Microscale and Macroscale Techniques in the Organic Laboratory
1. Laboratory Safety. 2. Advance Preparation and Laboratory Records. 3. Laboratory Glassware. 4. How to Find Data for Your Compound: Handbooks and Catalogues. 5. Measurement of Volume and Weight. 6. Heating and Cooling Methods. 7. Reaction Methods. 8. Filtration. 9. Physical Constants of Solids: The Melting Point. 10. Solubility. 11. Crystallization: Purification of Solids. 12. Extractions, Separations, and Drying Agents. 13. Physical Constants of Liquids: Boiling Point and Density. 14. Simple Distillation. 15. Fractional Distillation; Azeotropes. 16. Vacuum Distillation; Manometers. 17. Sublimation. 18. Steam Distillation. 19. Column Chromatography. 20. Thin-Layer Chromatography. 21. High-Performance Liquid Chromatography (HPLC). 22. Gas Chromatography. 23. Polarimetry. 24. Refractometry. 25. Infrared Spectroscopy. 26. Nuclear Magnetic Resonance Spectroscopy (Proton NMR). 27. Carbon-13 Nuclear Magnetic Resonance Spectroscopy. 28. Mass Spectrometry. 29. Computational Chemistry. 30. Guide to the Chemical Literature.