Missouri Code of State Regulations › Title 10 - DEPARTMENT OF NATURAL RESOURCES › Division 10 - Air Conservation Commission › Chapter 6 - Air Quality Standards, Definitions, Sampling and Reference Methods and Air Pollution Control Regulations for the Entire State of Missouri › Section 10 CSR 10-6.040 - Reference Methods

Current through Register Vol. 49, No. 14, July 15, 2024
PURPOSE: This rule provides reference methods for
				  determining ambient air/atmosphere data and information necessary for the
				  enforcement of air pollution control regulations throughout
				  Missouri.
PUBLISHER'S NOTE: The secretary of state has
				  determined that the publication of the entire text of the material which is
				  incorporated by reference as a portion of this rule would be unduly cumbersome
				  or expensive. This material as incorporated by reference in this rule shall be
				  maintained by the agency at its headquarters and shall be made available to the
				  public for inspection and copying at no more than the actual cost of
				  reproduction. This note applies only to the reference material. The entire text
				  of the rule is printed here.
(1) The percent sulfur in solid fuels shall
				be determined as specified by American Society of Testing and Materials (ASTM)
				D4239 - 17 Standard Test Method for Sulfur in the Analysis Sample of Coal and
				Coke Using High-Temperature Tube Furnace Combustion, as approved and published
				in 2017, as specified in section (36) of this rule.
(2) The heat content or higher heating value
				(HHV) of solid fuels shall be determined by use of the Adiabatic Bomb
				Calorimeter as specified by ASTM D5865 - 13 Standard Test Method for Gross
				Calorific Value of Coal and Coke, as approved and published in 2013, as
				specified in section (36) of this rule.
(3) The heat content or HHV of liquid
				hydrocarbons shall be determined as specified by ASTM D240 - 17 Standard Test
				Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter,
				as approved and published in 2017, as specified in section (36) of this
				rule.
(4) The methods for
				determining the concentrations of the following air contaminants shall be as
				specified in 40 CFR 50, Appendices A- R or equivalent methods as specified in
				40 CFR 53. The provisions of 40 CFR 50, Appendices A-R, and 40 CFR 53, both
				promulgated as of July 1, 2018, apply and are hereby incorporated by reference
				in this rule, as published by the Office of the Federal Register. Copies can be
				obtained from the U.S. Publishing Office Bookstore, 710 N. Capitol Street N W,
				Washington DC 20401.
This rule does not incorporate any subsequent amendments or
				  additions.
(A) The concentration of
				sulfur dioxide shall be determined as specified in 40 CFR 50, Appendix
				A-Reference Method for the Determination of Sulfur Dioxide in the Atmosphere
				(Pararosaniline Method) or an equivalent method as approved by 40 CFR 53, as
				incorporated by reference in section (4) of this rule.
(B) The concentration of total suspended
				particulate shall be determined as specified in 40 CFR 50, Appendix B-Reference
				Method for the Determination of Suspended Particulate Matter in the Atmosphere
				(High-Volume Method), as incorporated by reference in section (4) of this
				rule.
(C) The concentration of
				carbon monoxide shall be determined as specified in 40 CFR 50, Appendix
				C-Measurement Principle and Calibration Procedure for the Measurement of Carbon
				Monoxide in the Atmosphere (Non-Dispersive Infrared Photometry) or equivalent
				methods as approved by 40 CFR 53, as incorporated by reference in section (4)
				of this rule.
(D) The concentration
				of ozone shall be determined as specified in 40 CFR 50, Appendix D-Measurement
				Principle and Calibration Procedure for the Measurement of Ozone in the
				Atmosphere or equivalent methods as approved by 40 CFR 53, as incorporated by
				reference in section (4) of this rule.
(E) Reserved.
(F) The concentration of nitrogen dioxide
				shall be determined as specified in 40 CFR 50, Appendix F-Measurement Principle
				and Calibration Procedure for the Measurement of Nitrogen Dioxide in the
				Atmosphere (Gas Phase Chemiluminescence) or equivalent methods as approved by
				40 CFR 53, as incorporated by reference in section (4) of this rule.
(G) The concentration of lead shall be
				determined as specified in 40 CFR 50, Appendix G-Reference Method for the
				Determination of Lead in Suspended Particulate Matter Collected From Ambient
				Air or in 40 CFR 50, Appendix Q-Reference Method for the Determination of Lead
				in Particulate Matter as PM10 Collected From Ambient Air
				or equivalent methods as approved by 40 CFR 53, as incorporated by reference in
				section (4) of this rule.
(H)
				Compliance with the one (1) hour ozone standard shall be determined as
				specified in 40 CFR 50, Appendix H-Interpretation of the 1-Hour Primary and
				Secondary National Ambient Air Quality Standards for Ozone, as incorporated by
				reference in section (4) of this rule.
(I) Compliance with the eight (8) hour ozone
				standards shall be determined as specified in 40 CFR 50, Appendix
				I-Interpretation of the 8-Hour Primary and Secondary National Ambient Air
				Quality Standards for Ozone, as incorporated by reference in section (4) of
				this rule.
(J) The concentration of
				particulate matter 10 micron (PM10) shall be determined
				as specified in 40 CFR 50, Appendix J-Reference Method for the Determination of
				Particulate Matter as PM10 in the Atmosphere, or an
				equivalent method as approved in 40 CFR 53, as incorporated by reference in
				section (4) of this rule.
(K)
				Compliance with particulate matter 10 PM10 standards
				shall be determined as specified in 40 CFR 50, Appendix K- Interpretation of
				the National Ambient Air Quality Standards for Particulate Matter, as
				incorporated by reference in section (4) of this rule.
(L) The concentration of particulate matter
				2.5 micron (PM2.5) shall be determined as specified in
				40 CFR 50, Appendix L- Reference Method for the Determination of Fine
				Particulate Matter as PM2.5 in the Atmosphere, or an
				equivalent method as approved in 40 CFR 53, as incorporated by reference in
				section (4) of this rule.
(M)
				Compliance with particulate matter 2.5 (PM2.5) standards
				shall be determined as specified in 40 CFR 50, Appendix N- Interpretation of
				the National Ambient Air Quality Standards for PM2.5, as
				incorporated by reference in section (4) of this rule.
(N) Compliance with the eight (8)-hour ozone
				standards shall be determined as specified in 40 CFR 50, Appendix
				P-Interpretation of the Primary and Secondary National Ambient Air Quality
				Standards for Ozone, as incorporated by reference in section (4) of this
				rule.
(O) Compliance with the lead
				standards shall be determined as specified in 40 CFR 50, Appendix
				R-Interpretation of the National Ambient Air Quality Standards for Lead, as
				incorporated by reference in section (4) of this rule.