## 3 Results
### Volatile Organic Compounds
\begin{table}
\begin{tabular}{c c c c c c c c c} \hline  & \multicolumn{2}{c}{**25\({}^{\circ}\)C**} & \multicolumn{2}{c}{**40\({}^{\circ}\)C**} \\ \hline  & \multicolumn{2}{c}{**Time 0**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} \\ \hline
**Compound** & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} \\ \hline \(\Sigma\) Furans & 36.47 \(\pm\) 0.30 & 42.47 \(\pm\) 0.06 \({}^{\circ}\) & 45.35 \(\pm\) 0.08 \({}^{\circ}\) & 42.86 \(\pm\) 0.15 \({}^{\circ}\) & 49.65 \(\pm\) 0.06 \({}^{\circ}\) & 40.03 \(\pm\) 0.10 \({}^{\circ}\) & 50.13 \(\pm\) 0.15 \({}^{\circ}\) & 40.64 \(\pm\) 0.20 \({}^{\circ}\) & 49.11 \(\pm\) 0.20 \({}^{\circ}\) \\ \hline
2-Parammethanol & 18.88 \(\pm\) 0.37 & 20.02 \(\pm\) 0.08 \({}^{\circ}\) & 25.27 \(\pm\) 0.10 \({}^{\circ}\) & 24.14 \(\pm\) 0.36 \({}^{\circ}\) & 29.82 \(\pm\) 0.03 \({}^{\circ}\) & 19.95 \(\pm\) 0.20 \({}^{\circ}\) & 25.21 \(\pm\) 0.01 \({}^{\circ}\) & 23.09 \(\pm\) 0.67 \({}^{\circ}\) & 29.94 \(\pm\) 0.32 \({}^{\circ}\) \\ \hline Furfuryl acetate & 7.28 \(\pm\) 0.59 & 9.82 \(\pm\) 0.04 \({}^{\circ}\) & 7.93 \(\pm\) 0.29 \({}^{\circ}\) & 8.76 \(\pm\) 0.17 \({}^{\circ}\) & 7.35 \(\pm\) 0.04 \({}^{\circ}\) & 9.08 \(\pm\) 0.07 \({}^{\circ}\) & 10.62 \(\pm\) 0.46 \({}^{\circ}\) & 8.86 \(\pm\) 0.31 \({}^{\circ}\) & 8.51 \(\pm\) 0.06 \({}^{\circ}\) \\ \hline Furfuryl isovalerate & 0.13 \(\pm\) 0.03 & 0.45 \(\pm\) 0.01 \({}^{\circ}\) & 0.39 \(\pm\) 0.01 \({}^{\circ}\) & 0.39 \(\pm\) 0.04 \({}^{\circ}\) & 0.36 \(\pm\) 0.02 \({}^{\circ}\) & 0.39 \(\pm\) 0.03 \({}^{\circ}\) & 0.31 \(\pm\) 0.01 \({}^{\circ}\) & 0.39 \(\pm\) 0.01 \({}^{\circ}\) & 0.36 \(\pm\) 0.02 \({}^{\circ}\) \\ \hline Furfuryl & 4.51 \(\pm\) 0.66 & 4.02 \(\pm\) 0.13 \({}^{\circ}\) & 3.92 \(\pm\) 0.13 \({}^{\circ}\) & 2.41 \(\pm\) 0.05 \({}^{\circ}\) & 5.04 \(\pm\) 0.17 \({}^{\circ}\) & 4.04 \(\pm\) 0.10 \({}^{\circ}\) & 5.21 \(\pm\) 0.08 \({}^{\circ}\) & 2.10 \(\pm\) 0.06 \({}^{\circ}\) & 2.75 \(\pm\) 0.04 \({}^{\circ}\) \\ \hline Dihydro-2-methyl-3-furanone & 1.49 \(\pm\) 0.31 & 0.89 \(\pm\) 0.04 \({}^{\circ}\) & 0.84 \(\pm\) 0.03 \({}^{\circ}\) & 1.00 \(\pm\) 0.06 \({}^{\circ}\) & 0.90 \(\pm\) 0.05 \({}^{\circ}\) & 3.93 \(\pm\) 0.08 \({}^{\circ}\) & 6.33 \(\pm\) 0.30 \({}^{\circ}\) & 3.41 \(\pm\) 0.15 \({}^{\circ}\) & 5.11 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline
5-methyl-Fururland & 3.37 \(\pm\) 0.11 & 5.15 \(\pm\) 0.01 \({}^{\circ}\) & 5.37 \(\pm\) 0.01 \({}^{\circ}\) & 4.51 \(\pm\) 0.14 \({}^{\circ}\) & 4.76 \(\pm\) 0.06 \({}^{\circ}\) & 0.88 \(\pm\) 0.03 \({}^{\circ}\) & 0.81 \(\pm\) 0.02 \({}^{\circ}\) & 1.01 \(\pm\) 0.05 \({}^{\circ}\) & 0.96 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline
2-Marathevichan & 0.53 \(\pm\) 0.03 & 1.71 \(\pm\) 0.02 \({}^{\circ}\) & 12.48 \(\pm\) 0.03 \({}^{\circ}\) & 1.32 \(\pm\) 0.13 \({}^{\circ}\) & 0.95 \(\pm\) 0.02 \({}^{\circ}\) & 1.45 \(\pm\) 0.30 \({}^{\circ}\) & 1.25 \(\pm\) 0.10 \({}^{\circ}\) & 1.41 \(\pm\) 0.03 \({}^{\circ}\) & 1.18 \(\pm\) 0.06 \({}^{\circ}\) \\ \hline Durfuryl  
\begin{table}
\begin{tabular}{c c c c c c c c c c} \hline \hline \multicolumn{1}{c}{} & \multicolumn{4}{c}{**25 \({}^{\circ}\)C**} & \multicolumn{4}{c}{**40 \({}^{\circ}\)C**} \\ \hline  & **Time 0** & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} \\ \hline
**Compound** & \multicolumn{2}{c}{**STD**} & \multicolumn  
\begin{table}
\begin{tabular}{c c c c c c c c c c} \hline \hline  & \multicolumn{4}{c}{**25 \({}^{\circ}\)C**} & \multicolumn{4}{c}{**40 \({}^{\circ}\)C**} \\ \hline  & \multicolumn{2}{c}{**Time 0**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} \\ \hline
**Compound** & & **STD** & **ALT** & **STD** & **ALT** & **STD** & **ALT** & **STD** & **ALT** & **STD** & **ALT** \\ \hline
2-Acetypyrrole & 0.31 \(\pm\) 0.06 & 0.99 \(\pm\) 0.02 \({}^{\circ}\) & 0.99 \(\pm\) 0.03 \({}^{\circ}\) & 0.77 \(\pm\) 0.02 \({}^{\circ}\) & 1.09 \(\pm\) 0.02 \({}^{\circ}\) & 0.94 \(\pm\) 0.01 \({}^{\circ}\) & 1.01 \(\pm\) 0.02 \({}^{\circ}\) & 0.81 \(\pm\) 0.06 \({}^{\circ}\) & 1.12 \(\pm\) 0.05 \({}^{\circ}\) \\ \hline
1H-pyrrole-2-carboxaldehyde & n.d. & 0.28 \(\pm\) 0.02 \({}^{\circ}\) & 0.22 \(\pm\) 0.01 \({}^{\circ}\) & 0.23 \(\pm\) 0.01 \({}^{\circ}\) & 0.23 \(\pm\) 0.02 \({}^{\circ}\) & 0.19 \(\pm\) 0.01 \({}^{\circ}\) & 0.15 \(\pm\) 0.03 \({}^{\circ}\) & 0.17 \(\pm\) 0.02 \({}^{\circ}\) & 0.19 \(\pm\) 0.04 \({}^{\circ}\) \\ \hline \(\Sigma\) Aldehydes & 0.76 \(\pm\) 0.29 & 1.68 \(\pm\) 0.03 \({}^{\circ}\) & 1.20 \(\pm\) 0.02 \({}^{\circ}\) & 1.82 \(\pm\) 0.02 \({}^{\circ}\) & 1.05 \(\pm\) 0.03 \({}^{\circ}\) & 1.72 \(\pm\) 0.01 \({}^{\circ}\) & 0.88 \(\pm\) 0.01 \({}^{\circ}\) & 1.92 \(\pm\) 0.05 \({}^{\circ}\) & 0.79 \(\pm\) 0.02 \({}^{\circ}\) \\ \hline
2-Butenal & 0.45 \(\pm\) 0.06 & 1.19 \(\pm\) 0.06 \({}^{\circ}\) & 1.20 \(\pm\) 0.02 \({}^{\circ}\) & 1.24 \(\pm\) 0.01 \({}^{\circ}\) & 1.05 \(\pm\) 0.03 \({}^{\circ}\) & 1.27 \(\pm\) 0.01 \({}^{\circ}\) & 0.88 \(\pm\) 0.01 \({}^{\circ}\) & 1.13 \(\pm\) 0.06 \({}^{\circ}\) & 0.79 \(\pm\) 0.02 \({}^{\circ}\) \\ \hline Benzaldehyde & 0.31 \(\pm\) 0.23 & 0.49 \(\pm\) 0.01 \({}^{\circ}\) & n.d. & 0.58 \(\pm\) 0.02 \({}^{\circ}\) & n.d. & 0.45 \(\pm\) 0.01 \({}^{\circ}\) & n.d. & 0.79 \(\pm\) 0.04 \({}^{\circ}\) & n.d. \\ \hline \(\Sigma\) Others & 7.58 \(\pm\) 0.39 & 6.52 \(\pm\) 0.02 \({}^{\circ}\) & 8.23 \(\pm\) 0.07 \({}^{\circ}\) & 9.30 \(\pm\) 0.09 \({}^{\circ}\) & 9.18 \(\pm\) 0.04 \({}^{\circ}\) & 9.38 \(\pm\) 0.07 \({}^{\circ}\) & 9.24 \(\pm\) 0.14 \({}^{\circ}\) & 10.66 \(\pm\) 0.10 \({}^{\circ}\) & 10.77 \(\pm\) 0.03 \({}^{\circ}\) \\ \hline Acetic acid & 7.11 \(\pm\) 0.34 & 5.26 \(\pm\) 0.04 \({}^{\circ}\) & 6.98 \(\pm\) 0.25 \({}^{\circ}\) & 8.24 \(\pm\) 0.31 \({}^{\circ}\) & 8.50 \(\pm\) 0.08 \({}^{\circ}\) & 8.73 \(\pm\) 0.20 \({}^{\circ}\) & 8.87 \(\pm\) 0.46 \({}^{\circ}\) & 10.11 \(\pm\) 0.35 \({}^{\circ}\) & 10.27 \(\pm\) 0.05 \({}^{\circ}\) \\ \hline Maltol & 0.43 \(\pm\) 0.07 & 1.21 \(\pm\) 0.02 \({}^{\circ}\) & 1.21 \(\pm\) 0.01 \({}^{\circ}\) & 0.99 \(\pm\) 0.01 \({}^{\circ}\) & 0.63 \(\pm\) 0.01 \({}^{\circ}\) & 0.61 \(\pm\) 0.02 \({}^{\circ}\) & 0.32 \(\pm\) 0.06 \({}^{\circ}\) & 0.50 \(\pm\) 0.02 \({}^{\circ}\) & 0.44 \(\pm\) 0.05 \({}^{\circ}\) \\ \hline
3,4-Dimethoxystyrene & 0.04 \(\pm\) 0.05 & 0.05 \(\pm\) 0.03 \({}^{\circ}\) & 0.04 \(\pm\) 0.02 \({}^{\circ}\) & 0.07 \(\pm\) 0.03 \({}^{\circ}\) & 0.05 \(\pm\) 0.01 \({}^{\circ}\) & 0.04 \(\pm\) 0.03 \({}^{\circ}\) & 0.05 \(\pm\) 0.01 \({}^{\circ}\) & 0.