Patent Document:

the invention is further described and illustrated by the following embodiments and examples . as a particular description of a tuning example , the following is done . an initial frequency range of either 1 +/− 0 . 3 ghz or 2 . 5 +/− 0 . 5 ghz is considered likely to be optimal . an initial tuning scan of that frequency range is employed starting at 1 ghz . at 1 ghz , an assessment is made of the absorption by the sample in the system . if the absorption is not sufficiently optimized , then an incremental increase in the frequency is made and the absorption is observed at the new frequency . the initial tuning scan is conducted until the absorption is maximal . if the absorption is maximal , then a fine tuning scan is optionally employed to further improve absorption . for tuning , an incremental change in frequency is selected to be approximately an order of magnitude lower than the initial frequency . for fine tuning , an incremental change is selected to be between about an order of magnitude to about three orders of magnitude lower than the initial frequency . for example , if the initial frequency is 1 ghz , then a tuning scan increment can be 0 . 1 ghz and a fine tuning scan increment can be 5 mhz . the increment size for tuning and fine tuning is particularly significant at the lower initial frequencies . the frequency selection , including initial frequency selection and that achieved by tuning and fine tuning , can be influenced by the category of corn . corn categories can include soft , medium , and hard corn . the process can include the delivery of a first volume of corn with treatment of the first volume , followed by delivery of a second volume of corn with treatment of the second volume . the determination of cracking in kernels is known in the art and can be performed using microscopy , back - illumination techniques , or other techniques . as a particular description of a pulse profile , the following is done . an emf is pulsed on for a pulse width of one second followed by a delay ( pulse off ) of 50 seconds . this cycle of pulse and delay is repeated for a period of one hour . next , there is a rest period of between 2 to 8 hours at about less than 75 % r . h ., depending on the desired final moisture level of the drying product . during the rest period , significant migration of moisture from the inside of a corn kernel to the outside continues to occur after the pulsed emf treatment . reduction of moisture in the corn sample can continue to occur immediately following the one hour pulse period and also can continue during later portions of the 8 hour rest period , including portions beyond the initial 45 minutes after the one hour pulse period . the pulse width can vary from about 100 microseconds to about 60 seconds . the delay width can vary from about 1 second to about 3600 seconds . in a particular embodiment the pulse width will have a range from about 0 . 5 seconds to about 5 seconds , and the delay width will range from about 10 seconds to about 5 minutes . in specific embodiments , the invention contemplates application of pulsed emf wherein there is a cycle of pulse and delay , ranging from about 10 minutes to several hours . following such a cycle , the rest period can extend from about 2 hours to about 24 hours . for large scale systems , a power source capable of generating from about 5 to about 20 kw is used . for a particular large scale system , the power source is capable of generating about 10 kw . a conventional fan is optionally used to facilitate removal of moist air and evaporation from the kernel surface . in another example , multiple sources of electromagnetic fields are used . the multiple emf sources can use the same frequency or different frequencies . in a particular embodiment , there is safety equipment for protection of the operator from the emf . for example , a metallic enclosure can be used , such as a metallic storage bin , also equipped with a safety relay capable of automatically shutting down the electrical power to the emf source . as a more foolproof operation , a locked door should be also installed behind the safety relay , that could only be unlocked after the mains power to the emf source was shut down automatically by the relay . corn harvests from two consecutive years were employed for corn drying tests by pulsed emf . the corn selected for such tests was divided into three categories according to the corn hardness : soft corn , medium hardness corn , and hard corn . complete drying curves by both pulsed emf and conventional oven drying , as well as water sorption isotherms of corn were obtained for all three categories of corn . such corn drying curves were found to be significantly different from each other . pulsed emf frequencies that were tested span the range from 30 mhz to 2 . 45 ghz . fastest drying of corn was obtained at 2 . 45 ghz , whereas the lowest percentage of cracks in corn was obtained at 200 mhz for 6 hr exposure to pulsed emf , and an effective applied power level of 1 kw . high - resolution , solid - state ( cp - mass ) nmr and nir techniques were employed to evaluate corn composition and quality factors related to composition . drying of corn at 2 . 45 ghz and microwave pulsed power levels of 500 w achieved corn drying with 1 . 5 hr of pemf energy use , with less than 6 % cracks , for a 10 % r . f . heating cycle . such tests indicate that efficient corn drying from a level of 24 - 20 % moisture to 12 % is feasible by pulsed emf , and that energy savings of about 50 % are practically attained without causing an unacceptably large percentage of cracked corn . the nmr methodology was described in a previous publication ( baianu and kumosinski , 1994 ). the most difficult of the three categories to dry without cracks was found to be the soft corn , with an initial moisture content at harvest of about 24 %. table 1 shows drying efficiency and corn quality results for a pulsed emf application at indicated times for different types and masses of corn . table 2 indicates data corresponding to larger volumes of corn on the order of kilograms . the results of table 2 are consistent with higher efficiency and energy savings at the kilogram scale in comparison to tests of lots about one order of magnitude lower . a greater sample load can translate into such benefits due to the contribution of the favorable filling factor . the combined results at the kilogram scale and the 0 . 1 kg scale indicate the scalable nature of the methods and apparatus of the invention . although applicant does not wish to be bound by a particular theory , a possible simplified explanation of a mechanism , or sequence of events , is as follows . the filling factor , or q - factor , of the equipment is defined as the ratio of the total volume occupied by the wet corn , or any other sample to be treated , to the total volume irradiated by the pulsed emf source in the enclosed system containing the corn , or any other sample . the q - factor is therefore , a unitless real number which is less than 1 . 0 and larger than zero . this factor contributes to the determination of how effectively the energy of the pulsed emf is being used for drying corn . as an example , data from drying several pounds of wet corn when compared to several ounces of wet corn , show a marked increase in the effectiveness of energy usage for drying corn in the case of samples from 2 lbs to 5 lbs , as the q - factor increases from about 0 . 02 to about 0 . 4 , e . g . about twenty - fold . note that an additional contribution to the pemf efficiency for drying is the dielectric ‘ constant ’, or ‘ permitivity ’, ∈ wc , of the wet corn , which — in its turn — depends on both moisture level in the corn and the pemf frequency range . soft , hard , and medium hardness corn from consecutive harvest years was collected in illinois at incoming moisture levels of about 24 %. several sets of fresh corn were dried by pulsed emf within a week from harvesting each year ; the remainder of the corn harvest was stored in 4 separate lots ( see table 3 ). the fewest cracks and best results were obtained only with fresh corn and lot # 1 ( helium - classified corn , stored at 4 ° c .). pulsed emf drying of corn was carried out with laboratory - built , or commercial , resonant probe circuits tuned at frequencies of 30 mhz , 200 mhz , 360 mhz and 2 , 450 mhz ( 2 . 45 ghz ). pulsed emf power sources were operated at 10 levels ranging from 100 w to 1000 w ( 1 kw ). to cover this wide range of frequencies and power levels , four different setups of lab equipment were employed . water sorption isotherm of individual seeds of soft , medium hardness and hard corn were obtained with the isopiestic method , and the aoac salt solution standards , as previously reported ( lioutas et al ., 1986 ). such measurements allowed us to determine specific hydration levels in terms of the total amounts of ‘ bound ’ water ( nb ) for soft , medium , and hard corn , as well as the amounts of ‘ weakly ’ bound , or trapped , water in each type of corn for various relative vapor pressures of water in the corn kernels . this information is useful for both determining the optimum drying level of corn and for selecting the most appropriate corn drying curves / drying rates . corn drying curves demonstrate that pulsed emf does achieve similar results to conventional ( electrical ) oven drying at 95 f , but in a shorter time , and with potential energy savings of about 50 to about 85 % in comparison with conventional , electrical oven drying , as well as natural gas - based drying . fig1 illustrates exemplary drying curves for corn drying by pulsed emf . the invention is further illustrated by fig2 and 3 . in fig2 , a treatment system is depicted , for example for treating a plant product . fig2 specifically illustrates application to corn drying . the system includes a computer operatively connected to a pulsed electromagnetic field generator . a first power source is operatively connected to the computer , and a second power source is operatively connected to the pemf generator . the first and second power source can be the same source or different sources . the generator is connected to an output means for distributing the pulsed emf energy . the output means can treat the product while the product is transported by a conveyor belt . a conventional fan is connected to the corn storage area for facilitating movement of ambient air to assist in removal of moist air and evaporation from the product surface . the computer controls treatment conditions , for example the pulse length and delay , the frequency selection , and can facilitate drying while optimizing energy usage and achieving desired corn quality . a power source 30 is connected to a computer / pulse controller 10 which is further connected to a pemf generator source 20 . a waveguide 24 is used to deliver waves directed to a sample chamber 40 . a low power fan 50 is mounted to the chamber 40 . a conveyer 70 is used to transport a sample 60 for exposure to the waves . the treated sample 80 is conveyed to a receptacle 90 or support surface . the receptacle 90 is operatively connected to a fan 100 . the corn to be treated or wet corn is represented by the open circles , and the treated corn or dried corn is represented by the filled circles . the receptacle 90 can be a storage bin or conventional corn drying bin or system for further processing . fig3 illustrates another system for drying agricultural products , particularly applicable for drying corn or other grains . the system includes a computer operatively connected to a pulsed electromagnetic field generator . the generator is connected to an output means for distributing the pemf energy . the output means can be variably placed along a vertical axis that is perpendicular to the product container bottom . upon distribution of a sample material in a layer within the container , the treatment can occur while the output means is located vertically so as to maximize irradiation of the sample layer . irradiation is applied until a desired level of drying is achieved for the layer . upon further distribution of a second layer , the output means may be moved so as to maximize irradiation for the second layer . additional layers are further contemplated with analogous treatment . a conventional fan is optionally connected to the corn storage area for facilitating movement of ambient air to assist in removal of moist air and evaporation from the product surface . the computer controls treatment conditions , for example the pulse length and delay , the frequency selection , and can facilitate drying while optimizing energy usage and achieving desired corn quality . a power source 30 is connected to a computer / pulse controller 10 which is further connected to a pemf generator source 20 . a waveguide 24 is used to deliver waves directed to a sample chamber 94 . the waveguide 24 is mounted to 94 in an adjustable , such as vertically adjustable manner . optionally it can be horizontally adjustable or rotatably adjustable around the perimeter of the chamber . a transporting or delivery means 74 is used to provide a sample 60 for exposure to the waves . the treated sample 80 is retained in a storage chamber 94 or support surface . the chamber 94 is operatively connected to a fan 100 . the corn to be treated or wet corn is represented by the open circles , and the treated corn or dried corn is represented by the filled circles . as the corn is deposited in the chamber , layers are formed . in a specific embodiment , the waveguide is positioned initially towards a bottom layer and after time is moved up to be adjacent to an upper layer . soybeans obtained in the united states were treated with a method and apparatus of the invention . results are shown in table 4 . soybeans are sensitive to harsh drying conditions in that certain valuable oils can be reduced or degraded . therefore , the application of pemf is useful in enhancing the optimal retention of such compounds . fig4 and fig5 illustrate processes in embodiments of the invention . fig4 illustrates a process system that has a feedback feature . the feedback is accomplished using an nir monitor . an nir monitor can monitor spectra for water but can also be used to monitor the whole corn composition including extractable starch and protein content . fig5 illustrates a process system without a feedback feature . an example of a potential advantage of a system with feedback ( as illustrated in fig5 ) is the optimization of results such as corn quality and drying efficiency . in contrast , a system without feedback is likely to produce dried corn of suboptimal , or inferior , quality . in a feedback system , the nir monitor can be used to signal / control further treatment depending on the drying state as measured on a continuous , regular , or intermittent basis . if a desired moisture content for corn is 12 % and the nir monitor reflects a determination corresponding to 18 %, then further treatment cycles can be signaled . if the nir monitor reflects an observed drying curve that deviates from a desired standard drying curve , a signal can alter the pulse profile . for example , if the observed drying data indicates too rapid drying that could degrade corn quality , a signal can delay or alter further treatment , such as by temporally spacing pulses further apart or reducing the number of pulses . on the other hand , observed drying data that correlates with a drying process that is proceeding too slowly can lead to a signal that increases the number of pulses or decreases pulse delay times . the nir monitor thus accomplishes the optimization of a drying curve resulting in advantages such as one or more of energy efficiency , time efficiency , and quality control . fig6 illustrates a computer program in flow chart form . the diagram depicts logical steps of the computer program that was employed for controlling the emf source with dc square pulses . the program is implemented in the basic language ( ibm co ., usa ) and was also tested under microsoft windows (™) 1998 , 2000 , and xp . the program is also performed as known in the art , for example in visual basic or higher level languages ( e . g . c - language ), as well as older programming languages such as fortran and algol . the program in basic is preferred because of the simpler hardware and lower operation costs for the dc pulse generating board / source . fig7 illustrates an apparatus embodiment . the apparatus employs an emf generator and demonstrates applicable connections among a sample load , applicator , dummy load , tuner , and terminator or short - circuit . here , a tuner matches impedance between an emf source and a sample load ( a bin at least partially filled with corn , for example ), so that power transmission is optimal when the impedance at source and at sample load are equal . the circulator next to the tuner assists in protecting the emf source from reflected power in an open circuit situation ( in this case the impedance matching is occurring either through the dummy load or the power out is short - circuited by the shown terminator at the end of the waveguide or ‘ horn ’). the applicator is also useful for proper handling of emf power to the sample . the equipment has an electrical circuit that can be adjusted to obtain maximum emf output for the same power type employed , for example either direct current ( dc ) or more typically , alternating current ( ac ) power . this circuit can therefore be specified as a matching network . in some instances for emf systems , such an adjustment is carried out by a manufacturer either under “ no load ” conditions , with no sample in the emf enclosure of selected design but with a ‘ dummy ’ load instead , or with an average load for the expected most frequent samples to be treated . further energy savings and increased effectiveness of energy use are however achieved by matching the impedance of a sample , for example , wet corn , with that of the matching network in the emf source . achievement of such matching impedance thus allows for maximum transfer of energy from the emf source to the sample to be treated , or dried , such as wet corn . the matching impedance can be established at the beginning of the drying process . optionally , the matching impedance can be established subsequently on an intermittent or continuous basis during the drying process . the establishment of matching networks and matching impedance can result in efficient tuning and operation over a wide range of emf frequencies and with pulsed emf power . a suggested computer component is a personal computer ( pc ) with windows or dos operating system and basica (™) or visualbasic (™) installed . a pulse controller component can be a pc , dc - pulse board , either 8 - bit , 12 - or 16 - bit . a near infrared monitoring system can be an nir spectrometer system obtained from ocean optics ( dunedin , fla ., usa ), a nir spectrometer system such as model no . zx - 50 from zeltex , inc . ( hagerstown , md .) or other equivalent as known in the art . other components for apparatus that are suggested include a high power , continuously controllable emf source , such as those manufactured by boonton electronics ( parsippany , n . j . ), ca , varian , bruker ( usa ) or ge ( schenectady , n . y .) models , 1 kw emf power , either cw ( continuous wave ) or pulsed power ( pw ), the latter being preferred . further appropriate options for emf power source include an industrial cw magnetron capable of 896 mhz and 915 mhz transmission such as model cwm - 50l by california tube laboratory , inc . ( watsonville , calif . ); and a 1 to 6 kw emf power magnetron model such as those manufactured by varian , inc . ( palo alto , calif .). a suggested power source component for a particular application can have specifications dependent on the particular application and variables such as bin size . for a corn drying application , the emf power range is specified as a 1 kw to 50 kw emf source , for example from varian , inc . or ge . preferred ranges are about 1 kw to about 10 kw and about 1 kw to about 20 kw . the emf can be either pulsed or continuous . in a preferred example , the emf is capable of pulsed operation with an external trigger . all references throughout this application , for example publications , patents , and patent documents , are hereby incorporated by reference herein in their entireties , as though individually incorporated by reference , to the extent each reference is at least partially not inconsistent with the disclosure in this application ( for example , a reference that is partially inconsistent is incorporated by reference except for the partially inconsistent portion of the reference ). the invention has been described with reference to various specific and preferred embodiments and techniques . however , it should be understood that many variations and modifications may be made while remaining within the spirit and scope of the invention . it will be apparent to one of ordinary skill in the art that methods , devices , device elements , materials , procedures and techniques other than those specifically described herein can be applied to the practice of the invention as broadly disclosed herein without resort to undue experimentation . all art - known functional equivalents of methods , devices , device elements , materials , procedures and techniques described herein are intended to be encompassed by this invention . whenever a range is disclosed , all subranges and individual values are intended to be encompassed . this invention is not to be limited by the embodiments disclosed , including any shown in the drawings or exemplified in the specification , which are given by way of example and not of limitation . lioutas , t ., baianu , i . c . & amp ; m . p . steinberg . 1986 . arch . biochem . biophys . 23 : 236 - 247 . baianu , i . c . & amp ; kumosinski , t . 1994 . ; “ nmr principles and applications to the structure and hydration of food systems with emphasis on proteins ,” ch . 9 in ‘ physical chemistry of food processes : advanced techniques , structures and applications ’. vol . 2 . , i . c . baianu , h . pessen & amp ; t . kumosinski , t ., eds ., new york : van nostrand reinhold -. intl . thompson pubis ., pp . 338 - 420 . baianu , i . c ., k . a . rubinson and j . patterson . 1979 . ferromagnetic resonance and spin wave excitations in metallic glasses . j . phys . chem . solids , 40 : 940 - 951 . baianu , i . c ., j . patterson and k . a . rubinson . 1979 . ferromagnetic resonance observations of surface effects , magnetic ordering and inhomogeneous anisotropy in a metallic glass , material sci . and engineering , 40 : 273 - 284 . baianu , i . c ., k . a . rubinson and j . patterson . 1979 . the observation of structural relaxation in a fenipb glass by x - ray scattering and ferromagnetic resonance ., physica status solidi ( a ), 53 : k133 - 135 . scott , t . c ., klungness , j ., lentz , m , horn , e . and akhtar , m . 2002 . microwaving logs for energy savings and improved paper properties for mechanical pulps . in : proceed . 2002 tappi technical conf . trade fair , san diego , calif ., tappi press : atlanta , ga ., 10 pp . emam o a , farag s a , aziz n h , z lebensm unters forsch . 1995 , dec . 201 ( 6 ): 557 - 61 , comparative effects of gamma and microwave irradiation on the quality of black pepper .

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