Indiana Administrative Code › Title 327 - WATER POLLUTION CONTROL DIVISION › Article 8 - PUBLIC WATER SUPPLY › Rule 2.5 - Disinfectants and Disinfection › Section 2.5-5 - Analytical requirements; disinfectant residuals, disinfection byproducts, and disinfection byproducts precursors

Current through July 10, 2024
Authority: IC 13-13-5-1; IC 13-14-8-2; IC 13-14-8-7; IC
				  13-18-3-2
Affected: IC 13-12-3-1; IC 13-13-5-2; IC 13-14-9; IC
				  13-18-11
Sec. 5.
(a) Systems
				shall use only one (1) or more of the analytical methods specified in this
				subsection or an EPA-approved equivalent method to demonstrate compliance with
				this rule. These methods are incorporated by reference and may be obtained as
				follows:
(1) EPA Method 552.1 is in Methods
				for the Determination of Organic Compounds in Drinking Water-Supplement II,
				U.S. EPA, August 1992, EPA/600/R-92/129 (available through National Information
				Technical Service (NTIS), PB92-207703).
(2) EPA Methods 502.2, 524.2, 551.1, and
				552.2 are in Methods for the Determination of Organic Compounds in Drinking
				Water-Supplement III, U.S. EPA, August 1995, EPA/600/R-95/131 (available
				through NTIS, PB95-261616).
(3) EPA
				Methods 300.0 and 150.1 are in Methods for the Determination of Inorganic
				Substances in Environmental Samples, U.S. EPA, August 1993, EPA/600/R-93/100
				(available through NTIS, PB94-121811).
(4) EPA Methods 300.1 and 321.8 are in
				Methods for the Determination of Organic and Inorganic Compounds in Drinking
				Water Volume 1, U.S. EPA, August 2000, EPA 815-R-00-014 (available through
				NTIS, PB2000-106981).
(5) EPA
				Method 317.0, Revision 2.0, "Determination of Inorganic Oxyhalide Disinfection
				By-Products in Drinking Water Using Ion Chromatography with the Addition of a
				Postcolumn Reagent for Trace Bromate Analysis", U.S. EPA, July 2001, EPA
				815-B-01-001 may be accessed and downloaded directly online at
				http://www.epa.gov/safewater/methods/sourcalt.html.
(6) EPA Method 326.0, Revision 1.0,
				"Determination of Oxyhalide Disinfection By-Products in Drinking Water Using
				Ion Chromatography Incorporating the Addition of a Suppressor Acidified
				Postcolumn Reagent for Trace Bromate Analysis", U.S. EPA, June 2002, EPA
				815-R-03-007 may be accessed and downloaded directly online at
				http://www.epa.gov/safewater/methods/sourcalt.html.
(7) EPA Method 327.0, Revision 1.1,
				"Determination of Chlorine Dioxide and Chlorite Ion in Drinking Water Using
				Lissamine Green B and Horseradish Peroxidase with Detection by Visible
				Spectrophotometry", U.S. EPA, May 2005, EPA 815-R-05-008 may be accessed and
				downloaded directly online at
				http://www.epa.gov/safewater/methods/sourcalt.html.
(8) EPA Method 552.3, Revision 1.0.
				"Determination of Haloacetic Acids and Dalapon in Drinking Water by
				Liquid-liquid Microextraction, Derivitization, and Gas Chromatography with
				Electron Capture Detection", U.S. EPA, July 2003, EPA 815-B-03-002 may be
				accessed and downloaded directly online at
				http://www.epa.gov/safewater/methods/sourcalt.html.
(9) EPA Method 415.3, Revision 1.1,
				"Determination of Total Organic Carbon and Specific UV Absorbance at 254 nm in
				Source Water and Drinking Water", U.S. EPA, February 2005, EPA/600-R-05/055 may
				be accessed and downloaded directly online at
				http://www.epa.gov/nerlcwww/ordmeth.html.
(10) EPA Method 200.7 is found in "Methods
				for the Determination of Metals in Environmental Samples - Supplement I", U.S.
				EPA, May 1994, EPA 600-R-94-111(available through NTIS PB95-125472).
(11) Standard Methods 3111 B and 3500-Mg E
				must be followed in accordance with Standard Methods for the Examination of
				Water and Wastewater, 18th Edition or 19th Edition, American Public Health
				Association, 1992 and 1995, respectively. The cited method published in either
				edition may be used. Copies may be obtained from the American Public Health
				Association, 1015 Fifteenth Street NW, Washington, D.C. 2000Sec. 5.
(12) Standard Method 3120 B must be followed
				in accordance with the Standard Methods for the Examination of Water and
				Wastewater, 18th Edition, 19th Edition, or 20th Edition, American Public Health
				Association, 1992, 1995, and 1998 respectively. The cited method published in
				any of these three (3) editions may be used. Copies may be obtained from the
				American Public Health Association, 1015 Fifteenth Street NW, Washington, D.C.
				2000Sec. 5.
(13) Standard Methods
				4500-Cl D, 4500-Cl E, 4500-Cl F, 4500-Cl G, 4500-Cl H, 4500-Cl I,
				4500-ClO2 D, 4500-ClO2 E,
				4500-H+ B, 6251 B, and 5910 B shall be followed in
				accordance with Standard Methods for the Examination of Water and Wastewater,
				19th Edition or 20th Edition, American Public Health Association, 1996 and
				1998, respectively. The cited methods published in either edition may be used.
				Copies may be obtained from the American Public Health Association, 1015
				Fifteenth Street NW, Washington, D.C. 2000Sec. 5.
(14) Standard Method 3500-Mg B must be
				followed in accordance with Standard Methods for the Examination of Water and
				Wastewater, 20th Edition, American Public Health Association, 1998. Copies may
				be obtained from the American Public Health Association, 1015 Fifteenth Street
				NW, Washington, D.C. 2000Sec. 5.
(15) Standard Methods 5310 B, 5310 C, and
				5310 D shall be followed in accordance with the Supplement to the 19th Edition
				of Standard Methods for the Examination of Water and Wastewater, American
				Public Health Association, 1996 or the Standard Methods for the Examination of
				Water and Wastewater, 20th Edition, 1998. The cited methods published in either
				edition may be used. Copies may be obtained from the American Public Health
				Association, 1015 Fifteenth Street NW, Washington, D.C. 2000Sec. 5.
(16) Standard Methods 4500-Cl D-00, 4500-Cl
				E-00, 4500-Cl F-00, 4500-Cl G-00, 4500-Cl H-00, 4500-Cl I-00,
				4500-ClO2 E-00, 6251 B-94, 5310 B-00, 5310 C-00, 5310
				D-00, and 5910 B-00 are available at http://www.standardmethods.org or at EPA's
				Water Docket at 1301 Constitution Avenue NW, EPA West, Room B, Washington, D.C.
				20460. The year in which each method was approved by the Standard Methods
				Committee is designated by the last two (2) digits in the method number. The
				methods listed are the only online versions that are IBR-approved.
(17) ASTM Methods D 1253-86 and D 1253-86
				(reapproved 1996) shall be followed in accordance with the Annual Book of ASTM
				Standards, Volume 11.01, American Society for Testing and Materials, 1996
				edition, or any ASTM edition containing the IBR-approved version of the method
				may be used. Copies may be obtained from the American Society for Testing and
				Materials, 100 Barr Harbor Drive, West Conshohocken, Pennsylvania
				19428.
(18) ASTM Methods D 511-93A
				and D 511-93B shall be followed in accordance with the Annual Book of ASTM
				Standards, Volumes 11.01 and 11.02, American Society for Testing and Materials,
				1994, 1996, 1999, or any ASTM edition containing the IBR-approved version of
				the method may be used. Copies may be obtained from the American Society for
				Testing and Materials, 100 Barr Harbor Drive, West Conshohocken, Pennsylvania
				19428.
(19) ASTM Method D 1253-03
				shall be followed in accordance with the Annual Book of ASTM Standards, Volume
				11.01, American Society for Testing and Materials, 2004 or any ASTM edition
				containing the IBR-approved version of the method may be used. Copies may be
				obtained from the American Society for Testing and Materials, 100 Barr Harbor
				Drive, West Conshohocken, Pennsylvania 19428.
(20) ASTM Method D 6581-00 shall be followed
				in accordance with the Annual Book of ASTM Standards, Volume 11.01, American
				Society for Testing and Materials, 2001 or any ASTM edition containing the
				IBR-approved version of the method may be used. Copies may be obtained from the
				American Society for Testing and Materials, 100 Barr Harbor Drive, West
				Conshohocken, Pennsylvania 19428.
These methods are also available for copying at the Indiana
				  Department of Environmental Management, Office of Water Quality, 100 North
				  Senate Avenue, Room N1255, Indianapolis, Indiana 46204.