Arizona Administrative Code › Title 9 - HEALTH SERVICES › Chapter 14 - DEPARTMENT OF HEALTH SERVICES - LABORATORIES › Article 6 - LICENSING OF ENVIRONMENTAL LABORATORIES › Table 6.2.C - Approved Methods and Method Fees for Waste Parameters

Current through Register Vol. 30, No. 28, July 12, 2024
1. Microbiology of Waste
Description
Reference
Method/s
Fee Per Method
Coliforms, Total, by Membrane Filter
F
9132
$228
Coliforms, Total, by Multiple Tube
								Fermentation
F
9131
$228
2. Sample Preparation for Waste
Acid Digestion of Water
F
3005A
$7
Alkaline Digestion for Hex Chome
F
3060A
$7
Bomb Preparation Method for Solid Waste
F
5050
$7
EP for Oily Wastes
F
1330A
$76
EP Toxicity
F
1310B
$76
Microwave Assisted Digestions Multiple EP
F
F
3015A
$7
3051A
$7
3052
$7
3546
$7
1320
$152
Oils, Greases, and Waxes
F
3040A
$7
Oils
F
3031
$7
Sediments, Sludges, and Soils
F
3050B
$7
SPLP
F
1312
$303
TCLP
F
1311
$303
Total Metals
F
3010A
$7
3020A
$7
Total Recoverable in Water
F
3005A
$7
3. Inorganic Chemistry and Metals of Solid
								Waste
Aluminum
Ammonia
F
F and F13
A
6010C
$10
6020A
$26
7000B
$26
6010D
$10
6020B
$26
350.3
$39
Antimony
Arsenic
F
F and F13
F
6010C
$10
6020A
$26
7062
$76
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
6020A
$26
7010
$26
7061A
$76
7062
$76
7063
$76
F and F13
6010D
$10
6020B
$26
Barium
Beryllium
Boron
Bromide
F
F and F13
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
F and F13
6010D
$10
F
9056A
$26
9211
$39
Cadmium
Calcium
Cation-Exchange Capacity of Soils
F
F and F13
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
6020A
$26
7000B
$26
6010D
$10
6020B
$26
9080
$34
9081
$34
Chloride
F
9056A
$26
9057
$76
9212
$39
9250
$76
9251
$76
9253
$39
Chlorine, Total, in New and Used Petroleum
								Products
F
9075
$76
9076
$39
9077
$39
Chromium, Hexavalent
F
7195
$26
7196A
$76
7197
$26
7198
$40
7199
$76
Chromium, Total
F
F and F13
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
Cobalt
Compatibility Test for Wastes and Membrane
								Liners
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
9090A
$152
Copper
Corrosive to Steel
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
1110A
$63
Corrosivity pH Determination
F
9040C
$63
Cyanide
F
9010C
$13
9012B
$76
9213
$76
9014
$76
F9
9015
$76
Cyanide Extraction for Solids and Oils
F10
9013A
$39
Dermal Corrosion
F
1120
$63
Ignitability of Solids
F
1030
$32
Flash Point by Pensky Martems Cup
F
1010A
$32
Flash Point by Set-a Flash
F
1020B
$32
Fluoride
F
9056A
$26
9214
$39
Iron
Kjeldahl Total, Nitrogen
F
F and F13
A
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
351.4
$76
Lead
Liquid Release Test Procedure
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
9096
$39
Lithium
Magnesium
F
F and F13
6010C
$10
7000B
$26
6010D
$10
F
F and F13
6010C
$10
6020A
$26
7000B
$26
6010D
$10
6020B
$26
Manganese
Mercury
Molybdenum
Nickel
Nitrate
F
F and F13
F
F and F13
F
F and F13
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
6020A
$26
7470A
$52
7471B
$52
7472
$152
7473
$152
7474
$152
6010D
$10
6020B
$26
6010C
$10
7000B
$26
7010
$26
6010D
$10
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
9210A
$39
9056A
$26
Nitrite
Oil and Grease and Petroleum Hydrocarbons
F
A4.24
9056A
$26
9216
$39
1664B
$76
O-Phosphate-P
F
9056A
$26
Osmium
F
7000B
$26
Paint Filter Liquids Test
F
9095B
$19
Perchlorate
pH (Hydrogen Ion)
A5
314.0
$76
F
6850
$152
F
9041A
$39
9045D
$39
Phosphorus
Phosphorus, Total
F
6010C
$10
F and F13
6010D
$10
A
365.3
$76
Potassium
Saturated Hydraulic and Leachate Conductivity and
								Intrinsic Permeability
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
6010D
$10
6020B
$26
9100
$152
Selenium
Silica Silver
Sodium
Sodium Azide
F
6010C
$10
6020A
$26
7010
$26
7741A
$26
7742
$76
F and F13
F
6010D
$10
6020B
$26
6010C
$10
F and F13
6010D
$10
F
F and F13
F
F and F13
C
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
6020A
$26
7000B
$26
6010D
$10
6020B
$26
4110C (2011)
$76
Specific Conductance
F
9050A
$39
Strontium
Sulfate
F
F and F13
6010C
$10
7000B
$26
6010D
$10
F
9035
$76
9036
$76
9038
$76
9056A
$26
Sulfides
F
9030B
$76
9031
$76
9034
$76
9215
$76
Thallium
Tin
Titanium
F
F and F13
F
F and F13
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
6010C
$10
7000B
$26
6010D
$10
F
6010C
$10
Vanadium
Water
F
F and F13
F
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
9000
$32
9001
$32
White Phosphorus by GC
F
7580
$116
Zinc
F
F and F13
6010C
$10
6020A
$26
7000B
$26
7010
$26
6010D
$10
6020B
$26
4. Organics Procedures in Waste
Separatory Funnel Liquid-Liquid Extraction
F
3510C
$13
Organic Compounds in Water by
								Microextraction
F5
3511
$13
Continuous Liquid-Liquid Extraction
F
3520C
$13
SPE
F
3535A
$13
Soxhlet Extraction
F
3540C
$13
Automated Soxhlet Extraction
F
3541
$13
Pressurized Fluid Extraction
F
3545A
$13
Ultrasonic Extraction
F
3550C
$13
Supercritical Fluid Extraction of Total Recoverable
								Petroleum Hydrocarbons
F
3560
$13
Supercritical Fluid Extraction of PAHs
F
3561
$13
SFE of PCBs and Organochlorine Pesticides
F
3562
$13
MSE
F4
3570
$13
Waste Dilution
F
3580A
$13
Waste Dilution for Volatile Organics
F
3585
$13
Alumina Cleanup
F
3610B
$13
Alumina Column Cleanup and Separation of Petroleum
								Wastes
F
3611B
$13
Florisil Cleanup
F
3620C
$13
Silica Gel Cleanup
F
3630C
$13
Gel-Permeation Cleanup
F
3640A
$13
Acid-Base Partition Cleanup
F
3650B
$13
Sulfur Cleanup
F
3660B
$13
Sulfuric Acid/Permanganate Cleanup
F
3665A
$13
Screening Solids for VOCs
F
3815
$76
Hexadecane Extraction and Screening for Purgeable
								Organics
F
3820
$76
Screening for Pentachlorophenol by
								Immunoassay
F
4010A
$76
Screening for 2,4-Dichlorophenoxyacetic Acid by
								Immunoas-say
F
4015
$76
Screening for PCBs by Immunoassay
F
4020
$76
Screening for PCDDs and PCDFs by Immunoassay
F3
4025
$76
Soil Screening for Petroleum Hydrocarbons by
								Immunoassay
F
4030
$76
Soil Screening for PAHs by Immunoassay
F
4035
$76
Soil Screening for Toxaphene by Immunoassay
F
4040
$76
Soil Screening for Chlordane by Immunoassay
F
4041
$76
Soil Screening for DDT by Immunoassay
F
4042
$76
TNT Explosives in Soil by Immunoassay
F
4050
$76
RDX in Soil by Immunoassay
F
4051
$76
Screening Environmental Samples for Planar Organic
								Compounds
F
4425
$76
Triazine Herbicides by Quantitative
								Immunoassay
F
4670
$76
VOCs in Various Sample Matrices Using Equilibrium
								Head-space Analysis
F8
5021A
$13
Purge-and-Trap for Aqueous Samples
F6
5030C
$13
Volatile, Nonpurgeable, Water-Soluble Compounds by
								Azeo-tropic Distillation
F
5031
$13
VOCs by Vacuum Distillation
F
5032
$13
Closed-System Purge-and-Trap and Extraction for
								Volatile Organics in Soil and Waste Samples
F2
5035A
$13
Analysis for Desorption of Sorbent Cartridges from
								VOST
F
5041A
$13
EDB and DBCP by Microextraction and GC
F
8011
$116
C10 -
								C32 Hydrocarbons
K
8015AZ 1
$116
Nonhalogenated Organics Using GC/FID
F7
8015D
$116
Aromatic and Halogenated Volatiles by GC Using
								Photoionization and/or Electrolytic Conductivity Detectors
F
8021B
$152
Acrylonitrile by GC
F
8031
$76
Acrylamide by GC
F
8032A
$76
Acetonitrile by GC with Nitrogen-Phosphorus
								Detection
F
8033
$76
Phenols by GC
F
8041A
$116
Phthalate Esters by GC/ECD
F
8061A
$116
Nitrosamines by GC
F
8070A
$116
Organochlorine Pesticides by GC
F
8081B
$152
Elemental Quantitation by GC/AED
F
8085
$116
PCBs by GC
F
8082A
$152
Nitroaromatics and Cyclic Ketones by GC
F
8091
$116
Explosives by GC
F
8095
$116
PAHs
F
8100
$116
Haloethers by GC
F
8111
$116
Chlorinated Hydrocarbons by GC: Capillary Column
								Technique
F
8121
$116
Aniline and Selected Derivatives by GC
F
8131
$116
Organophosphorus Compounds by GC
F
8141B
$152
Chlorinated Herbicides by GC Using Methylation or
								Pentafluo-robenzylation Derivatization
F
8151A
$152
VOCs by GC/MS, including n-Hexane VOCs by
								VD/GC/MS
F
8260B
$152
F12 and F13
8260C/8000D
$152
F
8261
$152
Semivolatile Organic Compounds by GC/MS
Semivolatile Organic Compounds (PAHs and PCBs) in
								Soils/ Sludges and Solid Wastes Using TE/GC/MS
F
8270C
$152
F and F13
8270D/8000D
$152
F
8275A
$152
8280A: Polychlorinated Dibenzo-p-Dioxins and PCDFs
								by HRGC/LRMS
F
8280B
$258
PCDDs and PCDFs by HRGC/HRMS
F
8290A
$258
PAHs
F
8310
$116
Determination of Carbonyl Compounds by HPLC
F
8315A
$116
Acrylamide, Acrylonitrile, and Acrolein by
								HPLC
F
8316
$116
N-Methylcarbamates by HPLC
F
8318A
$116
Solvent-Extractable Nonvolatile Compounds by
								HPLC/TS/MS or UV Detection
F
8321B
$152
Solvent Extractable Nonvolatile Compounds by
								HPLC/PB/MS
F
8325
$152
Nitroaromatics and Nitramines by HPLC
F
8330A
$116
Nitroaromatics, Nitramines, and Nitrate
								Esters
F11
8330B
$116
Tetrazene by Reverse Phase HPLC
F
8331
$116
Nitroglycerin by HPLC
F
8332
$116
GC/FT-IR Spectrometry for Semivolatile Organics:
								Capillary Column
F
8410
$116
Analysis of Bis (2-chloroethyl) Ether and
								Hydrolysis Products by Direct Aqueous Injection GC/FT-IR
F
8430
$116
Total Recoverable Petroleum Hydrocarbons by
								Infrared Spec-trophotometry
F
8440
$116
Screening for RDX/MDX in Soil
F
8510
$76
Colorimetric Screening Method for TNT in
								Soil
F
8515
$76
Screening for Total VOH in Water
F
8535
$76
PCP by UV Colorimetry
F
8540
$108
TOX
F
9020B
$76
POX
F
9021
$76
TOX by Neutron Activation Analysis
F
9022
$114
EOX in Solids
F
9023
$114
TOCs
F
9060A
$76
Phenolics
F
9065
$152
9066
$152
9067
$152
HEM for Aqueous Samples
F
9070A
$76
HEM for Sludge, Sediment, and Solid Samples
F
9071B
$76
Screening for TRPH in Soil
F
9074
$76
Screening for PCBs in Soil
F
9078
$76
Screening for PCBs in Oil
F
9079
$76
PCBs in Waste Oil
A4.28
600/4-81-045
$152
5. Bulk Asbestos Analysis of
								Waste
Bulk Asbestos Analysis Fiber Counting
A4.29
Bulk Asbestos
$228
G
9002
$228
G1 and A4.29
Bulk Asbestos
$228
G
7400
$228
7402
$228
6. Radiochemistry of Waste
Alpha-Emitting Radium Isotopes
F
9315
$206
Gross Alpha and Beta
F
9310
$206
Radium-228
F
9320
$206