Louisiana Administrative Code › Title 33 - ENVIRONMENTAL QUALITY › Part IX - Water Quality › Subpart 2 - The Louisiana Pollutant Discharge Elimination System (LPDES) Program › Chapter 71 - Appendices › Section IX-7107 - Appendix D-Permit Application Testing Requirements (LAC 33:IX.2501)

Current through Register Vol. 50, No. 6, June 20, 2024
Table I.
Testing Requirements for Organic Toxic
								Pollutants by Industrial Category for Existing Dischargers
GC/MS
								Fraction(1)
Industrial Category
Volatile
Acid
Base/Neutral
Pesticides
Adhesives and Sealants
*
*
*
Aluminum Forming
*
*
*
Auto and Other Laundries
*
*
*
*
Battery Manufacturing
*
*
Coal Mining
*
*
*
*
Coil Coating
*
*
*
Copper Forming
*
*
*
Electric and Electronic Components
*
*
*
*
Electroplating
*
*
*
Explosives Manufacturing
*
*
Foundries
*
*
*
Gum and Wood Chemicals
*
*
*
*
Inorganic Chemicals Manufacturing
*
*
*
Iron and Steel Manufacturing
*
*
*
Leather Tanning and Finishing
*
*
*
*
Mechanical Products Manufacturing
*
*
*
Nonferrous Metals Manufacturing
*
*
*
*
Ore Mining
*
*
*
*
Organic Chemicals Manufacturing
*
*
*
*
Paint and Ink Formulation
*
*
*
*
Pesticides
*
*
*
*
Petroleum Refining
*
*
*
*
Pharmaceutical Preparations
*
*
*
Photographic Equipment and Supplies
*
*
*
*
Plastic and Synthetic Materials Manufacturing
*
*
*
*
Plastic Processing
*
Porcelain Enameling
*
*
*
Printing and Publishing
*
*
*
*
Pulp and Paper Mills
*
*
*
*
Rubber Processing
*
*
*
Soap and Detergent Manufacturing
*
*
*
Steam Electric Power Plants
*
*
*
Textile Mills
*
*
*
*
Timber Products Processing
*
*
*
*
(1) The toxic
				  pollutants in each fraction are listed in Table II.
* Testing required.
Table II
Organic Toxic Pollutants in Each of Four
								Fractions
in Analysis by Gas Chromatography/Mass
								Spectroscopy (GS/MS)
Volatiles
1V
Acrolein
2V
Acrylonitrile
3V
Benzene
5V
Bromoform
6V
Carbon tetrachloride
7V
Chlorobenzene
8V
Chlorodibromomethane
9V
Chloroethane
10V
2-chloroethyl vinyl ether
11V
Chloroform
12V
Dichlorobromomethane
14V
1,1-dichloroethane
15V
1,2-dichloroethane
16V
1,1-dichloroethylene
17V
1,2-dichloropropane
18V
1,3-dichloropropylene
19V
Ethylbenezene
20V
Methyl bromide
21V
Methyl chloride
22V
Methylene chloride
23V
1,1,2,2-tetrachloroethane
24V
Tetrachloroethylene
25V
Toluene
26V
1,2-trans-dichloroethylene
27V
1,1,1-trichloroethane
28V
1,1,2-trichloroethane
29V
Trichloroethylene
31V
Vinyl chloride
Acid Compounds
1A
2-chlorophenol
2A
2,4-dichlorophenol
3A
2,4-dimethylphenol
4A
4,6-dinitro-o-cresol
5A
2,4-dinitrophenol
6A
2-nitrophenol
7A
4-nitrophenol
8A
p-chloro-m-cresol
9A
Pentachlorophenol
10A
Phenol
11A
2,4,6-trichlorophenol
Pesticides
1P
Aldrin
2P
Alpha-BHC
3P
Beta-BHC
4P
Gamma-BHC
5P
Delta-BHC
6P
Chlordane
7P
4,4'-DDT
8P
4,4'-DDE
9P
4,4'-DDD
10P
Dieldrin
11P
Alpha-endosulfan
12P
Beta-endosulfan
13P
Endosulfan sulfate
14P
Endrin
15P
Endrin aldehyde
16P
Heptachlor
17P
Heptachlor epoxide
18P
PCB-1242
19P
PCB-1254
20P
PCB-1221
21P
PCB-1232
22P
PCB-1248
23P
PCB-1260
24P
PCB-1016
25P
Toxaphene
Base/Neutral Compounds
1B
Acenaphthene
2B
Acenaphthylene
3B
Anthracene
4B
Benzidine
5B
Benzo(a)anthracene
6B
Benzo(a)pyrene
7B
3,4-benzofluoranthene
8B
Benzo(ghi)perylene
9B
Benzo(k)fluoranthene
10B
Bis(2-chloroethoxy)methane
11B
Bis(2-chloroethyl)ether
12B
Bis(2-chloroisopropyl)ether
13B
Bis(2-ethylhexyl)phthalate
14B
4-bromophenyl phenyl ether
15B
Butylbenzyl phthalate
16B
2-chloronaphthalene
17B
4-chlorophenyl phenyl ether
18B
Chrysene
19B
Dibenzo(a,h)anthracene
20B
1,2-dichlorobenzene
21B
1,3-dichlorobenzene
22B
1,4-dichlorobenzene
23B
3,3'-dichlorobenzidine
24B
Diethyl phthalate
25B
Dimethyl phthalate
26B
Di-n-butyl phthalate
27B
2,4-dinitrotoluene
28B
2,6-dinitrotoluene
29B
Di-n-octyl phthalate
30B
1,2-diphenylhydrazine (as azobenzene)
31B
Fluoranthene
32B
Fluorene
33B
Hexachlorobenzene
34B
Hexachlorobutadiene
35B
Hexachlorocyclopentadiene
36B
Hexachloroethane
37B
Indeno (1,2,3-cd)pyrene
38B
Isophorone
39B
Naphthalene
40B
Nitrobenzene
41B
N-nitrosodimethylamine
42B
N-nitrosodi-n-propylamine
43B
N-nitrosodiphenylamine
44B
Phenanthrene
45B
Pyrene
46B
1,2,4-trichlorobenzene
Table III
Other Toxic Pollutants (Metals and Cyanide)
								and Total Phenols
Antimony, Total
Arsenic, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Copper, Total
Lead, Total
Mercury, Total
Nickel, Total
Selenium, Total
Silver, Total
Thallium, Total
Zinc, Total
Cyanide, Total
Phenols, Total
Table IV
Conventional and Nonconventional Pollutants
Required to be Tested by Existing
								Dischargers if Expected to be Present
Bromide
Chlorine, Total Residual
Color
Fecal Coliform
Fluoride
Nitrate-Nitrite
Nitrogen, Total Organic
Oil and Grease
Phosphorous, Total
Radioactivity
Sulfate
Sulfide
Sulfite
Surfactants
Aluminum, Total
Barium, Total
Boron, Total
Cobalt, Total
Iron, Total
Magnesium, Total
Molybdenum, Total
Manganese, Total
Tin, Total
Titanium, Total
Table V
Toxic Pollutants and Hazardous Substances
Required to be Identified by Existing
								Dischargers if Expected to be Present
Toxic Pollutants
Asbestos
Hazardous Substances
Acetaldehyde
Allyl alcohol
Allyl chloride
Amyl acetate
Aniline
Benzonitrile
Benzyl chloride
Butyl acetate
Butylamine
Captan
Carbaryl
Carbofuran
Carbon disulfide
Chlorpyrifos
Coumaphos
Cresol
Crotonaldehyde
Cyclohexane
2,4-D (2,4-Dichlorophenoxy acetic acid)
Diazinon
Dicamba
Dichlobenil
Dichlone
2,2-Dichloropropionic acid
Dichlorvos
Diethyl amine
Dimethyl amine
Dinitrobenzene
Diquat
Disulfoton
Diuron
Epichlorohydrin
Ethion
Ethylene diamine
Ethylene dibromide
Formaldehyde
Furfural
Guthion
Isoprene
Isopropanolamine Dodecylbenzenesulfonate
Kelthane
Kepone
Malathion
Mercaptodimethur
Methoxychlor
Methyl mercaptan
Methyl methacrylate
Methyl parathion
Mevinphos
Mexacarbate
Monoethyl amine
Monomethyl amine
Naled
Napthenic acid
Nitrotoluene
Parathion
Phenolsulfanate
Phosgene
Propargite
Propylene oxide
Pyrethrins
Quinoline
Resorcinol
Strontium
Strychnine
Styrene
2,4,5-T (2,4,5-Trichlorophenoxy acetic acid)
TDE (Tetrachlorodiphenylethane)
2,4,5-TP[2- (2,4,5-Trichlorophenoxy) propanoic
								acid]
Trichlorfon
Triethanolamine Dodecylbenzenesulfonate
Triethylamine
Trimethylamine
Uranium
Vanadium
Vinyl Acetate
Xylene
Xylenol
Zirconium
[Note 1: The Environmental Protection Agency has suspended
					 the requirements of
					 40 CFR
					 122.21(g)(7)(ii)(A) and
					 Table I of Appendix D (LAC 33:IX.2501.G.7.b.i and LAC 33:IX.7107.Appendix
					 D.Table I) as they apply to certain industrial categories. The suspensions are
					 as follows.
a. At 46 FR 2046, January
				  8, 1981, the Environmental Protection Agency suspended until further notice
				  40 CFR
				  122.21(g)(7)(ii)(A) (LAC
				  33:IX.2501.G.7.b.i) as it applies to coal mines.
b. At 46 FR 22585, April 20, 1981, the
				  Environmental Protection Agency suspended until further notice
				  40 CFR
				  122.21(g)(7)(ii)(A) (LAC
				  33:IX.2501.G.7.b.i) and the corresponding portions of Item V-C of the NPDES
				  application Form 2c as they apply to:
1.
				  Testing and reporting for all four organic fractions in the Greige Mills
				  Subcategory of the Textile Mills industry (Subpart C-Low water use processing
				  of  40 CFR Part 410 ), and testing and reporting for the pesticide fraction in
				  all other subcategories of this industrial category.
2. Testing and reporting for the volatile,
				  base/neutral and pesticide fractions in the Base and Precious Metals
				  Subcategory of the Ore Mining and Dressing industry (Subpart B of 40 CFR Part
				  440), and testing and reporting for all four fractions in all other
				  subcategories of this industrial category.
3. Testing and reporting for all four GC/MS
				  fractions in the Porcelain Enameling industry.
c. At 46 FR 35090, July 1, 1981, the
				  Environmental Protection Agency suspended until further notice
				  40 CFR
				  122.21(g)(7)(ii)(A) (LAC
				  33:IX.2501.G.7.b.i) and the corresponding portions of Item V-C of the NPDES
				  application Form 2c as they apply to:
1.
				  Testing and reporting for the pesticide fraction in the Tall Oil Rosin
				  Subcategory (Subpart D) and Rosin-Based Derivatives Subcategory (Subpart F) of
				  the Gum and Wood Chemicals industry ( 40 CFR Part 454 ), and testing and
				  reporting for the pesticide and base/neutral fractions in all other
				  subcategories of this industrial category.
2. Testing and reporting for the pesticide
				  fraction in the Leather Tanning and Finishing, Paint and Ink Formulation, and
				  Photographic Supplies industrial categories.
3. Testing and reporting for the acid,
				  base/neutral and pesticide fractions in the Petroleum Refining industrial
				  category.
4. Testing and reporting
				  for the pesticide fraction in the Papergrade Sulfite subcategories (Subparts J
				  and U) of the Pulp and Paper industry (  40 CFR Part 430  ); testing and reporting
				  for the base/neutral and pesticide fractions in the following subcategories:
				  Deink (Subpart Q), Dissolving Kraft (Subpart F), and Paperboard from Waste
				  Paper (Subpart E); testing and reporting for the volatile, base/neutral and
				  pesticide fractions in the following subcategories: BCT Bleached Kraft (Subpart
				  H), Semi-Chemical (Subparts B and C), and Nonintegrated-Fine Papers (Subpart
				  R); and testing and reporting for the acid, base/neutral, and pesticide
				  fractions in the following subcategories: Fine Bleached Kraft (Subpart I),
				  Dissolving Sulfite Pulp (Subpart K), Groundwood-Fine Papers (Subpart O), Market
				  Bleached Kraft (Subpart G), Tissue from Wastepaper (Subpart T), and
				  Nonintegrated-Tissue Papers (Subpart S).
5. Testing and reporting for the base/neutral
				  fraction in the Once-Through Cooling Water, Fly Ash and Bottom Ash Transport
				  Water process wastestreams of the Steam Electric Power Plant industrial
				  category. This revision continues these suspensions. "See Note 1"]
Editorial Note: The words "This revision" refers to the
					 document published at 48 FR 14153, April 1, 1983.
For the duration of the suspensions, therefore, Table 1
					 effectively reads:
Table 1. Testing Requirements for Organic
								Toxic Pollutants by Industry Category
GC/MS
								Fraction(1)
Industrial Category
Volatile
Acid
Base/Neutral
Pesticides
Adhesives and Sealants
*
*
*
Aluminum Forming
*
*
*
Auto and Other Laundries
*
*
*
*
Battery Manufacturing
*
*
Coal Mining
Coil Coating
*
*
*
Copper Forming
*
*
*
Electric and Electronic Components
*
*
*
*
Electroplating
*
*
*
Explosives Manufacturing
*
*
Foundries
*
*
*
Gum and Wood (All Subparts except D and F)
*
*
Subpart D- tall oil rosin
*
*
*
Subpart F-rosin-based derivatives
*
*
*
Inorganic Chemicals Manufacturing
*
*
*
Iron and Steel Manufacturing
*
*
*
Leather Tanning and Finishing
*
*
*
Mechanical Products and Manufacturing
*
*
*
Nonferrous Metal Manufacturing
*
*
*
*
Ore Mining (Applies to the base and precious
								metals/Subpart B)
*
Organic Chemicals Manufacturing
*
*
*
*
Paint and Ink Formulation
*
*
*
Pesticides
*
*
*
*
Petroleum Refining
*
Pharmaceutical Preparations
*
*
*
Photographic Equipment and Supplies
*
*
*
Plastic and Synthetic Materials Manufacturing
*
*
*
*
Plastic Processing
*
Porcelain Enameling
Printing and Publishing
*
*
*
*
Pulp and Paper Mills (See Table 1.A below)
Rubber Processing
*
*
*
Soap and Detergent Manufacturing
*
*
*
Steam Electric Power Plants
*
*
Textile Mills (Subpart C-Griege Mills are exempt
								from this table)
*
*
*
Timber Products Processing
*
*
*
*
(1) The
				  pollutants in each fraction are listed in Item V-C in the NPDES permit
				  application.
*Testing required.
Table 1.A
Pulp and Paperboard Mills - Exceptions
GC/MS
								Fraction(1)
40 CFR Part 430 Subpart
Volatile
Acid
Base/Neutral
Pesticide
A
[DAGGER]
*
[DAGGER]
*
B
[DAGGER]
*
[DAGGER]
[DAGGER]
C
[DAGGER]
*
[DAGGER]
[DAGGER]
D
[DAGGER]
*
[DAGGER]
[DAGGER]
E
*
*
[DAGGER]
*
F
*
*
[DAGGER]
[DAGGER]
G
*
*
[DAGGER]
[DAGGER]
H
*
*
[DAGGER]
[DAGGER]
I
*
*
[DAGGER]
[DAGGER]
J
*
*
*
[DAGGER]
K
*
*
[DAGGER]
[DAGGER]
L
*
*
[DAGGER]
[DAGGER]
M
*
*
[DAGGER]
[DAGGER]
N
*
*
[DAGGER]
[DAGGER]
O
*
*
[DAGGER]
[DAGGER]
P
*
*
[DAGGER]
[DAGGER]
Q
*
*
[DAGGER]
*
R
[DAGGER]
*
[DAGGER]
[DAGGER]
S
*
*
[DAGGER]
*
T
*
*
[DAGGER]
*
U
*
*
*
[DAGGER]
(1) The pollutants in each fraction are
				  listed in Item V-C in the NPDES permit application.
*Testing required.
[DAGGER] Do not test unless "reason to believe" it is
					 discharged.