NMR Spectroscopy of Polymers
By: by Koichi Hatada, Tatsuki Kitayama
Contributors: Kitayama, Tatsuki
Series: Springer Laboratory; Springer Laboratory
Publisher: Springer Berlin Heidelberg
Published: 2004
Place of publication: Berlin, Heidelberg
Language: eng
Format: [electronic resource] /
Number of pages: 222
ISBN-13: 9783642072932; 9783662089828
Subjects: Physical organic chemistry; Analytical biochemistry; Chemistry; Polymers
Description: NMR Spectroscopy of Polymers places emphasis on the practical use of NMR spectroscopy in polymer chemistry rather than the theoretical treatments. Based on the authors' extensive experimental experience, topics covered include (1) experimental problems such as preparation of sample solution, selection of solvent, internal standard and tube, and contaminants in sample solution, (2) accuracy and precision of NMR measurements required in the analysis of polymer structure such as tacticity, copolymer composition and chain end structures, (3) volume magnetic susceptibility by NMR, (4) stereochemistry of polymer chains, chemical composition and comonomer sequence distribution in copolymers, and end groups and irregular linkages, (5) on-line coupled size exclusion chromatography(SEC) and NMR spectroscopy(SEC/NMR) in which an NMR spectrometer is set in the SEC system as a detector.
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Table of contents: title: Introduction to NMR Spectroscopy; title: Measurement of Spectrum with High Quality Including Quantitative Analysis; title: Stereochemistry of Polymers; title: Copolymer; title: NMR for the Study of Polymerization Reaction; title: Two-dimensional NMR Spectroscopy; title: NMR Relaxation; title: On-line SEC/NMR Analysis of Polymers.