Year: 1898

page_text: I, EDMOND HAAS, of the Firm of A Raynaud & Co., of 11, Place de la Madeleine,
Paris, in the Republic of France, Perfumer, do hereby declare the nature of this
invention to be as follows..
This invention relates to a novel manufacture of articles of perfumery such as
sachets, plaquettes, crayons, sticks, pastilles, amulets, medals, envelopes, statuettes,
flowers and all such articles of any shape, size and colour, the said articles being
composed essentially of pure cellulose which is impregnated with perfume adapted
to be given off by fiction, contact or simple volatilisation
The basis of the perfumed articles manufactured according to my invention
is cellulose or pulp of rags, etc., brought to a high degree of purity and which I
propose to designate "lulosine," the said cellulose being obtained by ordinary and
known processes The paste of lulosine from which any one of the above named
articles is to be manufactured, is more or less sized, homogeneous, porous or
compressed according to the hardness and the fragility which it is desired to impart
to the article to be manufactured
When it is desired to obtain the perfume with which the article is impiegnated
by fiction, I advantageously add to the paste a substance wluch can be dısın-
tegrated such for example as carbonate of magnesium, sulphate or carbonate of
lime etc, in varying proportions
According to the nature of the product to be obtained the manufacture can be
effected by hand through the medium of moulds or mechanically. As an example
I will explain the method of manufacture of sachet-plaquettes for all kinds of
perfume
The pure cellulose, being obtained by the ordinary processes and diluted with
water more or less mixed with glue, for example in the proportion of from 10 to
12%, 19 dried by being passed through a press and it is then ready to be directly
placed in the moulds, or 18 formed into a compact block which is then subjected
to as complete a diving or dessication as 18 possible
The block is then formed into sheets or the like of any desired shape, for
example a rectangular shape of varying thickness The sheet thus obtained 18
then pressed in a mould where it acquires the desired shape, reliefs and inscrip-
tions, which latter can, however, be cemented directly upon the said sheet
sheets thus moulded are soaked for a suitable length of time in baths of the desired
perfume, then, after they have been thoroughly impregnated, they are allowed to
drin and are then diied in stoves.
The
My novel method of manufacture of lulosine impregnated with perfume can
be advantageously employed for the manufacture of artificial flowers, not contain-

page_text: ing any other analogous material
Flowers manufactured by this method differ
considerably from those made of paper by the ordinary methods; the perfume
penetrating the pores of the pure cellulose is preserved practically indefinitely
whilst it volatilises rapidly fiom all articles obtained by processes hitherto in
vogue.
I may remark that lulosine can be scented not only after the finished article
18 obtained but in the course of the manufacture in the paste itself by means of
essences, extracts, colouring matters or powders so that it acquires an inalterable
basis of perfume independently of the impregnation with perfume which it under-
goes when the article is manufactured.
Furthermore, lulosine 18 not only adapted to receive all possible shapes, but it
can also be coloured in any shade; for example, in the case of artificial flowers
the colours can be incorporated in the paste during the manufacture thereof
or they can be applied to the finished article.
The various articles of perfumery manufactured as above described possess the
property of preserving the scents or perfumes which are incorporated in them prac-
tically indefinitely and they can also take any desired shape, the past from which
they are formed lending itself easily during the manufacture to shaping in moulds by
hand or mechanically These various articles thus form new commercial products
Dated this 9th day of June 1898
G F. REDFERN & Co,
4, South Street, Finsbury, London, Agents for the Applicant.
I, EDMOND HAAS, of the Firm of A Raynaud & Co., of 11, Place de la Madeleine,
Paris, in the Republic of France, Perfumer, do hereby declare the nature of this
invention and in what manner the same 18 to be performed, to be particularly
described and ascertained in and by the following statements-
This invention relates to a novel manufacture of articles of perfumery such as
sachets, plaquettes, crayons, sticks, pastilles, amulets, medals, envelopes, statuettes,
flowers and all such articles of any shape, size and colour, the said articles being
composed essentially of pure cellulose which 18 impregnated with perfume adapted
to be given off by friction, contact or simple volatilisation
The basis of the perfumed articles manufactured according to my invention
is cellulose or pulp of rags, etc., brought to a high degree of purity and which I
propose to designate "lulosine," the said cellulose being obtained by ordinary and
known рrосеваев
The paste of lulosine from which any one of the above named
articles is to be manufactured, is more or less sized, homogeneous, porous or
compressed according to the hardness and the fragility which it is desired to impart
to the article to be manufactured
When it is desired to obtain the perfume with which the article 18 impregnated
by friction, I advantageously add to the paste a substance which can be disin-
tegrated such for example as carbonate of magnesium, sulphate or carbonate of
lime etc., in varving proportions.
According to the nature of the product to be obtained the manufacture can be
effected by hand through the medium of moulds, or mechanically. As an example

page_text: I will explain the method of manufacture of sachet-plaquettes for all kinds of
perfume.
The pure cellulose, being obtained by the ordinary processes and diluted with
water more or less mixed with glue, for example in the proportion of from 10 to
12%, 18 dried by being passed through a press and 18 then ready to be directly
placed in the moulds, or is formed into a compact block which is then subjected
to as complete a dying on dessication as is possible
The block 18 then formed into sheets or the like of any desired shape, for
example a rectangular shape of varying or suitable thickness The sheet thus obtained
is pressed in a mould where it acquires the desned shape, reliefs and inscrip-
tions, which latter can, however, be cemented duectly upon the said sheet The
sheets thus moulded are soaked for a suitable length of time in baths of the desired
perfume, then, after they have been thoroughly impregnated, they are allowed to
drip and are afterwards dried in stoves.
My novel method of manufacture of lulosine impregnated with perfume can
be advantageously employed for the manufacture of artificial floweis Flowers
manufactured by this method differ considerably from those made of paper by the
ordinary methods; the perfume penetrating the pores of the pure cellulose is
presei ved practically indefinitely whilst it volatilises rapidly from all articles
obtained by processes hitherto in vogue
I may remark that lulosine can be scented not only after the finished article
is obtained but in the course of the manufacture in the paste itself by means of
essences, extracts, colouring matters or powders so that it acquires an inalterable
basis of perfume independently of the impregnation with perfume which it under-
goes when the article is manufactured
Furthermore, lulosine is not only adapted to receive all possible shapes, but it
can also be coloured in any shade, for example, in the case of artificial flowers
the colours can be incorporated in the paste during the manufacture thereof
or they can be applied to the finished article.
The various articles of perfumery manufactured as above described possess the
property of preserving the scents or perfumes which are incorporated in them prac-
tically indefinitely and they can also take any desired shape, the paste from which
they are formed lending itself easily during the manufacture to shaping in moulds by
hand or mechanically These various articles thus form new commercial products
Having now particularly described and ascertained the nature of my said
invention and in what manner the same is to be performed, I declare that what
I claim is:-
1. An improved manufacture of articles of perfumery consisting in the employ-
ment of pure cellulose or rag pulp (termed lulosine) impregnated with the desired
perfume, the pure cellulose being prepared in the ordinary manner, treated with
water (with or without glue) and dried by means of a press, the blocks formed
being then placed in suitable moulds, or being treated mechanically or by hand,
to form the desired article which is then soaked in a bath of the desired perfume
for a suitable time, allowed to drip or drain and afterwards dried in a stove,
substantially as, and for the purpose, hereinbefore described.
2 In a process of the kind described in Claim 1 and in the case where the
perfume is to be given off by friction the incorporation in the lulosine of any
substance which is easily disintegrated, such as magnesium carbonate sulphate, or
carbonate of lime, etc., in varying proportions, substantially as, and for the
purpose, herein before described.
3. In a process of the kind described in Claim 1, the incorporation in the lulosine
during its manufacture of perfumes and colours for the purpose of giving to the
articles manufactured a more permanent scent and colour, substantially as herein-
before described
4 As new articles of manufacture, articles made of pure cellulose impregnated
with scents and colours in the manner described in the preceding claiming clauses

page_text: such for example as sachets, placquettes, crayons, sticks, pastilles, amulets, medals,
envelopes, statuettes, flowers, and all ordinary articles of perfumery of any shape,
size or colour
Data
1
ML 1900
G F. REDFERN & Co,
4, South Street, Finsbury, London, Agents for the Applicant