 the supplementary crystallographic data for this paper. These data can be obtained free of charge via [www.ccdc.cam.ac.uk/data_request/cif](http://www.ccdc.cam.ac.uk/data_request/cif), or by emailing <data_request@ccdc.cam.ac.uk>, or by contacting The Cambridge Crystallographic Data Centre, 00 Union Road, Cambridge CB0 0EZ, UK; fax: +00 0000 000000.  The 