Patent ID: 10118831

Abstract:
The invention provides for a method of making a magnesium aluminate spinel including an alumina compound and a magnesium compound, the method including the steps of; dispersing the alumina compound by dispersing it in a aqueous solution, to form an alumina dispersion, the aqueous solution having a pH of between 2 and 5; preferably between 2 and 4, flocculating the alumina by increasing the pH of the alumina dispersion to a pH of between 8 and 10 by adding a base; adding the alumina dispersion to an aqueous dispersion of the magnesium compound to form a slurry; drying the slurry to produce a dried spinel precursor; and calcining the dried spinel precursor to produce the magnesium aluminate spinel. Dispersing at such a low pH results in a conversion to spinel as well as allows for the control of the surface area of the spinel.