Assertion: crystalline maltose | /r/HasProperty | converted by the ethanol treatment
Facets:
value: in example
type: OTHER
Source sentences:
text: 9 shows powdery X-ray diffraction diagrams of an anhydrous crystalline maltose converted by the ethanol treatment and those of the hydrous crystalline β-maltose of Control 1, anhydrous crystalline α-maltose of Control 2, and anhydrous crystalline β-maltose of Control 3.
text: 10 shows endothermic patterns on differential scanning calorimetry (DSC) of an anhydrous crystalline maltose converted by the ethanol treatment and those of the anhydrous crystalline α-maltose of Control 2 and
text: 11 shows a GLC chromatogram for measuring an α/β anomer ratio of an anhydrous crystalline maltose converted by the ethanol treatment.
text: a: Anhydrous crystalline maltose converted by the ethanol treatment (Present Invention) b: Anhydrous crystalline β-maltose (Control 3)
text: ↓: Characteristic diffraction peaks of the anhydrous crystalline maltose converted by the ethanol treatment
text: a: Anhydrous crystalline maltose converted by the ethanol treatment (Present Invention) b: Anhydrous crystalline β-maltose (Control 3)
text: Anhydrous crystalline maltose converted by the ethanol treatment (Present Invention) :
text: Hereinafter, the anhydrous crystalline maltose, obtained by heating and dehydrating in ethanol, is called as “the anhydrous crystalline maltose converted by the ethanol treatment” in distinction to conventional anhydrous crystalline maltose.
text: The following maltose preparations, (i), (ii), and (iii), were used as Control 1, Control 2, and Control 3, respectively, for comparing the physical properties with those of the anhydrous crystalline maltose converted by the ethanol treatment:
text: SEM photographs of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1, are shown in FIG.
text: Powdery X-ray diffractometry of the anhydrous crystalline maltose converted by the ethanol treatment was carried out using Cu
text: The powdery X-ray diffraction diagram of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 and those of crystalline maltose preparations, Controls 1 to 3, are shown in FIG.
text: 9 , the powdery X-ray diffraction diagram of the anhydrous crystalline maltose converted by the ethanol treatment ( FIG. 9
text: The anhydrous crystalline maltose converted by the ethanol treatment showed characteristic peaks on a powdery X-ray diffraction diagram at diffraction angles (20) of 7.8°, 19.5°, 20.7°, and 22.6°, which are not detected in the crystalline maltoses of Controls 1 to 3.
text: The results indicate that the anhydrous crystalline maltose converted by the ethanol treatment has a crystal form completely different from those of well-known crystalline maltose.
text: The endothermic pattern of the anhydrous crystalline maltose, converted by the ethanol treatment in Example 1, and those of the anhydrous crystalline maltoses of Control 2 and Control 3 are shown in FIG.
text: 10 , an endothermic pattern of the anhydrous crystalline maltose converted by the ethanol treatment ( FIG. 10
text: The endothermic pattern of the anhydrous crystalline maltose converted by the ethanol treatment was completely different from those of the anhydrous crystalline maltoses of Control 2 and Control 3.
text: Based on the facts that a powdery X-ray diffraction diagram and an endothermic pattern on DSC analysis of the anhydrous crystalline maltose converted by the ethanol treatment were completely different from those of the conventional well-known anhydrous crystalline maltoses used as Control 2 and Control 3, the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 is concluded to be a novel anhydrous crystalline maltose.
text: Based on the facts that a powdery X-ray diffraction diagram and an endothermic pattern on DSC analysis of the anhydrous crystalline maltose converted by the ethanol treatment were completely different from those of the conventional well-known anhydrous crystalline maltoses used as Control 2 and Control 3, the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 is concluded to be a novel anhydrous crystalline maltose.
text: Successively, a melting point and an anomer ratio of the anhydrous crystalline maltose converted by the ethanol treatment were measured and the results were compared with those of the conventional anhydrous crystalline maltoses of Control 2 and Control 3 in the following Examples 2-4 and 2-5.
text: The melting point of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 was measured by conventional method using
text: As a result, it was revealed that the melting point of the anhydrous crystalline maltose converted by the ethanol treatment is 154 to 159° C.
text: The anhydrous crystalline maltose converted by the ethanol treatment in Example 1 is completely different from the conventional well-known anhydrous crystalline
text: About 70 mg of an anhydrous crystalline maltose, converted by the ethanol treatment in Example 1, was dissolved in 5 ml of anhydrous pyridine.
text: A GLC chromatogram of the anhydrous crystalline maltose converted by the ethanol treatment is shown in FIG.
text: 11 , Symbol “b”) contents of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 were 5.5% and 94.5%, respectively, and the anhydrous crystalline maltose was made up of a majority of β-anomer.
text: From the results in Example 2-5, it was revealed that the anhydrous crystalline maltose converted by the ethanol treatment is a β-maltose.
text: Based on the result, the anhydrous crystalline maltose converted by the ethanol treatment is called as “the anhydrous crystalline β-maltose converted by the ethanol treatment”, hereinafter.
text: 9 shows powdery X-ray diffraction diagrams of an anhydrous crystalline maltose converted by the ethanol treatment and those of the hydrous crystalline β-maltose of Control 1, anhydrous crystalline α-maltose of Control 2, and anhydrous crystalline β-maltose of Control 3.
text: 10 shows endothermic patterns on differential scanning calorimetry (DSC) of an anhydrous crystalline maltose converted by the ethanol treatment and those of the anhydrous crystalline α-maltose of Control 2 and
text: 11 shows a GLC chromatogram for measuring an α/β anomer ratio of an anhydrous crystalline maltose converted by the ethanol treatment.
text: a: Anhydrous crystalline maltose converted by the ethanol treatment (Present Invention) b: Anhydrous crystalline β-maltose (Control 3)
text: ↓: Characteristic diffraction peaks of the anhydrous crystalline maltose converted by the ethanol treatment
text: a: Anhydrous crystalline maltose converted by the ethanol treatment (Present Invention) b: Anhydrous crystalline β-maltose (Control 3)
text: Hereinafter, the anhydrous crystalline maltose, obtained by heating and dehydrating in ethanol, is called as “the anhydrous crystalline maltose converted by the ethanol treatment” in distinction to conventional anhydrous crystalline maltose.
text: The following maltose preparations, (i), (ii), and (iii), were used as Control 1, Control 2, and Control 3, respectively, for comparing the physical properties with those of the anhydrous crystalline maltose converted by the ethanol treatment:
text: SEM photographs of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1, are shown in FIG.
text: Powdery X-ray diffractometry of the anhydrous crystalline maltose converted by the ethanol treatment was carried out using Cu
text: The powdery X-ray diffraction diagram of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 and those of crystalline maltose preparations, Controls 1 to 3, are shown in FIG.
text: 9 , the powdery X-ray diffraction diagram of the anhydrous crystalline maltose converted by the ethanol treatment ( FIG. 9
text: The anhydrous crystalline maltose converted by the ethanol treatment showed characteristic peaks on a powdery X-ray diffraction diagram at diffraction angles (20) of 7.8°, 19.5°, 20.7°, and 22.6°, which are not detected in the crystalline maltoses of Controls 1 to 3.
text: The results indicate that the anhydrous crystalline maltose converted by the ethanol treatment has a crystal form completely different from those of well-known crystalline maltose.
text: The endothermic pattern of the anhydrous crystalline maltose, converted by the ethanol treatment in Example 1, and those of the anhydrous crystalline maltoses of Control 2 and Control 3 are shown in FIG.
text: 10 , an endothermic pattern of the anhydrous crystalline maltose converted by the ethanol treatment ( FIG. 10
text: The endothermic pattern of the anhydrous crystalline maltose converted by the ethanol treatment was completely different from those of the anhydrous crystalline maltoses of Control 2 and Control 3.
text: Based on the facts that a powdery X-ray diffraction diagram and an endothermic pattern on DSC analysis of the anhydrous crystalline maltose converted by the ethanol treatment were completely different from those of the conventional well-known anhydrous crystalline maltoses used as Control 2 and Control 3, the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 is concluded to be a novel anhydrous crystalline maltose.
text: Based on the facts that a powdery X-ray diffraction diagram and an endothermic pattern on DSC analysis of the anhydrous crystalline maltose converted by the ethanol treatment were completely different from those of the conventional well-known anhydrous crystalline maltoses used as Control 2 and Control 3, the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 is concluded to be a novel anhydrous crystalline maltose.
text: Successively, a melting point and an anomer ratio of the anhydrous crystalline maltose converted by the ethanol treatment were measured and the results were compared with those of the conventional anhydrous crystalline maltoses of Control 2 and Control 3 in the following Examples 2-4 and 2-5.
text: The melting point of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 was measured by conventional method using
text: As a result, it was revealed that the melting point of the anhydrous crystalline maltose converted by the ethanol treatment is 154 to 159° C.
text: The anhydrous crystalline maltose converted by the ethanol treatment in Example 1 is completely different from the conventional well-known anhydrous crystalline
text: About 70 mg of an anhydrous crystalline maltose, converted by the ethanol treatment in Example 1, was dissolved in 5 ml of anhydrous pyridine.
text: A GLC chromatogram of the anhydrous crystalline maltose converted by the ethanol treatment is shown in FIG.
text: 11 , Symbol “b”) contents of the anhydrous crystalline maltose converted by the ethanol treatment in Example 1 were 5.5% and 94.5%, respectively, and the anhydrous crystalline maltose was made up of a majority of β-anomer.
text: From the results in Example 2-5, it was revealed that the anhydrous crystalline maltose converted by the ethanol treatment is a β-maltose.
text: Based on the result, the anhydrous crystalline maltose converted by the ethanol treatment is called as “the anhydrous crystalline β-maltose converted by the ethanol treatment”, hereinafter.