# Effect of Process Parameters on Repeatability Precision of Weight for Microinjection Molding Products

Authors: Quan Wang; Jinrong Wang; Chongying Yang; Kaihui Du; Wenli Zhu; Xiaoli Zhang
Journal: Advances in Polymer Technology
 (2019)

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## Abstract

The repeatability precision of weight for injection molded products is important technical parameter to measure the quality and accuracy of injection molded products and evaluate the performance of injection molding machine. The influence of mold temperature, melt temperature, packing pressure, and packing time on the weight of microinjection molding products was studied by Taguchi orthogonal experiment. The influence of peak cavity pressure on the weight of products also was analysed. The experimental results show that the packing pressure is the most important process parameter affecting both the weight of the tensile and the impact specimens. With the increase of the packing pressure, the weight of the tensile and the impact specimens increases. When the peak cavity pressure reaches a certain value, the pressure value of the tensile specimen is 65 MPa, and the pressure value of the impact specimen is 68 MPa, the weight of the product increases quickly. The packing pressure increased from 85 MPa to 100 MPa, the weight of the tensile specimen increased from 0.544g to 0.559g, an increase of 2.7%, and the weight of the impact specimen increased from 0.418g to 0.425g, an increase of 1.7%.


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## Body

## 1. Introduction

With the development of the synthesis and molding technology of polymer materials, more and more polymer precision products are applied to the advanced technology fields such as aerospace, medical instruments, biological engineering, precision optics, electronic communication, and so on [1–5]. More than 90% of the plastic molding products are the two main molding methods in the process of polymer molding, extrusion molding, and injection molding. This puts forward higher requirements for the quality precision of the polymer molding products, and the research on the factors affecting the quality precision and how to evaluate the quality of the molded products scientifically and effectively is the precondition of improving the precision of the molding quality.Plastic injection molding is a widely used and complex process and is a highly efficient technique for producing a large quantity of plastic products, with high production requirement and tight tolerance. It is well-known as the manufacturing technique to produce products with various shapes and complex geometry at low cost [6–8]. The quality of parts produced by injection molding is a function of plastic material, part geometry, mold structure, and process conditions [9, 10].The repeatability accuracy of injection molded products includes three aspects, such as size, appearance, and injection weight. It can measure the quality and accuracy of injection products [11–14]. However, the size and appearance of the products are different because of different products shape. It cannot be used to realize the quantitative comparison of the performance of different products and different machines. Therefore, the repetition precision of injection weight is usually used as a technical index to measure the quality accuracy of injection products and evaluate the performance of the injection molding machine [15]. The weight repetition precision of the ordinary injection molding machine is about l%, which can reach 0.8%. The precision injection machine is lower than 0.5%, and the highest international level is less than 0.15% at present [16]. The improvement of the repetition precision of injection weight depends on the accuracy of mold processing and the rationality of the structure design, the performance of the raw materials, the rationality of the process parameters, and the control performance of the machine [17, 18]. Therefore, it is instructive for improving the repetition accuracy of injection weight to study the process parameters affecting the injection weight and the algorithm of repetition accuracy of injection weight which conforms to the characteristics of injection molding.


## 2. Calculation Method

The injection weight is the weight of the polymer melt from the nozzle of injection molding machine. The conventional injection weight based on the injection volume control method is related to the diameter of the injection screw and the injection stroke. The theoretical calculation formula is such as (1).(1)W=δπ4Ds2Sρ=VaρVa=δπ4Ds2SwhereW is the injection weight,g; ρ is density of polymer resin in room temperature, g/cm3; Ds is the diameter of the screw, cm;S is the stroke of screw, cm; Va is actual injection capacity, cm3; δ is injection coefficient, which varies with different raw materials.In (1), the diameter Ds of the screw is given by the injection machine and δ is the empirical coefficient. The injection stroke S of the screw is accurately measured by the displacement sensor and controlled by the servo motor driving the ball screw; that is to say, Va is kept constant. In the traditional injection volume control method, ρ is a constant value. The injection weight obtained from (1) is the weight of the injection product. However, in the actual injection process, ρ is not really constant. The change rate of melt density of polypropylene (Trademark T30S, MFR=3.2g/10min, supplied by Mao Ming Phoenix Ltd., China) is 6.44% when the pressure rises from 2 MPa to 30 MPa in temperature 190°C. When the temperature is 200°C, the change rate of polypropylene under the same pressure is 6.64% [19]. Therefore, the injection weight obtained by formula (1) is not the real weight of the injection molded product. Of course, the traditional volume control method cannot achieve the consistency of weight of injection products. According to the control technology of PVT in the injection process, the molding process, especially the temperature and pressure, has an important influence on the polymer meltρ [20, 21]. Therefore, the effect of molding process on the injection weight accuracy of microinjection molding products is studied in this paper.Repetitive precision refers to the degree of consistency between the results of continuous measurements of the same object under the same measurement conditions. It is the degree of repetition error in the measurement results. Therefore, the repetition accuracy of injection weight can be understood as the consistency between the weight of injection molded parts and the ideal weight of injection molded parts, which is a concept based on statistical process. There are two formulas for calculating the weight repeatability of products which are given as follows:(2)δG=wmax-wminw-×100%(3)δG=1/n-1∑i=1nwi-w-2w-×100%(4)w-=∑inwinwheren is the number of sample products; wi is the weight of the i product, g; wmax is the maximum weight of the product, g; wmin is the minimum weight of the product, g; w- is the average weight of the sample, g; δG is the repetition precision of the product weight.The denominators of (2) and (3) denote the arithmetic average weight of the sample product, and the numerator denotes the fluctuation of the sample data. Equation (2) is the sample range; and (3) is the sample standard deviation. Therefore, (2) is the polar difference algorithm, and (3) is the standard deviation algorithm. In order to objectively calculate the weight repetition accuracy of the products and eliminate the influence of abnormal values, (3) is chosen in the paper.


## 3. Experimental

### 3.1. Materials

The sample material used in this work was polypropylene in the form of pellets and with a trade mark 5090T (MFI=15g/10min), supplied by the Formosa petrochemical Corp, Taiwan.


### 3.2. Microinjection Molding Machine

The experimental work was carried out on an injection molding machine of type BOX XS concept having a maximum injection pressure 2298 bar, with screw diameter for plastication 14 mm and maximum weight of the product 6.1g as shown in Figure1.Figure 1
Experimental setup.


### 3.3. Mold

The multispline injection mold constructed from two parts (tensile specimen and impact specimen). The mold cavity thickness is 1 mm. The cavity pressure and temperature is measured in the mold cavity by the quartz sensor for mold cavity pressure type Kistler 6190CA, which has a front of 4.0 mm diameter. Data output from the amplifier is collected using a Kistler 5865 Como injection system. Computer is used to record the output reading of the acquisition system through an interface cart by the help of lab view program. The pressure sensors are installed in the middle of the specimens, respectively. The distance from the gate is 8 mm. The dimensions of specimen and gate are shown in Figure2.Figure 2
Dimension of specimen and gate.


### 3.4. Mold Temperature Controller

The mold temperature controller (model TP6ZE) was adopted using PIOVAN Co. Ltd., Italia.


### 3.5. Chiller

Chiller (model ML-CA03) was adopted Ming Lee Co. Ltd., Hong Kong, China.


### 3.6. Electronic Balance

Electronic balance (model CP214) was adopted OHAUS Co. Ltd., America. The accuracy is 0.1 mg.Melt temperature, mold temperature, packing pressure, packing time, and injection pressure were chosen as the process parameters. Parameters of injection molding process are reported in Table1.Table 1
Parameters of injection molding process.
Level melt temperature mold temperature Packing pressure Packing time Injection pressure (°C) (°C) (MPa) (s) (MPa) 1 220 40 85 5 85 2 230 50 90 10 90 3 240 60 95 15 95 4 250 70 100 20 100Orthogonal design is a high-efficiency design method for tests to arrange multifactor tests and seek optimal level combinations. The design method of orthogonal tests is able to determine optimal parameters by simply calculating influences of each factor on test results, showing the influences in charts, and then comprehensively comparing differences. The calculation is carried out on orthogonal tables, so the whole process is simple and clear. In this way, enough information can be obtained through a few tests, thus saving costs. An L16(45) orthogonal array was selected for the experimental design for each of the five factors. The four levels for the five parameters were identified during the 16 experiments. The data of injection five molds were recorded under the same conditions and the peak cavity pressure also was recorded. Then, the process parameters were changed to continue the same procedures. The values of these parameters are presented in Table 2.Table 2
Proposed L16 orthogonal array.
Level A B C D E 1 1 1 1 1 1 2 1 2 2 2 2 3 1 3 3 3 3 4 1 4 4 4 4 5 2 1 2 3 4 6 2 2 1 4 3 7 2 3 4 1 2 8 2 4 3 2 1 9 3 1 3 4 2 10 3 2 4 3 1 11 3 3 1 2 4 12 3 4 2 1 3 13 4 1 4 2 3 14 4 2 3 1 4 15 4 3 2 4 1 16 4 4 1 3 2


## 3.1. Materials

The sample material used in this work was polypropylene in the form of pellets and with a trade mark 5090T (MFI=15g/10min), supplied by the Formosa petrochemical Corp, Taiwan.


## 3.2. Microinjection Molding Machine

The experimental work was carried out on an injection molding machine of type BOX XS concept having a maximum injection pressure 2298 bar, with screw diameter for plastication 14 mm and maximum weight of the product 6.1g as shown in Figure1.Figure 1
Experimental setup.


## 3.3. Mold

The multispline injection mold constructed from two parts (tensile specimen and impact specimen). The mold cavity thickness is 1 mm. The cavity pressure and temperature is measured in the mold cavity by the quartz sensor for mold cavity pressure type Kistler 6190CA, which has a front of 4.0 mm diameter. Data output from the amplifier is collected using a Kistler 5865 Como injection system. Computer is used to record the output reading of the acquisition system through an interface cart by the help of lab view program. The pressure sensors are installed in the middle of the specimens, respectively. The distance from the gate is 8 mm. The dimensions of specimen and gate are shown in Figure2.Figure 2
Dimension of specimen and gate.


## 3.4. Mold Temperature Controller

The mold temperature controller (model TP6ZE) was adopted using PIOVAN Co. Ltd., Italia.


## 3.5. Chiller

Chiller (model ML-CA03) was adopted Ming Lee Co. Ltd., Hong Kong, China.


## 3.6. Electronic Balance

Electronic balance (model CP214) was adopted OHAUS Co. Ltd., America. The accuracy is 0.1 mg.Melt temperature, mold temperature, packing pressure, packing time, and injection pressure were chosen as the process parameters. Parameters of injection molding process are reported in Table1.Table 1
Parameters of injection molding process.
Level melt temperature mold temperature Packing pressure Packing time Injection pressure (°C) (°C) (MPa) (s) (MPa) 1 220 40 85 5 85 2 230 50 90 10 90 3 240 60 95 15 95 4 250 70 100 20 100Orthogonal design is a high-efficiency design method for tests to arrange multifactor tests and seek optimal level combinations. The design method of orthogonal tests is able to determine optimal parameters by simply calculating influences of each factor on test results, showing the influences in charts, and then comprehensively comparing differences. The calculation is carried out on orthogonal tables, so the whole process is simple and clear. In this way, enough information can be obtained through a few tests, thus saving costs. An L16(45) orthogonal array was selected for the experimental design for each of the five factors. The four levels for the five parameters were identified during the 16 experiments. The data of injection five molds were recorded under the same conditions and the peak cavity pressure also was recorded. Then, the process parameters were changed to continue the same procedures. The values of these parameters are presented in Table 2.Table 2
Proposed L16 orthogonal array.
Level A B C D E 1 1 1 1 1 1 2 1 2 2 2 2 3 1 3 3 3 3 4 1 4 4 4 4 5 2 1 2 3 4 6 2 2 1 4 3 7 2 3 4 1 2 8 2 4 3 2 1 9 3 1 3 4 2 10 3 2 4 3 1 11 3 3 1 2 4 12 3 4 2 1 3 13 4 1 4 2 3 14 4 2 3 1 4 15 4 3 2 4 1 16 4 4 1 3 2


## 4. Results and Discussion

The variance analysis of the relationship between the specimen weight and the process parameters was carried out, in which A stands for melt temperature (°C), B stands for mold temperature (°C), C stands for packing pressure (MPa), D stands for packing time (s), and E stands for injection pressure (MPa). Figure3 shows that the packing pressure, mold temperature, and melt temperature have great influence on the weight of the product, while the packing time and injection pressure have little influence on the weight of the product.Figure 3
Horizontal trend chart of tensile and impact specimen.The weight of the tensile and impact specimens increases with the increase of the melt temperature as illustrated in Figure4. The weight of the tensile specimen increases faster than that of the impact specimen in the melt temperature range of 230°C to 240°C. When the melt temperature rises from 220°C to 250°C, the weight of the tensile specimen increases from 0.548g to 0.554g, by 1.1%. The weight increased from 0.419g to 0.423g, an increase of 0.9% for the impact specimen.Figure 4
Influence of melt temperature on product weight.Figure5 shows the effect of mold temperature on the weight of the product. The weight of the tensile specimen increases with the increase of mold temperature, but the impact specimen shows the opposite situation. This may be due to the filling unbalance of the two mold cavities because of different dimensions and weight of product. The cavity of impact specimen is filled before the tensile specimen, resulting in a large residual stress and shrinkage. In molding process, reasonable adjustment of process parameters should be made to achieve the best balance filling of two cavities. The weight of tensile specimen increased from 0.544g to 0.551g, an increase of 1.3%, and the weight of impact specimen decreased from 0.422g to 0.420g, a decrease of 0.47%. The increase of mold temperature can promote the filling of melt, the specimen is more compact, the melt fluidity will be guaranteed, and the mechanical properties of the specimen are improved.Figure 5
Influence of mold temperature on product weight.Figure6 is the effect of packing pressure on the weight. The weight of tensile and impact specimens increases with the increase of packing pressure, which is due to the increase of packing pressure, filling more melt in the cavity at the same time, the specimen is more compact, but excessive packing pressure will cause stress of products. The packing pressure increased from 85 MPa to 100 MPa, the weight of tensile specimen increased from 0.544g to 0.559g, an increase of 2.7%, and the weight of impact specimen increased from 0.418 g to 0.425 g, an increase of 1.7%.Figure 6
Influence of packing pressure on product weight.Influence of packing time on product weight is illustrated in Figure7. The packing time has little effect on the weight of the product, indicating that when the product is small, the gate has cooled, and increasing the packing time has little effect on the weight of the product.Figure 7
Influence of packing time on product weight.Because the filling process of the cavity is not known in the molding process, the weights of the parts become important basis for verifying the defects of parts. In the process of injection molding, the pressure is not large enough to fill the cavity; short shots and other phenomena will occur. Injection molding pressure is one of the key processing parameters mentioned in several research works [22–25]. The peak cavity pressure and product weight have a certain relationship. Because the cavity pressure curve records the change of cavity pressure during the whole injection molding process, the relationship between them is studied to guide the production better.The weight of the tensile and impact specimen increases with the increase of the peak cavity pressure as illustrated in Figure8. This is because the larger the peak cavity pressure, the better the fluidity of melt, the more the melt injected into the cavity at the same time, and the greater the density of the specimen. At the same time, the weight of the specimen does not increase significantly before the cavity pressure reaches 65 MPa for tensile specimen. After the peak pressure reaches 65 MPa, the weight increases rapidly. The peak cavity pressure increases; the more melt is filled into the cavity in the same time. The density of specimen is enhanced, and the weight of the specimen increases. The pressure continues to pack in additional material which is low in viscosity. Therefore, the less viscous melt is able to fill up the cavity thoroughly and even created some flash without causing significant increase in pressure. Due to the fact that more material is in the cavity, the parts produced are heavier and denser although peak cavity pressure does not increase much. The maximum weight of impact specimen appears about 71 MPa. Because the peak cavity pressure has a high correlation with the weight of specimen, the pressure value and the actual parts can be recorded in actual molding process. It can be used as a reference in molding process. It can also be used to judge the actual injection process of specimen according to the peak cavity pressure.Figure 8
Effect of the peak cavity pressure on the tensile and impact specimen weight.


## 5. Conclusions

An experimental work is carried out to study the effect of the microinjection molding parameters on the product weight in this paper. For the tensile and impact specimens, the packing pressure is the most important parameter affecting their weight. With the increase of packing pressure, the weight of both the tensile and impact specimens increases. The cavity pressure of impact specimen is larger than that of tensile specimen during injection molding because of unbalance filled. When the cavity pressure increases, the weight of the specimen will increase; when the peak cavity pressure reaches a certain value, the peak cavity pressure is about 65 MPa for tensile specimen and peak cavity pressure is about 68 MPa for impact specimen; when the peak cavity pressure increases, the weight of specimen increases significantly.



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