Table S1. Analytical method validation data No. Name Retention time (Min) Quantifier transition Collision Energy (V) Qualifier transition Collision Energy (V) LOQ (mg kg-1) Recovery (%RSD) at Spiking level (mg kg-1) 0.01 0.05 0.10 1 Dichlorvos 6.15 185.00>93.00 14 14 0.008 79.2 (6) 73.3 (13) 83.4 (7) 2 Novaluron 6.57 335.00>168.00 16 25 0.009 – 97.8 (6) 119.6 (9) 3 4-bromo 6.64 207.90>63.00 25 22 0.008 115.3 (13) 93.6 (13) 96.9 (10) 4 Disulfoton sulfoxide 6.77 125.00>96.95 7 26 0.009 108.4 (20) 96.5(18) 102.4(14) 5 Dichlobenil 7.23 170.90>100.00 24 14 0.010 71.5 (5) 78.1 (8) 81.8 (6) 6 Diflubenzuron 7.25 157.05>141.05 9 25 0.009 98.9 (10) 77.8 (6) 93.4 (16) 7 Butylate 7.97 174.10>146.10 6 8 0.009 93.0 (18) 71.8 (4) 80.3 (9) 8 Mevinphos 8.04 192.00>127.00 12 4 0.010 85.9 (8) 87.1 (7) 96.8 (9) 9 Chlormephos 8.16 233.90>121.00 12 6 0.008 85.2 (7) 84.3 (9) 91.7 (8)
10 Etridiazole 8.34 210.90>182.90 10 22 0.009 74.0 (10) 76.1 (9) 84.8 (10) 11 Nitrapyrin 8.36 193.90>133.00 16 20 0.010 87.6 (13) 77.0 (9) 85.6 (9) 12 Propham 8.48 179.10>137.00 8 17 0.009 84.6 (15) 99.0 (16) 112.1 (11) 13 Methacrifos 8.96 208.00>179.95 8 19 0.009 100.4 (9) 93.0 (6) 97.4 (8) 14 Triflumuron 8.96 155.00>139.00 9 24 0.009 110.2 (8) 73.0 (17) 85.3 (11) 15 Crimidine 9.40 156.10>120.10 8 22 0.009 83.0 (17) 79.0 (19) 88.1 (16) 16 Triflusulfuron 9.62 237.10>208.00 6 13 0.009 – 70.3 (10) 78.9 (7) 17 Tebuthiuron 9.74 171.10>156.10 10 26 0.009 107.5 (16) 88.6 (7) 112.8 (12) 18 Molinate 9.76 126.10>55.00 14 6 0.007 – 72.8 (19) 87.5 (11) 19 Tritosulfuron 9.83 161.05>141.05 11 22 0.009 94.1 (17) 113.9(18) 98.8(10) 20 Picloram 9.99 196.00>161.00 15 23 0.009 116.3 (14) 85.8 (14) 81.4 (14) 21 Propachlor 11.04 176.10>57.10 10 24 0.009 98.6 (19) 103.4(12)
22 Ethoprophos 11.45 158.00>96.95 18 8 0.006 92.4 (8) 92.9 (6) 100.1 (7) 23 Diphenylamine 11.45 169.10>66.00 24 28 0.008 106.5 (12) 77.2 (12) 99.8 (12) 24 Omethoate 11.57 156.05>110.00 8 22 0.010 – 84.7(15) 98.9(19) 25 Flonicamid 11.65 174.00>146.05 13 24 0.009 84.9 (21) 108.3(10) 106.6(10) 26 Ethalfluralin 11.67 316.10>276.00 10 24 0.008 78.3 (6) 80.2 (5) 89.4 (9) 27 Trifluralin 12.01 306.10>264.10 8 14 0.009 70.6 (9) 78.9 (2) 89.1 (10) 28 Benfluraline 12.12 292.10>264.00 8 22 0.006 103.3 (10) 84.9 (11) 88.0 (9) 29 Sulfotep 12.14 322.00>202.00 10 18 0.007 86.9 (14) 86.2 (10) 101.7 (14) 30 Bendiocarb 12.33 166.10>151.10 10 20 0.010 116.8 (5) 102.8 (17) 112.1 (8) 31 Pencycuron 12.61 209.00>180.00 8 20 0.008 – 95.2 (19) 72.6 (17) 32 α-HCH 12.90 218.90>182.90 8 20 0.009 71.1 (10) 85.1 (5) 99.2 (11) 33 Thiometon 13.15 246.00>88.00 6 15 0.009 79.5 (15) 93.5 (16) 98.0 (13)
34 Dimethoate 13.15 125.00>79.00 8 14 0.010 – 79.6 (12) 90.3 (16) 35 Prosulfuron 13.40 188.00>168.05 8 16 0.009 – 75.6 (16) 78.2 (8) 36 Ethoxyquin 13.61 202.15>174.10 16 21 0.010 – 76.9 (5) 74.1 (9) 37 Carbofuran 13.87 164.10>149.10 8 18 0.010 107.8 (14) 89.8 (13) 93.9 (14) 38 Dicloran 13.97 205.95>176.00 13 26 0.010 84.4 (10) 74.7 (16) 82.4 (19) 39 Clomazone 14.13 204.10>107.00 20 26 0.009 119.0 (17) 98.1 (19) 101.4 (12) 40 Simazine 14.18 201.10>173.10 6 6 0.010 74.2 (20) 79.9(13) 82.6(16) 41 Monolinuron 14.28 214.05>61.05 9 27 0.009 110.4 (11) 72.9 (9) 74.2 (11) 42 Propazine 14.36 229.10>58.00 14 8 0.010 77.3 (13) 77.1 (10) 95.5 (12) 43 β-HCH 14.39 218.90>182.90 8 20 0.007 81.0 (17) 82.0 (7) 96.4 (14) 44 Chlorbufam 14.44 223.05>171.05 9 20 0.009 – 89.2 (16) 93.7 (20) 45 Terbufos 14.48 231.00>128.90 26 14 0.008 102.2 (12) 88.1 (7) 99.5 (9)
46 Disulfoton 14.48 153.00>96.95 11 6 0.010 82.1 (13) 78.0 (13) 87.9 (11) 47 Swep 14.68 218.90>186.90 8 14 0.010 – 87.7 (18) 91.8 (12) 48 Lindane 14.71 218.90>182.90 8 20 0.008 119.8 (3) 90.2 (4) 90.8 (10) 49 Cyanophos 14.73 243.00>109.00 14 6 0.009 102.7 (18) 95.6 (9) 100.0 (14) 50 Diazinon 14.89 304.10>179.10 10 8 0.006 83.1 (18) 85.2 (5) 97.4 (9) 51 Propyzamide 15.04 172.95>144.90 17 27 0.009 – 75.3 (15) 104.5 (10) 52 Pyroquilon 15.17 173.10>130.10 24 22 0.009 111.3 (16) 89.6 (15) 86.1 (13) 53 Dinoterb 15.19 225.05>177.10 9 17 0.008 – 81.6 (16) 73.3 (15) 54 Triallate 15.68 268.10>184.00 20 14 0.010 82.8 (10) 78.5 (13) 96.2 (14) 55 Etrimphos 15.71 292.10>181.10 8 20 0.007 80.9 (7) 91.0 (5) 100.9 (10) 56 Tebupirimfos 15.98 318.10>152.10 14 12 0.010 – 73.1 (13) 82.5 (10) 57 Paraoxon methyl 16.09 230.05>106.00 20 9 0.009 77.1 (16) 72.5(20) 106.9(19)
58 Iprobenphos 16.15 204.00>91.00 8 12 0.010 88.5 (4) 92.8 (7) 104.0 (9) 59 Pirimicarb 16.22 238.10>166.10 12 24 0.008 79.2 (14) 86.2 (6) 98.7 (11) 60 δ-HCH 16.30 218.90>182.90 10 20 0.010 115.5 (13) 89.4 (6) 86.5 (9) 61 Benoxacor 16.32 259.00>120.00 18 8 0.006 98.5 (4) 88.9 (4) 97.9 (10) 62 16.61 269.00>254.00 17 27 0.009 – 75.6 (10) 87.8 (16) 63 Phosphamidon 16.98 264.10>127.10 14 8 0.010 98.5 (5) 96.4 (5) 103.2 (7) 64 Acetochlor 17.15 223.10>132.10 22 10 0.005 82.4 (9) 90.2 (5) 103.3 (11) 65 Chlorpyriphos methyl 17.22 285.90>93.00 22 14 0.010 – 81.3 (6) 89.3 (12) 66 Vinchlozolin 17.53 284.95>212.00 12 14 0.009 98.2 (5) 99.8 (5) 110.5 (9) 67 Alachlor 17.60 188.10>160.10 10 18 0.006 99.2 (12) 91.4 (3) 98.6 (9) 68 Malaoxon 17.62 194.95>109.00 18 11 0.010 88.6 (11) 82.0 (19) 107.2 (9) 69 sulphone 17.62 169.05>125.00 9 14 0.009 – 80.8 (16) 97.5 (13)
82 Malathion 19.44 173.10>127.05 7 17 0.009 – 88.0 (17) 86.6 (10) 83 Aldrin 19.52 262.90>193.00 28 34 0.010 75.8 (9) 70.0 (13) 78.0 (11) 84 Metholachlor-s 19.56 238.10>162.15 14 27 0.008 80.1 (7) 94.1 (2) 107.7 (10) 85 19.61 298.00>241.85 16 7 0.010 – 71.2 (11) 80.9 (19) 86 Chlorpyriphos ethyl 19.72 313.90>257.85 16 9 0.006 77.2 (12) 83.4 (6) 91.6 (9) 87 Thiobencarb 19.80 257.10>100.00 8 20 0.010 87.5 (16) 75.7 (13) 91.4 (12) 88 19.97 300.90>222.85 25 17 0.005 96.2 (4) 87.6 (8) 97.4 (11) 89 Fenthion 20.00 278.00>109.00 20 14 0.006 – 80.0 (5) 97.9 (12) 90 Fenpropimorph 20.05 128.15>71.10 16 10 0.008 107.0 (12) 73.1 (16) 89.4 (16) 91 Diethofencarb 20.21 267.15>225.10 9 19 0.009 119.4 (5) 88.8 (11) 101.8 (8) 92 Parathion ethyl 20.24 291.10>109.00 14 6 0.009 103.0 (10) 83.2 (6) 92.0 (10) 93 Triadimefon 20.42 208.10>181.00 10 14 0.009 88.0 (15) 98.0 (8) 105.8 (11)
94 Flufenacet 20.46 210.90>123.00 10 6 0.010 82.8 (17) 86.3 (11) 106.3 (13) 95 4,4 20.70 249.95>139.00 16 8 0.010 110.5 (17) 90.5 (9) 86.2 (9) 96 Butraline 20.73 266.15>174.15 25 14 0.006 119.6 (4) 81.9 (9) 87.7 (9) 97 Tetraconazole 20.76 336.05>204.10 28 14 0.009 – 84.0 (8) 101.0 (16) 98 Fosthiazate-1 21.09 283.05>195.00 8 19 0.010 – 96.1 (13) 90.6 (17) 99 21.13 311.00>174.10 17 17 0.010 116.9 (4) 71.6 (13) 88.4 (16) 100 21.21 311.00>174.10 17 17 0.010 118.8 (4) 74.2 (19) 86.1 (13) 101 Fosthiazate-2 21.28 283.05>195.00 8 19 0.010 – 70.9 (9) 87.9 (13) 102 Pendimethalin 21.56 252.10>162.10 10 8 0.009 118.6 (7) 89.5 (14) 74.1 (13) 103 Metazachlor 21.67 209.10>132.10 16 35 0.007 103.9 (8) 97.9 (7) 110.3 (12) 104 Cyprodinil 21.82 224.10>208.10 16 22 0.010 71.9 (16) 72.8 (8) 74.8 (13) 105 Tolylfluanid 22.02 238.00>137.05 16 29 0.009 – 69.3 (18) 113.6 (13)
106 Penconazole 22.09 248.10>157.10 26 14 0.009 116.7 (19) 102.9 (7) 107.3 (13) 107 22.27 322.95>266.90 16 6 0.010 90.7 (17) 90.1 (4) 96.4 (8) 108 Mecarbam 22.38 160.05>132.00 8 19 0.010 72.2 (14) 89.5 (18) 110.0 (14) 109 Phenthoate 22.38 273.90>125.00 20 6 0.010 98.3 (11) 87.7 (8) 107.2 (12) 110 Prallethrin 22.47 123.00>81.00 11 9 0.010 – 88.5 (13) 72.2 (13) 111 Quinalphos 22.49 157.10>129.00 14 24 0.010 74.3 (17) 96.3 (12) 111.6 (13) 112 Pethoxamid 22.51 260.15>147.10 15 20 0.009 112.9 (8) 92.8 (8) 103.3 (18) 113 Fipronil 22.68 366.90>212.90 30 22 0.010 82.9 (8) 89.1 (10) 105.5 (12) 114 Zoxamide 22.75 242.05>214.10 12 21 0.010 – 76.9 (18) 94.5 (14) 115 Procymidone 22.76 283.00>96.05 10 24 0.009 85.9 (12) 93.0 (7) 98.0 (12) 116 Beflubutamid 22.80 355.15>176.15 8 24 0.010 93.4 (20) 89.2 (10) 103.1 (12) 117 Triadimenol 22.87 168.10>70.00 10 4 0.009 117.9 (15) 105.1 (5) 109.0 (16)
118 Folpet 22.92 259.90>130.00 14 20 0.009 – 97.2 (12) 73.8 (19) 119 Triflumizole 23.02 278.10>73.00 6 12 0.010 – 110.4 (11) 117.1 (8) 120 cis-Chlordane 23.04 372.80>265.90 22 10 0.009 73.8 (14) 70.0 (6) 87.4 (7) 121 Bromophos-ethyl 23.10 358.90>302.90 16 10 0.009 84.3 (9) 71.6 (1) 83.9 (9) 122 Methidathion 23.20 145.00>85.05 8 14 0.010 – 86.7 (5) 82.0 (10) 123 α-Endosulfan 23.55 338.90>160.00 18 20 0.009 84.7 (19) 78.0 (20) 94.6 (15) 124 trans-Chlordane 23.59 372.80>265.90 22 12 0.006 73.7 (18) 73.8 (3) 88.3 (18) 125 Butachlor 23.62 188.10>160.10 12 18 0.009 78.9 (18) 90.4 (15) 118.1 (10) 126 Paclobutrazole 23.64 236.10>167.00 10 16 0.010 114.9 (12) 90.9 (8) 110.4 (16) 127 Chlorbenside 23.64 125.00>89.00 16 18 0.010 115.2 (11) 95.4 (15) 103.7 (9) 128 Disulfoton sulfone 23.66 213.05>153.00 8 19 0.010 77.5 (15) 115.3(13) 110.0(18) 129 Flutriafol 24.15 219.10>123.05 16 28 0.010 115.4 (4) 101.5 (8) 110.2 (10)
130 Napropamide 24.18 271.15>128.15 7 17 0.006 75.9 (9) 87.1 (10) 96.9 (13) 131 Mepanipyrim 24.30 222.10>220.00 21 19 0.010 113.2 (8) 72.3 (5) 72.4 (11) 132 Hexaconazole 24.40 214.00>159.00 20 20 0.010 119.6 (17) 99.6 (16) 115.3 (16) 133 Fenamiphos 24.49 303.10>195.10 8 18 0.010 – 72.9 (10) 87.2 (13) 134 Pretilachlor 24.50 262.10>202.10 10 26 0.008 103.4 (6) 89.3 (4) 98.7 (9) 135 Isoprothiolane 24.54 290.10>118.00 14 6 0.010 101.9 (10) 87.0 (12) 102.5 (14) 136 Flutolanil 24.59 323.10>173.05 20 39 0.010 117.3 (6) 92.0 (11) 99.1 (9) 137 Profenophos 24.61 336.90>266.90 14 6 0.009 95.2 (18) 79.5 (9) 92.6 (13) 138 Dieldrin 24.69 276.90>241.00 8 38 0.010 71.1 (18) 72.0 (17) 90.9 (16) 139 p,p-DDE 24.70 246.00>176.05 30 22 0.009 74.2 (7) 71.1 (5) 76.2 (7) 140 Oxadiazon 24.85 258.00>175.00 8 28 0.010 88.9 (20) 87.9(7) 92.6(7) 141 Buprofezin 25.03 172.10>116.10 8 6 0.007 81.1 (19) 76.4 (16) 107.7 (16)
142 25.17 206.10>131.10 14 6 0.007 103.6 (17) 85.9 (10) 99.6 (12) 143 Flusilazole 25.20 233.10>165.10 14 14 0.007 117.4 (16) 108.3 (11) 116.8 (15) 144 Oxyfluorfen 25.22 361.10>299.95 14 6 0.010 117.5 (6) 73.0 (13) 83.9 (11) 145 Myclobutanil 25.22 179.10>125.00 14 8 0.009 79.2 (17) 87.9 (9) 105.4 (13) 146 Endrin 25.47 262.90>193.00 28 22 0.010 91.5 (15) 83.1 (11) 102.2 (12) 147 Cyflufenamid 25.50 412.15>295.10 8 23 0.009 91.6 (10) 85.6 (11) 98.2 (15) 148 Chlorfenapyr 25.54 247.10>227.00 16 24 0.009 86.2 (18) 98.9 (14) 104.5 (16) 149 Fipronilsulphone 25.64 382.95>254.95 21 15 0.008 102.0 (16) 86.1 (9) 98.0 (8) 150 β-Endosulfan 26.03 338.90>160.00 18 8 0.010 71.0 (19) 76.5 (11) 102.6 (20) 151 Chlorobenzilate 26.08 251.05>139.00 16 28 0.008 77.0 (20) 84.2(10) 108.0(14) 152 Oxadiargyl 26.19 340.00>150.00 22 8 0.010 – 70.5 (9) 81.4 (13) 153 Diniconazole 26.24 268.00>232.05 12 24 0.007 108.0 (7) 87.4 (5) 95.6 (9)
154 o,p–DDT 26.26 235.00>165.10 24 16 0.010 105.8 (5) 78.3 (2) 81.5 (9) 155 Fenthion-D 26.34 278.00>169.00 14 20 0.010 – 104.2 (10) 78.9 (9) 156 26.34 279.00>169.05 17 19 0.010 84.9 (9) 73.7 (9) 77.7 (12) 157 Oxadixyl 26.42 233.10>146.10 14 26 0.007 – 91.0 (13) 105.9 (10) 158 Triazophos 27.01 257.00>162.00 8 22 0.010 118.5 (16) 79.7 (19) 100.5 (12) 159 Benalaxyl 27.04 148.15>105.05 16 14 0.007 112.1 (4) 82.9 (5) 97.0 (9) 160 Mepronil 27.07 269.15>119.05 17 6 0.008 109.3 (17) 89.0 (9) 95.6 (9) 161 Carfentrazone 27.19 340.10>312.10 14 28 0.005 103.5 (5) 92.4 (9) 106.4 (12) 162 Edifenfos 27.28 310.00>173.00 14 8 0.010 118.7 (12) 77.4 (7) 87.2 (13) 163 Trifloxystrobin 27.35 222.10>162.10 10 4 0.008 77.4 (14) 85.2 (15) 100.9 (15) 164 27.37 386.80>252.90 16 10 0.010 – 97.0 (10) 97.9 (10) 165 27.37 259.00>69.00 14 8 0.010 – 88.2 (18) 112.6 (13)
166 Chlordecone 27.39 271.85>236.80 17 36 0.009 75.7 (16) 70.3 (7) 79.9 (12) 167 Quinoxyfen 27.42 272.05>237.00 21 36 0.006 70.5 (11) 70.3 (7) 80.0 (12) 168 p,p-DDT 27.49 235.00>165.10 24 16 0.010 89.5 (6) 70.5 (6) 74.2 (10) 169 27.56 259.00>69.05 14 8 0.009 – 107.2 (10) 117.4 (9) 170 Fenhexamid 27.66 301.05>97.15 17 27 0.008 – 95.7 (12) 93.1 (15) 171 27.67 412.00>349.00 16 24 0.009 – 89.2 (8) 101.5 (8) 172 27.71 349.05>266.05 12 17 0.010 – 78.1 (11) 90.2 (15) 173 Fluopicolide 27.79 347.00>173.00 26 35 0.010 91.0 (19) 87.4 (13) 98.4 (11) 174 Diclofop 28.06 340.00>252.95 13 26 0.010 – 112.9 (8) 107.0 (15) 175 Proquinazid 28.09 329.95>287.75 9 24 0.006 – 62.2 (11) 72.0 (8) 176 Triphenyl phosphate 28.12 325.05>169.10 23 23 0.005 101.7 (12) 91.7 (5) 102.2 (7) 177 Diflufenican 28.19 394.10>266.00 14 4 0.008 71.1 (11) 76.4 (2) 86.0 (9)
178 Resmethrin-1 28.28 171.10>128.00 12 6 0.010 – 74.7 (17) 72.4 (11) 179 Resmethrin-2 28.35 171.10>128.00 12 6 0.010 – 93.6 (15) 72.0 (3) 180 Spiromesifen 28.42 272.10>254.10 6 23 0.010 70.2 (14) 82.5 (6) 90.5 (8) 181 Epoxiconazole 28.47 192.05>138.00 14 25 0.007 107.5 (13) 97.1 (7) 106.6 (11) 182 Dimoxystrobin 28.84 205.10>116.10 11 19 0.010 111.9 (10) 91.6 (8) 101.7 (9) 183 Bromuconazole-1 28.92 294.90>172.90 14 28 0.009 107.7 (10) 92.6 (3) 108.2 (11) 184 Bifenthrin 28.94 181.10>166.10 12 12 0.009 71.2 (15) 70.0 (6) 76.1 (7) 185 Iprodione 28.97 314.00>271.00 8 12 0.010 118.7 (4) 81.8 (18) 83.7 (18) 186 29.00 340.90>184.90 20 18 0.006 71.3 (8) 81.1 (5) 90.5 (9) 187 Phenothrin-1 29.00 183.10>153.10 14 14 0.010 – 77.6 (5) 84.8 (9) 188 Phosmet 29.03 160.05>77.05 24 14 0.010 – 74.0 (20) 90.2 (11) 189 Fluxapyoxad 29.12 381.10>159.05 4 16 0.010 118.1 (4) 86.7 (10) 96.9 (10)
190 Methoxychlor 29.18 227.10>169.10 24 14 0.009 115.5 (13) 77.9 (7) 82.1 (13) 191 Etoxazole 29.20 204.15>176.15 12 28 0.010 70.5 (12) 75.0 (15) 85.5 (6) 192 Fenpropathrin 29.24 181.05>152.10 24 24 0.009 74.6 (16) 84.4 (8) 89.7 (6) 193 Fenamidone 29.36 268.10>180.10 16 28 0.008 117.7 (9) 93.8 (7) 107.3 (11) 194 Tebufenpyrad 29.40 333.15>171.10 22 9 0.008 92.0 (7) 82.0 (12) 90.7 (11) 195 Fenazaquin 29.50 160.15>145.10 9 21 0.010 117.1 (6) 72.6 (8) 70.3 (10) 196 Bifenox 29.59 340.95>309.95 10 16 0.010 119.7 (3) 71.4 (13) 72.2 (14) 197 Bromuconazole-2 29.59 294.90>172.90 14 28 0.010 119.5 (2) 83.8 (4) 93.4 (8) 198 Metconazole 29.62 125.05>99.00 19 19 0.009 112.6 (14) 101.7 (15) 100.2 (11) 199 Phenothrin-2 29.77 183.10>153.10 14 14 0.009 – 81.9 (14) 93.7 (17) 200 Tetradifon 29.81 355.85>159.00 13 13 0.009 95.5 (11) 70.6 (8) 82.6 (15) 201 Phosalone 29.99 182.00>111.00 14 8 0.008 71.3 (7) 79.7 (11) 92.4 (10)
202 Triticonazole 30.05 235.10>182.10 14 6 0.009 118.6 (13) 94.7 (7) 108.3 (12) 203 Valifenalate 30.25 212.05>138.05 22 12 0.009 73.8 (20) 79.8 (9) 85.4 (14) 204 30.32 357.10>256.10 10 14 0.006 85.1 (12) 86.4 (7) 99.3 (10) 205 Tralkoxydim 30.43 283.00>227.00 8 23 0.010 79.3 (19) 79.4 (12) 83.7 (18) 206 λ-Cyhalothrin 30.44 197.05>141.10 12 8 0.010 83.5 (17) 78.0 (11) 86.0 (7) 207 Lactofen 30.52 344.00>223.00 17 26 0.007 111.8 (9) 78.0 (9) 81.8 (9) 208 Acrinathrin 30.68 289.10>93.00 14 26 0.007 72.5 (16) 75.5 (7) 86.5 (7) 209 Benfuracarbe 30.68 353.10>190.10 12 20 0.010 116.0 (12) 71.8 (14) 76.5 (13) 210 Pyrazophos 30.74 221.10>193.05 11 17 0.009 – 82.6 (11) 100.8 (11) 211 Fenarimol 30.75 251.00>139.00 14 26 0.009 104.6 (11) 93.2 (6) 102.0 (11) 212 Dialifos 30.94 208.00>181.00 8 24 0.007 95.9 (9) 92.5 (8) 102.8 (11) 213 Azinphos-ethyl 30.96 160.10>132.10 4 12 0.008 140.1 (1) 75.8 (7) 89.2 (13)
214 Isopyrazam 31.02 303.15>159.10 26 16 0.009 72.5 (16) 87.0 (6) 98.1 (6) 215 Permethrin-1 31.49 183.10>153.10 14 14 0.008 78.5 (16) 71.4 (13) 81.7 (9) 216 Bitertanol 31.53 170.10>141.10 22 28 0.008 93.8 (7) 97.5 (6) 104.5 (9) 217 Permethrin-2 31.68 183.10>153.10 14 14 0.010 96.0 (19) 70.5 (17) 81.0 (13) 218 Dioxathion 31.73 271.00>153.05 8 14 0.008 119.6 (10) 97.6 (6) 108.8 (13) 219 Pyridaben 31.74 147.10>117.10 22 14 0.006 108.0 (15) 81.7 (6) 87.7 (8) 220 Prochloraz 31.98 180.10>138.10 12 20 0.010 – 106.5 (8) 114.4 (11) 221 Cyfluthrin-1 32.27 163.00>127.00 5 5 0.010 78.0 (19) 78.2 (16) 85.3 (18) 222 Cyfluthrin-2 32.41 163.00>127.00 5 5 0.010 115.6 (9) 70.5 (5) 73.7 (15) 223 Fenbuconazole 32.44 198.10>129.10 9 27 0.009 101.6 (7) 94.1 (6) 107.6 (10) 224 Cyfluthrin-3 32.55 163.00>127.00 5 5 0.010 84.2 (18) 71.2 (5) 74.0 (13) 225 Cyfluthrin-4 32.69 163.00>127.00 5 5 0.010 76.1 (18) 72.5 (14) 80.8 (9)
226 Cypermethrin-1 32.85 163.00>127.00 5 5 0.009 75.7 (18) 82.4 (8) 85.6 (5) 227 Flucythrinate-1 32.93 199.10>157.10 10 22 0.006 112.3 (7) 89.0 (4) 93.1 (11) 228 Boscalid 32.94 342.10>140.10 14 28 0.005 78.4 (11) 87.0 (4) 102.6 (11) 229 Cypermethrin-2 32.98 163.00>127.00 5 5 0.009 78.0 (12) 113.1 (8) 81.8 (16) 230 Cypermethrin-3 32.98 163.00>127.00 5 5 0.010 92.5 (5) 90.7 (5) 87.9 (7) 231 Cypermethrin-4 32.98 163.00>127.00 5 5 0.010 92.5 (5) 90.7 (5) 94.8 (14) 232 Etofenprox 33.10 163.10>135.10 10 18 0.009 96.3 (12) 72.0 (3) 78.8 (8) 233 Flucythrinate-2 33.22 199.10>157.10 10 22 0.006 70.8 (11) 75.3 (11) 88.7 (11) 234 Fenvalerate 34.03 419.10>225.10 6 12 0.005 114.2 (8) 79.2 (8) 93.4 (13) 235 Tau-fluvalinate-1 34.23 250.10>200.00 20 20 0.010 76.0 (11) 70.5 (8) 81.4 (11) 236 Tau-fluvalinate-2 34.36 250.10>200.00 20 20 0.009 89.6 (14) 73.9 (7) 80.7 (10) 237 Esfenvalerate 34.38 419.10>225.10 6 12 0.008 76.9 (9) 74.4 (11) 86.5 (10)