Assertion: crystalline acetone solvate | /r/CapableOf | comprise acetone
Facets:
value: in the range
type: LOCATION
Source sentences:
text: Therefore, the present invention also relates to above-described process, wherein subjecting said preferably crystalline acetone solvate to said atmosphere is performed at a temperature in the range of from 20 to 25° C. at ambient pressure for a time in the range of from 72 to 120 h, wherein the relative humidity of the atmosphere is in the range of from 41 to 45%, and wherein, according to an even more preferred embodiment, said crystalline acetone solvate of the compound of formula (I) comprises acetone in the range of from 0.8 to 1.1 mol per mol of the compound of formula (I), has an ICH class 2 solvent content of less than 5 ppm and exhibits monoclinic unit cells having space group P2 1 and having the parameters a=5.72+/−0.05 Angstrom, b=11.82+/−0.05
text: Yet further, the present invention relates to said crystalline compounds of formula (I) wherein said compounds are obtainable or obtained by the above-described process, most preferably by a process wherein a crystalline acetone solvate of the compound of formula (I) is subjected to an atmosphere having a relative humidity in the range of from 41 to 45%, said subjecting being performed at a temperature in the range of from 20 to 25° C. at ambient pressure for a time in the range of from 72 to 120 h, wherein before, during or after said subjecting, exclusively an atmosphere of gaseous water in air is brought into contact with the crystalline acetone solvate of the compound of formula (I), and wherein, preferably, said crystalline acetone solvate of the compound of formula (I) comprises acetone in the range of from 0.8 to 1.1 mol per mol of the compound of formula (I), has an ICH class 2 solvent content of less than 5 ppm and exhibits monoclinic unit cells having space group P2 1 and having the parameters a=5.72+/−0.05 Angstrom, b=11.82+/−0.05