제17579호                              관             보                 2011. 8.25.(목요일)
8.2.2 모든 농도결과는 방법검출한계를 적용하여 나타내고 방법검출한계 미만은 N.D.로 표시하고 방
법검출한계값을 같이 제시한다.
8.2.3 결과보고 양식은 부록에 제시한 양식에 따른다.
9.0 참고자료
9.1 ISO 25101: 2009(E) Water quality-Determinationof perfluorooctanesulfonate (PFOS) and
perfluorooctanoate (PFOA)-Method for unfiltered samples using solid phase extraction and liquid
chromatography/mass spectrometry.
9.2 EPA Method 537. Determination of selected perfluorinated alkyl acids in drinking water by
solid phase extraction and liquid chromatography/tandem mass spectrometry (LC/MSMS). US
EPA, 2009.
9.3 FDA: Validation of analytical procedures: Methodology, recommended for implementation at
step 7 of the VICH process on 22 October 1998 by the VICH steering committee(64. guidance for
industry), FDA, DHHS, 1998.
9.4 NIOSH. Guidelines for air sampling and analytical method development and
evaluation(DHHS[NIOSH]) Pub. No. 95-117 .Cincinnati, OH: NIOSH, 1995.
9.5 OSHA. Evaluation scheme for methods that use filters as collection medium. In OSHA
analytical manual, 2ed ed. Salt Lake City: OSHA, 1990.
10.0 부록
표1. 과불화합물(PFCs) 분석을 위한 내부표준물질
              분류                          분석물질                       보정용 실린지첨가
                                                                       내부표준물질
                               PFHxA                                      IS#1
                               PFHpA                                      IS#1
  Perfluorocarboxylic acid     PFOA                                       IS#1
                               PFNA                                       IS#1
  (PFCAs)                      PFDA                                       IS#1
                               PFUnDA                                     IS#1
                               PFDoDA                                     IS#1
                               PFTrDA                                     IS#1
  Perfluoroalkyl sulfonate     PFHxS                                      IS#2
  (PFASs)                      PFOS                                       IS#2
                               PFDS                                       IS#2
                               8:2 FTUCA                                  IS#3
  Intermediate                 N-MeFOSAA                                  IS#3
                               N-EtFOSAA
                               13C2-PFHxA
                                                                          IS#3
                               13C5-PFNA
                                                                          IS#1
                               13C2-PFDA
                                                                          IS#1
                               13C2-PFUnDA
                                                                          IS#1
                                                                          IS#1
  정제용 내부표준물질                   13C2-PFDoDA                                IS#1
                               18O2-PFHxS                                 IS#2
                               d5-N-EtFOSAA
                               13C2-8:2FTUCA
                                                                          IS#3
                               13C4-PFOA - IS#1
                                                                          IS#3
  실린지첨가용                                                                    -
                               13C4-PFOS - IS#2                             -
  내부표준물질                       d3-N-MeFOSAA - IS#3                          -
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