A process of making a fluff pulp sheet, comprising: adding a first debonder surfactant at the wet-end with fluff pulp fibers to form a mixture; raising the pH to a second pH, which is higher than the first pH; drying the mixture to form a web; and adding a second debonder surfactant to the web to form the fluff pulp sheet, wherein the first and the second debonder surfactants comprise independently from each other one or more of linear or branched monoalkyl amine, linear or branched dialkyl amine, linear or branched tertiary alkyl amine, linear or branched quarternary alkyl amine, ethoxylated alcohol, linear or branched, saturated or unsaturated hydrocarbon surfactant, fatty acid amide, fatty acid amide quaternary ammonium salt, dialkyl dimethyl quaternary ammonium salt, dialkylimidazolinium quaternary ammonium salt, dialkyl ester quaternary ammonium salt, triethanolamine-ditallow fatty acid, fatty acid ester of ethoxylated primary amine, ethoxylated quarternary ammonium salt, dialkyl amide of fatty acid, cationic surfactant, anionic surfactant, C 16 -C 18 unsaturated alkyl alcohol ethoxylate, compound having CAS Registry No. 68155-01-1, compound having CAS Registry No. 26316-40-5, or a combination thereof; wherein the first pH is < 5.0, the second pH is ≥ 5.0, and the application of the first debonder surfactant is carried out before, during, or after the raising of the pH to the second pH, or a combination thereof; and wherein all the debonder surfactants are present in a total amount of from 0.45 - 9.07 kg per ton of the fluff pulp fibers. adding a first debonder surfactant at the wet-end with fluff pulp fibers to form a mixture; raising the pH to a second pH, which is higher than the first pH; drying the mixture to form a web; and adding a second debonder surfactant to the web to form the fluff pulp sheet, wherein the first and the second debonder surfactants comprise independently from each other one or more of linear or branched monoalkyl amine, linear or branched dialkyl amine, linear or branched tertiary alkyl amine, linear or branched quarternary alkyl amine, ethoxylated alcohol, linear or branched, saturated or unsaturated hydrocarbon surfactant, fatty acid amide, fatty acid amide quaternary ammonium salt, dialkyl dimethyl quaternary ammonium salt, dialkylimidazolinium quaternary ammonium salt, dialkyl ester quaternary ammonium salt, triethanolamine-ditallow fatty acid, fatty acid ester of ethoxylated primary amine, ethoxylated quarternary ammonium salt, dialkyl amide of fatty acid, cationic surfactant, anionic surfactant, C 16 -C 18 unsaturated alkyl alcohol ethoxylate, compound having CAS Registry No. 68155-01-1, compound having CAS Registry No. 26316-40-5, or a combination thereof; wherein the first pH is < 5.0, the second pH is ≥ 5.0, and the application of the first debonder surfactant is carried out before, during, or after the raising of the pH to the second pH, or a combination thereof; and wherein all the debonder surfactants are present in a total amount of from 0.45 - 9.07 kg per ton of the fluff pulp fibers. wherein the first and the second debonder surfactants comprise independently from each other one or more of linear or branched monoalkyl amine, linear or branched dialkyl amine, linear or branched tertiary alkyl amine, linear or branched quarternary alkyl amine, ethoxylated alcohol, linear or branched, saturated or unsaturated hydrocarbon surfactant, fatty acid amide, fatty acid amide quaternary ammonium salt, dialkyl dimethyl quaternary ammonium salt, dialkylimidazolinium quaternary ammonium salt, dialkyl ester quaternary ammonium salt, triethanolamine-ditallow fatty acid, fatty acid ester of ethoxylated primary amine, ethoxylated quarternary ammonium salt, dialkyl amide of fatty acid, cationic surfactant, anionic surfactant, C 16 -C 18 unsaturated alkyl alcohol ethoxylate, compound having CAS Registry No. 68155-01-1, compound having CAS Registry No. 26316-40-5, or a combination thereof; wherein the first pH is < 5.0, the second pH is ≥ 5.0, and the application of the first debonder surfactant is carried out before, during, or after the raising of the pH to the second pH, or a combination thereof; and wherein all the debonder surfactants are present in a total amount of from 0.45 - 9.07 kg per ton of the fluff pulp fibers.