Arizona Administrative Code › Title 9 - HEALTH SERVICES › Chapter 14 - DEPARTMENT OF HEALTH SERVICES - LABORATORIES › Article 6 - LICENSING OF ENVIRONMENTAL LABORATORIES › Section R9-14-610 - Approved Methods and References

Current through Register Vol. 30, No. 28, July 12, 2024
A. A licensee or applicant shall ensure that
				compliance testing is performed according to an approved method and may use
				method alterations approved by the Department under subsection (C).
B. The approved methods listed by parameter
				in Tables 6.2.A through 6.2.D are found in the following references, which are
				incorporated by reference with the modifications described below; are on file
				with the Department; include no future editions or amendments; and are
				available as provided below.
Table 1. Key Reference
A Environmental Monitoring and Support Laboratory-Cincinnati,
				  EPA, Pub. No. EPA/600/4-79-020 (600479020), Methods for Chemical Analysis of
				  Water and Wastes (rev. March 1983), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
A1 Environmental Monitoring and Support
				  Laboratory-Cincinnati, EPA, Pub. No. EPA/600/R-94/111 (600R94111), Methods for
				  the Determination of Metals in Environmental Samples: Supplement I (May 1994),
				  available at http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling
				  (800) 490-9198.
A2 Environmental Monitoring Systems Laboratory, EPA, Pub. No.
				  EPA/600/R-93/100 (600R93100), Methods for the Determination of Inorganic
				  Substances in Environmental Samples (August 1993), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
A3 Technicon Industrial Systems, Industrial Method No.
				  380-75WE, Fluoride in Water and Wastewater (February 1976), available from
				  Mequon Technology Center, 10520-C North Baehr Road, Mequon, WI 53092 or by
				  calling (262) 241-7900.
A4 National Service Center for Environmental Publications
				  (NSCEP), Online EPA Publication Title List available at
				  http://nepis.epa.gov/EPA/html/Pubs/pubtitle.html or by calling (800) 490-9198.
				  Publication numbers for the methods that are listed under this reference
				  are:
1. Method 317.0, Rev 2.0, July
				2001, EPA 815-B-01-001
2. Method
				314.1, Rev 1.0, May 2005, EPA 815-R-05-009
3. Method 326.0, Rev 1.0, June 2000, EPA
				815-R-03-007
4. Method 327.0, Rev
				1.1, May 2005, EPA 815-R-05-008
5.
				Method 331.0, Rev 1.0, January 2005, EPA 815-R-05-007
6. Method 515.4, Rev 1.0, April 2000, EPA
				800-R-00-016
7. Method 527, Rev
				1.0, April 2005, EPA 815-R-05-005
8. Method 531.2, Rev 1.0, September 2001, EPA
				815-B-01-002
9. Method 552.3, Rev
				1.0, July 2003, EPA 815-B-03-002
10. Method 200.5, Rev 4.2, October 2003, EPA
				600-R-06-115
11. Method 332, Rev
				1.0, March 2005, EPA 600-R-05-049
12. Method 415.3, Rev 1.1, February2005, EPA
				600-R-05-055
13. Method 415.3, Rev
				1.2, September 2009, EPA 600-R-09-122
14. Method 521, Version 1.0, September 2004,
				EPA 600-R-05-054
15. Method 529,
				Rev 1.0, September 2002, EPA 600-R-05-052
16. Method 535, Rev 1.1, April 2005, EPA
				600-R-05-053
17. Method 1631, Rev
				E, August 2002, EPA 821-R-02-019
18. Method 557, Version 1.0, September 2009,
				EPA 815-B-09-012
19. Method 524.4,
				May 2013, EPA 815-R-13-002
20.
				Method 524.3, Version 1.0, June 2009, EPA 815-B-09-009
21. Method 522, Version 1.0, September 2008,
				EPA 600-R-08-101
22. Method 1613,
				Rev B, October 1994, EPA 821-B-94-005
23. Method 245.7, Rev 2.0, February 2005, EPA
				821-R-05-001
24. Method 1664, Rev
				B, February 2010, EPA 821-R-10-001
25. Method 1638, April 1995, EPA
				821-R-95-031
26. Method OIA-1677
				DW, January 2004, EPA 821-R-04-001
27. Method 1627, December 2011, Acid Mine
				Drainage, EPA 821-R-09-002
28. PCBs
				in Transformer Fluid and Oils, September 1982, EPA 600/4-81-045
29. Asbestos in Bulk Samples, December 1982,
				EPA 600/M4-82-020
30. Method 100.1,
				Asbestos Fibers, September 1993, EPA 600/4-83-043
31. Method 100.2, Asbestos Structures over
				10m in Length, EPA/600/R-94/134
32.
				Method 1622, Cryptosporidium in Water, December 2005, EPA
				815-R-05-001
33. Method 1623.1,
				Cryptosporidium and Giardia in Water, January 2012, EPA 816-R-12-001
34. Method 1682, Salmonella in Sewage Sludge,
				July 2006, EPA 821-R-06-014
35.
				Method 1605, Aeromonas in Finished Water by MF, October 2001, EPA
				821-/R/01/034
36. Method 1604,
				Total coliforms and E.coli by MF, September 2002, EPA-821-02-024
37. Method 1601, Coliphage, April 2001, EPA
				821-R-01-030
38. Method 1602,
				Coliphage, April 2001, EPA 821-R-01-029
39. Method 1623, Cryptosporidium and Giardia,
				December 2005, EPA 815-R-05-002
40.
				Method 537, September 2009, EPA/600/R-08/092
41. Method 302.0, September 2009,
				EPA-815-B-09-014
42. Method 539,
				November 2010, EPA 815-B-10-001
43.
				Method 218.7, November 2011, EPA 815-R-11-005
44. Method 334.0. September 2009, EPA
				815-B-09-013
A5 EPA Pub. No. EPA 815-R-00-014 (815R00014), Volume 1,
				  Methods for the Determination of Organic and Inorganic Compounds in Drinking
				  Water (August 2000), available at
				  http://nepis.epa.gov/EPA/html/Pubs/pubtitle.html or by calling (800) 490-9198,
				  modified to require the following when testing for bromate using method 321.8:
				  Samples must be preserved at the time of sampling with 50 mg ethylenediamine
				  (EDA)/L of sample and must be analyzed within 28 days. Ion chromatography and
				  post-column reaction or IC/ICP-MS must be used for monitoring of bromate for
				  purposes of demonstrating eligibility of reduced monitoring, as prescribed in
				  40 CFR
				  141.132(b)(3)(ii).
A6 Lachat Instruments, QuikChem Method 10-204-00-1-X,
				  Digestion and Distillation of Total Cyanide in Drinking and Wastewaters Using
				  MICRO DIST and Determination of Cyanide by Flow Injection Analysis (rev. 2.1
				  November 30, 2000), available from Lachat Instruments, 6645 W. Mill Rd.,
				  Milwaukee, WI 53218-0204.
A7 Standard Test Methods for Trace Uranium in Water by
				  Pulsed-Laser Phosphorimetry, ASTM D5174-97, 02, available from ASTM
				  International, 100 Barr Harbor Dr., P.O. Box C700, W. Conshohocken, PA
				  19428-2959 or through
www.astm.org
.
B Herman L. Krieger, EPA, Pub. No. EPA-600/4-75-008
				  (6004755008), Interim Radiochemical Methodology for Drinking Water (March
				  1976), available at http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by
				  calling (800) 490-9198.
C American Public Health Association et al., Standard Methods
				  for the Examination of Water and Wastewater ( 22nd edition 2012), available
				  from American Public Health Association, 800 I Street, NW, Washington, DC 20001
				  or at
http://www.standardmethods.org
,
				  with the approved method having the same last two digits in the method number
				  as the year in which the method was approved by the Standard Methods Committee,
				  as published for the individual methods in the 22nd edition.
C1 Hach Company, Hach Water Analysis Handbook ( 5th edition
				  2008), available from Hach Company, P.O. Box 389, Loveland, CO
				  80539-0389.
C2 American Public Health Association et al., Standard
				  Methods for the Examination of Water and Wastewater (21st edition 2005),
				  available from American Public Health Association, 800 I St., NW, Washington,
				  DC 20001.
C3 Hach Method 10360, Luminescence Measurement of Dissolved
				  Oxygen in Water and Wastewater and for Use in the Determination of BOD5 and
				  cBOD5, Revision 1.2, October 2011, available from Hach Company, P.O. Box 389,
				  Love-land, CO 80539-0389.
C4 Expedited Approval of Test Procedures for the Analysis of
				  Contaminants Under the Safe Drinking Water Act, August 04, 2014, available at
				  https://www.gpo.gov/fdsys/pkg/FR-2014-06-19/html/2014-14369.htm.
C5 Guidelines Establishing Test Procedures for the Analysis
				  of Pollutants Under the Clean Water Act; Analysis and Sampling Procedures;
				  Final Rule, May 18, 2012, available at
				  http://www.gpo.gov/fdsys/pkg/FR-2012-05-18/pdf/2012-10210.pdf.
C6 The quality control criteria and the modifications listed
				  in the "Guidelines Establishing Test Procedures for the Analysis of Pollutants;
				  Analytical Methods for Biological Pollutants in Wastewater and Sewage Sludge,"
				  March 26, 2007, available at
				  http://www.epa.gov/fedrgstr/EPA-WATER/2007/March/Day-26/w1455.pdf.
C7 ChlordioX Plus "Chlorine Dioxide and Chlorite in Drinking
				  Water by Amperometry using Disposable Sensors," November 2013, available from
				  Palintest Ltd., Jamike Avenue, Suite 100, Erlanger, KY 41018.
C8 American Public Health Association et al., Standard
				  Methods for the Examination of Water and Wastewater (20th ed. 1998), available
				  from American Public Health Association, 800 I St., NW, Washington, DC
				  20001.
D Environmental Monitoring Systems Laboratory-Cincinnati,
				  EPA, Pub. No. EPA/600/4-88/039 (600488039), Methods for the Determination of
				  Organic Compounds in Drinking Water (rev. July 1991), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D1 Environmental Monitoring Systems Laboratory-Cincinnati,
				  EPA, Pub. No. EPA/600/4-90/020 (600490020), Methods for the Determination of
				  Organic Compounds in Drinking Water: Supplement I (July 1990), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D2 Environmental Monitoring Systems Laboratory-Cincinnati,
				  EPA, Pub. No. EPA/600/R-92/129 (600R92129), Methods for the Determination of
				  Organic Compounds in Drinking Water: Supplement II (August 1992), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D3 National Exposure Research Laboratory-Cincinnati, EPA,
				  Pub. No. EPA/600/R-95/131 (600R95131), Methods for the Determination of Organic
				  Compounds in Drinking Water: Supplement III (August 1995), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D4 Office of Ground Water and Drinking Water Technical
				  Support Center, EPA, Pub. No. EPA 815-R-05-004 (815R05004), Manual for the
				  Certification of Laboratories Analyzing Drinking Water: Criteria and Procedures
				  Quality Assurance (5th edition January 2005), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D5 Supplement I to the 5th edition of the Manual for the
				  Certification of Laboratories Analyzing Drinking Water; EPA 815-F-08-006, June
				  2008, available at
				  http://water.epa.gov/scitech/drinkingwater/labcert/index.cfm.
D6 Supplement II to the 5th edition of the Manual for the
				  Certification of Laboratories Analyzing Drinking Water; EPA 815-F-12-006,
				  November 2012, available at
				  http://water.epa.gov/scitech/drinkingwater/labcert/index.cfm.
D7 LT2 Enhanced Surface Water Treatment Rule, January 05,
				  2006; available at
				  http://water.epa.gov/lawsregs/rulesregs/sdwa/lt2/regulations.cfm .
D8 Modified Colitag®, ATP D05-0035-"Modified
				  ColitagTM Test Method for the Simultaneous Detection
				  of
E. coli
and other Total Coliforms in Water,'' August 28,
				  2009, available from CPI International, Inc., 5580 Skylane Blvd., Santa Rosa,
				  CA, 95403 or by calling (800) 878-7654.
D9 Stage 2 Disinfectants and Disinfection Byproducts Rule,
				  January 04, 2006, available at https://www.federalregister.gov/
				  articles/2006/01/04/06-3/national-primary-drinking-water-regulations-stage-2-disinfectants-and-disinfection-byprod-ucts-rule.
D10 National Primary Drinking Water Regulations: Ground Water
				  Rule, 11/08/2006; available at
				  https://www.federalregister.gov/articles/2006/11/08/06-8763/national-primary-drinking-water-regulations-ground-water-rule.
D11 Source Water Monitoring Guidance Manual for Public Water
				  Systems for the Final Long Term 2 Enhanced Surface Water Treatment Rule; EPA
				  815-R06-005 (815R06005), February 2006, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D12 Analytical Methods Recommended for Drinking Water
				  Monitoring of Secondary Contaminants (PDF), EPA 815-B-14-005 (815B14005),
				  January 2014, available at http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or
				  by calling (800) 490-9198.
D13 Analytical Methods Approved for Drinking Water Compliance
				  Monitoring under the Disinfection Byproduct Rules, EPA 815-B-14-004
				  (815B14004), January 2014, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
D14 National Primary Drinking Water Regulations: Revisions to
				  the Total Coliform Rule; Final Rule; Federal Register / Vol. 78, No. 30 /
				  Wednesday, February 13, 2013 / Rules and Regulations.
E 40 CFR Part 136 app. A (January 2016), available through
http://www.ecfr.gov/cgi-bin/text-idx?tpl=/ecfrbrowse/Title40/40cfr136_main_02.tpl
.
E1 Office of Water Engineering and Analysis Division, EPA,
				  Pub. No. EPA-821-R-93-010-A (821R93010A), Methods for the Determination of
				  Nonconventional Pesticides in Municipal and Industrial Wastewater: Volume I
				  (rev. 1 August 1993), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
E2 EPA Methods 608.1, 608.2, 614, 614.1, 615, 617, 619, 622,
				  622.1, 627, and 632, found in Methods for the Determination of Nonconventional
				  Pesticides in Municipal and Industrial Wastewater, EPA 821-R-92-002
				  (821R92002), April 1992, U.S. EPA, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
E3 "White House Document" Environmental Regulations and
				  Technology-Control of Pathogens and Vector Attraction in Sewage Sludge, EPA
				  625/R-92/013 (625R92013), revised July 2003, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
E4 Organochlorine Pesticides and PCBs in Wastewater Using
				  Empore TM Disk; revised October 28, 1994, 3M Corporation, available from 3M
				  Corporation, at
http://www.horizontechinc.com/PDF/epa_methods/method_608_3m.pdf
or by calling (800) 440-2966, ext. 67.
E5 American Public Health Association, et al., Standard
				  Methods for the Examination of Water and Wastewater (18th edition 1992),
				  available from American Public Health Association, 800 I St., NW, Washington,
				  DC 20001.
E6 CEM Corporation, Closed Vessel Microwave Digestion of
				  Wastewater Samples for Determination of Metals (April 1992), available from CEM
				  Corporation, P.O. Box 200, 3100 Farm Road, Matthews, NC 28106-0200.
E7 Kelada-01, Kelada Automated Test Methods for Total
				  Cyanide, Acid Dissociable Cyanide, and Thiocyanate, EPA 821- B-01-009, revision
				  1.2, August 2001, available from NTIS, 5285 Port Royal Road, Springfield, VA
				  22161 or by calling (800) 490-9198. EPA Note: A 450-W UV lamp may be used in
				  this method instead of the 550-W lamp specified if it provides performance
				  within the quality control acceptance criteria of the method in a given
				  instrument. Similarly, modified flow cell configurations and flow conditions
				  may be used in the method, provided that the quality control acceptance
				  criteria are met.
E8 Methods for Analysis of Inorganic Substances in Water and
				  Fluvial Sediments, Techniques of Water-Resource Investigations of the U.S.
				  Geological Survey, Book 5, Chapter A1, 1985, USGS, available at U.S. Geological
				  Survey Information Services, Box 25286, Federal Center, Denver, CO
				  80225-0425.
F Office of Solid Waste and Emergency Response, EPA, Pub. No.
				  SW-846, Test Methods for Evaluating Solid Waste, Physical/Chemical Methods (3rd
				  edition 1986), as amended by Update I, July 1992; Update IIA, August 1993;
				  Update II, September 1994; Update IIB, January 1995; Update III, December 1996;
				  Update IIIA, April 1998; Update IIIB, November 2004; Update IV, February 2007;
				  and Update V, August 18, 2015, available from NTIS, 5285 Port Royal Rd.,
				  Springfield, VA 22161, by calling (800) 490-9198, and at
				  http://www.epa.gov/epaoswer/hazwaste/test/main.htm.
F1 8260B AZ Vapor Method for the Determination of VOCs in
				  Vapor Samples, Revision 0.0, dated April 14, 2009, available at
http://www.azdhs.gov/documents/preparedness/state-laboratory/lab-licensure-certification/technical-resources/additional-resources/az-vapor-method.pdf.
F2 EPA, Method 5035A: Closed-System Purge-and-Trap and
				  Extraction for Volatile Organics in Soil and Waste Samples (draft rev. 1 July
				  2002), available at
				  https://www.epa.gov/homeland-security-research/epa-method-5035a-sw-846-closed-system-purge-and-trap-and-extraction
				  .
F3 EPA, Method 4025: Screening for Polychlorinated
				  Dibenzodioxins and Polychlorinated Dibenzofurans (PCDD/Fs) by Immunoassay (rev.
				  0 October 2002), available at https://
				  www.epa.gov/hw-sw846/sw-846-test-method-4025-screening-polychlorinated-dibenzodioxins-and-polychlorinated
				  .
F4 EPA, Method 3570: Microscale Solvent Extraction (MSE)
				  (rev. 0 November 2002), available at
				  https://www.epa.gov/homeland-security-research/epa-method-3570-sw-846-microscale-solvent-extraction-mse.
F5 EPA, Method 3511: Organic Compounds in Water by
				  Microextraction (rev. 0 November 2002), available at
				  https://www.epa.gov/hw-sw846/sw-846-test-method-3511-organic-compounds-water-microextraction.
F6 EPA, Method 5030C: Purge-and-Trap for Aqueous Samples
				  (rev. 3 May 2003), available at
				  https://www.epa.gov/homeland-security-research/epa-method-5030c-sw-846-purge-and-trap-aqueous-samples.
F7 EPA, Method 8015D: Nonhalogenated Organics Using GC/FID
				  (rev. 4 June 2003), available at
				  https://www.epa.gov/hw-sw846/validated-test-method-8015d-nonhalogenated-organics-using-gas-chromatographyflame.
F8 EPA, Method 5021A: Volatile Organic Compounds in Various
				  Sample Matrices Using Equilibrium Headspace Analysis (rev. 1 June 2003),
				  available at
				  https://www.epa.gov/hw-sw846/validated-test-method-5021a-volatile-organic-compounds-vocs-various-sample-matrices-using
				  .
F9 EPA, Method 9015: Metal Cyanide Complexes by Anion
				  Exchange Chromatography and UV Detection (rev. 0 November 2004), available
				  athttps://www.epa.gov/hw-sw846/sw-846-test-method-9015-metal-cyanide-complexes-waters-and-waste-extracts-using-anion.
				  .
F10 EPA, Method 9013A: Cyanide Extraction Procedure for
				  Solids and Oils (rev. 1 November 2004), available at
				  nide-extraction-procedure-solids-and-oils.
F11 Method 8330B, Nitroaromatics, Nitramines, and Nitrate
				  Esters by High Performance Liquid Chromatography, Revision 2, October 2006,
				  available at
				  https://www.epa.gov/hw-sw846/validated-method-8330b-nitroaromatics-nitramines-and-nitrate-esters-high-performance-liquid.
F12 EPA 8260C (SW-846) Volatile Organic Compounds by Gas
				  Chromatography-Mass Spectrometry (GC-MS), Revision 3, 2006,available at
				  https://www.epa.gov/hw-sw846/validated-test-method-8260c-volatile-organic-compounds-gas-chro-matographymass-spectrometry.
F13 SW 846 Update V, Revision 2, July 2014, Chapters ONE
				  through FIVE, applicable to 6010D, 6020B, 8260C, and 8270D, available at
				  https://www.epa.gov/hw-sw846/sw-846-compendium.
F14 EPA Method 8000C: Determinative Chromatographic
				  Separations (rev. 3 March 2003), available at
				  https://archive.epa.gov/epawaste/hazard/testmethods/web/pdf/method_208000c,_20revision_203_20-_202003.pdf.
G National Institute for Occupational Safety and Health, U.S.
				  Department of Health and Human Services, Pub. No. 94-113, NIOSH Manual of
				  Analytical Methods (4th edition, August 1994), available from Superintendent of
				  Documents, Government Printing Office, Washington, DC 20402-9325.
G1 Method for the Determination of Asbestos in Bulk Building
				  Materials, EPA/600R-93/116, July 1993, available at
http://www.nist.gov/nvlap/upload/EPA-600-R-93-116.pdf
. A concurrent certification is also required for Asbestos in Bulk samples,
				  December 1982, EPA 600/M4-82-020 (A4.29), as outlined in NVLAP Lab Bulletin,
				  LB-68-2012, available at
http://www.nist.gov/nvlap/upload/LB_68_2012.pdf
.
H National Environmental Laboratory Accreditation Conference,
				  2009 NELAC, available from the National Environmental Laboratory Accreditation
				  Conference, P.O. Box 2439, Weatherford, TX 76086 or at
www.nelac-institute.org
.
I ASTM, individual standards available from ASTM
				  International, 100 Barr Harbor Dr., P.O. Box C700, W. Conshohocken, PA
				  19428-2959 or at
www.astm.org
.
J L.L. Thatcher et
				  al., U.S. Department of the Interior, "Methods for Determination of Radioactive
				  Substances in Water and Fluvial Sediments," Chapter A5 in Book of Techniques of
				  Water-Resources Investigations of the United States Geological Survey, 1977,
				  available from U.S. Geological Survey Information Services, Box 25286, Federal
				  Center, Denver, CO 80225-0425.
K Bureau of State Laboratory Services, Arizona Department of
				  Health Services, Method No. BLS-188, Ethylene Glycol in Waste Water (rev. April
				  1991); and Bureau of State Laboratory Services, Arizona Department of Health
				  Services, C10 - C32 Hydrocarbons
				  in Soil - 8015AZ (rev. 1.0 September 1998), available from the Bureau of State
				  Laboratory Services, 250 N. 17th Ave., Phoenix, AZ 85007, and at
http://www.azdhs.gov/preparedness/state-laboratory/lab-licensure-certification/index.php#technical-resources-additional
.
K1 Office of Water,
				  EPA, Pub. No. EPA-821-B-98-016 (821B98016), Analytical Methods for the
				  Determination of Pollutants in Pharmaceutical Manufacturing Industry Wastewater
				  (July 1998), available at http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or
				  by calling (800) 490-9198.
L Herman L. Krieger and Earl L. Whittaker, EPA, Pub. No.
				  EPA-600/4-80-032 (600480032), Prescribed Procedures for Measurement of
				  Radioactivity in Drinking Water (August 1980), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
M1 Environmental Monitoring Systems Laboratory-Cincinnati,
				  EPA, Pub. No. EPA/600/4-90/027F (600490027F), Methods for Measuring the Acute
				  Toxicity of Effluents and Receiving Waters to Freshwater and Marine Organisms
				  (4th edition August 1993), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
N1 Environmental Monitoring Systems Laboratory-Cincinnati,
				  EPA, Pub. No. EPA-600-4-91-002 (600491002), Short-Term Methods for Estimating
				  the Chronic Toxicity of Effluents and Receiving Water to Freshwater Organisms
				  (3rd edition July 1994), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
0 40 CFR Part 50, Chapter 1, Sub-chapter C (2015), available
				  at
http://www.ecfr.gov/cgi-bin/text-idx?tpl=/ecfrbrowse/Title40/40cfr50_main_02.tpl
.
01 Compendium of Methods for the Determination of Inorganic
				  Compounds in Ambient Air, Compendium Method IO-3.4, Determination of Metals in
				  Ambient Particulate Matter Using Inductively Coupled Plasma (ICP) Spectroscopy,
				  EPA/ 625/R-96/010AC (625R96010AC), June 1999, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
02 Compendium of Methods for the Determination of Inorganic
				  Compounds in Ambient Air, Compendium Method IO-3.5,
Determination of Metals in Ambient Particulate Matter Using
				  Inductively Coupled Plasma/Mass Spectrometry (ICP/ MS), EPA/625/R-96/010AB
				  (625R96010AB), June 1999, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
03 Compendium of Methods for the Determination of Inorganic
				  Compounds in Ambient Air, Compendium Method IO-3.1, Selection, Preparation and
				  Extraction, EPA/625/R-96/010AD (625R96010AD), June 1999, available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
04 Determination of Lead in TSP by Inductively Coupled Plasma
				  Mass Spectrometry (ICP-MS) with Heated Ultrasonic Nitric and Hydrochloric Acid
				  Filter Extraction; available from the Bureau of State Laboratory Services, 250
				  N. 17th Ave., Phoenix, AZ 85007, and at
http://www.azdhs.gov/documents/preparedness/state-laboratory/lab-licensure-certification/technical-resources/additional-resources/lead-in-ambient-air-by-icp-ms-eql-0510-191.pdf
.
P EPA, Pub. No. EPA/600/4-84/013, USEPA Manual of Methods for
				  Virology (rev. June 2001), Chapters 1 through 16 available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
P1 Jay Vasconcelos and Stephanie Harris, EPA, Pub. No. EPA
				  910/9-92-029 (910992029), Consensus Method for Determining Groundwaters Under
				  the Direct Influence of Surface Water Using Microscopic Particulate Analysis
				  (MPA) (October 1992), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
P2 G. Shay Fout et al., EPA, Pub. No. EPA/600/R-95/178
				  (600R95178), ICR Microbial Laboratory Manual (April 1996), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
P3 Charles P. Gerba, University of Arizona, U of A 2000:
				  Ascaris lumbricoides in Water (1999), available from the University of Arizona,
				  Microbial Analytical Laboratory, Building No. 90, Rm. 406, Tucson, AZ
				  85721.
Q 40 CFR Part 60 Chapter I, Subchapter C, Part 60 ( January
				  2008), available at
http://www.ecfr.gov/cgi-bin/text-idx?SID=059c1-fa5bb66be2b9393d76638c87a0c&node=pt40.8.60&rgn=div5
.
Q1 EPA Performance Specification PS-12B: Analysis of Vapor
				  Phase Mercury Emissions from Stationary Sources Using a Sorbent Trap Monitoring
				  System, available at http://www.epa.gov/ttnemc01/perfspec/ps-12B.pdf.
R Office of Air Quality, ADEQ, Arizona Testing Manual for Air
				  Pollutant Emissions (rev. F March 1992), available from the Office of Air
				  Quality, ADEQ, 1110 W. Washington St., Phoenix, AZ 85007 and at
http://www.azdeq.gov/environ/air/compliance/download/manual.pdf
.
S 40 CFR Part 61 apps. B and C ( January 2008), available at
http://www.ecfr.gov/cgi-bin/text-idx?tpl=/ecfrbrowse/Title40/40cfr61_main_02.tpl
.
S1 EPA, Pub. No. EPA/625/R-96/010b (625R96010b), Compendium
				  of Methods for the Determination of Toxic Organic Compounds in Ambient Air (2nd
				  edition January 1999), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800) 490-9198.
				  U Environmental Measurements Laboratory, U.S. Department of Energy, Pub. No.
				  HASL-300, EML Procedures Manual, Vol. I (28th edition February 1997), available
				  from NTIS, 5285 Port Royal Rd., Springfield, VA 22161.
V Eastern Environmental Radiation Facility, EPA, Pub. No. EPA
				  520/5-84-006 (520584006), Eastern Environmental Radiation Facility
				  Radiochemistry Procedures Manual ( December 1987), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
W Environmental Monitoring and Support Laboratory Las Vegas,
				  EPA, Pub. No. EMSL-LV-0539-17 (EMSLLV053917), Radiochemical Analytical
				  Procedures for Analysis of Environmental Samples (March 1979), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
X Office of Ground Water and Drinking Water, EPA, Pub. No.
				  EPA/600/4-91/016 (600491016), Test Methods for
Escherichia coli
in Drinking Water: EC Medium with Mug Tube Procedure, Nutrient Agar
				  with Mug Membrane Filter Procedure (July 1991), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
Y Method OIA-1677-09, Available Cyanide by Ligand Exchange
				  and Flow Injection Analysis (FIA). 2010, available from ALP-KEM, a Division of
				  OI Analytical, 151 Graham Road, College Station, TX 77845 or by calling (979)
				  690-1711.
Z IDEXX Colilert*-18 and Quanti-Tray* Test Method for the
				  Detection of Fecal Coliforms in Wastewater, available from IDEXX Laboratories,
				  Inc., One IDEXX Dr., Westbrook, ME 04092 or by calling 1-800-548-6733.
Z1 EPA Method 1681, July 2006, EPA-821-R-06-013, Fecal
				  Coliform in Sewage Sludge (Biosolids) by Multiple Tube Fermentation using A-1
				  Medium, available at http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by
				  calling (800) 490-9198.
Z2 EPA, Pub. No.
				  EPA-821-R-02-013 (821R02013), Short-term Methods for Estimating the Chronic
				  Toxicity of Effluents and Receiving Waters to Freshwater Organisms (4th edition
				  October 2002), available at http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or
				  by calling (800) 490-9198.
Z3 IDEXX Laboratories,
				  Inc., IDEXX SimPlate TM HPC Method for Heterotrophs in Water (November 2000),
				  available from IDEXX Laboratories, Inc., One IDEXX Dr., Westbrook, ME
				  04092.
Z4 William A. Yanko,
				  EPA, Pub. No. EPA/600/1-87/014 (600187014), Occurrence of Pathogens in
				  Distribution and Marketing Municipal Sludges (1987), available at
				  http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
Z5 CPI International Colitag® Product as a Test for
				  Detection and Identification of Coliforms and
E. coli
Bacteria
				  in Drinking Water and Source Water as Required in National Primary Drinking
				  Water Regulations, August 2001, available from CPI International, 5580 Skylane
				  Blvd, Santa Rosa, CA 95403, at
http://www.cpiinternational.com
,
				  or by calling 1-800-878-7654.
Z6 m-ColiBlue 24 Test, Total Coliforms and
E.
				  coli
Membrane Filtration Method with m-ColiBlue 24 Broth, Method No.
				  10029, Revision 2, August 17, 1999, available at Hach Company, P.O. Box 389,
				  Loveland, Colorado 80539-0389 or by calling 1-800-227-4224.
Z7 Colisure Test, IDEXX Laboratories Inc., February 28, 1994,
				  available from IDEXX Laboratories, Inc., One IDEXX Dr., Westbrook, ME 04092 or
				  by calling 1-800-548-6733.
Z8 Presence/Absence for Coliforms and
E.
				  coli
in Water, Charm Sciences, Inc., December 21, 1997, available at
				  659 Ando-ver Street, Lawrence, MA 01843, 987-687-9200,
http://www.charm.com
.
Z9 OI
				  Analytical/ALPKEM, Nitrogen, Total Kjeldahl, Method PAI-DK01 (Block Digestion,
				  Steam Distillation, Titri-metric Detection) (rev. December 22, 1994), available
				  from OI Analytical/ALPKEM, P.O. Box 9010, College Station, TX 77842.
Z10 OI
				  Analytical/ALPKEM, Nitrogen, Total Kjeldahl, Method PAI-DK02 (Block Digestion,
				  Steam Distillation, Colori-metric Detection) (rev. December 22, 1994),
				  available from OI Analytical/ALPKEM, P.O. Box 9010, College Station, TX
				  77842.
Z11 OI
				  Analytical/ALPKEM, Nitrogen, Total Kjeldahl, Method PAI-DK03 (Block Digestion,
				  Automated FIA Gas Diffusion) (rev. December 22, 1994), available from OI
				  Analytical/ALPKEM, P.O. Box 9010, College Station, TX 77842.
Z12 EPA, Pub. No.
				  EPA-821-R-02-012, Methods for Measuring the Acute Toxicity of Effluents and
				  Receiving Waters to Freshwater and Marine Organisms (5th edition October 2002),
				  available http://nepis.epa.gov/EPA/html/pubs/pubtitle.html or by calling (800)
				  490-9198.
Z13 Lozarchak, J. 2001, "Short-term Chronic Toxicity Tests on
				  Daphnia magna (Survival and Growth Tests)", USEPA, available from the
				  Department at 250 N. 17th Ave, Phoenix, AZ 85007, and at
http://www.azdhs.gov/documents/pre-paredness/state-laboratory/lab-licensure-certification/technical-resources/additional-resources/lazorchak-toxicity-method.pdf
.
Z14 ReadyCult Coliforms 100 Presence/Absence Test for
				  Detection and Identification of Coliform Bacteria and
Escherichia coli
in Finished Waters, Version 1.1, January 2007, available from EM
				  Science, EMD Millipore, 290 Concord Road, Billerica, MA 01821, at
				  http://www.emdmillipore.com, or by calling 781-533-6000.
Z15 Chromocult® Coliform Agar Presence/Absence Membrane
				  Filter Test Method for Detection and Identification of Coli-form Bacteria and
Escherichia coli
in Finished Waters, Version 1.0, November
				  2000, available from EM Science, EMD Millipore, 290 Concord Road, Billerica, MA
				  01821, at http://www.emdmillipore.com, or by calling 781-533-6000.