New Jersey Administrative Code › Title 7 - ENVIRONMENTAL PROTECTION › Chapter 26F - HEATING OIL TANK SYSTEM REMEDIATION RULES › Subchapter 2 - GENERAL REMEDIATION REQUIREMENTS › Section 7:26F-2.2 - Sample analysis

Current through Register Vol. 56, No. 14, July 15, 2024
(a) The owner shall have all soil and water samples collected in accordance with the requirements for Quality Assurance for Sampling and Laboratory Analysis in the Technical Requirements for Site Remediation at N.J.A.C. 7:26E-2.
(b) The owner shall have all soil and water samples collected and analyzed:
1. By a laboratory certified to analyze the contaminants in question pursuant to the Regulations Governing the Certification of Laboratories and Environmental Measurements, N.J.A.C. 7:18;
2. In accordance with the requirements for Quality Assurance for Sampling and Laboratory Analysis in the Technical Requirements for Site Remediation at N.J.A.C. 7:26E-2; and
3. For the applicable parameters listed in Table 2-1 below.
Table 2-1
Analytical Requirements for Samples from Heating Oil Tank System Discharges
Type of Heating Oil
Soil
Water
No. 2 Heating Oil
Extractable petroleum hydrocarbons (EPH)1 Analyze 25 percent of samples that contain EPH greater than 1,000 mg/kg for Naphthalene7 and 2-Methyl Naphthalene7, 8
VO+TICs2 SVO+TIC4
No. 4 and No. 6 Heating Oil
Extractable petroleum hydrocarbons(EPH)1 Analyze 25 percent of samples for PAH6 when EPH is detected over 100 mg/kg7
VO+TICs3, SVO+TICs5
Kerosene
VO+TICs3, Naphthalene, 2-Methyl Naphthalene
VO+TICs3, SVO+TICs5
Footnotes
1. Extractable petroleum hydrocarbons (EPH). Analyze for EPH using the method, "Analysis of extractable petroleum hydrocarbon (EPH) compounds in non-aqueous and aqueous matrices," at
www.nj.gov/dep/srp/guidance/srra/eph_protocol.pdf
, as supplemented or amended.
2. United States Environmental Protection Agency (EPA) Target Compound List volatile organic compounds including 1,2,4-Trimethylbenzene, but excluding 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, and 1,4-Dioxane with a library search of the 15 highest Tentatively Identified Compounds (TICs).
TICs for volatiles -- Identify up to 15 organic compounds of greatest concentration that are not surrogates, internal standards, or targeted compounds listed under TCL.
3. EPA Target Compound List volatile organic compounds excluding 1,2-Dibromo-3-chloropropane, 1,2-Dibromoethane, and 1,4-Dioxane with a library search of the 15 highest TICs.
TICs for volatiles -- Identify up to 15 organic compounds of greatest concentration that are not surrogates, internal standards, or targeted compounds listed under TCL.
4. EPA Target Compound List semi-volatile organic compounds including 1-Methyl Naphthalene, but excluding phenol and substituted phenols with a library search of the 15 highest TICs.
TICs for semi-volatiles -- Identify up to 15 organic compounds of greatest concentration that are not surrogates, internal standards, or targeted compounds listed under TCL.
5. EPA Target Compound List semi-volatile organic compounds excluding phenol and substituted phenols with a library search of the 15 highest TICs.
TICs for semi-volatiles -- Identify up to 15 organic compounds of greatest concentration that are not surrogates, internal standards, or targeted compounds listed under TCL.
6. EPA Target Compound List Polynuclear Aromatic Hydrocarbons (PAH).
7. Conduct the additional analyses on sample(s) with the highest EPH concentration(s), with a minimum of one sample.
8. May perform synthetic precipitation leaching procedure (SPLP) extraction to develop a site specific impact to ground water remediation standard for 2-Methyl Naphthalene (see
http://www.nj.gov/dep/srp/guidance/rs/index.html
, as supplemented or amended).