## 3 Results
\begin{table}
\begin{tabular}{c c c c c c c} \hline \hline
**Peak** & **RT** & **\% (Liq)** & **\% (HS)** & **\% (SPME)** & **Compound** & **Type** & **RI** \\ \hline
44 & 23.801 & traces & 0.10 &
\begin{tabular}{c} (_E_)-4-decenoic acid \\ methyl ester \\ \end{tabular} & fatty acid ester & 1299 \\ \hline
45 & 24.202 & traces & 0.10 & methyl decanoate & fatty acid ester & 1325 \\ \hline
46 & 24.939 & & traces & \(\alpha\)-cubebene & tricyclic sesquiterpene & 1351 \\ \hline
47 & 25.525 & traces & 0.24 & ylangene & tricyclic sesquiterpene & 1372 \\ \hline
48 & 25.685 & 0.11 & 0.48 & ethyl _trans_-4-decenoate & fatty acid ester & 1375 \\ \hline
49 & 25.837 & 0.09 & 0.36 & hexyl hexanoate & fatty acid ester & 1384 \\ \hline
50 & 25.990 & traces & 0.13 & _7-epi_-sesquithujene & bicyclic sesquiterpene & 1391 \\ \hline
51 & 26.086 & 0.10 & 0.38 & ethyl decanoate & fatty acid ester & 1396 \\ \hline
52 & 26.246 & & traces & tetradecane & hydrocarbon & 1400 \\ \hline
53 & 26.302 & & traces & cyperene & tricyclic sesquiterpene & 1399 \\ \hline
54 & 26.390 & 0.17 & 0.09 & & sesquithujene & bicyclic sesquiterpene & 1402 \\ \hline
55 & 26.463 & & traces & 0.72 & _cis_-caryophyllene & bicyclic sesquiterpene & 1406 \\ \hline
56 & 26.647 & 0.29 & 0.32 & _cis_-\(\alpha\)-bergamotene & bicyclic sesquiterpene & 1415 \\ \hline
57 & 26.807 & **21.80** & **15.85** & **30.19** & \(\beta\)**-caryophyllene** & bicyclic sesquiterpene & 1419 \\ \hline
58 & 27.047 & & & 0.66 &
\begin{tabular}{c} 10,10-dimethyl-2,6- \\ dimethylenebicycloclo \\ \end{tabular} & bicyclic sesquiterpene & 1440 \\ \hline
59 & 27.16 & **2.30** & **1.71** & **4.48** & \(\alpha\)-bergamotene & bicyclic sesquiterpene & 1435 \\ \hline
60 & 27.248 & 0.14 & traces & 0.35 & \(\alpha\)-guaiene & bicyclic sesquiterpene & 1439 \\ \hline
61 & 27.376 & & traces & guaia-6,9-diene & bicyclic sesquiterpene & 1444 \\ \hline
62 & 27.465 & & traces & _epi_-\(\beta\)-santalene & bicyclic sesquiterpene & 1448 \\ \hline
63 & 27.480 & & & 0.09 & \(\alpha\)-himachane & bicyclic sesquiterpene & \\ \hline
64 & 27.649 & **9.18** & **5.64** & **16.79** & \(\alpha\)**-humulene** & monocyclic sesquiterpene & 1454 \\ \hline
65 & 27.809 & & & traces & \(\beta\)-santalene & bicyclic sesquiterpene & 1462 \\ \hline
66 & 28.338 & & & 0.63 & \(\alpha\)-curcumene & aromatic sesquiterpene & 1483 \\ \hline
67 & 28.370 & 0.47 & 0.28 & & selina-4,11-diene & bicyclic sesquiterpene & 1474 \\ \hline
68 & 28.402 & & & 1.22 &
\begin{tabular}{c} 4a,8-dimethyl-2-(prop-1- \\ en-2-yl)-1,2,3,4,4a,5,6,7- \\ octahydronaphthalene \\ \end{tabular} & bicyclic sesquiterpene & 1492 \\ \hline
69 & 28.443 & 0.50 & 0.22 & 1.22 & \(\beta\)-seline & bicyclic sesquiterpene & 1486 \\ \hline
70 & 28.587 & & 0.27 & 1.26 & valencene & bicyclic sesquiterpene & 1492 \\ \hline
71 & 28.627 & 0.42 & 0.22 & 1.18 & \(\alpha\)-seline & bicyclic sesquiterpene & 1494 \\ \hline
72 & 28.747 & & traces & 0.11 & \(\beta\)-dihydroaagrofuran & tricyclic sesquiterpene & 1496 \\ \hline
73 & 28.819 & 1.56 & 0.74 & **2.77** & \(\alpha\)-farnesene & acyclic sesquiterpene & 1508 \\ \hline
74 & 28.931 & & & 0.19 & \(\beta\)-curcumene & monocyclic sesquiterpene & 1514 \\ \hline
75 & 28.972 & & traces & sesquicineole & bicyclic sesquiterpene & 1516 \\ \hline
76 & 29.140 & 0.65 & 0.29 & 1.38 & \(\beta\)-sesquiphellandrene & monocyclic sesquiterpene & 1524 \\ \hline
77 & 29.389 & 0.90 & 0.12 & 1.05 & \(\gamma\)-seline & bicyclic sesquiterpene & 1538 \\ \hline
78 & 29.493 & 0.85 & 0.27 & **1.55** & selina-3,7(11)-diene & bicyclic sesquiterpene & 1542 \\ \hline
79 & 29.757 & & 0.09 & & germacrene B & monocyclic sesquiterpene & 1557 \\ \hline
80 & 29.781 & 0.20 & & & nerolidol & acyclic sesquiterpene & 1544 \\ \hline \hline \end{tabular}
\end{table} 
Table 2: _Cont._In Table 3, limonene was the biggest peak in HS and SPME and selina-3,7(11)-diene in Liq. Next, 8 different compounds were above 5%; in Liq--5 above 5%, in HS--5 above 5%, and in SPME--6 above 5%.