 20 g of water, was prepared in a separate container. Under nitrogen purge, the reactor was heated to 80° C. by circulating temperature controlled water through the reactor jacket. After the temperature of the reactor charge had reached 80° C., the initial oxidizer solution was added to the reactor. Two minutes later, the monomer feed was conveyed to the reaction vessel over a 3 hour period by FMI (Fluid Metering Inc.) pumps using ⅛ inch Teflon tubing with continuous stirring while the reaction temperature was held between 79° and 81° C. The reaction was allowed to proceed at 80° C. for an additional hour after completion of the monomer feed. To the product was added 15% ammonium hydroxide solution to a pH of 9. To the cooled product was added 36.8 g of a 10% solution of adipic dihydrazide. 
     Example B 
     Styrene Acrylic Latex Binder Preparation 
     A first monomer mixture was prepared by charging 365 grams of butyl acrylate (BA), 470 grams of methyl methacrylate (MMA), 130 grams of styrene, 5.4 grams of methacrylic acid (MAA), 40 grams of diacetone acrylamide (DAAM), 40 grams of TRITON GR-9M (a disodium ethoxylated lauryl alcohol half ester of sulfosuccinic acid surfactant available from Union Carbide Corporation, Danbury, Conn.) and 450 grams of water to a 2-liter monomer feed cylinder. A two liter jacketed resin flask equipped with a four-blade stainless steel mechanical stirrer, Claisen connecting tube, Friedrichs water condenser, nitrogen sparge and bubble trap, thermometer, and monomer addition inlets was used as the reactor. To the reactor was charged 600 grams of water. An initial oxidizer solution, prepared by dissolving 4 grams of ammonium persulfate in 20 grams of water, was prepared in a separate container. Under nitrogen purge, the reactor was heated to 80° C. by circulating temperature controlled water through the reactor jacket. After the temperature of the reactor charge had reached 80° C., the initial oxidizer solution was added to the reactor. Two minutes later, the monomer feed was conveyed to the reaction vessel over a 3 hour period by FMI (Fluid Metering Inc.) pumps using ⅛ inch Teflon tubing with continuous stirring while the reaction temperature was held between 79° and 81° C. The reaction was allowed to proceed at 80° C. for an additional hour after completion of the monomer feed. 
     A second monomer mixture was prepared by charging 36 grams of methacrylic acid (MAA), 72 grams of methyl methacrylate, 120 grams of styrene, 12.5 grams diacetone acrylamide, 1.2 grams of ethylhexyl-3-mercaptopropionate as a chain transfer agent (CTA), 12.5 grams of the macromonomer of Example M1 and 12.5 grams of the macromonomer alpha, alpha-dimethyl-m-isopropenylbenzylisocyanate adduct with Bis-nonylphenoxy-propylpoly(ethyleneoxy) ethanol (large hydrophobe macromonomer of Example M2), 4 grams of Rhodacal DS-4 and 245 grams of water to a one 2-liter monomer feed cylinder. An additional 4 grams of ammonium persulfate in 20 grams of water, was prepared in a separate container and added to the reactor. The monomer feed was conveyed to the reaction vessel over a 3 hour period with continuous stirring while the reaction temperature was held between 79° and 81° C. The reaction was allowed to proceed at 80° C. for an additional hour after completion of the monomer feed. 
     To the product was added 15% ammonium hydroxide solution to a pH of 9. To the cooled product was added 0.75 molar amounts of adipic dihydrazide. 
     Table 1 below sets forth a variety of latexes made with the monomers as listed in accordance with the procedure of Example B. Ingredients are listed in grams. 
     
       
         
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
             
           
               
                 TABLE 1 
               
               
                   
               
               
                   
                 1st 
                   
                   
                   
                   
                   
               
               
                 Exam- 
                 Stage 
                 2nd Stage 
                 2nd Stage 
                 2nd Stage 
                 2nd Stage 
               
               
                 ple 
                 DAAM 
                 M1 
                 M2 
                 DAAM 
                 MAA 
                 CTA 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                 B1 
                 40 
                 0 
                 0 
                 12.5 
                 30 
                 0 
               
               
                 B2 
                 15 
                 0 
                 12.5 
                 5 
                 36 
                 1.2 
               
               
                 B3 
                 40 
                 12.5 
                 0 
                 12.5 
                 36 
                 0 
               
               
                 B4 
                 15 
                 12.5 
                 12.5 
                 5 
                 36 
                 0 
               
               
                 B5 
                 15 
                 12.5 
                 12.5 
                 5 
                 30 
                 1.2 
               
               
                 B6 
                 15 
                 12.5 
                 0 
                 5 
                 36 
                 1.2 
               
               
                 B7 
                 40 
                 0 
                 0 
                 12.5 
                 36 
                 1.2 
               
               
                 B8 
                 40 
                 12.5 
                 0 
                 12.5 
                 30 
                 1.2 
               
               
                 B9 
                 15 
                 12.5 
                 0 
                 5 
                 30 
                 0 
               
               
                 B10 
                 40 
                 12.5 
                 12.5 
                 12.5 
                 30 
                 0 
               
               
                 B11 
                 15 
                 0 
                 12.5 
                 5 
                 30 
                 0 
               
               
                 B12 
                 15 
                 0 
                 0 
                 5 
                 36 
                 0 
               
               
                 B13 
                 15 
                 0 
                 0 
                 5 
                 30 
                 1.2 
               
               
                 B14 
                 40 
                 0 
                 12.5 
                 12.5 
                 30 
                 1.2 
               
               
                 B15 
                 40 
                 12.5 
                 12.5 
                 12.5 
                 36 
                 1.2 
               
               
                 B16 
                 40 
                 0 
                 12.5 
                 12.5 
                 36 
                 0 
               
               
                 B17 
                 100  
                 0 
                 0 
                 25 
                 48 
                 1.2 
               
               
                 B18 
                 50 
                 0 
                 5 
                 12.5 
                 48 
                 1.2 
               
               
                 B19 
                 100  
                 0 
                 5 
                 25 
                 36 
                 1.2 
               
               
                 B20 
                 50 
                 0 
                 0 
                 12.5 
                 36 
                 1.2 
               
               
                 B21 
                 50 
                 0 
                 5 
                 12.5 
                 36 
                 1.2 
               
               
                 B22 
                 100  
                 0 
                 0 
                 25 
                 36 
                 1.2 
               
               
                 B23 
                 100  
                 0 
                 5 
                 25 
                 48 
                 1.2 
               
               
                 B24 
                 50 
                 0 
                 0 
                 12.5 
                 48 
                 1.2 
               
               
                 B25 1   
                 50 
                 0 
                 0 
                 12.5 
                 15 
                 1.2 
               
               
                 B26 1   
                 50 
                 0 
                 0 
                 12.5 
                 15 
                 1.2 
               
               
                 B27 2   
                 50 
                 0 
                 0 
                 12.5 
                 15 
                 1.2 
               
               
                 B28 2 * 
                 50 
                 0 
                 0 
                 12.5 
                 15 
                 1.2 
               
               
                 B29 2 * 
                 50 
                 0 
                 0 
                 12.5 
                 15 
                 1.2 
               
               
                   
               
               
                   1 Methylmethacrylate substituted for styrene monomer in stage1 and stage 2.  
               
               
                   2 Veo Val0 substituted for BA and styrene in stage 1 and stage2.  
               
               
                   3 MMA substituted for styrene and acrylonitrile substituted for 10% by weight of MMA in stage 1 and stage 2.  
               
               
                 *Surfactant used was Rhodafac RE-610  
               
             
          
         
       
     
     Example C 
     Latex Binder Preparation 
     A monomer mixture was prepared by charging 615 grams of VeoVa 10 (a vinyl versatate ester having 10 carbon atoms in the acid portion, commercially available from Shell Chemical), 368 grams of methyl methacrylate (MMA), 9.8 grams diacetone acrylamide (DAAM), 11 grams of methacrylic: acid (MAA), 40 grams of Rhodafac 610 (a nonylphenol ethoxylated phosphate ester surfactant available from Rhodia) and 365 grams of water to a 2-liter monomer feed cylinder. A two liter jacketed resin flask equipped with a four-bladed stainless steel mechanical stirrer, Claisen connecting tube, Freidrichs water condenser, nitrogen sparge and bubble trap, thermometer, and monomer addition inlets was used as the reactor. To the reactor was charged 560 grams of water. An initial oxidizer solution, prepared by dissolving 4 grams of ammonium persulfate in 20 grams of water, was prepared in a separate container. Under nitrogen purge, the reactor was heated to 80° C. by circulating temperature controlled water through the reactor jacket. After the temperature of the reactor charge had reached 80° C., the initial oxidizer solution was added to the reactor. Two minutes later, the monomer feed was conveyed to the reaction vessel over a 3 hour period by FMI pumps using ⅛″ Teflon tubing with continuous stirring while the reaction temperature was held between 79° and 81° C. The reaction was allowed to proceed at 80° C. for an additional hour after completion of the monomer feed. To the product was added 15% ammonium hydroxide solution to a pH of 9. To the cooled product was added 0.75 molar amounts of adipic dihydrazide. 
     Table 2 below sets forth other latexes made with monomers as listed in accordance with the procedure of Example C. Ingredients are listed in grams. 
     
       
         
               
               
               
               
               
             
           
               
                 TABLE 2 
               
               
                   
               
               
                 Example 
                 Veo Val0 
                 MMA 
                 MAA 
                 Surfactant 
               
               
                   
               
             
             
               
                 C1 
                 615 
                 368 
                 11 
                 Rhodafac RE-610 
               
               
                 C2 
                 487 
                 497 
                 11 
                 Rhodafac RE-610 
               
               
                   
               
             
          
         
       
     
     Example D 
     Acrylic Latex Binder Preparation 
     A monomer mixture was prepared by charging 530 grams (“g”) of butyl acrylate, 600 g of methyl methacrylate, 23 g diacetone acrylamide (DAAM), 5.4 g of methacrylic acid (MAA), 40 g of Rhodacal DS-4 (a surfactant available from Rhone-Poulenc) and 450 g of water to a one 2-liter monomer feed cylinder. A two liter jacketed resin flask equipped with a four-bladed stainless steel mechanical stirrer, Claisen connecting tube, Friedrichs water condenser, nitrogen sparge and bubble trap, thermometer, and monomer addition inlets were used to charge 800 g of water. An initial oxidizer solution, prepared by dissolving 4 g of ammonium persulfate in 20 g of water, was prepared in a separate container. Under nitrogen purge, the reactor was heated to 80° C. by circulating temperature controlled water through the reactor jacket. After the temperature of the reactor charge had reached 80° C., the initial oxidizer solution was added to the reactor. Two minutes later, the monomer feed was conveyed to the reaction vessel over a 3 hour period by FMI (Fluid Metering Inc.) pumps using ⅛″ Teflon tubing with continuous stirring while the reaction temperature was held between 79 and 81° C. The reaction was allowed to proceed at 80° C. for an additional hour after completion of the monomer feed. 
     A second monomer mixture was prepared by charging 7.35 grams of methacrylic acid (MAA), 21 grams of butyl acrylate, 7.5 grams diacetone acrylamide (DAAM), 7.35 grams of the macromonomer M1, 4 grams of Rhodacal DS-4 and 10 grams of ammonium persulfate in 20 grams of water, was prepared in a separate container and added to the reactor. The monomer feed was conveyed to the reaction vessel over a 3 hour period with continuous stirring while the reaction temperature was held between 79 and 81° C. The reaction was allowed to proceed at 80° C. for an additional hour after completion of the monomer feed. 
     To the product was added 15% ammonium hydroxide solution to a pH of 9. To the cooled product was added 0.75 molar amounts of adipic dihydrazide. 
     Table 3 sets forth a variety of latexes made with the monomers as listed in accordance with the procedure of Example D. Ingredients are listed in grams. 
     
       
         
               
               
               
               
               
             
               
               
               
               
               
             
           
               
                 TABLE 3 
               
               
                   
               
               
                   
                 1st Stage 
                 2nd Stage 
                 2nd Stage 
                 2nd Stage 
               
               
                 Example 
                 DAAM 
                 M1 
                 DAAM 
                 MAA 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                 D1 
                 23 
                 7.35 
                 7.3 
                 7.5 
               
               
                 D2 
                 58 
                 1.8 
                 1.8 
                 15 
               
               
                 D3 
                 58 
                 7.35 
                 1.8 
                 15 
               
               
                 D4 
                 23 
                 1.8 
                 7.3 
                 7.5 
               
               
                 D5 
                 23 
                 7.35 
                 7.3 
                 15 
               
               
                 D6 
                 58 
                 1.8 
                 1.8 
                 7.5 
               
               
                 D7 
                 23 
                 1.8 
                 7.3 
                 15 
               
               
                 D8 
                 58 
                 7.35 
                 1.8 
                 7.5 
               
               
                   
               
             
          
         
       
     
     Example E 
     Preparation of Crosslinkable Thickener 
     A monomer mixture (300 grams) was prepared by charging ethyl acrylate, methacrylic acid, diacetone acrylamide, macromonomer M1, 13 grams of a 75% solution of Aerosol® OT surfactant (American Cyanamid) and 3 grams of distilled deionized water to a bottle, and dispersing the contents with vigorous shaking. The ethyl acrylate, methacrylic acid, diacetone acrylamide and macromonomer M1 were added in amounts identified in Table 4 below. A catalyst feed mixture comprised of 0.53 grams of sodium persulfate and 52.47 grams of water was prepared in another container. To a 2 liter resin flask that had been immersed in a thermostated water bath and equipped with a 4-bladed stainless steel mechanical stirrer, Claisen connecting tube, water condenser, nitrogen sparge and bubble trap, thermometer and monomer and catalyst addition inlets, 1.20 grams of the sodium salt of vinyl sulfonic acid and 658.5 grams of water were charged. The monomer mixture was charged to a 1-liter graduated monomer feed cylinder, and the catalyst solution was charged to a 125 milliliter graduated catalyst feed cylinder. Under nitrogen purge, the reactor was heated to 70° C., whereupon 33 milliliters of the monomer mixture and 3 milliliters of the catalyst feed mixture were charged to the reaction vessel. The reaction vessel was subsequently heated to 80° C. After allowing the monomers to react for 20 minutes to form a seed product, the monomer and catalyst feed mixtures were conveyed to the reaction vessel by FMI pumps via ⅛ inch teflon tubing at a rate of 1.94 and 0.27 milliters/minute, respectively, under continuous stirring at a reaction temperature held between 76° and 82° C. The reaction was allowed to proceed for another hour, after which the product was cooled and filtered with a 200 mesh nylon cloth. The coagulum was collected from the reaction vessel and filter cloth. The product is a low viscosity latex of solids content of about 40% and pH of about 2.5. 
     Table 4 sets forth a variety of thickeners made with the monomers as listed, in accordance with the procedure of Example E. Ingredients are listed in percentages by weight based on the total weight of the polymer. 
     
       
         
               
               
               
               
               
               
               
             
           
               
                 TABLE 4 
               
               
                   
               
               
                 Example 
                 M1 
                 M2 
                 MAA 
                 EA 
                 DAAM 
                 Surfactant 
               
               
                   
               
             
             
               
                 E1 
                 15 
                   
                 40 
                 35 
                 10 
                 Rhodafac RE-610 
               
               
                 E2 
                  5 
                   
                 40 
                 45 
                 10 
                 Rhodafac RE-610 
               
               
                 E3 
                 15 
                   
                 40 
                 40 
                  5 
                 Rhodafac RE-610 
               
               
                 E4 
                  5 
                   
                 40 
                 50 
                  5 
                 Triton GR-9M 
               
               
                 E5 
                   
                 5 
                 40 
                 50 
                  5 
                 Triton GR-9M 
               
               
                 E6 
                   
                 5 
                 40 
                 45 
                 10 
                 Triton GR-9M 
               
               
                 E7 
                 15 
                   
                 40 
                 35 
                 10 
                 Triton GR-9M 
               
               
                 E8 
                 15 
                   
                 40 
                 40 
                  5 
                 Triton GR-9M 
               
               
                   
               
             
          
         
       
     
     Example F 
     Preparation of Crosslinkable Dispersant 
     A monomer mixture (300 grams) was prepared by charging ethyl acrylate, methacrylic acid, diacetone acrylamide, macromonomer M1, 13 grams of a 75% solution of Aerosol® OT surfactant (American Cyanamid) and 3 grams of distilled deionized water to a bottle, and dispersing the, contents with vigorous shaking. The ethyl acrylate, methacrylic acid, diacetone acrylamide and macromonomer M1 were added in amounts identified in Table 5 below. A catalyst feed mixture comprised of 0.53 grams of sodium persulfate and 52.47 grams of water was prepared in another container. To a 2 liter resin flask that had been immersed in a thermostated water bath and equipped with a 4-beaded stainless steel mechanical stirrer, Claisen connecting tube, water condenser, nitrogen sparge and bubble trap, thermometer and monomer and catalyst addition inlets, 1.20 grams of the sodium salt of vinyl sulfonic acid and 658.5 grams of water were charged. The monomer mixture was charged to a 1-liter graduated monomer feed cylinder, and the catalyst solution was charged to a 125 milliliter graduated catalyst feed cylinder. Under nitrogen purge, the reactor was heated to 70° C., whereupon 33 milliliters of the monomer mixture and 3 milliliters of the catalyst feed mixture were charged to the reaction vessel. The reaction vessel was subsequently heated to 80° C. After allowing the monomers to react for 20 minutes to form a seed product, the monomer and catalyst feed mixtures were conveyed to the reaction vessel by FMI pumps via ⅛ inch teflon tubing at a rate of 1.94 and 0.27 milliters/minute, respectively, under continuous stirring at a reaction temperature held between 76° and 82° C. The reaction was allowed to proceed for another hour, after which the product was cooled and filtered with a 200 mesh nylon cloth. The coagulum was collected from the reaction vessel and filter cloth. The product is a low viscosity latex of solids content of about 25%. The product was subsequently neutralized to a pH of about 9.0. 
     Table 5 sets forth a variety of dispersants made with the monomers as listed, in accordance with the procedure of Example F. Ingredients are listed in percentages by weight based on the total weight of the polymer. 
     
       
         
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
             
           
               
                 TABLE 5 
               
               
                   
               
               
                 Example 
                 M1 
                 M2 
                 MAA 
                 EA 
                 DAAM 
                 Surfactant 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                 F1 
                   
                   
                 40 
                 32.5 
                 20 
                 Rhodafac RE-610 
               
               
                 F2 
                   
                 30 
                 17 5 
                 47.5 
                  5 
                 Triton GR-9M 
               
               
                 F3 
                 30 
                   
                 17.5 
                 17.5 
                 35 
                 Triton GR-9M 
               
               
                 F4 
                 30 
                   
                 17.5 
                 32.5 
                 20 
                 Triton GR-9M 
               
               
                 F5 
                 37.5 
                   
                 17.5 
                 25 
                 20 
                 Rhodafac RE-610 
               
               
                 F6 
                 37.5 
                   
                 17.5 
                 10 
                 35 
                 Triton GR-9M 
               
               
                 F7 
                 45 
                   
                 17.5 
                 32.5 
                  5 
                 Triton GR-9M 
               
               
                 F8 
                   
                 37.5 
                 17.5 
                 40 
                  5 
                 Triton GR-9M 
               
               
                 F9 
                   
                 37.5 
                 17.5 
                 25 
                 20 
                 Triton GR-9M 
               
               
                 F10 
                   
                 45 
                 17.5 
                 17.5 
                 20 
                 Triton GR-9M 
               
               
                 F11 
                   
                 45 
                 17.7 
                 2.5 
                 35 
                 Triton GR-9M 
               
               
                 F12 
                 30 
                   
                 25 
                 35 
                 10 
                 Triton GR-9M 
               
               
                 F13 
                 30 
                   
                 25 
                 25 
                 20 
                 Triton GR-9M 
               
               
                 F14 
                 30 
                   
                 40 
                 20 
                 10 
                 Triton GR-9M 
               
               
                 F15 
                 30 
                   
                 25 
                 40 
                  5 
                 Triton GR-9M 
               
               
                 F16 
                 30 
                   
                 17.5 
                 25 
                  5 
                 Triton GR-9M 
               
               
                   
               
             
          
         
       
     
     The binders, thickeners and dispersants described above were used in the formulation of paints as described below. The paint formulations may, in addition to the polymers described herein, contain conventional additives, such as pigments, fillers, wetting agents, coalescants, biocides and anti-foaming agents and the like. 
     Example G 
     Preparation of Latex Paint 
     A pigment grind is prepared by adding the following ingredients in sequence: 54.96 grams of water, 5.92 grams of a 28% aqueous ammonia solution and 2.76 grams of Dispersant F9 to a HSD-type grinding apparatus with low agitation. Slowly added are 200.8 grams of TiPure R-706 titanium dioxide pigment (DuPont) while the agitation is increased. The mixture is ground for approximately 1 hour, or until a fineness of grind of 8 Hegman is obtained. The agitation is reduced and 25.6 grams of ethylene glycol and 1.8 grams of BYK 035 defoamer is added. 
     A thickener premix is prepared by adding 10.32 grams of water to a mix tank and under agitation, adding 0.25 grams of Thickener E5 and 0.05 grams of 28% aqueous ammonia solution to the tank. 
     The paint is prepared by adding 568.72 grams of Binder resin C2 to the grind mixture under agitation. After this mixture is agitated for about 30 minutes, the following ingredients are added in order: 21.64 grams of Exxate 1000 (Exxon), 5.44 grams of Arcosolve DPNB (dipropylene glycol n-butyl ether from Arco Chemicals) and 11.64 grams of Exxate 900 (oxononyl acetate from Exxon). The thickener premix is then added under agitation. Flash X-150 flash rust inhibitor (Halox) in an amount of 2.6 grams is then added, followed by 1.48 grams of Surfynol 104BC defoamer (Air Products) and 1.48 grams of Byk 307 (wetting agent from BYK-Chemie). Dispersant F9 is then added in an amount of 2.76 grams. The paint is mixed until it is homogeneous and then reduced with 54.57 grams of water to the desired application viscosity. 
     Example H 
     Preparation of Paint 
     A pigment grind is prepared by adding the following ingredients in sequence: 54.96 grams of water, 5.92 grams of a 28% aqueous ammonia solution and 2.55 grams of Dispersant F5 to a HSD-type grinding apparatus with low agitation. Slowly added are 200.8 grams of TiPure R-706 titanium dioxide pigment (DuPont) while the agitation is increased. The mixture is ground for approximately 1 hour, or until a fineness of grind of 8 Hegman is obtained. The agitation is reduced and 25.6 grams of ethylene glycol and 1.8 grams of BYK 035 defoamer is added. 
     A thickener premix is prepared by adding 10.32 grams of water to a mix tank and under agitation, adding 0.25 grams of Thickener E5 and 0.05 grams of 28% aqueous ammonia solution to the tank. 
     The paint is prepared by adding 581.48 grams of Binder resin B29 to the grind mixture under agitation. After this mixture is agitated for about 30 minutes, the following ingredients are added in order: 21.64 grams of Texanol (Eastman Chemicals), 5.44 grams of Arcosolve DPNB (dipropylene glycol n-butyl ether from Arco Chemicals) and 12.73 grams of Exxate 900 (oxononyl acetate from Exxon). The thickener premix is then added under agitation. Flash X-150 flash rust inhibitor in an amount of 2.6 grams is then added, followed by 1.48 grams of Surfynol 104BC defoamer (Air Products) and 1.48 grams of Byk 307 (wetting agent from BYK-Chemie). Dispersant F9 is then added in an amount of 2.76 grams. The paint is mixed until it is homogeneous and then reduced with 45.5 grams of water to the desired application viscosity. 
     Examples 1-88 were prepared substantially in accordance with the procedure of Example G. The following criteria were used to evaluate the quality of the coatings 1-88. For evaluation of the coatings for ambient cure chemical coating applications, each coating was applied to Bonderite 100 substrates. Adhesion was evaluated by applying the coatings to treated aluminum, Lexan, ABS, Noryl and Styron substrates. QUV evaluations were conducted on coatings applied to aluminum substrates. Table 7 shows the results of the evaluations of the coatings for ambient cure chemical coating applications. These coatings were compared to commercially available polyurethane coatings, Polane® 700T, a one-component waterborne polyurethane and Polane®HS Plus, a two-component solvent borne polyurethane. 
     For the evaluation of the coatings for industrial maintenance applications, the coatings were applied to cold rolled steel substrates. Adhesion was evaluated by applying the coatings to weathered aluminum and weathered galvanized steel substrates. Corrosion, humidity, salt spray and 24 hour water soak were evaluated by applying the coatings on biased steel panels. QUV evaluations were conducted on coatings applied to aluminum substrates. Table 8 shows the results of the evaluations of the coatings for industrial maintenance applications. These coatings were compared to commercially available coatings, Polylon® 1900, a two-component solvent borne polyurethane coating, Centurion™, a two-component waterborne polyurethane coating, and Sher-cryl™, an acrylic enamal coating. 
     For the evauation of the coatings for oven bake applications, the coatings were applied to Bonderite 1000 substrates. Adhesion was evaluated by applying the coatings to weathered aluminum and weathered galvanized steel substrates. QUV evaluations were conducted on coatings applied to aluminum substrates. Table 9 shows the results of the evaluations of the coatings for oven bake applications. These coatings were compared to commercially available coatings Kem Aqua® 1700T and Kem Aqua® 1400, both water reducible enamel coatings. 
     
       
         
               
               
               
             
               
             
               
               
               
             
               
             
               
               
               
             
           
               
                   
               
               
                 Property 
                 Test Method 
                 Measurement 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                 AMBIENT CURE 
               
             
          
           
               
                 Chemical Resistance 
                 ASTM D3912-80 24 hr. 
                 rating 
               
               
                   
                 exposure 
                 1. Total Failure 
               
               
                   
                 Key Chemicals: 
                 2. severe Failure 
               
               
                   
                 1. Formula 409 
                 3. slight failure 
               
               
                   
                 2. isopropanol 
                 4. minimal failure 
               
               
                   
                 3. MEK 
                 5. no effect 
               
               
                   
                 4. Toluene 
               
               
                   
                 5. 10% NaOH 
               
               
                   
                 6. 10% sulfuric acid 
               
               
                   
                 7. Deep Woods Off 
               
               
                   
                 Spray 
               
               
                   
                 8. Coppertone 30 
               
               
                 Pencil Hardness 
                 ASTM D3363 
                 Use film breakthrough 
               
               
                 Salt Spray 
                 ASTM B117 
                 200 hours 
               
               
                 MEK Rubs 
                   
                 Until substrate shows 
               
               
                 Gloss 
                   
                 60°, 20° 
               
               
                 Reverse Impact Test 
                 ASTM D2794 
                 Until film breakage 
               
               
                 Impact Resistance 
                 ASTM D2794 
                 Until film breakage 
               
               
                 QUV 
                 ASTM D4587-91 
                 1000 hours 
               
               
                   
                 Method B 
               
               
                 Storage Stability 
                 4 weeks at 120° F. 
                 4 weeks, check viscosity 
               
               
                   
                   
                 and settling 
               
               
                 Adhesion 
                 ASTM D3359 
                 Tape adhesion 
               
               
                   
                 Key substrates: 
               
               
                   
                 1. Treated Aluminum 
               
               
                   
                 2. Lexan 
               
               
                   
                 3. ABS 
               
               
                   
                 4. Noryl 
               
               
                   
                 5. Styron 
               
               
                 48 hr. Water 
                   
                 Blister, Rust, Tape 
               
               
                 Immersion 
                   
                 adhesion 
               
             
          
           
               
                 OVEN BAKE 
               
             
          
           
               
                 Chemical Resistance 
                 ASTM D3912-80 24 hr. 
                 rating 
               
               
                   
                 exposure 
                 1. Total Failure 
               
               
                   
                   
                 2. severe Failure 
               
               
                   
                   
                 3. slight failure 
               
               
                   
                   
                 4. minimal failure 
               
               
                   
                   
                 5. no effect 
               
               
                 QUV 
                 ASTM D4587-91 
                 1000 hours 
               
               
                   
                 Method B 
               
               
                 Pencil Hardness 
                 ASTM D3363 
                 Use film breakthrough 
               
               
                 Gloss 
                   
                 60°, 20° 
               
               
                 Corrosion- 
                 ASTM D5894-96 
                 6 cycles 
               
               
                 Weathering 
               
               
                 Salt Spray 
                 ASTM B117 
                 500 hrs. 
               
               
                 Reverse Impact Test 
                 ASTM D2794 
                 Until film breakage 
               
               
                 Impact Resistance 
                 ASTM D2794 
                 Until film breakage 
               
               
                 Storage Stability 
                 for 4 weeks at 140° F. 
                 Check Viscosity and 
               
               
                   
                   
                 Settling 
               
               
                 Early Blister 
                 2, 4, and 6 hrs after 
                 Blister and Rust 
               
               
                 Resistance 
                 application 
               
               
                 Adhesion 
                 ASTM D3359 
                 Tape Adhesion 
               
               
                   
                 Key Substrates: 
               
               
                   
                 1. Weathered Aluminum 
               
               
                   
                 2. Weathered Hotdipped 
               
               
                   
                 Galvanized 
               
               
                   
               
             
          
         
       
     
     
       
         
               
             
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
             
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
             
           
               
                 TABLE 7 
               
               
                   
               
               
                 AMBIENT CURE 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                   
                 Chemical Resistance 
               
             
          
           
               
                   
                   
                   
                 Dispersant 
                   
                 Film 
                 20 
                 60 
                   
                   
                   
                   
                   
                   
                 10% 
                   
               
               
                 Formula 
                 Resin 
                 Dispersant 
                 amount 
                 Thickener 
                 build 
                 gloss 
                 gloss 
                 Coppertone 
                 Toluene 
                 IPA 
                 MEK 
                 DWO 
                 10% Sulf 
                 NaOH 
                 F409 
               
               
                   
               
               
                 001 
                 3 
                 2 
                 1 
                 3 
                 1.76 
                 5.9 
                 29.4 
                 1 
                 3 
                 3 
                 3 
                 2 
                 5 
                 3 
                 5 
               
               
                 002 
                 3 
                 8 
                 1 
                 5 
                 1.95 
                 23.5 
                 58.6 
                 3 
                 3 
                 2 
                 2 
                 2 
                 3 
                 3 
                 5 
               
               
                 003 
                 3 
                 7 
                 1 
                 5 
                 2.01 
                 30.3 
                 64.6 
                 5 
                 3 
                 3 
                 5 
                 2.5 
                 4 
                 3 
                 5 
               
               
                 004 
                 3 
                 2 
                 1 
                 6 
                 2.24 
                 4.3 
                 24.8 
                 4 
                 3 
                 3 
                 3 
                 2.5 
                 5 
                 3 
                 5 
               
               
                 005 
                 3 
                 11 
                 1 
                 7 
                 1.95 
                 26.4 
                 61.9 
                 5 
                 2 
                 2 
                 2 
                 2 
                 4 
                 2 
                 5 
               
               
                 006 
                 3 
                 3 
                 1 
                 7 
                 1.71 
                 16.5 
                 51.3 
                 5 
                 2 
                 3 
                 3 
                 2 
                 4.5 
                 3 
                 5 
               
               
                 007 
                 4 
                 1 
                 2 
                 7 
                 2.03 
                 34.3 
                 67.8 
                 5 
                 4 
                 5 
                 5 
                 3.75 
                 5 
                 4 
                 5 
               
               
                 008 
                 4 
                 5 
                 2 
                 5 
                 1.77 
                 33.4 
                 67.9 
                 4.5 
                 3 
                 5 
                 5 
                 3.5 
                 5 
                 4 
                 5 
               
               
                 009 
                 4 
                 3 
                 2 
                 3 
                 1.82 
                 31.5 
                 65.0 
                 5 
                 3 
                 4 
                 4 
                 3.75 
                 5 
                 3 
                 3.5 
               
               
                 010 
                 4 
                 10 
                 2 
                 2 
                 2.04 
                 13.3 
                 48.0 
                 5 
                 3 
                 5 
                 3 
                 2.5 
                 5 
                 4 
                 4 
               
               
                 011 
                 4 
                 10 
                 2 
                 2 
                 1.78 
                 7.1 
                 35.5 
                 4 
                 3.5 
                 5 
                 4 
                 3.5 
                 5 
                 4 
                 5 
               
               
                 012 
                 4 
                 3 
                 2 
                 7 
                 1.74 
                 20.8 
                 56.6 
                 4 
                 3 
                 4.5 
                 3 
                 2 
                 5 
                 4 
                 5 
               
               
                 013 
                 4 
                 8 
                 2 
                 7 
                 1.89 
                 11.7 
                 43.0 
                 4 
                 3 
                 5 
                 3 
                 2 
                 5 
                 4 
                 5 
               
               
                 014 
                 4 
                 11 
                 2 
                 8 
                 2.01 
                 28.1 
                 64.5 
                 4 
                 3.5 
                 4 
                 3.5 
                 2 
                 5 
                 3 
                 5 
               
               
                 015 
                 4 
                 1 
                 1 
                 2 
                 1.8 
                 30.7 
                 64.8 
                 4.5 
                 3.5 
                 5 
                 3 
                 2 
                 5 
                 3.5 
                 4 
               
               
                 016 
                 4 
                 5 
                 1 
                 3 
                 1.56 
                 37.9 
                 68.7 
                 5 
                 3 
                 5 
                 3 
                 2 
                 4 
                 3 
                 5 
               
               
                 017 
                 4 
                 1 
                 1 
                 8 
                 1.84 
                 21.4 
                 57.8 
                 4.5 
                 3.5 
                 5 
                 3.5 
                 2 
                 5 
                 3 
                 5 
               
               
                 018 
                 4 
                 2 
                 1 
                 4 
                 1.69 
                 33.5 
                 66.9 
                 4.5 
                 3 
                 5 
                 5 
                 2 
                 5 
                 3 
                 5 
               
               
                 019 
                 4 
                 7 
                 1 
                 1 
                 1.73 
                 13.4 
                 46.3 
                 5 
                 3 
                 4 
                 3.5 
                 2 
                 5 
                 4.5 
                 5 
               
               
                 020 
                 4 
                 11 
                 1 
                 4 
                 1.76 
                 31.4 
                 66.0 
                 4 
                 3 
                 3 
                 3 
                 2 
                 1 
                 3.5 
                 5 
               
               
                 021 
                 4 
                 3 
                 1 
                 6 
                 1.8 
                 33.1 
                 67.4 
                 5 
                 3 
                 4 
                 4 
                 2 
                 5 
                 3.5 
                 5 
               
               
                 022 
                 4 
                 11 
                 1 
                 2 
                 1.78 
                 30.0 
                 65.2 
                 5 
                 3 
                 5 
                 5 
                 2 
                 5 
                 4 
                 5 
               
               
                 023 
                 4 
                 3 
                 1 
                 7 
                 2.06 
                 39.1 
                 69.1 
                 5 
                 3.5 
                 5 
                 3 
                 2 
                 4 
                 5 
                 5 
               
               
                 031 
                 2 
                 2 
                 2 
                 1 
                 1.98 
                 22.4 
                 56.7 
                 5 
                 2 
                 3 
                 2 
                 2 
                 4 
                 3 
                 4 
               
               
                 032 
                 2 
                 3 
                 2 
                 6 
                 1.82 
                 37.4 
                 67.9 
                 4.5 
                 2 
                 3 
                 2 
                 2 
                 4 
                 2 
                 3 
               
               
                 033 
                 2 
                 4 
                 2 
                 8 
                 1.99 
                 13.0 
                 44.8 
                 4.5 
                 2 
                 2.5 
                 2 
                 2 
                 3 
                 2 
                 5 
               
               
                 034 
                 2 
                 1 
                 1 
                 7 
                 1.88 
                 25.2 
                 59.9 
                 5 
                 2 
                 3 
                 2 
                 2 
                 4.5 
                 2 
                 4.5 
               
               
                 035 
                 2 
                 1 
                 1 
                 5 
                 1.91 
                 15.6 
                 48.9 
                 4 
                 2 
                 3 
                 2 
                 2 
                 5 
                 2.5 
                 4.5 
               
               
                 036 
                 2 
                 3 
                 1 
                 4 
                 2.09 
                 16.1 
                 50.2 
                 4 
                 2 
                 3 
                 2 
                 2 
                 4 
                 2.5 
                 5 
               
               
                 037 
                 2 
                 8 
                 1 
                 4 
                 2.06 
                 15.4 
                 48.5 
                 4 
                 1 
                 3 
                 1 
                 2 
                 4.5 
                 2 
                 4 
               
               
                 038 
                 2 
                 11 
                 1 
                 2 
                 1.98 
                 34.5 
                 67.1 
                 4 
                 2 
                 2 
                 2 
                 2 
                 5 
                 2 
                 3 
               
               
                 039 
                 2 
                 2 
                 1 
                 8 
                 1.85 
                 24.2 
                 58.7 
                 4 
                 2 
                 3 
                 2 
                 2 
                 3 
                 2 
                 4.5 
               
               
                 040 
                 2 
                 7 
                 1 
                 8 
                 1.72 
                 27.2 
                 62.3 
                 4.5 
                 2 
                 2 
                 2 
                 2 
                 5 
                 2 
                 4 
               
               
                 041 
                 2 
                 7 
                 1 
                 6 
                 2.16 
                 23.6 
                 58.7 
                 4 
                 2 
                 3 
                 2 
                 2 
                 5 
                 2 
                 4.5 
               
               
                 042 
                 3 
                 1 
                 2 
                 4 
                 1.78 
                 23.5 
                 59.2 
                 4 
                 2 
                 2 
                 2 
                 2 
                 2 
                 2 
                 4 
               
               
                 043 
                 3 
                 1 
                 2 
                 1 
                 1.52 
                 19.6 
                 54.2 
                 4 
                 2 
                 3 
                 2 
                 2 
                 5 
                 2 
                 5 
               
               
                 044 
                 3 
                 1 
                 2 
                 7 
                 1.72 
                 9.1 
                 38.4 
                 4 
                 2 
                 2 
                 2 
                 2 
                 4 
                 3 
                 4.5 
               
               
                 045 
                 3 
                 5 
                 2 
                 8 
                 1.50 
                 26.3 
                 62.0 
                 4 
                 2 
                 2 
                 2 
                 2 
                 3 
                 2 
                 4.5 
               
               
                 046 
                 3 
                 8 
                 2 
                 3 
                 1.45 
                 7.2 
                 32.5 
                 4.5 
                 2 
                 3 
                 2 
                 2 
                 5 
                 2 
                 5 
               
               
                 047 
                 3 
                 7 
                 2 
                 1 
                 1.74 
                 28.0 
                 62.5 
                 4 
                 2 
                 3 
                 2 
                 2 
                 5 
                 2 
                 4 
               
               
                 048 
                 3 
                 11 
                 2 
                 3 
                 1.70 
                 25.6 
                 61.0 
                 4 
                 2 
                 3 
                 3 
                 2 
                 4 
                 2 
                 5 
               
               
                 049 
                 3 
                 8 
                 2 
                 6 
                 1.64 
                 26.8 
                 63.6 
                 4.5 
                 2 
                 3 
                 2 
                 2 
                 3 
                 2 
                 5 
               
               
                 050 
                 3 
                 3 
                 2 
                 5 
                 1.75 
                 15.5 
                 49.9 
                 4 
                 2 
                 2 
                 2 
                 2 
                 5 
                 2 
                 5 
               
               
                 051 
                 3 
                 5 
                 1 
                 4 
                 2.30 
                 29.1 
                 63.6 
                 4 
                 2 
                 5 
                 2 
                 2 
                 5 
                 2 
                 5 
               
               
                 052 
                 3 
                 9 
                 1 
                 1 
                 2.18 
                 25.2 
                 59.4 
                 5 
                 2 
                 2.5 
                 2 
                 2 
                 4 
                 2 
                 5 
               
               
                 053 
                 3 
                 9 
                 1 
                 2 
                 2.34 
                 22.6 
                 57.9 
                 4 
                 2 
                 3 
                 2 
                 2 
                 5 
                 3 
                 5 
               
               
                 054 
                 2 
                 8 
                 1 
                 4 
                 3.53 
                 15.0 
                 48.9 
                 5 
                 3 
                 3 
                 2 
                 2.5 
                 5 
                 3 
                 5 
               
               
                 055 
                 3 
                 8 
                 2 
                 4 
                 1.77 
                 8.6 
                 35.8 
                 4 
                 3 
                 3 
                 3 
                 1 
                 5 
                 5 
                 5 
               
               
                 067 
                 1 
                 5 
                 2 
                 3 
                 1.64 
                 27.7 
                 65.0 
                 5 
                 5 
                 5 
                 5 
                 2.5 
                 3 
                 2 
                 5 
               
               
                 068 
                 1 
                 1 
                 2 
                 6 
                 1.60 
                 36.5 
                 70.8 
                 3 
                 3 
                 4 
                 4 
                 2.5 
                 2 
                 2 
                 4 
               
               
                 069 
                 1 
                 8 
                 2 
                 2 
                 1.61 
                 37.8 
                 71.3 
                 4 
                 4 
                 5 
                 3 
                 3.5 
                 3 
                 2 
                 5 
               
               
                 070 
                 1 
                 3 
                 2 
                 2 
                 1.68 
                 34.7 
                 69.8 
                 4.5 
                 3.5 
                 5 
                 3.5 
                 3 
                 2 
                 2 
                 5 
               
               
                 071 
                 1 
                 3 
                 2 
                 2 
                 1.64 
                 32.2 
                 87.5 
                 4 
                 4 
                 5 
                 3 
                 2 
                 3 
                 2 
                 3 
               
               
                 072 
                 1 
                 11 
                 2 
                 5 
                 1.48 
                 36.4 
                 69.8 
                 4.5 
                 5 
                 5 
                 5 
                 2.5 
                 3 
                 2 
                 5 
               
               
                 073 
                 1 
                 7 
                 2 
                 6 
                 1.58 
                 32.7 
                 69.3 
                 5 
                 4 
                 5 
                 5 
                 2 
                 3 
                 2 
                 5 
               
               
                 074 
                 1 
                 2 
                 2 
                 5 
                 1.76 
                 33.0 
                 67.8 
                 4.5 
                 4 
                 5 
                 3 
                 2 
                 2 
                 3 
                 4 
               
               
                 075 
                 1 
                 5 
                 1 
                 2 
                 2.10 
                 30.6 
                 67.1 
                 5 
                 3 
                 5 
                 5 
                 2 
                 3 
                 2 
                 5 
               
               
                 076 
                 1 
                 6 
                 1 
                 1 
                 2.03 
                 21.9 
                 59.2 
                 5 
                 3 
                 5 
                 3 
                 2 
                 3 
                 2 
                 4.5 
               
               
                 077 
                 1 
                 9 
                 1 
                 5 
                 2.00 
                 30.8 
                 66.5 
                 4.5 
                 3.5 
                 4 
                 3 
                 2 
                 3 
                 2 
                 4.5 
               
               
                 078 
                 1 
                 9 
                 1 
                 4 
                 1.62 
                 28.0 
                 65.8 
                 4.5 
                 3 
                 4.5 
                 3 
                 2 
                 3 
                 2 
                 5 
               
               
                 079 
                 1 
                 2 
                 1 
                 1 
                 1.89 
                 28.4 
                 62.9 
                 4 
                 3.5 
                 4 
                 4 
                 2 
                 3 
                 2 
                 5 
               
               
                 080 
                 1 
                 3 
                 1 
                 8 
                 1.93 
                 32.4 
                 67.7 
                 5 
                 3.5 
                 3 
                 3 
                 2 
                 3 
                 1 
                 5 
               
               
                 081 
                 1 
                 7 
                 1 
                 3 
                 1.88 
                 32.4 
                 67.0 
                 4 
                 3.5 
                 4.5 
                 3 
                 2 
                 4 
                 2 
                 5 
               
               
                 082 
                 1 
                 10 
                 1 
                 1 
                 1.82 
                 27.8 
                 62.5 
                 4.5 
                 2 
                 5 
                 2 
                 2.5 
                 4 
                 2 
                 5 
               
               
                 083 
                 1 
                 9 
                 1 
                 5 
                 1.56 
                 34.6 
                 68.8 
                 4.5 
                 3 
                 4 
                 3 
                 2.5 
                 3 
                 2 
                 3 
               
               
                 084 
                 1 
                 3 
                 1 
                 6 
                 2.06 
                 35.4 
                 69.0 
                 5 
                 3 
                 4.5 
                 3 
                 2 
                 3 
                 2 
                 5 
               
               
                 085 
                 2 
                 1 
                 2 
                 3 
                 1.70 
                 30.9 
                 64.6 
                 5 
                 2 
                 3 
                 2 
                 2.5 
                 3.5 
                 2 
                 4 
               
               
                 086 
                 2 
                 5 
                 2 
                 7 
                 1.38 
                 24.0 
                 60.2 
                 5 
                 2 
                 2 
                 2 
                 2 
                 5 
                 2 
                 2 
               
               
                 087 
                 2 
                 5 
                 2 
                 7 
                 1.67 
                 33.8 
                 66.5 
                 4 
                 2 
                 3 
                 2 
                 2 
                 5 
                 2 
                 3 
               
               
                 088 
                 2 
                 8 
                 2 
                 4 
                 1.90 
                 17.8 
                 53.6 
                 4 
                 2 
                 3 
                 2 
                 2 
                 4 
                 2 
                 3 
               
               
                 700T 
                   
                   
                   
                   
                 2.08 
                 2.5 
                 29.5 
                 2.5 
                 2 
                 3 
                 4.5 
                 1 
                 3.5 
                 2.5 
                 2 
               
               
                 HS+ 
                   
                   
                   
                   
                 1.96 
                 89.8 
                 90.1 
                 4 
                 5 
                 5 
                 5 
                 4 
                 5 
                 5 
                 5 
               
               
                   
               
             
          
           
               
                   
                 Humidity 200 hours 
                 Salt Spray-100 Hours 
                 Salt Spray-200 hours 
               
             
          
           
               
                   
                 Pencil 
                 Blister 
                 Blister 
                   
                 Flash rust- 
                   
                 % change 
                 Blister 
                 Blister 
                   
                   
                 Blister 
                 Blister 
                   
                   
               
               
                 Formula 
                 Hardness 
                 size 
                 density 
                 Rust 
                 Y or N 
                 Gloss 
                 gloss 
                 size 
                 density 
                 Rust 
                 Scribe 
                 size 
                 density 
                 Rust 
                 Scribe 
               
               
                   
               
               
                 001 
                 4 
                 8 
                 4 
                 8 
                 no 
                 23.8 
                 −19.05% 
                 2 
                 2 
                 6 
                 9 
                 2 
                 2 
                 6 
                 9 
               
               
                 002 
                 4 
                 8 
                 3 
                 6 
                 yes 
                 46.2 
                 −21.16% 
                 2 
                 1 
                 5 
                 9 
                 2 
                 1 
                 5 
                 9 
               
               
                 003 
                 5 
                 8 
                 2 
                 4 
                 yes 
                 42.7 
                 −33.90% 
                 2 
                 2 
                 5 
                 9 
                 2 
                 2 
                 5 
                 9 
               
               
                 004 
                 4 
                 8 
                 4 
                 10  
                 no 
                 24.4 
                  −1.61% 
                 2 
                 2 
                 7 
                 9 
                 2 
                 2 
                 7 
                 9 
               
               
                 005 
                 4 
                 8 
                 4 
                 7 
                 no 
                 54.4 
                 −12.12% 
                 2 
                 2 
                 5 
                 9 
                 2 
                 2 
                 5 
                 9 
               
               
                 006 
                 3 
                 6 
                 4 
                 7 
                 no 
                 42.3 
                 −17.54% 
                 2 
                 2 
                 6 
                 9 
                 2 
                 2 
                 6 
                 9 
               
               
                 007 
                 4 
                 8 
                 1 
                 5 
                 yes 
                 16 
                 −78.40% 
                 2 
                 2 
                 7 
                 9 
                 2 
                 2 
                 7 
                 9 
               
               
                 008 
                 6 
                 4 
                 1 
                 6 
                 yes 
                 16.8 
                 −75.26% 
                 2 
                 3 
                 8 
                 5 
                 2 
                 3 
                 8 
                 5 
               
               
                 009 
                 5 
                 6 
                 1 
                 6 
                 yes 
                 15.4 
                 −76.31% 
                 2 
                 3 
                 7 
                 6 
               
               
                 010 
                 5 
                 8 
                 1 
                 6 
                 yes 
                 16.7 
                 −85.21% 
                 2 
                 3 
                 8 
                 9 
                 2 
                 3 
                 8 
                 9 
               
               
                 011 
                 5 
                 8 
                 1 
                 6 
                 yes 
                 11.7 
                 −67.04% 
                 2 
                 4 
                 9 
                 4 
                 2 
                 4 
                 9 
                 4 
               
               
                 012 
                 5 
                 6 
                 1 
                 8 
                 yes 
                 15.2 
                 −73.14% 
                 2 
                 3 
                 7 
                 6 
                 2 
                 3 
                 7 
                 6 
               
               
                 013 
                 4 
                 8 
                 1 
                 7 
                 yes 
                 21.3 
                 −50.47% 
                 2 
                 4 
                 9 
                 6 
                 2 
                 4 
                 9 
                 6 
               
               
                 014 
                 5 
                 6 
                 1 
                 7 
                 yes 
                 16.1 
                 −75.04% 
                 2 
                 3 
                 8 
                 6 
                 2 
                 2 
                 8 
                 6 
               
               
                 015 
                 4 
                 6 
                 1 
                 8 
                 yes 
                 17.8 
                 −72.53% 
                 2 
                 3 
                 8 
                 7 
                 2 
                 3 
                 8 
                 7 
               
               
                 016 
                 5 
                 4 
                 2 
                 7 
                 yes 
                 18.9 
                 −72.49% 
                 4 
                 3 
                 7 
                 6 
                 4 
                 3 
                 7 
                 6 
               
               
                 017 
                 6 
                 8 
                 1 
                 6 
                 yes 
                 29.4 
                 −49.13% 
                 4 
                 3 
                 8 
                 6 
                 4 
                 3 
                 8 
                 6 
               
               
                 018 
                 4 
                 8 
                 1 
                 8 
                 yes 
                 27 
                 −59.64% 
                 4 
                 4 
                 9 
                 7 
                 4 
                 4 
                 9 
                 7 
               
               
                 019 
                 4 
                 8 
                 1 
                 7 
                 yes 
                 17.5 
                 −62.20% 
                 4 
                 3 
                 7 
                 6 
                 4 
                 3 
                 7 
                 6 
               
               
                 020 
                 5 
                 6 
                 1 
                 8 
                 yes 
                 16 
                 −75.78% 
                 4 
                 3 
                 7 
                 7 
                 4 
                 3 
                 7 
                 7 
               
               
                 021 
                 4 
                 6 
                 1 
                 8 
                 yes 
                 19.1 
                 −71.66% 
                 4 
                 3 
                 7 
                 6 
                 4 
                 3 
                 7 
                 6 
               
               
                 022 
                 4 
                 6 
                 1 
                 9 
                 yes 
                 17.3 
                 −73.47% 
                 4 
                 4 
                 9 
                 6 
                 4 
                 4 
                 9 
                 6 
               
               
                 023 
                 4 
                 4 
                 4 
                 9 
                 yes 
                 23.2 
                 −66.43% 
                 2 
                 3 
                 9 
                 7 
                 2 
                 3 
                 9 
                 7 
               
               
                 031 
                 4 
                 8 
                 2 
                 5 
                 yes 
                 42.4 
                 −25.22% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 032 
                 4 
                 8 
                 2 
                 6 
                 yes 
                 61.5 
                  −9.43% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 8 
                 9 
               
               
                 033 
                 5 
                 8 
                 3 
                 5 
                 yes 
                 38 
                 −15.18% 
                 2 
                 1 
                 7 
                 9 
                 2 
                 1 
                 7 
                 9 
               
               
                 034 
                 4 
                 6 
                 4 
                 9 
                 yes 
                 49.9 
                 −16.69% 
                 2 
                 1 
                 7 
                 9 
                 2 
                 1 
                 7 
                 9 
               
               
                 035 
                 4 
                 8 
                 4 
                 5 
                 yes 
                 43.5 
                 −11.04% 
                 2 
                 1 
                 5 
                 9 
                 2 
                 1 
                 5 
                 9 
               
               
                 036 
                 5 
                 8 
                 3 
                 6 
                 yes 
                 42.6 
                 −15.14% 
                 2 
                 1 
                 5 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 037 
                 4 
                 8 
                 3 
                 6 
                 yes 
                 38.4 
                 −20.82% 
                 2 
                 1 
                 4 
                 9 
                 2 
                 1 
                 4 
                 9 
               
               
                 038 
                 4 
                 6 
                 2 
                 7 
                 no 
                 49.6 
                 −26.08% 
                 2 
                 2 
                 6 
                 9 
                 2 
                 2 
                 6 
                 9 
               
               
                 039 
                 4 
                 8 
                 2 
                 8 
                 no 
                 39.5 
                 −32.71% 
                 2 
                 2 
                 8 
                 9 
                 2 
                 2 
                 8 
                 9 
               
               
                 040 
                 5 
                 8 
                 3 
                 5 
                 yes 
                 49 
                 −21.35% 
                 2 
                 2 
                 7 
                 9 
                 2 
                 2 
                 7 
                 9 
               
               
                 041 
                 4 
                 8 
                 3 
                 7 
                 yes 
                 47.3 
                 −19.42% 
                 2 
                 1 
                 7 
                 9 
                 2 
                 2 
                 7 
                 9 
               
               
                 042 
                 4 
                 8 
                 4 
                 9 
                 yes 
                 51.4 
                 −13.18% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 043 
                 4 
                 8 
                 4 
                 8 
                 no 
                 46.2 
                 −14.76% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 044 
                 5 
                 8 
                 4 
                 9 
                 no 
                 35.2 
                  −8.33% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 045 
                 4 
                 8 
                 4 
                 7 
                 yes 
                 45.6 
                 −26.45% 
                 2 
                 1 
                 6 
                 7 
                 2 
                 1 
                 6 
                 7 
               
               
                 046 
                 2 
                 8 
                 3 
                 7 
                 no 
                 25.7 
                 −20.92% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 047 
                 5 
                 8 
                 2 
                 9 
                 no 
                 43.7 
                 #REFI 
                 4 
                 2 
                 6 
                 9 
                 4 
                 2 
                 6 
                 9 
               
               
                 048 
                 5 
                 8 
                 4 
                 8 
                 yes 
                 40.1 
                 −35.84% 
                 4 
                 1 
                 6 
                 9 
                 4 
                 1 
                 6 
                 9 
               
               
                 049 
                 4 
                 8 
                 4 
                 9 
                 yes 
                 48.4 
                 −20.66% 
                 4 
                 2 
                 6 
                 9 
                 4 
                 2 
                 6 
                 9 
               
               
                 050 
                 5 
                 8 
                 4 
                 9 
                 no 
                 39.5 
                 −20.84% 
                 2 
                 2 
                 6 
                 9 
                 2 
                 2 
                 6 
                 9 
               
               
                 051 
                 4 
                 8 
                 3 
                 9 
                 yes 
                 44.4 
                 −30.19% 
                 2 
                 2 
                 8 
                 9 
                 2 
                 2 
                 8 
                 9 
               
               
                 052 
                 4 
                 8 
                 3 
                 9 
                 yes 
                 44.8 
                 −24.58% 
                 2 
                 2 
                 6 
                 7 
                 2 
                 2 
                 6 
                 7 
               
               
                 053 
                 4 
                 8 
                 4 
                 8 
                 yes 
                 51.1 
                 −11.74% 
                 4 
                 3 
                 1 
                 9 
                 4 
                 3 
                 8 
                 9 
               
               
                 054 
                 4 
                 8 
                 4 
                 7 
                 yes 
                 41.1 
                 −15.95% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 055 
                 4 
                 8 
                 4 
                 6 
                 no 
                 31.3 
                 −12.57% 
                 4 
                 1 
                 2 
                 9 
                 4 
                 1 
                 2 
                 9 
               
               
                 067 
                 2 
                 8 
                 2 
                 5 
                 yes 
                 27.8 
                 −57.23% 
                 6 
                 1 
                 2 
                 9 
                 6 
                 1 
                 2 
                 9 
               
               
                 068 
                 3 
                 8 
                 3 
                 5 
                 yes 
                 29.7 
                 −58.05% 
                 4 
                 2 
                 2 
                 9 
                 4 
                 2 
                 2 
                 9 
               
               
                 069 
                 2 
                 8 
                 4 
                 6 
                 yes 
                 22.1 
                 −69.00% 
                 6 
                 1 
                 2 
                 9 
                 6 
                 1 
                 2 
                 9 
               
               
                 070 
                 2 
                 8 
                 3 
                 4 
                 yes 
                 26.6 
                 −61.60% 
                 4 
                 2 
                 3 
                 9 
                 4 
                 2 
                 3 
                 9 
               
               
                 071 
                 4 
                 8 
                 3 
                 4 
                 yes 
                 28.3 
                 −58.07% 
                 4 
                 1 
                 3 
                 9 
                 4 
                 1 
                 3 
                 9 
               
               
                 072 
                 4 
                 8 
                 3 
                 4 
                 yes 
                 30 
                 −57.02% 
                 6 
                 1 
                 8 
                 9 
                 6 
                 1 
                 8 
                 9 
               
               
                 073 
                 4 
                 8 
                 2 
                 5 
                 yes 
                 29.4 
                 −57.58% 
                 4 
                 2 
                 7 
                 9 
                 4 
                 2 
                 7 
                 9 
               
               
                 074 
                 4 
                 8 
                 3 
                 7 
                 no 
                 33.8 
                 −50.15% 
                 4 
                 2 
                 7 
                 9 
                 4 
                 2 
                 7 
                 9 
               
               
                 075 
                 4 
                 8 
                 2 
                 6 
                 yes 
                 25 
                 −62.74% 
                 4 
                 1 
                 6 
                 9 
                 4 
                 1 
                 6 
                 9 
               
               
                 076 
                 2 
                 8 
                 2 
                 6 
                 yes 
                 27.5 
                 −53.55% 
                 4 
                 2 
                 6 
                 9 
                 4 
                 2 
                 6 
                 9 
               
               
                 077 
                 2 
                 8 
                 3 
                 8 
                 yes 
                 28.4 
                 −57.29% 
                 4 
                 2 
                 7 
                 9 
                 4 
                 2 
                 7 
                 9 
               
               
                 078 
                 4 
                 8 
                 3 
                 7 
                 yes 
                 28.3 
                 −56.99% 
                 4 
                 1 
                 8 
                 7 
                 4 
                 1 
                 8 
                 7 
               
               
                 079 
                 4 
                 8 
                 4 
                 7 
                 yes 
                 20.9 
                 −86.77% 
                 6 
                 2 
                 8 
                 8 
                 6 
                 2 
                 8 
                 8 
               
               
                 080 
                 3 
                 8 
                 3 
                 6 
                 yes 
                 18.6 
                 −72.53% 
                 4 
                 2 
                 7 
                 9 
                 4 
                 2 
                 7 
                 9 
               
               
                 081 
                 3 
                 8 
                 4 
                 8 
                 yes 
                 37.1 
                 −44.63% 
                 6 
                 2 
                 8 
                 9 
                 6 
                 2 
                 8 
                 9 
               
               
                 082 
                 4 
                 8 
                 2 
                 8 
                 yes 
                 24.2 
                 −61.28% 
                 2 
                 2 
                 8 
                 7 
                 2 
                 2 
                 8 
                 7 
               
               
                 083 
                 3 
                 8 
                 3 
                 7 
                 yes 
                 25.1 
                 −63.52% 
                 4 
                 1 
                 7 
                 7 
                 4 
                 1 
                 7 
                 7 
               
               
                 084 
                 2 
                 8 
                 3 
                 6 
                 yes 
                 18.8 
                 −75.65% 
                 4 
                 2 
                 7 
                 9 
                 4 
                 2 
                 7 
                 9 
               
               
                 085 
                 4 
                 6 
                 3 
                 5 
                 yes 
                 50.8 
                 −21.36% 
                 2 
                 1 
                 2 
                 9 
                 2 
                 1 
                 2 
                 9 
               
               
                 086 
                 4 
                 6 
                 3 
                 5 
                 yes 
                 47.6 
                 −20.93% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 2 
                 9 
               
               
                 087 
                 3 
                 8 
                 2 
                 7 
                 yes 
                 49.7 
                 −25.26% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 088 
                 3 
                 8 
                 2 
                 5 
                 yes 
                 44 
                 −17.91% 
                 2 
                 1 
                 6 
                 9 
                 2 
                 1 
                 6 
                 9 
               
               
                 700T 
                 6 
                 none 
                 none 
                 none 
                 no 
                 36.6 
                  24.07% 
                 6 
                 3 
                 7 
                 6 
                 6 
                 3 
                 7 
                 6 
               
               
                 HS+ 
                 6 
                 none 
                 none 
                 none 
                 no 
                 68.5 
                 −23.97% 
                 10  
                 5 
                 10  
                 9 
                 10  
                 5 
                 10  
                 9 
               
               
                   
               
             
          
           
               
                   
                 Impact 
                   
                 Adhesion 
                 48 Hr. Water Soak 
               
             
          
           
               
                 Formula 
                 Forward 
                 Reverse 
                 MEK rubs 
                 Treated aluminum 
                 Noryl 
                 ABS 
                 Lexan 
                 Styron 
                 Blister size 
                 Blister density 
                 Rust 
                 Adhesion 
               
               
                   
               
               
                 001 
                 36 
                 4 
                 132 
                 3 
                 0 
                 0 
                 1 
                 0 
                 10 
                 5 
                 10 
                 4 
               
               
                 002 
                 40 
                 4 
                 50 
                 4 
                 0 
                 0 
                 2 
                 1 
                 6 
                 4 
                 10 
                 3 
               
               
                 003 
                 44 
                 8 
                 100 
                 3 
                 −1 
                 0 
                 1 
                 −1 
                 8 
                 3 
                 10 
                 3 
               
               
                 004 
                 40 
                 4 
                 50 
                 3 
                 0 
                 3 
                 3 
                 2 
                 10 
                 5 
                 10 
                 4 
               
               
                 005 
                 40 
                 8 
                 50 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 10 
                 5 
                 10 
                 4 
               
               
                 006 
                 40 
                 8 
                 150 
                 3 
                 −1 
                 1 
                 0 
                 0 
                 10 
                 5 
                 10 
                 4 
               
               
                 007 
                 &gt;168 
                 &gt;168 
                 150 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 4 
                 3 
                 3 
                 0 
               
               
                 008 
                 &gt;168 
                 &gt;168 
                 750 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 6 
                 2 
                 3 
                 1 
               
               
                 009 
                 140 
                 &gt;168 
                 400 
                 4 
                 −1 
                 0 
                 0 
                 −1 
                 6 
                 1 
                 1 
                 0 
               
               
                 010 
                 &gt;168 
                 &gt;168 
                 46 
                 4 
                 −1 
                 0 
                 0 
                 −1 
                 6 
                 4 
                 10 
                 4 
               
               
                 011 
                 &gt;168 
                 &gt;168 
                 49 
                 4 
                 −1 
                 0 
                 0 
                 −1 
                 10 
                 5 
                 10 
                 5 
               
               
                 012 
                 &gt;168 
                 &gt;168 
                 1000 
                 2 
                 0 
                 0 
                 0 
                 0 
                 8 
                 1 
                 4 
                 3 
               
               
                 013 
                 &gt;168 
                 &gt;168 
                 40 
                 5 
                 −1 
                 0 
                 0 
                 −1 
                 10 
                 5 
                 10 
                 4 
               
               
                 014 
                 &gt;168 
                 &gt;168 
                 46 
                 5 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 2 
                 9 
                 4 
               
               
                 015 
                 &gt;168 
                 &gt;168 
                 45 
                 4 
                 −1 
                 −1 
                 0 
                 0 
                 8 
                 1 
                 8 
                 2 
               
               
                 016 
                 &gt;168 
                 &gt;168 
                 50 
                 2 
                 0 
                 0 
                 0 
                 −1 
                 8 
                 1 
                 10 
                 3 
               
               
                 017 
                 &gt;168 
                 &gt;168 
                 187 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 3 
                 10 
                 3 
               
               
                 018 
                 &gt;168 
                 &gt;168 
                 45 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 2 
                 6 
                 3 
               
               
                 019 
                 &gt;168 
                 &gt;168 
                 47 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 2 
                 10 
                 4 
               
               
                 020 
                 &gt;168 
                 &gt;168 
                 500 
                 4 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 1 
                 10 
                 3 
               
               
                 021 
                 &gt;168 
                 &gt;168 
                 750 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 1 
                 10 
                 3 
               
               
                 022 
                 &gt;168 
                 &gt;168 
                 150 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 2 
                 10 
                 3 
               
               
                 023 
                 &gt;168 
                 &gt;168 
                 150 
                 3 
                 −1 
                 2 
                 0 
                 −1 
                 8 
                 1 
                 4 
                 1 
               
               
                 031 
                 36 
                 &lt;4 
                 200 
                 3 
                 −1 
                 0 
                 3 
                 2 
                 8 
                 1 
                 10 
                 1 
               
               
                 032 
                 36 
                 &lt;4 
                 50 
                 3 
                 0 
                 0 
                 2 
                 0 
                 6 
                 2 
                 3 
                 0 
               
               
                 033 
                 32 
                 &lt;4 
                 400 
                 4 
                 0 
                 0 
                 0 
                 3 
                 8 
                 1 
                 3 
                 0 
               
               
                 034 
                 32 
                 &lt;4 
                 29 
                 3 
                 −1 
                 0 
                 1 
                 1 
                 6 
                 2 
                 10 
                 1 
               
               
                 035 
                 36 
                 &lt;4 
                 130 
                 4 
                 −1 
                 3 
                 −1 
                 3 
                 8 
                 1 
                 10 
                 0 
               
               
                 036 
                 32 
                 &lt;4 
                 100 
                 3 
                 −1 
                 0 
                 0 
                 3 
                 6 
                 3 
                 10 
                 1 
               
               
                 037 
                 32 
                 &lt;4 
                 46 
                 4 
                 −1 
                 0 
                 0 
                 0 
                 6 
                 4 
                 10 
                 1 
               
               
                 038 
                 36 
                 8 
                 300 
                 4 
                 −1 
                 −1 
                 0 
                 0 
                 6 
                 2 
                 10 
                 1 
               
               
                 039 
                 40 
                 4 
                 650 
                 3 
                 0 
                 0 
                 0 
                 0 
                 6 
                 3 
                 10 
                 2 
               
               
                 040 
                 32 
                 &lt;4 
                 42 
                 3 
                 −1 
                 0 
                 0 
                 2 
                 8 
                 1 
                 10 
                 1 
               
               
                 041 
                 32 
                 &lt;4 
                 38 
                 4 
                 0 
                 0 
                 2 
                 0 
                 8 
                 1 
                 10 
                 1 
               
               
                 042 
                 56 
                 8 
                 75 
                 4 
                 −1 
                 0 
                 0 
                 0 
                 6 
                 1 
                 10 
                 0 
               
               
                 043 
                 40 
                 4 
                 45 
                 4 
                 −1 
                 0 
                 0 
                 0 
                 10 
                 5 
                 10 
                 2 
               
               
                 044 
                 40 
                 4 
                 150 
                 4 
                 0 
                 0 
                 1 
                 −1 
                 8 
                 4 
                 10 
                 4 
               
               
                 045 
                 40 
                 8 
                 48 
                 4 
                 1 
                 0 
                 0 
                 −1 
                 8 
                 2 
                 10 
                 3 
               
               
                 046 
                 28 
                 &lt;4 
                 50 
                 3 
                 0 
                 0 
                 0 
                 −1 
                 8 
                 1 
                 10 
                 3 
               
               
                 047 
                 40 
                 8 
                 39 
                 3 
                 −1 
                 0 
                 0 
                 −1 
                 8 
                 3 
                 10 
                 3 
               
               
                 048 
                 44 
                 8 
                 146 
                 3 
                 0 
                 0 
                 0 
                 2 
                 8 
                 3 
                 10 
                 3 
               
               
                 049 
                 92 
                 40 
                 100 
                 4 
                 0 
                 0 
                 3 
                 0 
                 8 
                 1 
                 10 
                 0 
               
               
                 050 
                 76 
                 12 
                 300 
                 3 
                 0 
                 0 
                 2 
                 0 
                 8 
                 1 
                 10 
                 2 
               
               
                 051 
                 56 
                 6 
                 48 
                 3 
                 0 
                 0 
                 0 
                 0 
                 6 
                 3 
                 10 
                 3 
               
               
                 052 
                 36 
                 8 
                 42 
                 3 
                 −1 
                 −1 
                 0 
                 −1 
                 6 
                 3 
                 10 
                 3 
               
               
                 053 
                 36 
                 4 
                 200 
                 3 
                 −1 
                 0 
                 0 
                 0 
                 10 
                 5 
                 10 
                 3 
               
               
                 054 
                 44 
                 4 
                 200 
                 3 
                 1 
                 0 
                 2 
                 1 
                 8 
                 2 
                 9 
                 3 
               
               
                 055 
                 36 
                 4 
                 150 
                 3 
                 0 
                 0 
                 3 
                 1 
                 8 
                 2 
                 10 
                 3 
               
               
                 067 
                 56 
                 12 
                 800 
                 3 
                 0 
                 0 
                 0 
                 3 
                 10 
                 5 
                 10 
                 4 
               
               
                 068 
                 64 
                 20 
                 100 
                 3 
                 2 
                 0 
                 0 
                 2 
                 10 
                 5 
                 10 
                 4 
               
               
                 069 
                 84 
                 20 
                 800 
                 3 
                 4 
                 −1 
                 2 
                 3 
                 10 
                 5 
                 10 
                 5 
               
               
                 070 
                 56 
                 12 
                 200 
                 3 
                 2 
                 0 
                 2 
                 2 
                 10 
                 5 
                 10 
                 3 
               
               
                 071 
                 68 
                 16 
                 100 
                 3 
                 5 
                 0 
                 0 
                 4 
                 10 
                 5 
                 10 
                 3 
               
               
                 072 
                 52 
                 8 
                 1000 
                 3 
                 4 
                 0 
                 −1 
                 4 
                 10 
                 5 
                 10 
                 3 
               
               
                 073 
                 60 
                 8 
                 250 
                 3 
                 2 
                 0 
                 0 
                 3 
                 10 
                 5 
                 10 
                 4 
               
               
                 074 
                 64 
                 4 
                 300 
                 3 
                 3 
                 0 
                 0 
                 −1 
                 10 
                 5 
                 10 
                 4 
               
               
                 075 
                 56 
                 8 
                 43 
                 3 
                 0 
                 0 
                 0 
                 −1 
                 10 
                 5 
                 10 
                 4 
               
               
                 076 
                 56 
                 4 
                 50 
                 3 
                 0 
                 0 
                 3 
                 4 
                 10 
                 5 
                 10 
                 4 
               
               
                 077 
                 56 
                 8 
                 700 
                 3 
                 0 
                 0 
                 0 
                 3 
                 10 
                 5 
                 10 
                 3 
               
               
                 078 
                 60 
                 12 
                 100 
                 3 
                 0 
                 0 
                 2 
                 4 
                 10 
                 5 
                 10 
                 3 
               
               
                 079 
                 52 
                 8 
                 100 
                 3 
                 0 
                 0 
                 −1 
                 3 
                 10 
                 5 
                 10 
                 3 
               
               
                 080 
                 56 
                 4 
                 1000 
                 3 
                 3 
                 0 
                 0 
                 3 
                 10 
                 5 
                 10 
                 3 
               
               
                 081 
                 52 
                 8 
                 350 
                 3 
                 0 
                 0 
                 0 
                 2 
                 10 
                 5 
                 10 
                 4 
               
               
                 082 
                 60 
                 8 
                 300 
                 3 
                 4 
                 0 
                 0 
                 4 
                 10 
                 5 
                 10 
                 4 
               
               
                 083 
                 56 
                 4 
                 1000 
                 3 
                 0 
                 0 
                 −1 
                 3 
                 10 
                 5 
                 10 
                 3 
               
               
                 084 
                 60 
                 12 
                 350 
                 3 
                 0 
                 0 
                 0 
                 4 
                 10 
                 5 
                 10 
                 4 
               
               
                 085 
                 36 
                 &lt;4 
                 37 
                 4 
                 0 
                 0 
                 0 
                 0 
                 6 
                 2 
                 3 
                 1 
               
               
                 086 
                 36 
                 &lt;4 
                 250 
                 4 
                 0 
                 0 
                 1 
                 2 
                 6 
                 2 
                 1 
                 1 
               
               
                 087 
                 32 
                 4 
                 246 
                 3 
                 −1 
                 0 
                 0 
                 0 
                 6 
                 1 
                 1 
                 1 
               
               
                 088 
                 32 
                 &lt;4 
                 100 
                 3 
                 0 
                 0 
                 −1 
                 1 
                 4 
                 3 
                 10 
                 0 
               
               
                 700T 
                 &gt;168 
                 &gt;168 
                 150 
                 3 
                 −1 
                 5 
                 5 
                 −1 
                 8 
                 4 
                 10 
                 4 
               
               
                 HS+ 
                 68 
                 8 
                 1000 
                 3 
                 −1 
                 5 
                 5 
                 5 
                 10 
                 5 
                 10 
                 4 
               
               
                   
               
             
          
           
               
                   
                 QUV−500 hours 
                 QUV−1000 hrs. 
               
             
          
           
               
                   
                 Gloss (60 degree) 
                 Delta E 
                 Delta b 
                 Gloss (60 degree) 
                   
                   
               
             
          
           
               
                   
                   
                 at 
                   
                   
                 at 
                   
                   
                 at 
                   
                 1000 
                   
                 Delta E 
                 Delta b 
               
             
          
           
               
                 Formula 
                 Initial 
                 500 hrs 
                 % change 
                 Initial 
                 500 hrs 
                 change 
                 Initial 
                 500 hrs 
                 change 
                 hour 
                 % change 
                 Delta E 
                 change 
                 Delta b 
                 change 
               
               
                   
               
               
                 001 
                 32.60 
                 21.10 
                 −35.28 
                 0.94 
                 3.23 
                 2.29 
                 −0.85 
                 1.55 
                 2.40 
                 17.90 
                 −45.09 
                 2.88 
                 1.94 
                 1.13 
                 1.98 
               
               
                 002 
                 58.50 
                 40.10 
                 −29.03 
                 2.69 
                 5.10 
                 2.41 
                 0.41 
                 2.79 
                 2.38 
                 37.10 
                 −34.34 
                 5.70 
                 3.01 
                 2.95 
                 2.54 
               
               
                 003 
                 65.70 
                 50.70 
                 −22.83 
                 1.81 
                 2.72 
                 0.91 
                 0.79 
                 1.42 
                 0.63 
                 46.20 
                 −26.64 
                 3.02 
                 1.21 
                 1.25 
                 0.46 
               
               
                 004 
                 49.60 
                 29.80 
                 −39.92 
                 1.17 
                 2.66 
                 1.49 
                 −1.00 
                 1.36 
                 2.36 
                 26.50 
                 −46.57 
                 2.66 
                 1.49 
                 0.93 
                 1.93 
               
               
                 005 
                 61.00 
                 47.00 
                 −22.95 
                 2.05 
                 3.44 
                 1.39 
                 −0.36 
                 1.92 
                 2.28 
                 45.60 
                 −25.25 
                 4.04 
                 1.99 
                 1.84 
                 2.20 
               
               
                 006 
                 51.00 
                 35.80 
                 −29.80 
                 1.34 
                 3.16 
                 1.82 
                 −0.46 
                 1.76 
                 2.22 
                 32.80 
                 −35.69 
                 3.62 
                 2.28 
                 1.70 
                 2.16 
               
               
                 007 
                 69.40 
                 33.30 
                 −52.02 
                 1.81 
                 2.49 
                 0.68 
                 0.04 
                 1.43 
                 1.39 
                 21.90 
                 −68.44 
                 4.09 
                 2.28 
                 2.22 
                 2.18 
               
               
                 008 
                 70.30 
                 30.50 
                 −56.61 
                 1.17 
                 1.41 
                 0.24 
                 −0.32 
                 0.83 
                 1.15 
                 21.20 
                 −69.84 
                 2.58 
                 1.41 
                 1.22 
                 1.54 
               
               
                 009 
                 68.30 
                 21.90 
                 −67.94 
                 1.06 
                 1.98 
                 0.92 
                 −0.31 
                 1.06 
                 1.37 
                 15.20 
                 −77.75 
                 2.44 
                 1.38 
                 1.09 
                 1.40 
               
               
                 010 
                 52.00 
                 13.80 
                 −73.48 
                 1.05 
                 3.14 
                 2.09 
                 0.01 
                 1.83 
                 1.82 
                 9.80 
                 −81.15 
                 4.00 
                 2.95 
                 2.07 
                 2.06 
               
               
                 011 
                 40.60 
                 10.40 
                 −74.38 
                 0.26 
                 3.03 
                 2.77 
                 −0.13 
                 1.75 
                 1.88 
                 7.50 
                 −81.53 
                 3.85 
                 3.59 
                 1.97 
                 2.10 
               
               
                 012 
                 59.30 
                 16.50 
                 −72.18 
                 0.73 
                 1.95 
                 1.22 
                 −0.45 
                 0.95 
                 1.40 
                 12.70 
                 −78.58 
                 2.75 
                 2.02 
                 1.17 
                 1.62 
               
               
                 013 
                 46.80 
                 15.00 
                 −67.95 
                 1.31 
                 2.83 
                 1.52 
                 0.05 
                 1.60 
                 1.55 
                 12.30 
                 −73.72 
                 3.40 
                 2.09 
                 1.79 
                 1.74 
               
               
                 014 
                 69.10 
                 19.60 
                 −71.64 
                 1.10 
                 2.45 
                 1.35 
                 −0.32 
                 1.38 
                 1.70 
                 15.90 
                 −76.99 
                 3.01 
                 1.91 
                 1.56 
                 1.88 
               
               
                 015 
                 66.10 
                 18.20 
                 −72.47 
                 1.00 
                 2.01 
                 1.01 
                 −0.29 
                 1.03 
                 1.32 
                 15.50 
                 −76.55 
                 2.29 
                 1.29 
                 1.12 
                 1.41 
               
               
                 016 
                 70.70 
                 19.70 
                 −72.14 
                 1.39 
                 1.88 
                 0.49 
                 −0.44 
                 0.94 
                 1.38 
                 18.10 
                 −74.40 
                 2.36 
                 0.97 
                 1.12 
                 1.56 
               
               
                 017 
                 59.30 
                 14.50 
                 −75.55 
                 0.61 
                 1.80 
                 1.19 
                 −0.46 
                 0.66 
                 1.32 
                 12.30 
                 −79.26 
                 2.40 
                 1.79 
                 0.96 
                 1.42 
               
               
                 018 
                 69.00 
                 19.00 
                 −72.46 
                 0.92 
                 2.01 
                 1.09 
                 −0.26 
                 1.10 
                 1.38 
                 15.90 
                 −76.96 
                 2.58 
                 1.66 
                 1.24 
                 1.50 
               
               
                 019 
                 49.20 
                 12.90 
                 −73.78 
                 0.45 
                 2.25 
                 1.89 
                 −0.30 
                 1.16 
                 1.46 
                 10.40 
                 −78.86 
                 2.54 
                 2.09 
                 1.20 
                 1.50 
               
               
                 020 
                 68.70 
                 21.10 
                 −69.29 
                 1.37 
                 2.09 
                 0.72 
                 −0.29 
                 1.17 
                 1.46 
                 16.40 
                 −76.13 
                 2.72 
                 1.35 
                 1.32 
                 1.61 
               
               
                 021 
                 70.70 
                 22.00 
                 −68.88 
                 1.57 
                 2.34 
                 0.77 
                 −0.10 
                 1.24 
                 1.34 
                 14.90 
                 −78.93 
                 2.87 
                 1.30 
                 1.44 
                 1.54 
               
               
                 022 
                 67.80 
                 21.70 
                 −67.99 
                 1.31 
                 2.79 
                 1.46 
                 0.06 
                 1.63 
                 1.57 
                 16.00 
                 −76.40 
                 3.51 
                 2.20 
                 1.82 
                 1.76 
               
               
                 023 
                 71.80 
                 22.10 
                 −69.22 
                 1.31 
                 1.87 
                 0.56 
                 0.06 
                 0.95 
                 0.89 
                 23.20 
                 −67.69 
                 2.59 
                 1.28 
                 1.22 
                 1.16 
               
               
                 031 
                 57.70 
                 37.50 
                 −35.01 
                 1.65 
                 1.38 
                 0.27 
                 −0.98 
                 0.65 
                 1.63 
                 35.90 
                 −37.78 
                 1.42 
                 0.23 
                 0.60 
                 1.58 
               
               
                 032 
                 68.70 
                 47.10 
                 −31.44 
                 1.61 
                 0.77 
                 0.84 
                 −1.33 
                 0.15 
                 1.48 
                 54.90 
                 −20.09 
                 0.75 
                 0.86 
                 0.02 
                 1.35 
               
               
                 033 
                 47.10 
                 29.00 
                 −38.43 
                 1.38 
                 2.19 
                 0.81 
                 −0.69 
                 1.24 
                 2.13 
                 26.10 
                 −44.59 
                 1.93 
                 0.55 
                 1.06 
                 1.95 
               
               
                 034 
                 60.90 
                 44.40 
                 −27.09 
                 1.88 
                 1.79 
                 0.09 
                 −0.61 
                 0.86 
                 1.47 
                 47.80 
                 −21.51 
                 2.51 
                 0.63 
                 1.24 
                 1.85 
               
               
                 035 
                 52.50 
                 36.00 
                 −31.43 
                 1.42 
                 0.73 
                 0.69 
                 −1.18 
                 0.21 
                 1.39 
                 36.70 
                 −30.10 
                 1.33 
                 0.09 
                 0.41 
                 1.59 
               
               
                 036 
                 53.00 
                 40.00 
                 −24.53 
                 1.29 
                 1.18 
                 0.11 
                 −0.86 
                 0.59 
                 1.45 
                 39.20 
                 −26.04 
                 1.63 
                 0.34 
                 0.82 
                 1.68 
               
               
                 037 
                 51.80 
                 41.70 
                 −19.50 
                 1.78 
                 2.45 
                 0.67 
                 −0.82 
                 1.40 
                 2.22 
                 43.60 
                 −15.83 
                 2.30 
                 0.52 
                 1.08 
                 1.90 
               
               
                 038 
                 66.80 
                 57.30 
                 −14.22 
                 1.40 
                 1.36 
                 0.04 
                 −0.81 
                 0.65 
                 1.46 
                 58.70 
                 −12.13 
                 1.81 
                 0.41 
                 0.90 
                 1.71 
               
               
                 039 
                 60.00 
                 48.30 
                 −19.50 
                 1.86 
                 1.61 
                 0.25 
                 −0.80 
                 0.82 
                 1.62 
                 50.70 
                 −15.50 
                 1.89 
                 0.03 
                 0.92 
                 1.72 
               
               
                 040 
                 63.20 
                 47.60 
                 −24.68 
                 1.49 
                 1.37 
                 0.12 
                 −1.05 
                 0.71 
                 1.76 
                 49.40 
                 −21.84 
                 1.54 
                 0.05 
                 0.76 
                 1.81 
               
               
                 041 
                 60.50 
                 43.40 
                 −28.26 
                 1.63 
                 1.49 
                 0.14 
                 −0.83 
                 0.81 
                 1.64 
                 44.80 
                 −25.95 
                 2.12 
                 0.49 
                 1.19 
                 2.02 
               
               
                 042 
                 60.70 
                 40.50 
                 −33.28 
                 1.29 
                 1.82 
                 0.53 
                 −0.95 
                 0.89 
                 1.84 
                 40.00 
                 −34.10 
                 2.09 
                 0.80 
                 0.90 
                 1.85 
               
               
                 043 
                 55.20 
                 36.20 
                 −34.42 
                 1.36 
                 2.38 
                 1.02 
                 −0.88 
                 1.20 
                 2.08 
                 31.80 
                 −42.39 
                 2.67 
                 1.31 
                 1.34 
                 2.22 
               
               
                 044 
                 41.70 
                 23.80 
                 −42.93 
                 1.17 
                 2.51 
                 1.34 
                 −1.00 
                 1.21 
                 2.21 
                 20.10 
                 −51.80 
                 3.09 
                 1.92 
                 1.33 
                 2.33 
               
               
                 045 
                 63.20 
                 46.90 
                 −25.79 
                 1.48 
                 1.87 
                 0.39 
                 −1.15 
                 0.60 
                 1.95 
                 43.40 
                 −31.33 
                 1.79 
                 0.31 
                 0.74 
                 1.89 
               
               
                 046 
                 38.40 
                 25.60 
                 −33.33 
                 1.14 
                 2.33 
                 1.19 
                 −1.03 
                 1.04 
                 2.07 
                 25.20 
                 −34.38 
                 2.27 
                 1.13 
                 0.89 
                 1.92 
               
               
                 047 
                 63.00 
                 48.80 
                 −22.54 
                 1.52 
                 1.85 
                 0.33 
                 −1.15 
                 0.81 
                 1.96 
                 49.30 
                 −21.75 
                 1.47 
                 0.05 
                 0.49 
                 1.64 
               
               
                 048 
                 61.10 
                 42.50 
                 −30.44 
                 1.13 
                 2.28 
                 1.15 
                 −1.04 
                 1.02 
                 2.06 
                 40.80 
                 −33.22 
                 2.13 
                 1.00 
                 0.77 
                 1.81 
               
               
                 049 
                 64.60 
                 45.00 
                 −30.34 
                 1.43 
                 2.24 
                 0.81 
                 −1.25 
                 0.72 
                 1.97 
                 42.00 
                 −34.98 
                 1.81 
                 0.38 
                 0.41 
                 1.66 
               
               
                 050 
                 51.80 
                 30.10 
                 −41.89 
                 1.37 
                 2.28 
                 0.91 
                 −1.14 
                 0.80 
                 1.94 
                 28.70 
                 −44.59 
                 2.18 
                 0.81 
                 0.67 
                 1.81 
               
               
                 051 
                 61.70 
                 44.90 
                 −27.23 
                 1.41 
                 2.00 
                 0.59 
                 −1.09 
                 0.85 
                 1.94 
                 45.00 
                 −27.07 
                 1.69 
                 0.28 
                 0.54 
                 1.63 
               
               
                 052 
                 58.00 
                 42.40 
                 −26.90 
                 1.44 
                 2.83 
                 1.39 
                 −0.72 
                 1.35 
                 2.07 
                 43.50 
                 −25.00 
                 2.64 
                 1.20 
                 1.16 
                 1.88 
               
               
                 053 
                 58.00 
                 40.40 
                 −30.34 
                 1.20 
                 2.79 
                 1.59 
                 −0.87 
                 1.35 
                 2.22 
                 39.40 
                 −32.07 
                 2.69 
                 1.49 
                 1.17 
                 2.04 
               
               
                 054 
                 48.10 
                 30.60 
                 −36.38 
                 1.28 
                 2.50 
                 1.22 
                 −1.11 
                 1.05 
                 2.16 
                 29.10 
                 −39.50 
                 2.18 
                 0.90 
                 0.76 
                 1.87 
               
               
                 055 
                 37.50 
                 27.00 
                 −28.00 
                 0.98 
                 3.18 
                 2.20 
                 −0.75 
                 1.56 
                 2.33 
                 25.70 
                 −31.47 
                 3.08 
                 2.10 
                 1.49 
                 2.24 
               
               
                 067 
                 67.80 
                 39.00 
                 −42.48 
                 1.21 
                 0.98 
                 0.23 
                 −1.08 
                 0.45 
                 1.53 
                 26.40 
                 −61.06 
                 1.92 
                 0.71 
                 0.73 
                 1.81 
               
               
                 068 
                 72.60 
                 42.90 
                 −40.91 
                 1.38 
                 1.78 
                 0.40 
                 −0.56 
                 0.98 
                 1.54 
                 36.10 
                 −50.28 
                 2.75 
                 1.37 
                 1.46 
                 2.02 
               
               
                 069 
                 73.70 
                 43.70 
                 −40.71 
                 1.61 
                 1.33 
                 0.28 
                 −0.92 
                 0.63 
                 1.55 
                 42.70 
                 −42.06 
                 2.00 
                 0.39 
                 1.00 
                 1.92 
               
               
                 070 
                 73.10 
                 40.50 
                 −44.60 
                 1.15 
                 1.23 
                 0.08 
                 −0.81 
                 0.71 
                 1.52 
                 30.10 
                 −58.82 
                 2.28 
                 1.13 
                 1.16 
                 1.97 
               
               
                 071 
                 70.40 
                 34.40 
                 −51.14 
                 1.18 
                 1.22 
                 0.04 
                 −0.89 
                 0.65 
                 1.54 
                 32.40 
                 −53.98 
                 2.03 
                 0.85 
                 1.00 
                 1.89 
               
               
                 072 
                 72.00 
                 39.80 
                 −44.72 
                 1.43 
                 0.86 
                 0.57 
                 −1.04 
                 0.39 
                 1.43 
                 33.50 
                 −53.47 
                 1.62 
                 0.19 
                 0.75 
                 1.79 
               
               
                 073 
                 70.90 
                 33.40 
                 −52.89 
                 1.23 
                 0.95 
                 0.28 
                 −1.10 
                 0.35 
                 1.45 
                 34.30 
                 −51.62 
                 1.71 
                 0.48 
                 0.62 
                 1.72 
               
               
                 074 
                 71.80 
                 35.70 
                 −50.28 
                 1.43 
                 1.16 
                 0.27 
                 −0.63 
                 0.67 
                 1.50 
                 29.40 
                 −59.05 
                 1.98 
                 0.55 
                 0.94 
                 1.77 
               
               
                 075 
                 69.70 
                 35.30 
                 −49.35 
                 1.06 
                 1.00 
                 0.06 
                 −0.86 
                 0.57 
                 1.43 
                 36.80 
                 −47.20 
                 1.61 
                 0.55 
                 0.67 
                 1.53 
               
               
                 076 
                 59.40 
                 37.50 
                 −36.87 
                 1.38 
                 1.56 
                 0.18 
                 −0.82 
                 0.94 
                 1.76 
                 43.50 
                 −26.77 
                 2.26 
                 0.88 
                 1.09 
                 1.91 
               
               
                 077 
                 70.00 
                 34.60 
                 −50.57 
                 1.37 
                 1.76 
                 0.39 
                 −0.77 
                 0.93 
                 1.70 
                 30.80 
                 −56.00 
                 2.18 
                 0.81 
                 1.02 
                 1.79 
               
               
                 078 
                 69.20 
                 33.30 
                 −51.88 
                 1.46 
                 1.70 
                 0.24 
                 −0.82 
                 0.90 
                 1.72 
                 30.10 
                 −56.50 
                 2.03 
                 0.57 
                 1.19 
                 2.01 
               
               
                 079 
                 68.50 
                 33.60 
                 −49.47 
                 1.61 
                 1.48 
                 0.13 
                 −0.88 
                 0.99 
                 1.67 
                 31.60 
                 −52.48 
                 2.07 
                 0.46 
                 1.07 
                 1.75 
               
               
                 080 
                 69.70 
                 33.20 
                 −52.37 
                 1.42 
                 1.64 
                 0.22 
                 −0.82 
                 0.76 
                 1.58 
                 32.00 
                 −54.09 
                 1.66 
                 0.24 
                 0.80 
                 1.62 
               
               
                 081 
                 69.70 
                 33.80 
                 −51.61 
                 1.48 
                 1.46 
                 0.02 
                 −0.90 
                 0.78 
                 1.68 
                 32.10 
                 −53.95 
                 1.97 
                 0.49 
                 1.02 
                 1.92 
               
               
                 082 
                 64.90 
                 30.20 
                 −53.47 
                 1.43 
                 1.81 
                 0.38 
                 −0.95 
                 0.92 
                 1.87 
                 29.10 
                 −55.16 
                 2.34 
                 0.91 
                 1.27 
                 2.22 
               
               
                 083 
                 72.10 
                 32.40 
                 −55.06 
                 1.33 
                 1.67 
                 0.34 
                 −0.77 
                 0.90 
                 1.67 
                 26.20 
                 −63.66 
                 1.86 
                 0.53 
                 0.92 
                 1.69 
               
               
                 084 
                 72.40 
                 33.10 
                 −54.26 
                 1.57 
                 2.02 
                 0.45 
                 −0.70 
                 1.00 
                 1.70 
                 32.70 
                 −54.83 
                 2.26 
                 0.69 
                 1.20 
                 1.90 
               
               
                 085 
                 64.90 
                 40.30 
                 −37.90 
                 1.61 
                 0.92 
                 0.69 
                 −1.11 
                 0.34 
                 1.45 
                 45.30 
                 −30.20 
                 0.86 
                 0.75 
                 0.32 
                 1.43 
               
               
                 086 
                 62.20 
                 37.30 
                 −40.03 
                 1.55 
                 1.08 
                 0.47 
                 −1.24 
                 0.43 
                 1.67 
                 37.10 
                 −40.35 
                 0.99 
                 0.56 
                 0.28 
                 1.52 
               
               
                 087 
                 68.60 
                 40.40 
                 −39.34 
                 1.51 
                 0.66 
                 0.85 
                 −1.26 
                 0.19 
                 1.45 
                 40.70 
                 −38.89 
                 0.83 
                 0.68 
                 0.21 
                 1.47 
               
               
                 088 
                 54.40 
                 35.50 
                 −34.74 
                 1.54 
                 0.87 
                 0.67 
                 −1.12 
                 0.36 
                 1.48 
                 36.50 
                 −32.90 
                 1.21 
                 0.33 
                 −0.46 
                 0.66 
               
               
                 700T 
                 31.80 
                 13.30 
                 −58.18 
                 0.14 
                 0.45 
                 0.31 
                 0.11 
                 −0.41 
                 −0.52 
                 11.20 
                 −64.78 
                 0.52 
                 0.38 
                 −0.10 
                 −0.21 
               
               
                 HS+ 
                 86.50 
                 69.80 
                 −19.31 
                 3.04 
                 4.02 
                 0.98 
                 3.89 
                 2.53 
                 −1.36 
                 82.90 
                 −4.16 
                 4.11 
                 1.07 
                 2.59 
                 −1.30 
               
               
                   
               
             
          
           
               
                   
                 Viscosity, settling, and pH Stability (4 weeks at 120° F.) 
               
             
          
           
               
                 Formula 
                 Initial KU 
                 final KU 
                 % change 
                 Initial ICI 
                 final ICI 
                 % change 
                 Initial pH 
                 final pH 
                 % change 
                 settling amount 
                 settling type 
               
               
                   
               
               
                 001 
                 96 
                 gelled 
                   
                 1.6 
                 gelled 
                   
                 9.58 
                 n/a 
                   
                 n/a 
               
               
                 002 
                 140 
                 gelled 
                   
                 1.18 
                 gelled 
                   
                 9.59 
                 n/a 
                   
                 n/a 
               
               
                 003 
                 94 
                 gelled 
                   
                 1.16 
                 gelled 
                   
                 9.43 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 004 
                 79 
                 gelled 
                   
                 1.88 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 005 
                 136 
                 no sampl 
                   
                 0.69 
                 no sampl 
                   
                 9.61 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 006 
                 108 
                 gelled 
                   
                 1.83 
                 gelled 
                   
                 9.3 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 007 
                 91 
                 gelled 
                   
                 1.88 
                 gelled 
                   
                 9.48 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 008 
                 95 
                 gelled 
                   
                 1.88 
                 gelled 
                   
                 9.32 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 009 
                 68 
                 gelled 
                   
                 1.11 
                 gelled 
                   
                 9.42 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 010 
                 85 
                 98 
                 15.29 
                 0.492 
                 0.39 
                 −20.33 
                 9.09 
                 8.43 
                 −7.26 
                 30 
                 med-hard 
               
               
                 011 
                 83 
                 85 
                 2.41 
                 9.42 
                 0.48 
                 −94.87 
                 9.14 
                 n/a 
                   
                 20 
                 med-hard 
               
               
                 012 
                 69 
                 gelled 
                   
                 0.66 
                 gelled 
                   
                 9.45 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 013 
                 74 
                 gelled 
                   
                 0.77 
                 gelled 
                   
                 9.32 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 014 
                 88 
                 no sampl 
                   
                 0.56 
                 no sampl 
                   
                 9.56 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 015 
                 61 
                 gelled 
                   
                 1.17 
                 gelled 
                   
                 9.52 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 016 
                 68 
                 gelled 
                   
                 1.12 
                 gelled 
                   
                 9.38 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 017 
                 61 
                 gelled 
                   
                 1.63 
                 gelled 
                   
                 9.52 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 018 
                 58 
                 gelled 
                   
                 0.68 
                 gelled 
                   
                 1.697 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 019 
                 63 
                 no sampl 
                   
                 1.28 
                 no sampl 
                   
                 9.47 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 020 
                 78 
                 gelled 
                   
                 2.34 
                 gelled 
                   
                 9.64 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 021 
                 69 
                 gelled 
                   
                 1.19 
                 gelled 
                   
                 9.53 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 022 
                 80 
                 gelled 
                   
                 0.78 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 023 
                 70 
                 gelled 
                   
                 0.88 
                 gelled 
                   
                 9.48 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 031 
                 93 
                 gelled 
                   
                 1.37 
                 gelled 
                   
                 9.57 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 032 
                 72 
                 gelled 
                   
                 1.5 
                 gelled 
                   
                 9.24 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 033 
                 86 
                 71 
                 −17.44 
                 0.9 
                 0.45 
                 −49.56 
                 9.01 
                 8.31 
                 −7.77 
                 10 
                 soft 
               
               
                 034 
                 90 
                 gelled 
                   
                 1.13 
                 gelled 
                   
                 9.44 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 035 
                 83 
                 105  
                 26.51 
                 1.95 
                 1.67 
                 −14.31 
                 9.44 
                 8.9 
                 −5.72 
                 40 
                 med 
               
               
                 036 
                 88 
                 no sampl 
                   
                 1.17 
                 no sampl 
                   
                 9.33 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 037 
                 92 
                 gelled 
                   
                 0.85 
                 gelled 
                   
                 9.23 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 038 
                 86 
                 gelled 
                   
                 1.38 
                 gelled 
                   
                 9.55 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 039 
                 101 
                 gelled 
                   
                 0.77 
                 gelled 
                   
                 9.56 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 040 
                 86 
                 gelled 
                   
                 0.54 
                 gelled 
                   
                 9.4 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 041 
                 92 
                 no sampl 
                   
                 1.79 
                 no sampl 
                   
                 9.39 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 042 
                 85 
                 gelled 
                   
                 0.86 
                 gelled 
                   
                 9.44 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 043 
                 81 
                 gelled 
                   
                 0.7 
                 gelled 
                   
                 9.5 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 044 
                 85 
                 gelled 
                   
                 1.35 
                 gelled 
                   
                 9.49 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 045 
                 75 
                 gelled 
                   
                 1.16 
                 gelled 
                   
                 9.3 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 046 
                 73 
                 gelled 
                   
                 1.11 
                 gelled 
                   
                 9.22 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 047 
                 84 
                 no sampl 
                   
                 0.7 
                 no sampl 
                   
                 9.37 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 048 
                 80 
                 gelled 
                   
                 1.34 
                 gelled 
                   
                 9.53 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 049 
                 86 
                 gelled 
                   
                 1.66 
                 gelled 
                   
                 9.07 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 050 
                 68 
                 gelled 
                   
                 0.63 
                 gelled 
                   
                 9.4 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 051 
                 64 
                 gelled 
                   
                 2.68 
                 gelled 
                   
                 9.43 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 052 
                 138 
                 gelled 
                   
                 1.62 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 053 
                 78 
                 gelled 
                   
                 1.34 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 054 
                 58 
                 gelled 
                   
                 1.48 
                 gelled 
                   
                 9.72 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 055 
                 87 
                 gelled 
                   
                 1.74 
                 gelled 
                   
                 9.32 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 067 
                 89 
                 122 
                 37.08 
                 0.85 
                 0.76 
                 −10.82 
                 9.81 
                 9.25 
                 −5.71 
                 80 
                 medium 
               
               
                 068 
                 87 
                 97 
                 11.49 
                 0.51 
                 0.83 
                 62.55 
                 9.7 
                 9.13 
                 −5.88 
                 70 
                 medium 
               
               
                 069 
                 98 
                 119 
                 21.43 
                 0.51 
                 0.95 
                 85.49 
                 9.71 
                 9.33 
                 −3.91 
                 90 
                 medium 
               
               
                 070 
                 77 
                 89 
                 15.58 
                 0.73 
                 1.34 
                 83.84 
                 9.75 
                 9.16 
                 −6.05 
                 60 
                 medium 
               
               
                 071 
                 85 
                 81 
                 −4.71 
                 1.55 
                 0.87 
                 −44.06 
                 9.76 
                 9.21 
                 −5.64 
                 30 
                 soft 
               
               
                 072 
                 96 
                 93 
                 −3.13 
                 0.52 
                 0.55 
                 5.77 
                 9.8 
                 9.25 
                 −5.61 
                 slight 
                 soft 
               
               
                 073 
                 90 
                 107 
                 18.89 
                 0.41 
                 0.63 
                 53.41 
                 9.73 
                 9.35 
                 −3.91 
                 80 
                 medium 
               
               
                 074 
                 90 
                 132 
                 46.67 
                 0.85 
                 0.72 
                 −15.18 
                 9.91 
                 9.34 
                 −5.75 
                 80 
                 soft 
               
               
                 075 
                 90 
                 107 
                 18.89 
                 0.8 
                 0.71 
                 −11.50 
                 9.73 
                 9.13 
                 −6.17 
                 80 
                 soft 
               
               
                 076 
                 84 
                 76 
                 −9.52 
                 0.84 
                 0.33 
                 −60.36 
                 9.67 
                 9.11 
                 −5.79 
                 none 
                 n/a 
               
               
                 077 
                 96 
                 114 
                 18.75 
                 0.69 
                 1.10 
                 60.00 
                 9.9 
                 9.38 
                 −5.25 
                 90 
                 med-hard 
               
               
                 078 
                 94 
                 113 
                 20.21 
                 0.63 
                 0.76 
                 21.11 
                 9.9 
                 9.39 
                 −5.15 
                 80 
                 soft 
               
               
                 079 
                 77 
                 105 
                 36.36 
                 1.1 
                 0.73 
                 −33.36 
                 9.92 
                 9.48 
                 −4.44 
                 none 
                 n/a 
               
               
                 080 
                 85 
                 88 
                 3.53 
                 0.97 
                 1.00 
                 2.89 
                 9.78 
                 9.24 
                 −5.52 
                 40 
                 soft 
               
               
                 081 
                 94 
                 138 
                 46.81 
                 1.06 
                 0.92 
                 −13.49 
                 9.8 
                 9.35 
                 −4.59 
                 35 
                 medium 
               
               
                 082 
                 83 
                 86 
                 3.61 
                 0.71 
                 0.81 
                 14.51 
                 9.67 
                 9.23 
                 −4.55 
                 10 
                 soft 
               
               
                 083 
                 91 
                 111 
                 21.98 
                 1.1 
                 0.65 
                 −40.55 
                 9.82 
                 9.23 
                 −6.01 
                 90 
                 medium 
               
               
                 084 
                 83 
                 105 
                 26.51 
                 0.74 
                 0.71 
                 −4.32 
                 9.78 
                 9.23 
                 −5.62 
                 90 
                 soft 
               
               
                 085 
                 87 
                 gelled 
                   
                 0.84 
                 gelled 
                   
                 9.01 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 086 
                 72 
                 88 
                 22.22 
                 1.05 
                 1.09 
                 3.82 
                 9.33 
                 8.83 
                 −7.50 
                 20 
                 medium 
               
               
                 087 
                 83 
                 106 
                 27.71 
                 0.78 
                 1.69 
                 116.41 
                 9.35 
                 8.66 
                 −7.38 
                 80 
                 soft 
               
               
                 088 
                 90 
                 gelled 
                   
                 0.95 
                 gelled 
                   
                 9.18 
                 n/a 
                   
                 n/a 
                 n/a 
               
             
          
           
               
                 700T 
                 % settling is the relative ht on stirring stick that adheres w/o easily falling away 
               
               
                 HS+ 
               
               
                   
               
             
          
         
       
     
     
       
         
               
             
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
             
               
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
               
             
               
               
               
               
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
               
             
               
               
             
               
               
               
               
               
               
               
               
               
               
               
               
             
           
               
                 TABLE 8 
               
               
                   
               
               
                 INDUSTRIAL MAINTENANCE 
               
               
                   
               
             
             
               
                   
               
             
          
           
               
                   
                 Chemical Resistance 
                 Pencil 
               
             
          
           
               
                 Formula 
                 Resin 
                 Dispersant 
                 Dispersant Amount 
                 Thickener 
                 Film Thickness 
                 20 Gloss 
                 60 Gloss 
                 Toluene 
                 Ethanol 
                 MEK 
                 10% Sulf 
                 10% NaOH 
                 DL Water 
                 hardness 
               
               
                   
               
               
                 001 
                 3 
                 2 
                 1 
                 3 
                 2.61 
                 6.6 
                 31.2 
                 1 
                 3 
                 1 
                 5 
                 3 
                 4.5 
                 1 
               
               
                 002 
                 3 
                 8 
                 1 
                 5 
                 2.69 
                 23.6 
                 59.6 
                 1 
                 3 
                 1 
                 5 
                 2 
                 4 
                 0 
               
               
                 003 
                 3 
                 7 
                 1 
                 5 
                 2.37 
                 28.8 
                 63.6 
                 1 
                 3 
                 1.5 
                 5 
                 2 
                 4 
                 1 
               
               
                 004 
                 3 
                 2 
                 1 
                 6 
                 2.75 
                 4.6 
                 25.7 
                 1 
                 4 
                 1.5 
                 5 
                 3 
                 5 
                 1 
               
               
                 005 
                 3 
                 11 
                 1 
                 7 
                 2.36 
                 25.6 
                 61.6 
                 1 
                 3 
                 1.5 
                 5 
                 2 
                 3 
                 1 
               
               
                 006 
                 3 
                 3 
                 1 
                 7 
                 2.60 
                 17.2 
                 52.7 
                 1 
                 3 
                 1.6 
                 4.5 
                 3 
                 4.5 
                 1 
               
               
                 007 
                 4 
                 1 
                 2 
                 7 
                 2.72 
                 34.7 
                 67.9 
                 1.5 
                 4.5 
                 1.6 
                 5 
                 2 
                 3 
                 0 
               
               
                 008 
                 4 
                 5 
                 2 
                 5 
                 2.80 
                 35.9 
                 68.3 
                 4 
                 4 
                 1.5 
                 4 
                 3 
                 3 
                 0 
               
               
                 009 
                 4 
                 3 
                 2 
                 3 
                 2.34 
                 30.8 
                 65.5 
                 3 
                 4 
                 1 
                 3 
                 3 
                 3 
                 0 
               
               
                 010 
                 4 
                 10 
                 2 
                 2 
                 2.28 
                 13.9 
                 49.8 
                 3 
                 3 
                 1.5 
                 3 
                 3 
                 3 
                 1 
               
               
                 011 
                 4 
                 10 
                 2 
                 2 
                 2.30 
                 8.0 
                 37.9 
                 4 
                 4 
                 1.5 
                 5 
                 4 
                 5 
                 1 
               
               
                 012 
                 4 
                 3 
                 2 
                 7 
                 2.43 
                 20.1 
                 57.9 
                 1.5 
                 4.5 
                 1.5 
                 4.5 
                 4 
                 3 
                 0 
               
               
                 013 
                 4 
                 8 
                 2 
                 7 
                 2.58 
                 11.7 
                 44.4 
                 1 
                 3 
                 4 
                 4 
                 3 
                 3 
                 0 
               
               
                 014 
                 4 
                 11 
                 2 
                 8 
                 2.49 
                 29.6 
                 65.4 
                 4 
                 3 
                 1.6 
                 5 
                 3 
                 3 
                 0 
               
               
                 015 
                 4 
                 1 
                 1 
                 2 
                 2.55 
                 28.9 
                 63.7 
                 1.5 
                 4.5 
                 2 
                 5 
                 1.5 
                 3 
                 0 
               
               
                 016 
                 4 
                 5 
                 1 
                 3 
                 2.76 
                 36.0 
                 67.5 
                 3 
                 3 
                 2 
                 3 
                 3 
                 3 
                 0 
               
               
                 017 
                 4 
                 1 
                 1 
                 8 
                 2.63 
                 21.2 
                 57.2 
                 1.5 
                 4.5 
                 2 
                 5 
                 4.5 
                 3 
                 0 
               
               
                 018 
                 4 
                 2 
                 1 
                 4 
                 2.51 
                 33.7 
                 66.8 
                 1.5 
                 3 
                 1.5 
                 4.5 
                 2 
                 3 
                 0 
               
               
                 019 
                 4 
                 7 
                 1 
                 1 
                 2.70 
                 14.3 
                 48.0 
                 1.5 
                 4 
                 1 
                 4 
                 3 
                 3 
                 0 
               
               
                 020 
                 4 
                 11 
                 1 
                 4 
                 2.65 
                 33.5 
                 67.2 
                 4 
                 3 
                 1.5 
                 4.5 
                 4 
                 3 
                 0 
               
               
                 021 
                 4 
                 3 
                 1 
                 6 
                 2.71 
                 34.2 
                 69.0 
                 3 
                 3 
                 1.5 
                 4.5 
                 4 
                 3 
                 0 
               
               
                 022 
                 4 
                 11 
                 1 
                 2 
                 2.60 
                 30.8 
                 66.3 
                 3 
                 4 
                 2 
                 5 
                 3 
                 3 
                 0 
               
               
                 023 
                 4 
                 3 
                 1 
                 7 
                 2.51 
                 36.9 
                 68.1 
                 3 
                 1.5 
                 3 
                 5 
                 3 
                 3 
                 0 
               
               
                 031 
                 2 
                 2 
                 2 
                 1 
                 2.38 
                 21.5 
                 56.1 
                 1.5 
                 4 
                 1.5 
                 5 
                 3 
                 5 
                 0 
               
               
                 032 
                 2 
                 3 
                 2 
                 6 
                 1.93 
                 31.0 
                 66.9 
                 1.5 
                 3.5 
                 1.5 
                 5 
                 3 
                 2 
                 0 
               
               
                 033 
                 2 
                 4 
                 2 
                 8 
                 2.09 
                 12.5 
                 44.7 
                 1.5 
                 3.5 
                 1.5 
                 5 
                 4 
                 2 
                 0 
               
               
                 034 
                 2 
                 1 
                 1 
                 7 
                 2.49 
                 25.4 
                 60.2 
                 1.5 
                 4 
                 1.6 
                 5 
                 3 
                 2 
                 0 
               
               
                 035 
                 2 
                 1 
                 1 
                 5 
                 2.47 
                 15.4 
                 49.3 
                 1.5 
                 4 
                 1.5 
                 5 
                 3 
                 2 
                 0 
               
               
                 036 
                 2 
                 3 
                 1 
                 4 
                 2.51 
                 16.6 
                 51.2 
                 1.5 
                 3 
                 1 
                 5 
                 2 
                 2 
                 0 
               
               
                 037 
                 2 
                 8 
                 1 
                 4 
                 2.54 
                 15.1 
                 49.1 
                 1 
                 2 
                 1 
                 4 
                 2 
                 5 
                 0 
               
               
                 038 
                 2 
                 11 
                 1 
                 2 
                 2.43 
                 33.0 
                 67.3 
                 1.5 
                 3 
                 1.6 
                 5 
                 2 
                 2.5 
                 0 
               
               
                 039 
                 2 
                 2 
                 1 
                 8 
                 2.61 
                 21.7 
                 58.5 
                 1.5 
                 3 
                 1.6 
                 5 
                 2 
                 2 
                 0 
               
               
                 040 
                 2 
                 7 
                 1 
                 8 
                 2.32 
                 27.4 
                 62.5 
                 1.5 
                 3 
                 1 
                 5 
                 2 
                 2 
                 0 
               
               
                 041 
                 2 
                 7 
                 1 
                 6 
                 2.49 
                 23.8 
                 59.4 
                 1.5 
                 3 
                 1.5 
                 5 
                 2 
                 2 
                 0 
               
               
                 042 
                 3 
                 1 
                 2 
                 4 
                 3.01 
                 25.7 
                 61.0 
                 1 
                 3 
                 1.5 
                 5 
                 2 
                 5 
                 0 
               
               
                 043 
                 3 
                 1 
                 2 
                 1 
                 2.34 
                 18.9 
                 54.4 
                 1 
                 3 
                 1 
                 5 
                 2 
                 2 
                 1 
               
               
                 044 
                 3 
                 1 
                 2 
                 7 
                 2.34 
                 9.7 
                 39.9 
                 1 
                 3 
                 1.5 
                 5 
                 2 
                 5 
                 1 
               
               
                 045 
                 3 
                 5 
                 2 
                 8 
                 2.36 
                 26.6 
                 62.4 
                 1 
                 3 
                 1 
                 4 
                 2 
                 4.5 
                 1 
               
               
                 046 
                 3 
                 8 
                 2 
                 3 
                 2.09 
                 6.9 
                 31.5 
                 1.5 
                 3 
                 1.5 
                 5 
                 3 
                 5 
                 1 
               
               
                 047 
                 3 
                 7 
                 2 
                 1 
                 1.94 
                 25.0 
                 61.4 
                 1.5 
                 3 
                 1.5 
                 5 
                 2 
                 2.5 
                 1 
               
               
                 048 
                 3 
                 11 
                 2 
                 3 
                 2.15 
                 23.6 
                 59.8 
                 1 
                 3 
                 1.5 
                 5 
                 2 
                 3 
                 1 
               
               
                 049 
                 3 
                 8 
                 2 
                 6 
                 2.02 
                 24.9 
                 63.6 
                 1.5 
                 4 
                 1.5 
                 5 
                 4 
                 4 
                 2 
               
               
                 050 
                 3 
                 3 
                 2 
                 5 
                 2.20 
                 15.4 
                 50.3 
                 1 
                 3 
                 1.5 
                 5 
                 2 
                 4.5 
                 1 
               
               
                 051 
                 3 
                 5 
                 1 
                 4 
                 2.56 
                 26.3 
                 63.0 
                 1 
                 3.5 
                 1 
                 5 
                 2 
                 3 
                 0 
               
               
                 052 
                 3 
                 9 
                 1 
                 1 
                 2.54 
                 22.6 
                 57.7 
                 4 
                 1 
                 1 
                 5 
                 2 
                 2 
                 1 
               
               
                 053 
                 3 
                 9 
                 1 
                 2 
                 2.47 
                 21.7 
                 57.3 
                 1 
                 3 
                 1 
                 6 
                 2 
                 2 
                 1 
               
               
                 054 
                 2 
                 8 
                 1 
                 4 
                 2.47 
                 14.9 
                 49.1 
                 1 
                 3 
                 1 
                 4.5 
                 2.5 
                 2 
                 1 
               
               
                 055 
                 3 
                 8 
                 2 
                 4 
                 2.79 
                 8.9 
                 37.3 
                 1 
                 3 
                 1 
                 4.5 
                 3 
                 4.5 
                 1 
               
               
                 067 
                 1 
                 5 
                 2 
                 3 
                 2.40 
                 29.1 
                 65.5 
                 1.5 
                 4 
                 1.5 
                 3 
                 2 
                 3 
                 0 
               
               
                 068 
                 1 
                 1 
                 2 
                 6 
                 2.28 
                 37.0 
                 70.9 
                 1.5 
                 4 
                 1.5 
                 4 
                 3 
                 3 
                 0 
               
               
                 069 
                 1 
                 8 
                 2 
                 2 
                 2.38 
                 38.6 
                 71.5 
                 1.5 
                 3 
                 1.5 
                 3 
                 2 
                 3 
                 0 
               
               
                 070 
                 1 
                 3 
                 2 
                 2 
                 2.38 
                 36.1 
                 69.4 
                 1.5 
                 3 
                 1.5 
                 4 
                 2 
                 4 
                 0 
               
               
                 071 
                 1 
                 3 
                 2 
                 2 
                 2.24 
                 32.0 
                 67.3 
                 1.5 
                 5 
                 1.5 
                 3 
                 2 
                 2 
                 0 
               
               
                 072 
                 1 
                 11 
                 2 
                 5 
                 2.09 
                 35.9 
                 69.2 
                 1.5 
                 2 
                 1.5 
                 4 
                 3 
                 3 
                 0 
               
               
                 073 
                 1 
                 7 
                 2 
                 6 
                 2.19 
                 32.2 
                 67.4 
                 1.5 
                 3.5 
                 1.5 
                 3 
                 2 
                 4 
                 0 
               
               
                 074 
                 1 
                 2 
                 2 
                 5 
                 2.57 
                 33.7 
                 68.2 
                 1.5 
                 5 
                 1.5 
                 4 
                 2 
                 3 
                 0 
               
               
                 075 
                 1 
                 5 
                 1 
                 2 
                 2.44 
                 32.2 
                 67.7 
                 1.5 
                 5 
                 1.5 
                 4.5 
                 3 
                 4 
                 0 
               
               
                 076 
                 1 
                 6 
                 1 
                 1 
                 2.49 
                 24.3 
                 59.7 
                 1.5 
                 4 
                 1.5 
                 4 
                 2 
                 4 
                 0 
               
               
                 077 
                 1 
                 9 
                 1 
                 6 
                 2.40 
                 31.9 
                 67.4 
                 1.5 
                 4 
                 1.5 
                 4 
                 2 
                 4.5 
                 0 
               
               
                 078 
                 1 
                 9 
                 1 
                 4 
                 2.25 
                 30.4 
                 66.7 
                 1.5 
                 4 
                 1.5 
                 4.5 
                 2 
                 4 
                 0 
               
               
                 079 
                 1 
                 2 
                 1 
                 1 
                 2.87 
                 28.2 
                 63.9 
                 1.5 
                 4 
                 1.5 
                 4 
                 2 
                 3 
                 0 
               
               
                 080 
                 1 
                 3 
                 1 
                 8 
                 2.55 
                 33.8 
                 67.5 
                 2 
                 3 
                 1 
                 4 
                 2 
                 2 
                 0 
               
               
                 081 
                 1 
                 7 
                 1 
                 3 
                 2.94 
                 34.5 
                 66.6 
                 1.5 
                 4 
                 2 
                 3 
                 3 
                 4 
                 0 
               
               
                 082 
                 1 
                 10 
                 1 
                 1 
                 2.95 
                 28.8 
                 61.7 
                 1.5 
                 5 
                 1.5 
                 4 
                 4 
                 5 
                 0 
               
               
                 083 
                 1 
                 9 
                 1 
                 5 
                 2.88 
                 36.2 
                 69.4 
                 1.5 
                 4 
                 1.5 
                 3 
                 2 
                 2 
                 0 
               
               
                 084 
                 1 
                 3 
                 1 
                 6 
                 3.24 
                 38.0 
                 69.7 
                 1.5 
                 2 
                 1 
                 3 
                 2 
                 2 
                 0 
               
               
                 085 
                 2 
                 1 
                 2 
                 3 
                 1.95 
                 27.0 
                 63.5 
                 1.5 
                 3 
                 1.5 
                 5 
                 2 
                 2 
                 0 
               
               
                 086 
                 2 
                 5 
                 2 
                 7 
                 2.34 
                 24.7 
                 60.4 
                 1 
                 3 
                 1 
                 5 
                 2 
                 2 
                 0 
               
               
                 087 
                 2 
                 6 
                 2 
                 7 
                 2.52 
                 30.9 
                 65.5 
                 1.5 
                 3.5 
                 1.5 
                 4.5 
                 2 
                 2 
                 0 
               
               
                 088 
                 2 
                 8 
                 2 
                 4 
                 2.43 
                 17.5 
                 52.7 
                 1.5 
                 4.5 
                 1.5 
                 5 
                 2 
                 5 
                 0 
               
               
                 Polylon 1900 
                   
                   
                 Control #1 
                   
                 3.30 
                 83.3 
                 94.4 
                 1.5 
                 1.5 
                 1.5 
                 4 
                 4.5 
                 4.5 
                 5 
               
               
                 Centurion 
                   
                   
                 Control #2 
                   
                 3.66 
                 72.8 
                 88.8 
                 1.5 
                 1.5 
                 1.5 
                 5 
                 5 
                 5 
                 4 
               
               
                 Sher-cryl 
                   
                   
                 Control #3 
                   
                 1.97 
                 46.3 
                 78.0 
                 1 
                 3 
                 1.5 
                 5 
                 3 
                 4 
                 0 
               
               
                   
               
             
          
           
               
                   
                 Humidity 
                 Salt Spray (200 hours) 
                 Salt Spray (375 hours) 
                 Forward 
                 Reverse 
               
             
          
           
               
                 Formula 
                 Blister size 
                 Blister density 
                 Rust 
                 Gloss 
                 % Change gloss 
                 Blister size 
                 Blister density 
                 Rust 
                 Scribe 
                 Blister size 
                 Blister density 
                 Rust 
                 Scribe 
                 Impact 
                 Impact 
               
               
                   
               
               
                 001 
                 4 
                 2 
                 9 
                 19.9 
                 −36.22% 
                 2 
                 2 
                 10 
                 8 
                 2 
                 1 
                 9 
                 7 
                 40 
                 &lt;4 
               
               
                 002 
                 6 
                 3 
                 10 
                 40.2 
                 −32.78% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 1 
                 8 
                 7 
                 44 
                 4 
               
               
                 003 
                 8 
                 2 
                 9 
                 46.3 
                 −27.43% 
                 2 
                 2 
                 6 
                 8 
                 2 
                 1 
                 7 
                 7 
                 36 
                 4 
               
               
                 004 
                 4 
                 2 
                 7 
                 15.4 
                 −40.08% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 1 
                 8 
                 7 
                 40 
                 &lt;4 
               
               
                 005 
                 8 
                 3 
                 8 
                 47.9 
                 −22.24% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 1 
                 8 
                 7 
                 44 
                 8 
               
               
                 006 
                 8 
                 3 
                 9 
                 41.6 
                 −21.06% 
                 2 
                 3 
                 8 
                 8 
                 2 
                 2 
                 8 
                 8 
                 40 
                 4 
               
               
                 007 
                 6 
                 2 
                 1 
                 26.5 
                 −60.97% 
                 6 
                 3 
                 8 
                 8 
                 2 
                 3 
                 7 
                 8 
                 &gt;168 
                 &gt;168 
               
               
                 008 
                 6 
                 2 
                 9 
                 20.5 
                 −69.99% 
                 6 
                 4 
                 10 
                 8 
                 4 
                 3 
                 9 
                 8 
                 &gt;168 
                 &gt;168 
               
               
                 009 
                 6 
                 2 
                 6 
                 26.0 
                 −60.31% 
                 6 
                 4 
                 10 
                 8 
                 6 
                 3 
                 9 
                 8 
                 &gt;168 
                 &gt;168 
               
               
                 010 
                 8 
                 1 
                 1 
                 19.6 
                 −60.64% 
                 6 
                 4 
                 6 
                 8 
                 4 
                 3 
                 8 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 011 
                 4 
                 3 
                 5 
                 16.9 
                 −55.41% 
                 6 
                 4 
                 8 
                 8 
                 4 
                 3 
                 8 
                 6 
                 &gt;168 
                 &gt;168 
               
               
                 012 
                 6 
                 2 
                 4 
                 25.6 
                 −55.79% 
                 6 
                 4 
                 8 
                 8 
                 2 
                 3 
                 8 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 013 
                 2 
                 2 
                 10 
                 11.7 
                 −73.65% 
                 6 
                 4 
                 9 
                 8 
                 4 
                 3 
                 9 
                 5 
                 &gt;168 
                 &gt;168 
               
               
                 014 
                 4 
                 1 
                 1 
                 9.0 
                 −86.24% 
                 6 
                 3 
                 7 
                 7 
                 4 
                 3 
                 8 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 015 
                 4 
                 1 
                 8 
                 18.2 
                 −71.43% 
                 2 
                 4 
                 9 
                 7 
                 4 
                 3 
                 9 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 016 
                 4 
                 2 
                 6 
                 36.3 
                 −46.22% 
                 6 
                 4 
                 8 
                 8 
                 4 
                 3 
                 8 
                 6 
                 &gt;168 
                 &gt;168 
               
               
                 017 
                 4 
                 1 
                 9 
                 10.0 
                 −82.52% 
                 6 
                 4 
                 8 
                 8 
                 4 
                 3 
                 8 
                 6 
                 &gt;168 
                 &gt;168 
               
               
                 018 
                 4 
                 1 
                 8 
                 10.5 
                 −54.28% 
                 6 
                 4 
                 8 
                 8 
                 2 
                 3 
                 8 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 019 
                 2 
                 1 
                 8 
                 7.8 
                 −83.75% 
                 6 
                 4 
                 8 
                 8 
                 4 
                 3 
                 9 
                 6 
                 &gt;168 
                 &gt;168 
               
               
                 020 
                 4 
                 2 
                 8 
                 16.6 
                 −75.00% 
                 6 
                 4 
                 8 
                 8 
                 4 
                 3 
                 8 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 021 
                 4 
                 2 
                 4 
                 23.9 
                 −65.36% 
                 6 
                 4 
                 8 
                 8 
                 4 
                 3 
                 7 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 022 
                 4 
                 1 
                 2 
                 20.7 
                 −68.78% 
                 6 
                 4 
                 9 
                 8 
                 6 
                 2 
                 9 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 023 
                 2 
                 1 
                 6 
                 8.4 
                 −87.67% 
                 6 
                 4 
                 9 
                 8 
                 6 
                 3 
                 9 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                 031 
                 4 
                 1 
                 5 
                 31.0 
                 −44.74% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 2 
                 7 
                 7 
                 24 
                 &lt;4 
               
               
                 032 
                 6 
                 3 
                 9 
                 43.5 
                 −34.98% 
                 2 
                 2 
                 6 
                 9 
                 2 
                 1 
                 6 
                 7 
                 35 
                 4 
               
               
                 033 
                 6 
                 2 
                 5 
                 31.0 
                 −30.65% 
                 2 
                 2 
                 8 
                 9 
                 2 
                 1 
                 5 
                 7 
                 28 
                 &lt;4 
               
               
                 034 
                 4 
                 2 
                 4 
                 33.5 
                 −44.35% 
                 2 
                 2 
                 8 
                 9 
                 2 
                 1 
                 7 
                 8 
                 28 
                 &lt;4 
               
               
                 035 
                 4 
                 2 
                 5 
                 24.0 
                 −51.32% 
                 2 
                 2 
                 6 
                 9 
                 2 
                 1 
                 4 
                 8 
                 24 
                 &lt;4 
               
               
                 036 
                 4 
                 2 
                 7 
                 30.3 
                 −40.82% 
                 2 
                 2 
                 7 
                 9 
                 2 
                 1 
                 6 
                 9 
                 28 
                 &lt;4 
               
               
                 037 
                 4 
                 3 
                 8 
                 23.8 
                 −51.53% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 2 
                 7 
                 7 
                 24 
                 &lt;4 
               
               
                 038 
                 4 
                 3 
                 9 
                 36.4 
                 −45.91% 
                 2 
                 1 
                 7 
                 8 
                 2 
                 1 
                 6 
                 7 
                 28 
                 4 
               
               
                 039 
                 4 
                 2 
                 7 
                 26.3 
                 −51.62% 
                 2 
                 2 
                 10 
                 8 
                 2 
                 1 
                 7 
                 7 
                 40 
                 4 
               
               
                 040 
                 4 
                 2 
                 9 
                 25.2 
                 −59.68% 
                 2 
                 2 
                 7 
                 8 
                 2 
                 1 
                 5 
                 7 
                 28 
                 &lt;4 
               
               
                 041 
                 6 
                 2 
                 7 
                 33.0 
                 −44.44% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 1 
                 7 
                 7 
                 24 
                 &lt;4 
               
               
                 042 
                 4 
                 2 
                 8 
                 37.0 
                 −39.34% 
                 2 
                 2 
                 6 
                 6 
                 2 
                 1 
                 7 
                 7 
                 96 
                 16 
               
               
                 043 
                 6 
                 2 
                 9 
                 32.1 
                 −40.99% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 1 
                 8 
                 6 
                 40 
                 4 
               
               
                 044 
                 6 
                 2 
                 10 
                 28.0 
                 −29.82% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 1 
                 8 
                 6 
                 36 
                 &lt;4 
               
               
                 045 
                 8 
                 2 
                 6 
                 40.1 
                 −35.74% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 1 
                 8 
                 7 
                 40 
                 8 
               
               
                 046 
                 6 
                 2 
                 9 
                 22.5 
                 −28.57% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 1 
                 7 
                 7 
                 36 
                 4 
               
               
                 047 
                 8 
                 2 
                 8 
                 43.3 
                 −29.48% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 1 
                 7 
                 7 
                 36 
                 4 
               
               
                 048 
                 8 
                 3 
                 9 
                 42.2 
                 −29.43% 
                 2 
                 2 
                 7 
                 8 
                 2 
                 1 
                 5 
                 7 
                 40 
                 4 
               
               
                 049 
                 8 
                 2 
                 9 
                 33.2 
                 −47.80% 
                 2 
                 2 
                 5 
                 8 
                 2 
                 1 
                 5 
                 7 
                 60 
                 16 
               
               
                 050 
                 8 
                 3 
                 10 
                 32.6 
                 −35.19% 
                 2 
                 2 
                 6 
                 8 
                 2 
                 1 
                 6 
                 7 
                 48 
                 &lt;4 
               
               
                 051 
                 8 
                 3 
                 9 
                 48.2 
                 −23.49% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 2 
                 8 
                 8 
                 48 
                 4 
               
               
                 052 
                 8 
                 3 
                 9 
                 46.5 
                 −18.41% 
                 2 
                 2 
                 7 
                 8 
                 2 
                 1 
                 7 
                 6 
                 32 
                 4 
               
               
                 053 
                 8 
                 3 
                 10 
                 46.3 
                 −19.20% 
                 2 
                 2 
                 5 
                 8 
                 2 
                 2 
                 8 
                 8 
                 36 
                 4 
               
               
                 054 
                 8 
                 3 
                 10 
                 35.3 
                 −28.11% 
                 2 
                 3 
                 7 
                 8 
                 2 
                 3 
                 9 
                 7 
                 32 
                 &lt;4 
               
               
                 055 
                 4 
                 3 
                 9 
                 28.5 
                 −23.59% 
                 2 
                 2 
                 7 
                 8 
                 2 
                 1 
                 7 
                 7 
                 28 
                 &lt;4 
               
               
                 067 
                 6 
                 2 
                 9 
                 21.2 
                 −67.63% 
                 2 
                 3 
                 9 
                 8 
                 4 
                 2 
                 8 
                 7 
                 44 
                 8 
               
               
                 068 
                 6 
                 2 
                 10 
                 28.8 
                 −59.38% 
                 2 
                 3 
                 10 
                 8 
                 2 
                 3 
                 8 
                 8 
                 44 
                 4 
               
               
                 069 
                 4 
                 2 
                 9 
                 16.7 
                 −73.85% 
                 2 
                 3 
                 9 
                 8 
                 2 
                 2 
                 8 
                 8 
                 56 
                 8 
               
               
                 070 
                 8 
                 1 
                 9 
                 32.6 
                 −53.03% 
                 2 
                 3 
                 9 
                 8 
                 4 
                 2 
                 8 
                 8 
                 52 
                 12 
               
               
                 071 
                 6 
                 2 
                 9 
                 27.8 
                 −58.69% 
                 2 
                 2 
                 10 
                 8 
                 2 
                 2 
                 9 
                 8 
                 40 
                 12 
               
               
                 072 
                 6 
                 2 
                 9 
                 26.8 
                 −61.27% 
                 2 
                 3 
                 9 
                 7 
                 2 
                 2 
                 8 
                 8 
                 48 
                 4 
               
               
                 073 
                 6 
                 1 
                 9 
                 20.6 
                 −69.44% 
                 2 
                 1 
                 10 
                 8 
                 2 
                 2 
                 9 
                 8 
                 64 
                 12 
               
               
                 074 
                 4 
                 2 
                 9 
                 29.7 
                 −56.45% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 2 
                 8 
                 8 
                 44 
                 4 
               
               
                 075 
                 4 
                 2 
                 10 
                 19.6 
                 −71.05% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 2 
                 8 
                 8 
                 64 
                 16 
               
               
                 076 
                 6 
                 2 
                 10 
                 30.9 
                 −48.24% 
                 10 
                 5 
                 10 
                 7 
                 2 
                 4 
                 9 
                 8 
                 44 
                 4 
               
               
                 077 
                 4 
                 2 
                 10 
                 13.6 
                 −79.82% 
                 2 
                 4 
                 10 
                 8 
                 2 
                 2 
                 9 
                 8 
                 52 
                 8 
               
               
                 078 
                 4 
                 2 
                 9 
                 22.7 
                 −65.97% 
                 2 
                 3 
                 10 
                 8 
                 4 
                 3 
                 9 
                 7 
                 56 
                 8 
               
               
                 079 
                 4 
                 2 
                 9 
                 22.8 
                 −64.32% 
                 2 
                 3 
                 9 
                 8 
                 2 
                 2 
                 8 
                 7 
                 36 
                 8 
               
               
                 080 
                 4 
                 2 
                 9 
                 19.9 
                 −70.52% 
                 2 
                 3 
                 9 
                 8 
                 2 
                 3 
                 9 
                 8 
                 56 
                 16 
               
               
                 081 
                 4 
                 2 
                 10 
                 22.4 
                 −68.37% 
                 2 
                 3 
                 9 
                 8 
                 2 
                 3 
                 8 
                 7 
                 44 
                 4 
               
               
                 082 
                 4 
                 2 
                 9 
                 26.4 
                 −57.21% 
                 2 
                 3 
                 9 
                 8 
                 2 
                 1 
                 9 
                 8 
                 60 
                 8 
               
               
                 083 
                 4 
                 2 
                 10 
                 22.1 
                 −68.16% 
                 2 
                 2 
                 8 
                 8 
                 2 
                 2 
                 9 
                 9 
                 52 
                 8 
               
               
                 084 
                 4 
                 2 
                 10 
                 16.5 
                 −76.33% 
                 2 
                 2 
                 9 
                 8 
                 2 
                 2 
                 9 
                 8 
                 64 
                 24 
               
               
                 085 
                 4 
                 2 
                 9 
                 17.9 
                 −71.81% 
                 2 
                 1 
                 8 
                 9 
                 2 
                 2 
                 8 
                 9 
                 28 
                 &lt;4 
               
               
                 086 
                 4 
                 2 
                 9 
                 23.0 
                 −61.92% 
                 2 
                 2 
                 8 
                 9 
                 2 
                 2 
                 7 
                 9 
                 32 
                 4 
               
               
                 087 
                 6 
                 2 
                 9 
                 22.6 
                 −65.50% 
                 2 
                 2 
                 6 
                 8 
                 2 
                 1 
                 6 
                 7 
                 28 
                 &lt;4 
               
               
                 088 
                 6 
                 2 
                 9 
                 26.3 
                 −50.09% 
                 2 
                 2 
                 6 
                 8 
                 2 
                 1 
                 6 
                 7 
                 40 
                 &lt;4 
               
               
                 Polylon 1900 
                 2 
                 3 
                 10 
                 90.5 
                 −4.13% 
                 10 
                 5 
                 10 
                 9 
                 10 
                 5 
                 10 
                 3 
                 36 
                 &lt;4 
               
               
                 Centurion 
                 4 
                 2 
                 10 
                 31.2 
                 −64.86% 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 9 
                 8 
                 &gt;168 
                 &gt;168 
               
               
                 Sher-cryl 
                 8 
                 2 
                 9 
                 30.2 
                 −61.28% 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 7 
                 7 
                 &gt;168 
                 &gt;168 
               
               
                   
               
             
          
           
               
                   
                 Corrosion Weathering (4 cycles) 
                 Adhesion 
                 24 Hr. Water Soak 
                   
               
             
          
           
               
                 Formula 
                 Blister size 
                 Blister density 
                 Rust 
                 Scribe 
                 Weathered aluminum 
                 Weathered HD galvanized 
                 Blister size 
                 Blister density 
                 Rust 
                 Adhesion 
                 Mandrel bend 
               
               
                   
               
               
                 001 
                 10 
                 5 
                 10 
                 5 
                 4 
                 3 
                 10 
                 6 
                 10 
                 4 
                 PASS 
               
               
                 002 
                 10 
                 5 
                 10 
                 8 
                 4 
                 4 
                 6 
                 3 
                 10 
                 4 
                 PASS 
               
               
                 003 
                 10 
                 5 
                 10 
                 8 
                 4 
                 3 
                 6 
                 4 
                 9 
                 4 
                 PASS 
               
               
                 004 
                 10 
                 5 
                 10 
                 8 
                 5 
                 2 
                 10 
                 5 
                 10 
                 5 
                 PASS 
               
               
                 005 
                 10 
                 5 
                 10 
                 6 
                 3 
                 0 
                 6 
                 4 
                 9 
                 4 
                 PASS 
               
               
                 006 
                 10 
                 5 
                 10 
                 9 
                 4 
                 1 
                 10 
                 5 
                 10 
                 4 
                 PASS 
               
               
                 007 
                 10 
                 5 
                 10 
                 8 
                 5 
                 3 
                 10 
                 5 
                 10 
                 5 
                 PASS 
               
               
                 008 
                 10 
                 5 
                 10 
                 7 
                 5 
                 3 
                 10 
                 5 
                 9 
                 0 
                 PASS 
               
               
                 009 
                 10 
                 5 
                 10 
                 8 
                 5 
                 3 
                 10 
                 5 
                 9 
                 4 
                 PASS 
               
               
                 010 
                 6 
                 4 
                 9 
                 8 
                 5 
                 2 
                 6 
                 3 
                 9 
                 5 
                 PASS 
               
               
                 011 
                 10 
                 5 
                 10 
                 9 
                 5 
                 0 
                 6 
                 4 
                 10 
                 4 
                 PASS 
               
               
                 012 
                 10 
                 5 
                 10 
                 8 
                 5 
                 1 
                 8 
                 3 
                 9 
                 5 
                 PASS 
               
               
                 013 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 10 
                 5 
                 10 
                 2 
                 PASS 
               
               
                 014 
                 10 
                 5 
                 10 
                 8 
                 5 
                 2 
                 8 
                 2 
                 10 
                 5 
                 PASS 
               
               
                 015 
                 10 
                 5 
                 10 
                 8 
                 5 
                 3 
                 8 
                 3 
                 10 
                 5 
                 PASS 
               
               
                 016 
                 10 
                 5 
                 9 
                 9 
                 5 
                 2 
                 8 
                 4 
                 10 
                 1 
                 PASS 
               
               
                 017 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 6 
                 4 
                 10 
                 5 
                 PASS 
               
               
                 018 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 8 
                 4 
                 9 
                 5 
                 PASS 
               
               
                 019 
                 10 
                 5 
                 10 
                 8 
                 5 
                 3 
                 8 
                 3 
                 10 
                 2 
                 PASS 
               
               
                 020 
                 10 
                 5 
                 10 
                 7 
                 5 
                 3 
                 10 
                 5 
                 9 
                 3 
                 PASS 
               
               
                 021 
                 10 
                 5 
                 10 
                 7 
                 4 
                 4 
                 8 
                 3 
                 9 
                 0 
                 PASS 
               
               
                 022 
                 10 
                 5 
                 10 
                 7 
                 5 
                 3 
                 10 
                 5 
                 10 
                 0 
                 PASS 
               
               
                 023 
                 10 
                 5 
                 9 
                 8 
                 5 
                 2 
                 10 
                 5 
                 10 
                 1 
                 PASS 
               
               
                 031 
                 10 
                 5 
                 10 
                 7 
                 5 
                 4 
                 6 
                 1 
                 10 
                 3 
                 PASS 
               
               
                 032 
                 10 
                 5 
                 10 
                 7 
                 5 
                 4 
                 6 
                 2 
                 9 
                 4 
                 PASS 
               
               
                 033 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 6 
                 2 
                 8 
                 3 
                 PASS 
               
               
                 034 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 4 
                 2 
                 10 
                 4 
                 PASS 
               
               
                 035 
                 10 
                 5 
                 10 
                 9 
                 5 
                 4 
                 6 
                 1 
                 10 
                 3 
                 PASS 
               
               
                 036 
                 10 
                 5 
                 10 
                 6 
                 5 
                 2 
                 6 
                 3 
                 10 
                 4 
                 PASS 
               
               
                 037 
                 10 
                 5 
                 10 
                 9 
                 3 
                 1 
                 8 
                 3 
                 10 
                 3 
                 PASS 
               
               
                 038 
                 10 
                 5 
                 10 
                 8 
                 5 
                 1 
                 6 
                 2 
                 10 
                 3 
                 PASS 
               
               
                 039 
                 10 
                 5 
                 10 
                 8 
                 4 
                 0 
                 4 
                 1 
                 10 
                 4 
                 PASS 
               
               
                 040 
                 10 
                 5 
                 10 
                 8 
                 5 
                 0 
                 6 
                 3 
                 9 
                 3 
                 PASS 
               
               
                 041 
                 10 
                 5 
                 10 
                 5 
                 4 
                 0 
                 6 
                 2 
                 9 
                 3 
                 PASS 
               
               
                 042 
                 10 
                 5 
                 10 
                 8 
                 4 
                 0 
                 4 
                 3 
                 9 
                 4 
                 PASS 
               
               
                 043 
                 10 
                 5 
                 10 
                 8 
                 4 
                 0 
                 6 
                 2 
                 9 
                 4 
                 PASS 
               
               
                 044 
                 10 
                 5 
                 10 
                 8 
                 4 
                 0 
                 8 
                 3 
                 10 
                 4 
                 PASS 
               
               
                 045 
                 10 
                 5 
                 10 
                 8 
                 0 
                 0 
                 4 
                 3 
                 9 
                 3 
                 PASS 
               
               
                 046 
                 10 
                 5 
                 10 
                 7 
                 4 
                 0 
                 6 
                 4 
                 9 
                 4 
                 PASS 
               
               
                 047 
                 10 
                 5 
                 9 
                 7 
                 3 
                 0 
                 6 
                 4 
                 9 
                 4 
                 PASS 
               
               
                 048 
                 10 
                 5 
                 10 
                 6 
                 4 
                 1 
                 10 
                 5 
                 9 
                 4 
                 PASS 
               
               
                 049 
                 10 
                 5 
                 10 
                 8 
                 4 
                 1 
                 6 
                 4 
                 9 
                 3 
                 PASS 
               
               
                 050 
                 10 
                 5 
                 10 
                 7 
                 2 
                 0 
                 4 
                 4 
                 10 
                 3 
                 PASS 
               
               
                 051 
                 10 
                 5 
                 10 
                 9 
                 4 
                 0 
                 6 
                 3 
                 9 
                 4 
                 PASS 
               
               
                 052 
                 10 
                 5 
                 10 
                 9 
                 1 
                 0 
                 10 
                 5 
                 10 
                 4 
                 PASS 
               
               
                 053 
                 10 
                 5 
                 10 
                 9 
                 4 
                 0 
                 8 
                 4 
                 10 
                 5 
                 PASS 
               
               
                 054 
                 10 
                 5 
                 10 
                 7 
                 1 
                 3 
                 4 
                 4 
                 10 
                 4 
                 PASS 
               
               
                 055 
                 10 
                 5 
                 8 
                 7 
                 4 
                 4 
                 10 
                 5 
                 9 
                 4 
                 PASS 
               
               
                 067 
                 10 
                 5 
                 10 
                 8 
                 4 
                 1 
                 6 
                 3 
                 9 
                 3 
                 PASS 
               
               
                 068 
                 10 
                 5 
                 9 
                 8 
                 4 
                 1 
                 6 
                 2 
                 10 
                 5 
                 PASS 
               
               
                 069 
                 10 
                 5 
                 10 
                 9 
                 4 
                 2 
                 8 
                 2 
                 10 
                 3 
                 PASS 
               
               
                 070 
                 10 
                 5 
                 10 
                 8 
                 4 
                 2 
                 6 
                 3 
                 10 
                 3 
                 PASS 
               
               
                 071 
                 10 
                 5 
                 10 
                 7 
                 4 
                 2 
                 8 
                 3 
                 10 
                 3 
                 PASS 
               
               
                 072 
                 10 
                 5 
                 10 
                 8 
                 4 
                 1 
                 6 
                 2 
                 10 
                 0 
                 PASS 
               
               
                 073 
                 10 
                 5 
                 10 
                 8 
                 4 
                 2 
                 6 
                 3 
                 9 
                 2 
                 PASS 
               
               
                 074 
                 10 
                 5 
                 10 
                 6 
                 4 
                 1 
                 6 
                 1 
                 9 
                 0 
                 PASS 
               
               
                 075 
                 10 
                 5 
                 10 
                 8 
                 4 
                 2 
                 8 
                 3 
                 9 
                 0 
                 PASS 
               
               
                 076 
                 10 
                 5 
                 10 
                 8 
                 4 
                 0 
                 6 
                 3 
                 10 
                 4 
                 PASS 
               
               
                 077 
                 10 
                 5 
                 10 
                 8 
                 3 
                 0 
                 6 
                 2 
                 10 
                 2 
                 PASS 
               
               
                 078 
                 10 
                 5 
                 10 
                 7 
                 4 
                 1 
                 4 
                 3 
                 10 
                 4 
                 PASS 
               
               
                 079 
                 10 
                 5 
                 10 
                 6 
                 4 
                 3 
                 4 
                 2 
                 9 
                 3 
                 PASS 
               
               
                 080 
                 10 
                 5 
                 10 
                 8 
                 4 
                 2 
                 4 
                 2 
                 9 
                 0 
                 PASS 
               
               
                 081 
                 10 
                 5 
                 10 
                 8 
                 4 
                 3 
                 6 
                 2 
                 9 
                 0 
                 PASS 
               
               
                 082 
                 10 
                 5 
                 10 
                 8 
                 4 
                 3 
                 6 
                 3 
                 10 
                 0 
                 PASS 
               
               
                 083 
                 10 
                 5 
                 10 
                 8 
                 4 
                 2 
                 6 
                 2 
                 9 
                 0 
                 PASS 
               
               
                 084 
                 10 
                 5 
                 10 
                 8 
                 4 
                 3 
                 6 
                 3 
                 10 
                 3 
                 PASS 
               
               
                 085 
                 10 
                 5 
                 10 
                 7 
                 4 
                 4 
                 4 
                 1 
                 10 
                 3 
                 PASS 
               
               
                 086 
                 10 
                 5 
                 10 
                 9 
                 4 
                 3 
                 4 
                 2 
                 10 
                 3 
                 PASS 
               
               
                 087 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 4 
                 1 
                 10 
                 2 
                 PASS 
               
               
                 088 
                 10 
                 5 
                 10 
                 9 
                 5 
                 3 
                 4 
                 2 
                 10 
                 3 
                 PASS 
               
               
                 Polylon 1900 
                 10 
                 5 
                 10 
                 5 
                 −1 
                 2 
                 10 
                 5 
                 10 
                 0 
                 FAIL 
               
               
                 Centurion 
                 10 
                 5 
                 10 
                 7 
                 5 
                 0 
                 10 
                 5 
                 10 
                 2 
                 PASS 
               
               
                 Sher-cryl 
                 6 
                 4 
                 9 
                 6 
                 4 
                 2 
                 10 
                 5 
                 9 
                 0 
                 FAIL 
               
               
                   
               
             
          
           
               
                   
                 QUV-500 hours 
                 QUV-1000 hrs. 
               
             
          
           
               
                   
                 Gloss (60 degree) 
                 Delta E 
                 Delta b 
                 Gloss (60 degree) 
                 Delta E 
                 Delta b 
               
             
          
           
               
                 Formula 
                 Initial 
                 at 500 hrs 
                 % change 
                 Initial 
                 at 500 hrs 
                 change 
                 Initial 
                 at 500 hrs 
                 change 
                 1000 hour 
                 % change 
                 Delta E 
                 change 
                 Delta b 
                 change 
               
               
                   
               
               
                 001 
                 32.60 
                 21.10 
                 −35.26 
                 0.94 
                 3.23 
                 2.29 
                 −0.85 
                 1.65 
                 2.40 
                 17.90 
                 −45.09 
                 2.88 
                 1.94 
                 1.13 
                 1.98 
               
               
                 002 
                 56.50 
                 40.10 
                 −29.03 
                 2.69 
                 5.10 
                 2.41 
                 0.41 
                 2.79 
                 2.38 
                 37.10 
                 −34.34 
                 5.70 
                 3.01 
                 2.95 
                 2.54 
               
               
                 003 
                 65.70 
                 50.70 
                 −22.83 
                 1.61 
                 2.72 
                 0.91 
                 0.79 
                 1.42 
                 0.63 
                 48.20 
                 −26.64 
                 3.02 
                 1.21 
                 1.25 
                 0.46 
               
               
                 004 
                 49.60 
                 29.60 
                 −39.92 
                 1.17 
                 2.66 
                 1.49 
                 −1.00 
                 1.36 
                 2.38 
                 26.50 
                 −46.57 
                 2.66 
                 1.49 
                 0.93 
                 1.93 
               
               
                 005 
                 61.00 
                 47.00 
                 −22.95 
                 2.05 
                 3.44 
                 1.39 
                 −0.36 
                 1.92 
                 2.28 
                 45.60 
                 −25.25 
                 4.04 
                 1.89 
                 1.84 
                 2.20 
               
               
                 006 
                 51.00 
                 35.80 
                 −29.80 
                 1.34 
                 3.16 
                 1.82 
                 −0.46 
                 1.76 
                 2.22 
                 32.80 
                 −35.69 
                 3.62 
                 2.28 
                 1.70 
                 2.16 
               
               
                 007 
                 69.40 
                 33.30 
                 −52.02 
                 1.61 
                 2.49 
                 0.68 
                 0.04 
                 1.43 
                 1.39 
                 21.90 
                 −68.44 
                 4.09 
                 2.28 
                 2.22 
                 2.16 
               
               
                 008 
                 70.30 
                 30.50 
                 −56.61 
                 1.17 
                 1.41 
                 0.24 
                 −0.32 
                 0.83 
                 1.15 
                 21.20 
                 −69.84 
                 2.58 
                 1.41 
                 1.22 
                 1.54 
               
               
                 009 
                 68.30 
                 21.90 
                 −67.94 
                 1.06 
                 1.98 
                 0.92 
                 −0.31 
                 1.06 
                 1.37 
                 15.20 
                 −77.75 
                 2.44 
                 1.38 
                 1.09 
                 1.40 
               
               
                 010 
                 52.00 
                 13.60 
                 −73.46 
                 1.05 
                 3.14 
                 2.09 
                 0.01 
                 1.83 
                 1.82 
                 9.80 
                 −51.15 
                 4.00 
                 2.95 
                 2.07 
                 2.06 
               
               
                 011 
                 40.60 
                 10.40 
                 −74.38 
                 0.26 
                 3.03 
                 2.77 
                 −0.13 
                 1.75 
                 1.88 
                 7.50 
                 −81.53 
                 3.85 
                 3.59 
                 1.97 
                 2.10 
               
               
                 012 
                 59.30 
                 16.50 
                 −72.18 
                 0.73 
                 1.95 
                 1.22 
                 −0.45 
                 0.95 
                 1.40 
                 12.70 
                 −78.58 
                 2.75 
                 2.02 
                 1.17 
                 1.62 
               
               
                 013 
                 46.80 
                 15.00 
                 −67.95 
                 1.31 
                 2.83 
                 1.52 
                 0.05 
                 1.60 
                 1.55 
                 12.30 
                 −73.72 
                 3.40 
                 2.09 
                 1.79 
                 1.74 
               
               
                 014 
                 69.10 
                 19.60 
                 −71.64 
                 1.10 
                 2.45 
                 1.35 
                 −0.32 
                 1.38 
                 1.70 
                 15.90 
                 −76.99 
                 3.01 
                 1.91 
                 1.56 
                 1.88 
               
               
                 015 
                 66.10 
                 18.20 
                 −72.47 
                 1.00 
                 2.01 
                 1.01 
                 −0.29 
                 1.03 
                 1.32 
                 15.50 
                 −76.55 
                 2.29 
                 1.29 
                 1.12 
                 1.41 
               
               
                 016 
                 70.70 
                 19.70 
                 −72.14 
                 1.39 
                 1.88 
                 0.49 
                 −0.44 
                 0.94 
                 1.36 
                 18.10 
                 −74.40 
                 2.36 
                 0.97 
                 1.12 
                 1.56 
               
               
                 017 
                 59.30 
                 14.50 
                 −75.55 
                 0.61 
                 1.80 
                 1.19 
                 −0.48 
                 0.66 
                 1.32 
                 12.30 
                 −79.26 
                 2.40 
                 1.79 
                 0.96 
                 1.42 
               
               
                 018 
                 69.00 
                 19.00 
                 −72.46 
                 0.92 
                 2.01 
                 1.09 
                 −0.28 
                 1.10 
                 1.35 
                 15.90 
                 −76.96 
                 2.58 
                 1.66 
                 1.24 
                 1.50 
               
               
                 019 
                 49.20 
                 12.90 
                 −73.78 
                 0.45 
                 2.25 
                 1.80 
                 −0.30 
                 1.16 
                 1.46 
                 10.40 
                 −78.86 
                 2.54 
                 2.09 
                 1.20 
                 1.50 
               
               
                 020 
                 68.70 
                 21.10 
                 −69.29 
                 1.37 
                 2.09 
                 0.72 
                 −0.29 
                 1.17 
                 1.46 
                 16.40 
                 −76.13 
                 2.72 
                 1.35 
                 1.32 
                 1.61 
               
               
                 021 
                 70.70 
                 22.00 
                 −68.88 
                 1.57 
                 2.34 
                 0.77 
                 −0.10 
                 1.24 
                 1.34 
                 14.90 
                 −78.93 
                 2.87 
                 1.30 
                 1.44 
                 1.54 
               
               
                 022 
                 67.80 
                 21.70 
                 −67.99 
                 1.31 
                 2.79 
                 1.48 
                 0.06 
                 1.63 
                 1.57 
                 16.00 
                 −76.40 
                 3.51 
                 2.20 
                 1.82 
                 1.76 
               
               
                 023 
                 71.80 
                 22.10 
                 −69.22 
                 1.31 
                 1.87 
                 0.56 
                 0.06 
                 0.95 
                 0.89 
                 23.20 
                 −67.69 
                 2.59 
                 1.28 
                 1.22 
                 1.16 
               
               
                 031 
                 57.70 
                 37.60 
                 −35.01 
                 1.65 
                 1.38 
                 0.27 
                 −0.98 
                 0.65 
                 1.63 
                 35.90 
                 −37.78 
                 1.42 
                 0.23 
                 0.60 
                 1.58 
               
               
                 032 
                 68.70 
                 47.10 
                 −31.44 
                 1.61 
                 0.77 
                 0.84 
                 1.33 
                 0.15 
                 1.45 
                 54.90 
                 −20.09 
                 0.75 
                 0.86 
                 0.02 
                 1.35 
               
               
                 033 
                 47.10 
                 29.00 
                 −38.43 
                 1.38 
                 2.19 
                 0.81 
                 −0.89 
                 1.24 
                 2.13 
                 26.10 
                 −44.59 
                 1.93 
                 0.55 
                 1.06 
                 1.95 
               
               
                 034 
                 60.90 
                 44.40 
                 −27.09 
                 1.88 
                 1.79 
                 0.09 
                 −0.61 
                 0.86 
                 1.47 
                 47.80 
                 −21.51 
                 2.51 
                 0.63 
                 1.24 
                 1.65 
               
               
                 035 
                 52.50 
                 38.00 
                 −31.43 
                 1.42 
                 0.73 
                 0.69 
                 −1.18 
                 0.21 
                 1.39 
                 38.70 
                 −30.10 
                 1.33 
                 0.09 
                 0.41 
                 1.59 
               
               
                 036 
                 53.00 
                 40.00 
                 −24.53 
                 1.29 
                 1.18 
                 0.11 
                 −0.86 
                 0.59 
                 1.45 
                 39.20 
                 −26.04 
                 1.63 
                 0.34 
                 0.82 
                 1.66 
               
               
                 037 
                 51.80 
                 41.70 
                 −19.50 
                 1.78 
                 2.45 
                 0.67 
                 −0.82 
                 1.40 
                 2.22 
                 43.60 
                 −15.83 
                 2.30 
                 0.52 
                 1.08 
                 1.90 
               
               
                 038 
                 68.80 
                 57.30 
                 −14.22 
                 1.40 
                 1.36 
                 0.04 
                 −0.81 
                 0.65 
                 1.46 
                 58.70 
                 −12.13 
                 1.81 
                 0.41 
                 0.90 
                 1.71 
               
               
                 039 
                 60.00 
                 48.30 
                 −19.50 
                 1.86 
                 1.61 
                 0.25 
                 −0.80 
                 0.82 
                 1.82 
                 50.70 
                 −15.50 
                 1.89 
                 0.03 
                 0.92 
                 1.72 
               
               
                 040 
                 63.20 
                 47.60 
                 −24.68 
                 1.49 
                 1.37 
                 0.12 
                 −1.05 
                 0.71 
                 1.76 
                 49.40 
                 −21.84 
                 1.54 
                 0.05 
                 0.76 
                 1.81 
               
               
                 041 
                 60.50 
                 43.40 
                 −28.26 
                 1.63 
                 1.49 
                 0.14 
                 −0.83 
                 0.81 
                 1.64 
                 44.80 
                 −25.95 
                 2.12 
                 0.49 
                 1.19 
                 2.02 
               
               
                 042 
                 60.70 
                 40.50 
                 −33.28 
                 1.29 
                 1.82 
                 0.53 
                 −0.95 
                 0.89 
                 1.64 
                 40.00 
                 −34.10 
                 2.09 
                 0.80 
                 0.90 
                 1.85 
               
               
                 043 
                 55.20 
                 36.20 
                 −34.42 
                 1.36 
                 2.38 
                 1.02 
                 −0.88 
                 1.20 
                 2.08 
                 31.80 
                 −42.39 
                 2.67 
                 1.31 
                 1.34 
                 2.22 
               
               
                 044 
                 41.70 
                 23.80 
                 −42.93 
                 1.17 
                 2.51 
                 1.34 
                 −1.00 
                 1.21 
                 2.21 
                 20.10 
                 −51.80 
                 3.09 
                 1.92 
                 1.33 
                 2.33 
               
               
                 045 
                 63.20 
                 46.90 
                 −25.79 
                 1.48 
                 1.87 
                 0.39 
                 −1.15 
                 0.80 
                 1.95 
                 43.40 
                 −31.33 
                 1.79 
                 0.31 
                 0.74 
                 1.89 
               
               
                 046 
                 38.40 
                 25.60 
                 −33.33 
                 1.14 
                 2.33 
                 1.19 
                 −1.03 
                 1.04 
                 2.07 
                 25.20 
                 −34.38 
                 2.27 
                 1.13 
                 0.89 
                 1.92 
               
               
                 047 
                 63.00 
                 48.60 
                 −22.54 
                 1.52 
                 1.85 
                 0.33 
                 −1.15 
                 0.61 
                 1.96 
                 49.30 
                 −21.75 
                 1.47 
                 0.05 
                 0.49 
                 1.64 
               
               
                 048 
                 61.10 
                 42.50 
                 −30.44 
                 1.13 
                 2.28 
                 1.15 
                 −1.04 
                 1.02 
                 2.06 
                 40.80 
                 −33.22 
                 2.13 
                 1.00 
                 0.77 
                 1.81 
               
               
                 049 
                 64.60 
                 45.00 
                 −30.34 
                 1.43 
                 2.24 
                 0.81 
                 −1.25 
                 0.72 
                 1.97 
                 42.00 
                 −34.98 
                 1.81 
                 0.38 
                 0.41 
                 1.66 
               
               
                 050 
                 51.80 
                 30.10 
                 −41.89 
                 1.37 
                 2.28 
                 0.91 
                 −1.14 
                 0.60 
                 1.94 
                 28.70 
                 −44.59 
                 2.18 
                 0.81 
                 0.67 
                 1.81 
               
               
                 051 
                 61.70 
                 44.90 
                 −27.23 
                 1.41 
                 2.00 
                 0.69 
                 −1.09 
                 0.85 
                 1.94 
                 45.00 
                 −27.07 
                 1.69 
                 0.26 
                 0.54 
                 1.63 
               
               
                 052 
                 58.00 
                 42.40 
                 −26.90 
                 1.44 
                 2.83 
                 1.39 
                 −0.72 
                 1.35 
                 2.07 
                 43.50 
                 −25.00 
                 2.64 
                 1.20 
                 1.16 
                 1.88 
               
               
                 053 
                 58.00 
                 40.40 
                 −30.34 
                 1.20 
                 2.79 
                 1.59 
                 −0.87 
                 1.35 
                 2.22 
                 39.40 
                 −32.07 
                 2.69 
                 1.49 
                 1.17 
                 2.04 
               
               
                 054 
                 48.10 
                 30.60 
                 −36.38 
                 1.28 
                 2.50 
                 1.22 
                 −1.11 
                 1.05 
                 2.16 
                 29.10 
                 −39.50 
                 2.18 
                 0.90 
                 0.76 
                 1.87 
               
               
                 055 
                 37.50 
                 27.00 
                 −28.00 
                 0.98 
                 3.18 
                 2.20 
                 −0.75 
                 1.58 
                 2.33 
                 25.70 
                 −31.47 
                 3.08 
                 2.10 
                 1.49 
                 2.24 
               
               
                 067 
                 67.60 
                 39.00 
                 −42.48 
                 1.21 
                 0.98 
                 0.23 
                 −1.08 
                 0.45 
                 1.53 
                 26.40 
                 −61.06 
                 1.92 
                 0.71 
                 0.73 
                 1.81 
               
               
                 068 
                 72.60 
                 42.90 
                 −40.91 
                 1.38 
                 1.78 
                 0.40 
                 −0.58 
                 0.98 
                 1.54 
                 36.10 
                 −50.28 
                 2.75 
                 1.37 
                 1.46 
                 2.02 
               
               
                 069 
                 73.70 
                 43.70 
                 −40.71 
                 1.61 
                 1.33 
                 0.28 
                 −0.92 
                 0.83 
                 1.55 
                 42.70 
                 −42.06 
                 2.00 
                 0.39 
                 1.00 
                 1.92 
               
               
                 070 
                 73.10 
                 40.50 
                 −44.60 
                 1.15 
                 1.23 
                 0.08 
                 −0.81 
                 0.71 
                 1.52 
                 30.10 
                 −58.82 
                 2.28 
                 1.13 
                 1.16 
                 1.97 
               
               
                 071 
                 70.40 
                 34.40 
                 −51.14 
                 1.18 
                 1.22 
                 0.04 
                 −0.89 
                 0.65 
                 1.54 
                 32.40 
                 −53.98 
                 2.03 
                 0.85 
                 1.00 
                 1.89 
               
               
                 072 
                 72.00 
                 39.80 
                 −44.72 
                 1.43 
                 0.86 
                 0.57 
                 −1.04 
                 0.39 
                 1.43 
                 33.50 
                 −53.47 
                 1.62 
                 0.19 
                 0.75 
                 1.79 
               
               
                 073 
                 70.90 
                 33.40 
                 −52.69 
                 1.23 
                 0.95 
                 0.28 
                 −1.10 
                 0.35 
                 1.45 
                 34.30 
                 −51.62 
                 1.71 
                 0.48 
                 0.62 
                 1.72 
               
               
                 074 
                 71.80 
                 35.70 
                 −50.28 
                 1.43 
                 1.16 
                 0.27 
                 −0.83 
                 0.67 
                 1.50 
                 29.40 
                 −59.05 
                 1.98 
                 0.55 
                 0.94 
                 1.77 
               
               
                 075 
                 69.70 
                 35.30 
                 −49.35 
                 1.06 
                 1.00 
                 0.06 
                 −0.86 
                 0.87 
                 1.43 
                 36.60 
                 −47.20 
                 1.61 
                 0.55 
                 0.67 
                 1.53 
               
               
                 076 
                 59.40 
                 37.50 
                 −36.67 
                 1.38 
                 1.56 
                 0.18 
                 −0.82 
                 0.94 
                 1.76 
                 43.50 
                 −26.77 
                 2.26 
                 0.88 
                 1.09 
                 1.91 
               
               
                 077 
                 70.00 
                 34.60 
                 −50.57 
                 1.37 
                 1.76 
                 0.39 
                 −0.77 
                 0.93 
                 1.70 
                 30.80 
                 −56.00 
                 2.16 
                 0.81 
                 1.02 
                 1.79 
               
               
                 078 
                 89.20 
                 33.30 
                 −51.88 
                 1.46 
                 1.70 
                 0.24 
                 −0.82 
                 0.90 
                 1.72 
                 30.10 
                 −56.50 
                 2.03 
                 0.57 
                 1.19 
                 2.01 
               
               
                 079 
                 66.50 
                 33.60 
                 −49.47 
                 1.61 
                 1.48 
                 0.13 
                 −0.68 
                 0.99 
                 1.67 
                 31.60 
                 −52.48 
                 2.07 
                 0.46 
                 1.07 
                 1.75 
               
               
                 080 
                 69.70 
                 33.20 
                 −52.37 
                 1.42 
                 1.64 
                 0.22 
                 −0.82 
                 0.78 
                 1.58 
                 32.00 
                 −54.09 
                 1.68 
                 0.24 
                 0.80 
                 1.62 
               
               
                 081 
                 69.70 
                 33.80 
                 −51.51 
                 1.48 
                 1.46 
                 0.02 
                 −0.90 
                 0.78 
                 1.68 
                 32.10 
                 −53.95 
                 1.97 
                 0.49 
                 1.02 
                 1.92 
               
               
                 082 
                 64.90 
                 30.20 
                 −53.47 
                 1.43 
                 1.81 
                 0.38 
                 −0.95 
                 0.92 
                 1.87 
                 29.10 
                 −55.16 
                 2.34 
                 0.91 
                 1.27 
                 2.22 
               
               
                 083 
                 72.10 
                 32.40 
                 −55.06 
                 1.33 
                 1.67 
                 0.34 
                 −0.77 
                 0.90 
                 1.67 
                 26.20 
                 −63.66 
                 1.86 
                 0.53 
                 0.92 
                 1.89 
               
               
                 084 
                 72.40 
                 33.10 
                 −54.28 
                 1.57 
                 2.02 
                 0.45 
                 −0.70 
                 1.00 
                 1.70 
                 32.70 
                 −54.83 
                 2.26 
                 0.69 
                 1.20 
                 1.90 
               
               
                 085 
                 64.90 
                 40.30 
                 −37.90 
                 1.61 
                 0.92 
                 0.69 
                 −1.11 
                 0.34 
                 1.45 
                 45.30 
                 −30.20 
                 0.88 
                 0.75 
                 0.32 
                 1.43 
               
               
                 086 
                 62.20 
                 37.30 
                 −40.03 
                 1.55 
                 1.08 
                 0.47 
                 −1.24 
                 0.43 
                 1.67 
                 37.10 
                 −40.35 
                 0.99 
                 0.56 
                 0.28 
                 1.52 
               
               
                 087 
                 66.60 
                 40.40 
                 −39.34 
                 1.51 
                 0.66 
                 0.85 
                 −1.26 
                 0.19 
                 1.45 
                 40.70 
                 −38.89 
                 0.83 
                 0.68 
                 0.21 
                 1.47 
               
               
                 088 
                 54.40 
                 35.50 
                 −34.74 
                 1.64 
                 0.87 
                 0.67 
                 −1.12 
                 0.36 
                 1.48 
                 36.50 
                 −32.90 
                 1.21 
                 0.33 
                 −0.46 
                 0.66 
               
               
                 Polylon 1900 
                 94.50 
                 94.50 
                 0.00 
                 4.40 
                 4.80 
                 0.40 
                 0.14 
                 0.73 
                 0.59 
                 91.60 
                 −3.07 
                 4.96 
                 0.56 
                 0.70 
                 0.56 
               
               
                 Centurion 
                 56.20 
                 17.70 
                 −68.51 
                 10.09 
                 11.42 
                 1.33 
                 0.81 
                 3.56 
                 2.75 
                 12.30 
                 −78.11 
                 11.92 
                 1.63 
                 3.42 
                 2.61 
               
               
                 Sher-cryl 
                 80.60 
                 72.30 
                 −10.30 
                 5.76 
                 6.25 
                 0.49 
                 2.43 
                 1.53 
                 −0.90 
                 51.90 
                 −35.61 
                 6.34 
                 0.58 
                 1.22 
                 −1.21 
               
               
                 700T 
                 31.80 
                 13.30 
                 −56.18 
                 0.14 
                 0.45 
                 0.31 
                 0.11 
                 −0.41 
                 −0.52 
                 11.20 
                 −64.78 
                 0.52 
                 0.36 
                 −0.10 
                 −0.21 
               
               
                 HS+ 
                 86.50 
                 69.80 
                 −19.31 
                 3.04 
                 4.02 
                 0.98 
                 3.89 
                 2.63 
                 −1.38 
                 82.90 
                 −4.16 
                 4.11 
                 1.07 
                 2.59 
                 −1.30 
               
               
                   
               
             
          
           
               
                   
                 Early Blister Resistance 
                   
               
             
          
           
               
                   
                 2 Hour 
                 4 Hour 
                 5 Hour 
                 Corrosion Weathering (5 cycle 
                 Corrosion Weathering (6 cycles 
               
             
          
           
               
                   
                   
                 Blister 
                   
                   
                 Blister 
                   
                   
                 Blister 
                   
                   
                 Blister 
                   
                   
                   
                 Blister 
                   
                   
               
               
                 Formula 
                 Blister Size 
                 Density 
                 Rust 
                 Blister Size 
                 Density 
                 Rust 
                 Blister Size 
                 Density 
                 Rust 
                 Blister Size 
                 Density 
                 Rust 
                 Scribe 
                 Blister Size 
                 Density 
                 Rust 
                 Scribe 
               
               
                   
               
               
                 001 
                 4 
                 3 
                 2 
                 2 
                 2 
                 3 
                 4 
                 2 
                 4 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 6 
               
               
                 002 
                 2 
                 3 
                 1 
                 2 
                 2 
                 3 
                 10 
                 5 
                 2 
                 10 
                 5 
                 10 
                 7 
                 10 
                 5 
                 10 
                 8 
               
               
                 003 
                 10 
                 5 
                 1 
                 2 
                 3 
                 2 
                 2 
                 3 
                 3 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 6 
               
               
                 004 
                 6 
                 3 
                 2 
                 4 
                 3 
                 1 
                 6 
                 1 
                 2 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 9 
                 6 
               
               
                 005 
                 10 
                 5 
                 1 
                 4 
                 3 
                 2 
                 4 
                 3 
                 2 
                 10 
                 5 
                 8 
                 6 
                 6 
                 3 
                 8 
                 6 
               
               
                 006 
                 4 
                 3 
                 1 
                 2 
                 3 
                 2 
                 6 
                 3 
                 2 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 7 
               
               
                 007 
                 10 
                 5 
                 9 
                 10 
                 5 
                 9 
                 6 
                 3 
                 8 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 008 
                 10 
                 5 
                 9 
                 10 
                 5 
                 9 
                 2 
                 4 
                 10 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 8 
                 7 
               
               
                 009 
                 10 
                 5 
                 9 
                 10 
                 5 
                 9 
                 6 
                 2 
                 8 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 9 
                 7 
               
               
                 010 
                 10 
                 5 
                 8 
                 10 
                 5 
                 8 
                 6 
                 3 
                 8 
                 6 
                 4 
                 8 
                 7 
                 6 
                 4 
                 9 
                 7 
               
               
                 011 
                 10 
                 5 
                 8 
                 10 
                 5 
                 9 
                 4 
                 2 
                 8 
                 10 
                 5 
                 8 
                 8 
                 10 
                 5 
                 10 
                 9 
               
               
                 012 
                 4 
                 4 
                 3 
                 10 
                 5 
                 9 
                 6 
                 3 
                 9 
                 10 
                 5 
                 6 
                 6 
                 10 
                 5 
                 10 
                 6 
               
               
                 013 
                 10 
                 5 
                 9 
                 10 
                 5 
                 9 
                 6 
                 3 
                 9 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 9 
                 9 
               
               
                 014 
                 4 
                 2 
                 4 
                 4 
                 3 
                 10 
                 4 
                 3 
                 8 
                 10 
                 5 
                 8 
                 7 
                 8 
                 4 
                 10 
                 8 
               
               
                 015 
                 4 
                 4 
                 6 
                 4 
                 4 
                 9 
                 4 
                 3 
                 8 
                 10 
                 5 
                 8 
                 8 
                 10 
                 5 
                 9 
                 8 
               
               
                 016 
                 10 
                 5 
                 8 
                 6 
                 4 
                 9 
                 6 
                 2 
                 8 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 9 
                 7 
               
               
                 017 
                 10 
                 5 
                 8 
                 10 
                 5 
                 9 
                 6 
                 2 
                 8 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 9 
                 9 
               
               
                 018 
                 10 
                 5 
                 9 
                 4 
                 3 
                 9 
                 4 
                 3 
                 8 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 8 
               
               
                 019 
                 10 
                 5 
                 9 
                 4 
                 3 
                 9 
                 4 
                 1 
                 10 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 9 
                 8 
               
               
                 020 
                 10 
                 5 
                 6 
                 6 
                 3 
                 6 
                 4 
                 2 
                 7 
                 10 
                 5 
                 9 
                 6 
                 10 
                 5 
                 10 
                 6 
               
               
                 021 
                 10 
                 5 
                 9 
                 6 
                 3 
                 8 
                 6 
                 3 
                 7 
                 10 
                 5 
                 7 
                 7 
                 10 
                 5 
                 9 
                 8 
               
               
                 022 
                 10 
                 5 
                 9 
                 10 
                 5 
                 9 
                 4 
                 1 
                 8 
                 10 
                 5 
                 9 
                 7 
                 8 
                 4 
                 10 
                 8 
               
               
                 023 
                 10 
                 5 
                 2 
                 10 
                 5 
                 8 
                 6 
                 3 
                 6 
                 10 
                 5 
                 7 
                 7 
                 10 
                 5 
                 9 
                 8 
               
               
                 031 
                 2 
                 3 
                 2 
                 2 
                 1 
                 3 
                 2 
                 1 
                 5 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 032 
                 2 
                 2 
                 2 
                 4 
                 1 
                 4 
                 4 
                 1 
                 5 
                 10 
                 5 
                 8 
                 8 
                 10 
                 5 
                 10 
                 6 
               
               
                 033 
                 2 
                 3 
                 2 
                 2 
                 2 
                 4 
                 2 
                 2 
                 5 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 10 
                 6 
               
               
                 034 
                 2 
                 2 
                 1 
                 2 
                 1 
                 6 
                 2 
                 1 
                 5 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 8 
               
               
                 035 
                 2 
                 3 
                 1 
                 2 
                 1 
                 4 
                 2 
                 1 
                 5 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 7 
               
               
                 036 
                 2 
                 2 
                 2 
                 2 
                 1 
                 5 
                 2 
                 1 
                 6 
                 10 
                 5 
                 9 
                 6 
                 8 
                 3 
                 10 
                 7 
               
               
                 037 
                 2 
                 2 
                 1 
                 2 
                 3 
                 3 
                 2 
                 3 
                 10 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 8 
               
               
                 038 
                 8 
                 3 
                 3 
                 2 
                 1 
                 5 
                 2 
                 2 
                 6 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 8 
               
               
                 039 
                 2 
                 1 
                 2 
                 2 
                 1 
                 3 
                 2 
                 1 
                 7 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 6 
               
               
                 040 
                 2 
                 3 
                 1 
                 4 
                 1 
                 4 
                 4 
                 2 
                 5 
                 10 
                 5 
                 7 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 041 
                 2 
                 3 
                 3 
                 2 
                 1 
                 5 
                 4 
                 1 
                 4 
                 10 
                 5 
                 7 
                 6 
                 10 
                 5 
                 10 
                 4 
               
               
                 042 
                 6 
                 3 
                 1 
                 2 
                 3 
                 2 
                 4 
                 2 
                 3 
                 10 
                 5 
                 8 
                 8 
                 10 
                 5 
                 10 
                 9 
               
               
                 043 
                 4 
                 2 
                 1 
                 2 
                 3 
                 2 
                 4 
                 3 
                 3 
                 10 
                 5 
                 8 
                 8 
                 10 
                 5 
                 9 
                 6 
               
               
                 044 
                 4 
                 2 
                 1 
                 4 
                 3 
                 1 
                 4 
                 3 
                 3 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 9 
                 7 
               
               
                 045 
                 2 
                 3 
                 1 
                 2 
                 2 
                 2 
                 2 
                 3 
                 4 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 9 
                 7 
               
               
                 046 
                 6 
                 3 
                 1 
                 6 
                 3 
                 2 
                 4 
                 2 
                 3 
                 10 
                 5 
                 9 
                 6 
                 10 
                 5 
                 10 
                 5 
               
               
                 047 
                 2 
                 2 
                 1 
                 4 
                 2 
                 2 
                 4 
                 2 
                 3 
                 10 
                 5 
                 7 
                 7 
                 10 
                 5 
                 9 
                 6 
               
               
                 048 
                 2 
                 3 
                 1 
                 2 
                 2 
                 2 
                 4 
                 2 
                 3 
                 10 
                 5 
                 6 
                 7 
                 10 
                 5 
                 10 
                 6 
               
               
                 049 
                 4 
                 3 
                 1 
                 4 
                 2 
                 3 
                 4 
                 2 
                 4 
                 10 
                 5 
                 9 
                 6 
                 10 
                 5 
                 10 
                 7 
               
               
                 050 
                 2 
                 3 
                 1 
                 2 
                 3 
                 2 
                 2 
                 2 
                 3 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 051 
                 2 
                 3 
                 1 
                 4 
                 2 
                 2 
                 4 
                 2 
                 3 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 9 
               
               
                 052 
                 10 
                 5 
                 1 
                 6 
                 3 
                 2 
                 6 
                 3 
                 1 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 10 
                 8 
               
               
                 053 
                 4 
                 3 
                 1 
                 2 
                 2 
                 2 
                 2 
                 3 
                 3 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 10 
                 9 
               
               
                 054 
                 2 
                 1 
                 1 
                 2 
                 2 
                 3 
                 2 
                 2 
                 4 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 055 
                 2 
                 3 
                 1 
                 4 
                 2 
                 3 
                 4 
                 3 
                 6 
                 10 
                 5 
                 5 
                 6 
                 8 
                 4 
                 8 
                 6 
               
               
                 067 
                 2 
                 1 
                 1 
                 2 
                 1 
                 5 
                 2 
                 1 
                 10 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 6 
               
               
                 068 
                 2 
                 2 
                 2 
                 2 
                 2 
                 6 
                 2 
                 1 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 9 
                 6 
               
               
                 069 
                 2 
                 1 
                 4 
                 2 
                 1 
                 10 
                 2 
                 1 
                 10 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 8 
               
               
                 070 
                 2 
                 1 
                 2 
                 2 
                 1 
                 10 
                 2 
                 2 
                 10 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 7 
               
               
                 071 
                 2 
                 3 
                 4 
                 2 
                 2 
                 10 
                 4 
                 1 
                 10 
                 10 
                 5 
                 6 
                 7 
                 10 
                 5 
                 10 
                 6 
               
               
                 072 
                 2 
                 1 
                 1 
                 2 
                 2 
                 4 
                 2 
                 1 
                 10 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 10 
                 8 
               
               
                 073 
                 2 
                 1 
                 2 
                 2 
                 1 
                 10 
                 2 
                 2 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 6 
                 9 
                 7 
               
               
                 074 
                 2 
                 1 
                 4 
                 2 
                 1 
                 7 
                 2 
                 1 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 6 
                 9 
                 8 
               
               
                 075 
                 2 
                 1 
                 6 
                 2 
                 1 
                 10 
                 2 
                 1 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 9 
                 6 
               
               
                 076 
                 2 
                 1 
                 10 
                 4 
                 2 
                 10 
                 4 
                 2 
                 10 
                 10 
                 5 
                 8 
                 8 
                 10 
                 5 
                 10 
                 7 
               
               
                 077 
                 2 
                 1 
                 3 
                 2 
                 1 
                 10 
                 2 
                 4 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 078 
                 2 
                 1 
                 4 
                 2 
                 1 
                 8 
                 2 
                 1 
                 10 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 10 
                 7 
               
               
                 079 
                 2 
                 1 
                 5 
                 2 
                 1 
                 9 
                 2 
                 1 
                 10 
                 10 
                 5 
                 7 
                 7 
                 10 
                 5 
                 9 
                 6 
               
               
                 080 
                 2 
                 1 
                 7 
                 2 
                 1 
                 10 
                 2 
                 2 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 9 
                 7 
               
               
                 081 
                 2 
                 1 
                 10 
                 2 
                 1 
                 10 
                 4 
                 2 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 8 
               
               
                 082 
                 2 
                 1 
                 10 
                 2 
                 1 
                 10 
                 2 
                 2 
                 10 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 9 
                 8 
               
               
                 083 
                 2 
                 1 
                 4 
                 2 
                 1 
                 10 
                 2 
                 1 
                 10 
                 10 
                 5 
                 10 
                 7 
                 10 
                 5 
                 10 
                 8 
               
               
                 084 
                 2 
                 4 
                 10 
                 2 
                 1 
                 10 
                 2 
                 2 
                 10 
                 10 
                 5 
                 8 
                 7 
                 10 
                 5 
                 9 
                 7 
               
               
                 085 
                 2 
                 2 
                 2 
                 2 
                 1 
                 3 
                 2 
                 2 
                 6 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 10 
                 6 
               
               
                 086 
                 2 
                 1 
                 3 
                 2 
                 1 
                 3 
                 2 
                 1 
                 4 
                 10 
                 5 
                 10 
                 8 
                 10 
                 5 
                 10 
                 9 
               
               
                 087 
                 2 
                 2 
                 3 
                 2 
                 2 
                 3 
                 4 
                 2 
                 4 
                 10 
                 5 
                 9 
                 7 
                 10 
                 5 
                 10 
                 7 
               
               
                 088 
                 2 
                 3 
                 2 
                 4 
                 2 
                 4 
                 4 
                 3 
                 8 
                 10 
                 5 
                 8 
                 6 
                 10 
                 5 
                 9 
                 7 
               
               
                 Polylon 1900 
                 2 
                 4(GL) 
                 10 
                 2 
                 4 
                 10 
                 10 
                 5 
                 10 
                 10 
                 5 
                 10 
                 6 
                 10 
                 5 
                 10 
                 6 
               
               
                 Centurion 
                 2 
                 4(GL) 
                 10 
                 10 
                 5(GL) 
                 10 
                 10 
                 5 
                 10 
                 10 
                 5 
                 9 
                 8 
                 10 
                 5 
                 10 
                 7 
               
               
                 Sher-cryl 
                 10 
                 5(GL) 
                 10 
                 10 
                 5(GL) 
                 10 
                 10 
                 5 
                 10 
                 8 
                 4 
                 6 
                 6 
                 8 
                 3 
                 8 
                 5 
               
               
                   
               
             
          
           
               
                   
                 Viscosity, settling, and pH Stability (6 weeks at 140 F.) 
               
             
          
           
               
                 Formula 
                 initial KU 
                 final KU 
                 % change 
                 initial ICI 
                 final ICI 
                 % change 
                 initial pH 
                 final pH 
                 % change 
                 settling amount 
                 settling type 
               
               
                   
               
               
                 001 
                 96 
                 gelled 
                   
                 1.6 
                 gelled 
                   
                 9.58 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 002 
                 140 
                 gelled 
                   
                 1.18 
                 gelled 
                   
                 9.59 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 003 
                 94 
                 gelled 
                   
                 1.16 
                 gelled 
                   
                 9.43 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 004 
                 79 
                 gelled 
                   
                 1.88 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 005 
                 136 
                 gelled 
                   
                 0.59 
                 gelled 
                   
                 9.61 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 006 
                 108 
                 gelled 
                   
                 1.83 
                 gelled 
                   
                 9.3 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 007 
                 91 
                 gelled 
                   
                 1.66 
                 gelled 
                   
                 9.48 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 008 
                 95 
                 gelled 
                   
                 1.88 
                 gelled 
                   
                 9.32 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 009 
                 68 
                 gelled 
                   
                 1.11 
                 gelled 
                   
                 9.42 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 010 
                 85 
                 gelled 
                   
                 0.492 
                 gelled 
                   
                 9.09 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 011 
                 83 
                 gelled 
                   
                 9.42 
                 gelled 
                   
                 9.14 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 012 
                 69 
                 gelled 
                   
                 0.66 
                 gelled 
                   
                 9.45 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 013 
                 74 
                 gelled 
                   
                 0.77 
                 gelled 
                   
                 9.32 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 014 
                 88 
                 gelled 
                   
                 0.56 
                 gelled 
                   
                 9.56 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 015 
                 61 
                 gelled 
                   
                 1.17 
                 gelled 
                   
                 9.52 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 016 
                 68 
                 gelled 
                   
                 1.12 
                 gelled 
                   
                 9.38 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 017 
                 61 
                 gelled 
                   
                 1.63 
                 gelled 
                   
                 9.52 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 018 
                 58 
                 gelled 
                   
                 0.68 
                 gelled 
                   
                 1.697 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 019 
                 63 
                 gelled 
                   
                 1.28 
                 gelled 
                   
                 9.47 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 020 
                 78 
                 gelled 
                   
                 2.34 
                 gelled 
                   
                 9.64 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 021 
                 69 
                 gelled 
                   
                 1.19 
                 gelled 
                   
                 9.53 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 022 
                 80 
                 gelled 
                   
                 0.78 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 023 
                 70 
                 gelled 
                   
                 0.68 
                 gelled 
                   
                 9.48 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 031 
                 93 
                 gelled 
                   
                 1.37 
                 gelled 
                   
                 9.57 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 032 
                 72 
                 gelled 
                   
                 1.5 
                 gelled 
                   
                 9.24 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 033 
                 86 
                  70 
                 −16.60 
                 0.9 
                 1.40 
                 55.11 
                 9.01 
                 8.21 
                 −8.88 
                 10 
                 soft 
               
               
                 034 
                 90 
                 gelled 
                   
                 1.13 
                 gelled 
                   
                 9.44 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 035 
                 83 
                 gelled 
                   
                 1.95 
                 gelled 
                   
                 9.44 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 036 
                 88 
                 gelled 
                   
                 1.17 
                 gelled 
                   
                 9.33 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 037 
                 92 
                 gelled 
                   
                 0.85 
                 gelled 
                   
                 9.23 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 038 
                 86 
                 gelled 
                   
                 1.38 
                 gelled 
                   
                 9.55 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 039 
                 101 
                 gelled 
                   
                 0.77 
                 gelled 
                   
                 9.56 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 040 
                 88 
                 gelled 
                   
                 0.54 
                 gelled 
                   
                 9.4 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 041 
                 92 
                 gelled 
                   
                 1.79 
                 gelled 
                   
                 9.39 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 042 
                 85 
                 gelled 
                   
                 0.86 
                 gelled 
                   
                 9.44 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 043 
                 81 
                 gelled 
                   
                 0.7 
                 gelled 
                   
                 9.5 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 044 
                 85 
                 gelled 
                   
                 1.35 
                 gelled 
                   
                 9.49 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 045 
                 75 
                 gelled 
                   
                 1.16 
                 gelled 
                   
                 9.3 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 046 
                 73 
                 gelled 
                   
                 1.11 
                 gelled 
                   
                 9.22 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 047 
                 84 
                 gelled 
                   
                 0.7 
                 gelled 
                   
                 9.37 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 048 
                 80 
                 gelled 
                   
                 1.34 
                 gelled 
                   
                 9.53 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 049 
                 86 
                 gelled 
                   
                 1.66 
                 gelled 
                   
                 9.07 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 050 
                 68 
                 gelled 
                   
                 0.63 
                 gelled 
                   
                 9.4 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 051 
                 64 
                 gelled 
                   
                 2.88 
                 gelled 
                   
                 9.43 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 052 
                 138 
                 gelled 
                   
                 1.62 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 053 
                 78 
                 gelled 
                   
                 1.34 
                 gelled 
                   
                 9.65 
                 n/a 
                   
                 20 
                 medium 
               
               
                 054 
                 58 
                 gelled 
                   
                 1.48 
                 gelled 
                   
                 9.72 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 055 
                 87 
                 gelled 
                   
                 1.74 
                 gelled 
                   
                 9.32 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 067 
                 89 
                 110 
                 23.60 
                 0.85 
                 1.29 
                 51.53 
                 9.81 
                 9.05 
                 −7.75 
                 60 
                 medium 
               
               
                 068 
                 87 
                 1637  
                   
                 0.51 
                 1.22 
                 139.41 
                 9.7 
                 8.69 
                 −8.35 
                 50 
                 med-hard 
               
               
                 069 
                 98 
                 gelled 
                   
                 0.51 
                 gelled 
                   
                 9.71 
                 gelled 
                   
                 90 
                 med-hard 
               
               
                 070 
                 77 
                 gelled 
                   
                 0.73 
                 gelled 
                   
                 9.75 
                 gelled 
                   
                 50 
                 med-hard 
               
               
                 071 
                 85 
                  94 
                 10.59 
                 1.55 
                 0.67 
                 −58.71 
                 9.76 
                 9.04 
                 −7.38 
                 75 
                 medium 
               
               
                 072 
                 96 
                 n/a 
                   
                 0.52 
                 n/a 
                   
                 9.8 
                 n/a 
                   
                 n/a 
                 n/a 
               
               
                 073 
                 90 
                 107 
                 18.89 
                 0.41 
                 1.26 
                 208.05 
                 9.73 
                 9.08 
                 −6.68 
                 50 
                 soft 
               
               
                 074 
                 90 
                  99 
                 10.00 
                 0.85 
                 0.93 
                 9.29 
                 9.91 
                 9.12 
                 −7.97 
                 80 
                 soft 
               
               
                 075 
                 90 
                 gelled 
                   
                 0.8 
                 n/a 
                   
                 9.73 
                 gelled 
                   
                 70 
                 medium 
               
               
                 076 
                 84 
                  70 
                 −16.67 
                 0.84 
                 0.79 
                 −5.71 
                 9.67 
                 8.93 
                 −7.65 
                 20 
                 soft 
               
               
                 077 
                 96 
                 111 
                 15.63 
                 0.69 
                 1.10 
                 59.42 
                 9.9 
                 9.11 
                 −7.98 
                 70 
                 soft 
               
               
                 078 
                 94 
                 109 
                 15.96 
                 0.63 
                 0.88 
                 40.16 
                 9.9 
                 9.14 
                 −7.68 
                 50 
                 soft 
               
               
                 079 
                 77 
                  78 
                 1.30 
                 1.1 
                 0.79 
                 −28.36 
                 9.92 
                 9.37 
                 −5.54 
                 20 
                 medium 
               
               
                 080 
                 85 
                  93 
                 9.41 
                 0.97 
                 0.75 
                 −22.27 
                 9.78 
                 8.97 
                 −8.28 
                 60 
                 medium 
               
               
                 081 
                 94 
                 116 
                 23.40 
                 1.06 
                 0.58 
                 −45.00 
                 9.8 
                 9.16 
                 −6.53 
                 80 
                 soft 
               
               
                 082 
                 83 
                  86 
                 3.61 
                 0.71 
                 0.29 
                 −59.44 
                 9.67 
                 8.8  
                 −9.00 
                 20 
                 soft 
               
               
                 083 
                 91 
                 gelled 
                   
                 1.1 
                 gelled 
                   
                 9.82 
                 gelled 
                   
                 gelled 
                 gelled 
               
               
                 084 
                 83 
                  94 
                 13.25 
                 0.74 
                 0.98 
                 31.76 
                 9.78 
                 n/a 
                   
                 60 
                 medium 
               
               
                 085 
                 87 
                 gelled 
                   
                 0.64 
                 gelled 
                   
                 9.01 
                 gelled 
                   
                 gelled 
                 gelled 
               
               
                 086 
                 72 
                 gelled 
                   
                 1.05 
                 gelled 
                   
                 9.33 
                 gelled 
                   
                 gelled 
                 gelled 
               
               
                 087 
                 83 
                 gelled 
                   
                 0.78 
                 gelled 
                   
                 9.35 
                 gelled 
                   
                 gelled 
                 gelled 
               
               
                 088 
                 90 
                 gelled 
                   
                 0.95 
                 gelled 
                   
                 9.18 
                 gelled 
                   
                 gelled 
                 gelled 
               
               
                   
               
               
                 GL = Gloss Loss  
               
               
                 % settling is the relative ht on stirring stick that adheres w/o easily falling away  
               
             
          
         
       
     
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                 TABLE 9               OVEN BAKE                                    Chemical Resistance                        Dispersant       Film   Gloss                       10%   10%                Formula   Resin   Dispersant   amount   Thickener   Build   20   60   Coppertone   Toluene   IPA   MEK   DWO   Sulf   NaOH   F409               001   3   2   1   3   1.74   4.2   23.3   3   3   5   3   3   3   3   5       002   3   8   1   5   1.71   18.5   56.7   4   3   5   4   3   3   5   5       003   3   7   1   5   1.86   35.3   68.3   4   2   3.5   3   3   5   4   1       004   3   2   1   6   1.66   6.5   33.8   5   5   4.5   4   2.5   5   5   4       005   3   11   1   7   1.88   19.3   63.1   4   2   5   3   3   5   5   2       006   3   3   1   7   1.91   13.1   50.1   3   4   6   4   2.5   5   4   6       007   4   1   2   7   1.60   26.1   61.5   4   5   5   2   3   5   3   6       008   4   5   2   5   1.74   25.5   62.4   4.5   5   5   5   3.5   2   5   5       009   4   3   2   3   1.61   23.5   59.4   5   3   5   5   3.5   5   5   5       010   4   10   2   2   1.62   6.8   34.4   3   3   5   4   2   2   4.5   5       011   4   10   2   2   1.48   3.8   23.6   3   3   4   4   2   3   3   5       012   4   3   2   7   1.61   14.4   45.3   3   4   4   3   2   3   3   4.5       013   4   8   2   7   1.85   6.8   34.1   3   5   5   4   2   5   5   5       014   4   11   2   8   1.60   26.0   56.7   3.5   5   5   5   3.5   5   5   4       015   4   1   1   2   1.88   21.8   59.2   3.5   3   3   3   2   3   4.5   4       016   4   5   1   3   1.48   30.5   63.2   4   3.5   5   3   2   3   3   4       017   4   1   1   8   1.72   12.6   47.1   4.5   3   4   3   2   5   5   4.5       018   4   2   1   4   1.62   23.9   62.0   3   3   5   3   2   2   5   5       019   4   7   1   1   1.71   7.8   38.9   5   5   4   5   3.5   5   3   4       020   4   11   1   4   1.70   28.5   60.6   4   5   4   3   2   5   3   5       021   4   3   1   6   1.64   31.4   63.0   3.5   5   4.5   5   2.5   5   5   4.5       022   4   11   1   2   1.81   22.6   59.5   4   4   5   5   3   4   5   5       023   4   3   1   7   1.67   29.9   66.4   3   5   5   4   2   6   3   6       031   2   2   2   1   1.63   20.9   55.9   3   3   5   4   1   5   5   2       032   2   3   2   6   1.39   39.3   68.4   4   5   5   5   3.5   5   5   2       033   2   4   2   8   1.60   11.8   44.6   4   3   3.5   3   2   5   5   3       034   2   1   1   7   1.69   22.9   60.3   4   3   5   3.5   3.5   5   5   3       035   2   1   1   5   1.61   12.7   46.4   4   3   5   3   3   5   5   3       036   2   3   1   4   1.59   15.5   49.3   4   3   4.5   3   3   5   5   3       037   2   8   1   4   1.57   14.2   47.2   4.5   3   4.5   4   3   5   5   3       038   2   11   1   2   1.74   42.8   71.5   4   2   5   4   3   5   3   3       039   2   2   1   8   1.78   24.3   59.7   3.5   3   5   4   3.5   5   5   3       040   2   7   1   8   1.51   27.4   62.8   4   3   4   3   3   5   3   3       041   2   7   1   6   1.46   22.3   58.9   3   4   5   3   3   5   5   2       042   3   1   2   4   1.80   22.4   59.2   4   2   4   3   3.5   5   5   2       043   3   1   2   1   1.60   16.2   51.4   3.5   3.5   5   3   3   5   4.5   3       044   3   1   2   7   1.91   6.2   33.9   2   2   4   3   3   5   5   3       045   3   5   2   8   1.72   30.9   64.9   4   2   3   2   3   2   3   2       046   3   8   2   3   1.83   6.5   31.3   5   3   5   3   3.5   5   5   4       047   3   7   2   1   1.40   32.8   66.5   4   2   3   2   3.5   5   4   2       048   3   11   2   3   1.83   27.7   63.4   4   2   3   2   3   5   5   2       049   3   8   2   6   1.36   26.8   65.2   4   3   5   3   3   4   4   3.5       050   3   3   2   5   1.87   13.0   46.7   4   3   3   2.5   3   3.5   3   3       051   3   5   1   4   1.71   23.9   63.2   4   5   5   5   3.5   4.5   3   3       052   3   9   1   1   1.54   24.4   60.1   3   5   5   3   3.5   5   5   5       053   3   9   1   2   1.56   21.7   57.2   4.5   3   5   3   2.5   3   3   3       054   2   8   1   4   1.67   10.0   45.2   3   2   5   3   3.5   5   5   3       055   3   8   2   4   1.33   7.5   34.3   5   2   5   3.5   2.5   3   3   4       067   1   5   2   3   1.66   25.5   63.3   4   3   4   3   2   2   5   5       068   1   1   2   6   1.72   33.3   68.5   3   3   4.5   4   3   2   3   5       069   1   8   2   2   1.63   31.6   68.8   3   3   4   3   2   5   5   4       070   1   3   2   2   1.60   30.1   67.7   4   3   4   3   2   3   3   3       071   1   3   2   2   1.50   28.7   65.2   3.5   3   3   3   2.5   2   5   4       072   1   11   2   5   1.65   40.9   71.0   3   3   4.5   3.5   2   5   3   4       073   1   7   2   6   1.69   32.9   67.4   4   2   4   2   2   3   5   3       074   1   2   2   5   1.52   27.9   68.3   3.5   3.5   5   3.5   2   5   5   5       075   1   5   1   2   1.97   28.9   66.6   4   3   3.5   3   2.5   5   5   5       076   1   6   1   1   2.13   24.8   61.0   4   3   4   3   2   5   5   5       077   1   9   1   5   1.57   28.7   65.4   4   3   4   3   2   4.5   4   5       078   1   9   1   4   1.91   30.3   65.7   4   3.5   4   3   3   5   4   4       079   1   2   1   1   2.70   24.6   61.7   4   3   3   4.5   3   5   5   4.5       080   1   3   1   8   2.32   32.8   66.5   3.5   3   5   3   3   4   3   4       081   1   7   1   3   1.70   32.1   65.7   4   5   5   3   3   4.5   4.5   4.5       082   1   10   1   1   1.94   28.0   63.6   4   3   3   2.5   2   5   5   4       083   1   9   1   5   1.57   29.4   67.0   4   3   5   4   2   3   3   4       084   1   3   1   6   1.80   32.8   67.0   3   3   4   3   3   5   5   4.5       085   2   1   2   3   1.48   32.5   65.3   3   3   4   3   3.5   5   5   3       086   2   5   2   7   1.40   26.4   61.4   4   3   4   3   3.5   5   5   3       087   2   5   2   7   1.54   36.6   68.6   3   2.5   4   2   3.5   5   3   3       088   2   8   2   4   2.05   18.0   51.4   4   4   5   6   3.5   5   5   3       KA 1400                   1.28   77.8   96.7   4.5   4   5   2   5   5   5   5       KA 1700T                   1.49   4.1   25.4   4   3   5   4   4   2   5   5                        Humidity-200 hours   Salt Spray-100 HOURS                Pencil   Blister           Flash rust-       % change 60   Blister                   Formula   Hardness   size   Blister density   Rust   Y or N   Gloss 60   gloss   size   Blister density   Rust   Scribe               001   6   8   1   10   no   12.5   −46.35%   6   4   8   5       002   6   8   1   10   yes   17   −70.02%   6   4   8   4       003   6   8   1   8   yes   14.6   −78.62%   8   4   9   4       004   6   8   1   10   no   14.9   −55.92%   8   4   8   4       005   6   6   1   10   yes   16.7   −73.53%   8   4   8   4       006   6   8   1   10   Yes   15.6   −68.88%   8   3   9   5       007   8   6   1   9   yes   7.3   −88.13%   6   4   8   3       008   7   6   1   8   yes   7.4   −88.14%   6   4   9   3       009   6   4   1   10   yes   5.7   −90.40%   8   4   8   1       010   6   6   1   9   yes   5.7   −83.43%   6   3   8   1       011   6   6   1   10   yes   4.7   −80.08%   8   3   6   2       012   6   4   1   8   yes   5.7   −87.42%   6   4   7   2       013   6   6   1   9   yes   8.3   −75.66%   8   4   8   3       014   6   6   1   10   yes   9.9   −82.54%   8   4   8   3       015   6   2   1   9   no   6.7   −88.68%   8   4   7   3       016   6   4   1   10   no   7.4   −88.29%   8   4   9   2       017   6   4   1   9   yes   6.3   −86.62%   6   4   7   3       018   6   2   1   9   no   9.6   −84.19%   6   4   7   4       019   6   4   1   10   yes   4.4   −88.08%   6   3   5   0       020   6   4   1   9   no   8.1   −86.63%   6   4   6   2       021   5   4   1   10   yes   9.1   −85.56%   10   5   9   3       022   6   4   1   10   yes   7.9   −86.72%   6   4   7   3       023   6   4   1   7   no   11.9   −81.80%   8   4   8   3       031   6   8   1   5   yes   21.4   −61.72%   6   3   9   2       032   6   8   1   7   yes   25.7   −62.43%   8   4   8   3       033   6   8   1   8   yes   15   −66.37%   8   4   7   3       034   6   4   1   7   yes   24.6   −59.20%   10   5   10   4       035   6   8   1   6   yes   17.9   −61.42%   8   4   7   3       036   6   8   1   10   yes   15.7   −68.15%   8   4   9   3       037   6                       −100.00%   8   4   7   4       038   6   8   1   9   yes   22.2   −68.95%   6   3   7   3       039   4   8   1   10   no   16.3   −72.70%   6   4   6   4       040   5   6   1   6   yes   26.6   −57.64%   8   3   6   3       041   6   8   1   9   yes   22.1   −62.48%   8   4   7   4       042   6   6   1   7   yes   15.4   −73.99%   10   5   8   3       043   6   8   1   10   yes   16.8   −67.32%   6   4   6   3       044   6   8   1   10   no   20.1   −40.71%   8   3   9   4       045   6   8   1   10   yes   17   −73.81%   8   4   9   3       046   6   8   1   10   no   18.1   −42.17%   6   4   6   4       047   6   8   1   10   yes   23   −65.41%   6   3   8   4       048   6   8   1   10   yes   16.8   −73.50%   6   4   9   4       049   6   8   1   9   yes   25.7   −60.58%   8   4   8   4       050   6   8   1   10   yes   14.9   −68.09%   8   4   8   4       051   6   8   1   10   yes   13.7   −78.32%   6   3   9   4       052   6   8   1   10   yes   12.9   −78.54%   8   3   9   4       053   6   8   1   10   yes   15.7   −72.55%   8   4   9   4       054   6   8   1   10   yes   15   #REFI   8   4   8   4       055   6   8   1   10   no   15   #REFI   6   3   4   3       067   6   8   1   8   no   13.1   −79.30%   8   4   4   2       068   6   none       10   yes   19   −72.26%   10   5   8   2       069   6   8   1   7   yes   18.4   −73.26%   8   4   8   2       070   6   8   1   8   yes   19.5   −71.20%   10   5   10   2       071   6   8   1   8   yes   19.4   −70.25%    8   4   7   2       072   6   none       10   yes   19.6   −72.39%   8   3   8   1       073   6   8   1   10   no   16.4   −75.67%   8   4   9   2       074   6   8   1   10   yes   15.9   −76.02%   8   4   8   2       075   6   none       6   yes   14.5   −78.23%   8   4   8   2       076   6   8   1   9   yes   13.3   −78.20%   8   4   8   2       077   6   8   1   9   yes   15.7   −75.99%   8   4   8   2       078   6   8   4   10   no   23.8   −63.77%   8   4   9   3       079   6   8   1   9   yes   17.2   −72.12%   6   4   8   2       080   6   8   1   9   yes   14.7   −77.89%   8   4   9   2       081   6   8   1   10   yes   16.8   −74.43%   8   4   8   2       082   6   8   1   10   no   12.9   −79.72%   8   4   9   2       083   6   8   1   10   no   14.3   −78.68%   10   5   9   2       084   6   8   1   10   yes   21.7   −67.61%   8   4   9   2       085   6   8   1   7   yes   17.6   −73.05%   6   4   6   3       086   6   8   1   6   yes   16.8   −72.64%   8   4   8   3       087   6   8   1   7   yes   20.9   −69.53%   8   4   8   3       088   6   8   1   9   yes   16.8   −67.32%   10   5   8   4       KA 1400   4   none       10   no   96.5       8   4   10   2       KA 1700T   9   none       10   no   19.4       4   2   4   7                        Self Spray-200 HOURS               48 Hr. Water-Soak                    Blister           Impact       Adhesion treated   Blister   Blister                    Formula   Blister size   density   Rust   Scribe   Forward   Reverse   MEK Rubs   aluminum   size   density   Rust   Adhesion               001   6   4   8   5   24   &lt;4   100   4   10   5   10   5       002   6   4   8   4   24   &lt;4   150   5   10   5   10   5       003   8   4   9   4   24   &lt;4   500   4   10   5   10   5       004   8   4   8   4   24   &lt;4   150   3   10   5   9   4       005   8   4   8   4   20   &lt;4   250   4   10   5   10   4       006   8   3   9   5   24   &lt;4   200   3   10   5   10   5       007   8   4   8   3   20   &lt;4   700   4   4   3   9   2       008   6   4   9   2   28   &lt;4   1000   3   4   2   10   −1       009   8   4   6   0   28   &lt;4   1000   3   4   3   10   −1       010   6   3   8   2   24   &lt;4   800   4   10   5   10   3       011   8   3   5   2   24   &lt;4   1000   3   10   5   10   4       012   6   4   7   2   28   &lt;4   1000   4   6   2   5   5       013   8   4   8   3   24   8   650   4   10   5   10   4       014   8   4   8   3   32   &lt;4   450   5   4   3   10   2       015   8   4   7   3   28   4   1000   4   10   5   10   5       016   8   4   9   2   24   &lt;4   250   4   6   2   10   2       017   6   4   7   3   24   &lt;4   1000   3   6   3   5   4       018   6   4   6   4   24   &lt;4   450   3   8   2   2   4       019   6   3   6   0   24   4   800   3   4   3   4   3       020   6   4   6   2   28   &lt;4   1000   3   4   3   10   3       021   10   5   9   3   28   &lt;4   950   4   6   3   7   4       022   6   4   7   3   24   &lt;4   1000   3   8   4   10   5       023   8   4   4   2   24   &lt;4   1000   3   4   3   6   4       031   6   3   9   2   20   &lt;4   250   4   10   5   10   4       032   8   4   8   3   20   &lt;4   150   4   10   5   10   5       033   8   4   7   3   20   &lt;4   100   5   10   5   8   5       034   10   5   10   4   20   &lt;4   600   2   10   5   10   5       035   6   4   7   3   20   &lt;4   150   5   10   5   10   5       036   8   4   9   3   20   &lt;4   150   4   10   5   10   5       037   8   4   7   4   20   &lt;4   200   4   10   5   10   5       038   6   3   7   3   20   &lt;4   200   3   10   5   9   4       039   6   4   6   4   20   &lt;4   50   2   10   5   9   4       040   8   3   6   3   20   &lt;4   50   3   10   5   10   4       041   8   4   7   4   20   &lt;4   50   3   10   5   10   4       042   10   5   8   3   24   &lt;4   61   4   10   5   10   4       043   6   4   6   3   24   &lt;4   50   5   10   5   10   5       044   8   3   9   4   24   &lt;4   120   5   10   5   10   5       045   8   4   9   3   24   &lt;4   850   5   10   5   9   5       046   8   4   6   4   20   &lt;4   100   4   10   5   10   5       047   6   3   7   3   24   &lt;4   400   4   10   5   10   5       048   6   4   9   5   28   &lt;4   150   4   10   5   10   5       049   8   4   8   4   24   &lt;4   150   4   10   5   10   4       050   8   4   8   4   24   &lt;4   450   5   10   5   9   4       051   6   3   9   4   20   &lt;4   550   1   10   5   10   5       052   8   3   9   4   20   &lt;4   700   3   10   5   10   5       053   8   4   9   4   24   &lt;4   650   3   10   5   10   5       054   8   4   8   4   20   &lt;4   50   1   10   5   8   5       055   6   3   4   3   24   &lt;4   200   5   10   5   7   5       067   8   4   4   2   24   &lt;4   400   0   6   2   10   4       068   10   5   8   2   24   &lt;4   750   0   10   5   10   4       069   8   4   8   2   24   &lt;4   700   4   8   2   10   5       070   10   5   10   2   24   &lt;4   600   1   8   2   10   4       071   8   4   7   2   24   &lt;4   1000   1   6   2   10   4       072   8   3   8   1   24   &lt;4   500   0   10   5   10   5       073   8   4   9   2   24   &lt;4   650   1   8   2   10   3       074   8   4   8   2   24   &lt;4   750   0   10   5   10   5       075   8   4   8   2   24   &lt;4   50   0   6   4   10   4       076   8   4   8   2   20   &lt;4   800   0   10   5   10   5       077   8   4   8   2   24   &lt;4   1000   0   6   3   9   1       078   8   4   9   3   24   &lt;4   900   0   8   3   10   1       079   6   4   8   2   20   &lt;4   750   0   8   4   10   5       080   8   4   9   2   24   &lt;4   550   4   6   2   10   4       081   8   4   8   2   24   &lt;4   1000   0   8   4   10   4       082   8   4   9   2   24   &lt;4   1000   1   8   4   10   5       083   10   5   9   3   24   &lt;4   700   0   6   4   9   4       084   8   4   9   2   24   &lt;4   700   1   10   5   10   5       085   6   4   6   3   20   &lt;4   50   3   8   4   10   4       086   8   4   8   3   20   &lt;4   50   4   10   5   10   5       087   8   4   8   3   20   &lt;4   50   3   10   5   10   4       088   10   5   7   4   20   &lt;4   50   4   10   5   10   4       KA 1400   8   4   10   2   &gt;168   &gt;168   650   5   10   5   10   5       KA 1700T   4   2   4   7   66   4   1000   5   10   5   10   2                        QUV-Initial   QUV-500-HOUR   QUV-1000-HOUR                60°   Delta   Delta   60°   Delta   Delta   % Loss of   Change in   Change in   60°   Delta   Delta   % Loss of   Change in   Change in       Formula   Gloss   E   YB   Gloss   E   YB   60 gloss   delta E   YB   Gloss   E   YB   60 gloss   delta E   YB               001   29.1   0.98   −0.21   18.7   2.85   1.24   −35.74%   1.89   1.45   18.5   2.00   0.55   −36.43%   1.04   0.76            002   MISSING PANEL       MISSING       MISSING                       PANEL       PANEL            003   68.5   0.31   −0.21   53.1   2.03   0.92   −22.48%   1.72   1.13   54.9   1.55   0.49   −19.85%   1.24   0.70       004   46.9   1.65   −0.58   25.1   2.59   0.65   −46.48%   0.94   1.23   22.9   2.12   −0.05   −51.17%   0.47   0.53       005   63.7   1.47   0.44   42.7   3.41   1.98   −32.97%   1.94   1.54   47.4   3.32   1.67   −25.59%   1.85   1.23       006   50.2   0.25   −0.11   33.9   2.99   1.60   −32.47%   2.74   1.71   32.5   2.78   1.26   −35.26%   2.53   1.37       007   83.0   3.72   3.03   19.9   3.89   2.40   −68.41%   0.17   −0.63   17.2   3.49   1.98   −72.70%   0.23   −1.05       008   64.4   3.53   2.67   21.6   3.62   2.29   −66.46%   0.09   −0.58   16.9   3.15   1.72   −73.78%   0.38   −1.15       009   57.7   3.01   2.45   18.4   3.13   1.87   −68.11%   0.12   −0.58   16.8   2.62   1.39   −70.88%   0.39   −1.06       010   37.7   3.83   3.00   8.5   4.99   2.93   −77.45%   1.16   −0.07   8.9   4.47   2.37   −76.39%   0.64   −0.63       011   25.2   4.12   3.01   6.2   5.34   3.01   −75.40%   1.22   0.00   5.7   4.54   2.31   −77.38%   0.42   −0.70       012   49.8   3.85   3.03   14.1   3.98   2.40   −71.69%   0.11   −0.63   10.6   3.99   2.16   −78.71%   0.14   −0.87       013   36.0   4.74   3.73   12.6   5.51   3.34   −64.44%   0.77   −0.39   11.9   5.09   2.87   −66.94%   0.35   −0.86       014   63.7   3.30   2.50   17.9   3.91   2.36   −71.90%   0.61   −0.14   15.7   3.05   1.44   −75.35%   0.25   −1.06       015   62.4   4.32   3.42   23.0   4.49   2.75   −63.14%   0.17   −0.67   16.8   3.84   2.15   −73.08%   0.48   −1.27       016   70.3   4.08   3.30   29.1   4.07   2.54   −58.61%   0.01   −0.76   24.6   3.69   2.05   −65.01%   0.39   −1.25       017   49.5   4.90   3.87   16.3   5.10   3.21   −67.07%   0.20   −0.66   11.9   5.07   2.83   −75.96%   0.17   −1.04       018   67.5   4.79   3.74   26.1   4.50   2.85   −61.33%   0.29   −0.89   15.5   3.87   2.10   −77.04%   0.92   −1.64       019   36.7   5.34   4.20   11.4   5.16   3.37   −68.94%   0.18   −0.83   8.3   4.44   2.61   −77.38%   0.90   −1.69       020   68.3   4.31   3.48   30.3   4.64   2.98   −55.64%   0.33   −0.50   20.9   3.76   2.03   −69.40%   0.55   −1.45       021   68.5   4.56   3.71   24.9   4.52   2.76   −63.65%   0.06   −0.95   20.7   4.16   2.30   −69.78%   0.42   −1.41       022   64.8   5.02   3.96   16.3   4.84   2.94   −74.85%   0.18   −1.02   12.1   4.35   2.43   −81.33%   0.67   −1.53       023   73.6   4.95   3.92   34.6   4.28   2.72   −52.93%   0.67   −1.20   24.7   3.89   2.13   −66.39%   1.06   −1.79       031   59.2   0.51   0.05   50.4   1.23   0.69   −14.86%   0.72   0.64   51.5   1.45   0.71   −13.01%   0.94   0.66       032   72.0   0.37   −0.35   59.7   0.88   0.33   −17.08%   0.51   0.68   63.2   1.33   0.47   −12.22%   0.96   0.82       033   47.7   0.39   −0.02   33.3   1.05   1.11   −30.19%   0.66   1.13   38.8   1.71   0.88   −18.66%   1.32   0.90       034   62.1   0.94   0.21   49.1   1.62   1.07   −20.93%   0.88   0.86   53.4   2.10   1.10   −14.01%   1.16   0.89       035   48.1   0.82   −0.25   32.3   1.52   0.62   −32.85%   0.70   0.87   36.1   1.60   0.60   −24.95%   0.78   0.85       036   50.0   0.18   −0.09   33.8   1.52   0.60   −32.40%   1.34   0.69   37.4   1.23   0.30   −25.20%   1.05   0.39       037   48.5   0.59   0.06   34.9   2.25   1.22   −28.04%   1.66   1.16   41.5   2.13   1.08   −14.43%   1.54   1.02       038   67.6   1.63   1.22   59.1   2.02   1.26   −12.57%   0.39   0.04   59.8   2.16   1.15   −11.64%   0.53   −0.07       039   60.6   1.23   0.28   49.4   2.08   1.14   −18.48%   0.85   0.66   51.0   2.06   0.94   −15.84%   0.83   0.66       040   64.7   0.61   −0.42   49.1   1.25   0.44   −24.11%   0.64   0.66   53.7   0.81   −0.01   −17.00%   0.20   0.41       041   58.1   0.32   −0.15   42.9   1.58   0.75   −26.16%   1.26   0.90   48.8   1.60   0.69   −16.01%   1.28   0.84       042   59.3   0.24   −0.19   41.2   2.36   1.23   −30.52%   2.14   1.42   44.5   2.04   0.69   −24.96%   1.80   1.08       043   53.6   0.55   −0.53   41.6   1.95   0.91   −22.39%   1.40   1.44   44.6   2.05   0.75   −16.79%   1.50   1.28       044   35.3   0.43   −0.08   25.3   2.47   1.25   −28.33%   2.04   1.33   29.6   2.33   0.98   −16.15%   1.90   1.06       045   65.6   0.41   −0.41   58.1   2.16   1.19   −11.43%   1.75   1.60   59.7   2.44   1.09   −8.99%   2.03   1.50       046   36.1   0.42   −0.11   28.3   2.63   1.31   −21.61%   2.21   1.42   31.2   2.63   1.19   −13.57%   2.21   1.30       047   66.9   0.30   −0.08   58.8   1.93   0.99   −12.11%   1.83   1.07   61.7   2.01   0.77   −7.77%   1.71   0.85       048   64.0   0.57   −0.43   54.8   2.41   1.08   −14.38%   1.84   1.51   55.9   1.97   0.67   −12.66%   1.40   1.10       049   67.4   0.77   −0.57   53.9   1.95   0.47   −20.03%   1.18   1.04   54.0   1.43   0.16   −19.88%   0.66   0.73       050   46.8   0.84   −0.33   35.9   2.32   0.93   −23.29%   1.48   1.26   33.9   1.99   0.65   −27.56%   1.15   0.98       051   64.7   0.17   −0.16   52.3   2.40   1.13   −19.17%   2.23   1.29   54.8   2.14   0.86   −15.30%   1.97   1.02       052   62.7   0.48   −0.03   48.8   2.91   1.32   −22.49%   2.43   1.35   55.4   2.54   1.07   −11.64%   2.06   1.10       053   58.5   0.37   0.07   47.4   2.40   1.19   −18.97%   2.03   1.12   52.3   2.35   1.00   −10.60%   1.98   0.93       054   46.2   1.08   −0.21   30.3   2.48   0.91   −34.42%   1.40   1.12   32.8   2.00   0.48   −29.00%   0.92   0.69       055   35.2   0.27   −0.02   22.3   2.79   1.36   −36.85%   2.52   1.38   26.1   2.24   0.90   −25.85%   1.97   0.92       067   64.6   0.56   −0.55   45.6   0.96   0.39   −29.41%   0.40   0.94   40.1   1.63   0.83   −37.93%   1.07   1.38       068   68.2   0.50   −0.40   50.2   1.28   0.61   −26.39%   0.78   1.01   38.6   1.98   0.97   −43.40%   1.48   1.37       069   69.8   0.78   −0.53   53.5   0.93   0.40   −23.35%   0.15   0.93   48.2   1.76   0.80   −30.95%   0.98   1.33       070   88.5   0.63   −0.60   50.6   0.98   0.42   −26.13%   0.35   1.02   39.8   1.33   0.53   −41.90%   0.70   1.13       071   66.7   0.61   −0.57   47.5   1.03   0.25   −28.79%   0.42   0.82   36.6   1.75   0.78   −44.83%   1.14   1.35       072   69.8   0.79   −0.67   49.5   0.72   0.21   −29.08%   0.07   0.88   50.1   1.37   0.51   −28.22%   0.58   1.18       073   68.2   1.03   −0.88   40.8   0.91   0.16   −40.47%   0.12   1.04   38.9   1.13   0.26   −42.96%   0.10   1.14       074   68.6   0.54   −0.34   39.9   0.99   0.49   −41.84%   0.45   0.83   32.3   1.42   0.63   −52.92%   0.88   0.97       075   67.9   0.43   −0.32   38.0   1.39   0.71   −44.04%   0.96   1.03   32.8   1.38   0.70   −51.69%   0.95   1.02       076   61.2   0.63   −0.41   37.6   1.55   0.83   −38.56%   0.92   1.24   43.1   1.94   0.95   −29.58%   1.31   1.36       077   67.2   0.60   −0.26   37.8   1.62   0.87   −43.75%   1.02   1.13   36.3   1.62   0.82   −45.98%   1.02   1.08       078   67.3   0.62   −0.24   43.0   1.54   0.85   −36.11%   0.92   1.09   35.2   2.19   1.20   −47.70%   1.57   1.44       079   63.3   0.93   0.01   41.8   1.55   0.88   −33.97%   0.62   0.65   33.8   2.14   1.12   −46.60%   1.21   1.11       080   67.9   0.53   −0.33   44.4   1.20   0.63   −34.61%   0.67   0.96   37.9   2.02   1.05   −44.18%   1.49   1.38       081   67.8   0.50   −0.35   41.0   1.20   0.58   −39.53%   0.70   0.93   34.6   1.83   0.86   −48.97%   1.33   1.21       082   63.5   0.49   −0.47   44.2   1.62   0.85   −30.39%   1.13   1.32   41.3   1.83   0.89   −34.96%   1.34   1.36       083   69.3   0.55   −0.35   49.9   1.32   0.71   −27.99%   0.77   1.06   38.2   1.61   0.80   −44.86%   1.06   1.15       084   68.7   0.88   −0.23   46.4   1.68   0.84   −32.46%   0.82   1.07   38.5   2.00   0.97   −43.96%   1.14   1.20       085   67.9   0.50   −0.38   57.4   1.13   0.47   −15.46%   0.63   0.85   55.5   0.95   0.32   −18.26%   0.45   0.70       086   62.7   0.46   −0.26   48.7   1.13   0.41   −22.33%   0.67   0.67   51.1   1.28   0.45   −18.50%   0.82   0.71       087   68.8   0.31   −0.25   58.5   1.05   0.36   −17.88%   0.74   0.63   60.7   1.33   0.39   −11.77%   1.02   0.64       088   54.4   0.22   −0.11   45.2   1.46   0.75   −16.91%   1.24   0.86   47.0   1.45   0.71   −13.60%   1.23   0.82       KA 1400   97.0   2.86   −0.24   92.1   3.75   1.06   −5.05%   0.89   1.30   81.2   4.66   1.91   −18.29%   2.00   2.15       KA 1700T   26.5   4.14   0.42   25.0   4.14   −0.08   −5.66%   0.00   −0.50   23.0   4.07   0.19   −13.21%   0.07   −0.23       Sher-cryl   80.0   7.97   4.05   74.3   6.26   1.07   −7.13%   1.71   −2.98   60.6   5.96   0.74   −24.25%   2.01   −3.31       Centurion   50.7   10.50   1.92   32.9   11.32   4.46   −35.11%   0.82   2.54   25.0   11.07   3.84   −50.69%   0.57   1.92       HS+   80.0   7.95   6.40   78.0   3.58   2.46   −2.50%   4.37   −3.94   75.5   3.40   2.53   −5.63%   4.55   −3.87       700T   22.0   2.48   1.88   15.3   0.84   −0.25   −30.45%   1.64   −2.13   12.5   0.57   −0.17   −43.18%   1.91   −2.05                        Viscosity, settling, and pH Stability (6 weeks at 140° F.)            Formula   Initial KU   final KU   % change   Initial ICI   final ICI   % change   Initial pH   final pH   % change   settling amount   settling type               001   96   gelled       1.6   gelled       9.58   n/a       n/a   n/a       002   140   gelled       1.18   gelled       9.59   n/a       n/a   n/a       003   94   gelled       1.16   gelled       9.43   n/a       n/a   n/a       004   79   gelled       1.88   gelled       9.65   n/a       n/a   n/a       005   136   gelled       0.69   gelled       9.61   n/a       n/a   n/a       006   108   gelled       1.83   gelled       9.3   n/a       n/a   n/a       007   91   gelled       1.66   gelled       9.48   n/a       n/a   n/a       008   95   gelled       1.88   gelled       9.32   n/a       n/a   n/a       009   68   gelled       1.11   gelled       9.42   n/a       n/a   n/a       010   65   gelled       0.492   gelled       9.09   n/a       n/a   n/a       011   83   gelled       9.42   gelled       9.14   n/a       n/a   n/a       012   69   gelled       0.68   gelled       9.45   n/a       n/a   n/a       013   74   gelled       0.77   gelled       9.32   n/a       n/a   n/a       014   88   gelled       0.58   gelled       9.55   n/a       n/a   n/a       015   61   gelled       1.17   gelled       9.52   n/a       n/a   n/a       016   68   gelled       1.12   gelled       9.38   n/a       n/a   n/a       017   81   gelled       1.63   gelled       9.52   n/a       n/a   n/a       018   68   gelled       0.68   gelled       1.697   n/a       n/a   n/a       019   83   gelled       1.28   gelled       9.47   n/a       n/a   n/a       020   78   gelled       2.34   gelled       9.64   n/a       n/a   n/a       021   69   gelled       1.19   gelled       9.53   n/a       n/a   n/a       022   80   gelled       0.78   gelled       9.65   n/a       n/a   n/a       023   70   gelled       0.88   gelled       9.48   n/a       n/a   n/a       031   93   gelled       1.37   gelled       9.57   n/a       n/a   n/a       032   72   gelled       1.5   gelled       9.24   n/a       n/a   n/a       033   86   70   −18.60   0.9   1.40   55.11   9.01   8.21   −8.68   10   soft       034   90   gelled       1.13   gelled       9.44   n/a       n/a   n/a       035   83   gelled       1.95   gelled       9.44   n/a       n/a   n/a       036   88   gelled       1.17   gelled       9.33   n/a       n/a   n/a       037   92   gelled       0.65   gelled       9.23   n/a       n/a   n/a       038   68   gelled       1.38   gelled       9.55   n/a       n/a   n/a       039   101   gelled       0.77   gelled       9.56   n/a       n/a   n/a       040   88   gelled       0.54   gelled       9.4   n/a       n/a   n/a       041   92   gelled       1.79   gelled       9.39   n/a       n/a   n/a       042   85   gelled       0.88   gelled       9.44   n/a       n/a   n/a       043   81   gelled       0.7   gelled       9.5   n/a       n/a   n/a       044   85   gelled       1.35   gelled       9.49   n/a       n/a   n/a       045   75   gelled       1.18   gelled       9.3   n/a       n/a   n/a       046   73   gelled       1.11   gelled       9.22   n/a       n/a   n/a       047   84   gelled       0.7   gelled       9.37   n/a       n/a   n/a       048   80   gelled       1.34   gelled       9.53   n/a       n/a   n/a       049   88   gelled       1.66   gelled       9.07   n/a       n/a   n/a       050   68   gelled       0.63   gelled       9.4   n/a       n/a   n/a       051   64   gelled       2.88   gelled       9.43   n/a       n/a   n/a       052   138   gelled       1.62   gelled       9.55   n/a       n/a   n/a       053   78   gelled       1.34   gelled       9.65   n/a       20   medium       054   58   gelled       1.48   gelled       9.72   n/a       n/a   n/a       055   57   gelled       1.74   gelled       9.32   n/a       n/a   n/a       067   89   110    23.60   0.85   1.29   51.53   9.81   9.05   −7.78   60   medium       068   87   183?        0.51   1.22   139.41   9.7   8.89   −8.35   50   ed-hard       069   98   gelled       0.51   gelled       9.71   gelled       90   ed-hard       070   77   gelled       0.73   gelled       9.75   gelled       50   ed-hard       071   85   94   10.59   1.55   0.67   −56.71   9.78   9.04   −7.38   75   medium       072   96   n/a       0.52   n/a       9.8   n/a       n/a   n/a       073   90   107    18.69   0.41   1.26   208.05   9.73   9.08   −6.68   50   soft       074   90   99   10.00   0.85   0.93   9.29   9.91   9.12   −7.97   80   soft       075   90   gelled       0.8   n/a       9.73   gelled       70   medium       076   84   70   −18.87   0.84   0.79   −5.71   9.67   8.93   −7.65   20   soft       077   96   111    15.63   0.69   1.10   59.42   9.9   9.11   −7.98   70   soft       078   94   109    15.96   0.63   0.88   40.16   9.9   9.14   −7.68   50   soft       079   77   78   1.30   1.1   0.79   28.36   9.92   9.37   −5.64   20   medium       080   85   93   9.41   0.97   0.75   −22.27   9.78   8.97   −6.28   60   medium       081   94   116    23.40   1.06   0.58   −45.00   9.6   9.16   −6.53   80   soft       082   83   86   3.61   0.71   0.29   −59.44   9.87   8.8    −9.00   20   soft       083   91   gelled       1.1   gelled       9.82   gelled       gelled   gelled       084   83   94   13.25   0.74   0.98   31.76   9.78   n/a       60   medium       085   87   gelled       0.64   gelled       9.01   gelled       gelled   gelled       086   72   gelled       1.05   gelled       9.33   gelled       gelled   gelled       087   83   gelled       0.78   gelled       9.35   gelled       gelled   gelled       088   90   gelled       0.95   gelled       9.18   gelled       gelled   gelled               % settling is the relative ht on stirring stick that adheres w/o easily failing away             
(Key for Tables 7, 8 and 9)
     Resin 1=Binder resin C2   Resin 2=Binder resin B28   Resin 3=Binder resin B27   Resin 4=Binder resin B29
 
Dispersant Amount:
   1=Dispersant used in pigment grind as in Example G.   2=Dispersant used in pigment grind and in final mix as in Example H.
 
Pencil Hardness Ratings:
   0 &lt;3B   1 3B   2 2B   3 B   4 HB   5 F   6 H   7 2H   8 3H   9 4H
 
Blister Density:
   1 Dense   2 Medium dense   3 Medium   4 Few   5 No Blister   
     While this invention has been described by a specific number of embodiments, other variations and modifications may be made without departing from the spirit and scope of the invention as set forth in the appended claims. 
     The entire disclosure of all applications, patents and publications cited herein are hereby incorporated by reference.