## 3 Results and Discussion
### Evaluation of Volatile Compounds during the Processing of Smoked Dry-Cured Ham
\begin{table}
\begin{tabular}{c c c c c c c c c c} \hline
**Volatile Compounds** & **RI** & **Muscle** & **Raw Ham** & **After Salting** & **After Smoking** & **After Drying** & **After Ripening** & **Identification** \\ \hline \hline Aldehydes & & & & & & & & & & \\
3-Methylbutanal & 645 & BF & 0.30 \(\pm\) 0.06\({}^{\rm h,2}\) & 0.00 \(\pm\) 0.00\({}^{\rm a}\) & 0.03 \(\pm\) 0.00\({}^{\rm a}\) & 0.07 \(\pm\) 0.01 \({}^{\rm a}\) & 0.42 \(\pm\) 0.10\({}^{\rm h,2}\) & MS, RI \\  & & SM & 0.00 \(\pm\) 0.00\({}^{\rm a,1}\) & 0.00 \(\pm\) 0.00\({}^{\rm a}\) & 0.04 \(\pm\) 0.02\({}^{\rm a,b}\) & 0.08 \(\pm\) 0.02\({}^{\rm h}\) & 0.13 \(\pm\) 0.01\({}^{\rm c,1}\) & MS, RI \\
2-Methylbutanal & 654 & BF & 0.96 \(\pm\) 0.20\({}^{\rm h,2}\) & 0.00 \(\pm\) 0.00\({}^{\rm a}\) & 0.07 \(\pm\) 0.01 \({}^{\rm a}\) & 0.14 \(\pm\) 0.02\({}^{\rm a}\) & 0.30 \(\pm\) 0.08\({}^{\rm a,2}\) & MS, RI \\  & SM & 0.20 \(\pm\) 0.12\({}^{\rm h}\) & 0.04 \(\pm\) 0.03 & 0.05 \(\pm\) 0.00 & 0.09 \(\pm\) 0.05 & 0.10 \(\pm\) 0.01\({}^{\rm a}\) & MS, RI \\  & 657 & BF & 0.52 \(\pm\) 0.16\({}^{\rm h}\) & 0.33 \(\pm\) 0.08\({}^{\rm h}\) & 0.19 \(\pm\) 0.02\({}^{\rm h}\) & 0.30 \(\pm\) 0.05\({}^{\rm h}\) & 0.00 \(\pm\) 0.00\({}^{\rm a}\) & MS, RI \\  & & SM & 0.62 \(\pm\) 0.13\({}^{\rm h}\) & 0.29 \(\pm\) 0.05\({}^{\rm h}\) & 0.16 \(\pm\) 0.02\({}^{\rm h}\) & 0.24 \(\pm\) 0.2\({}^{\rm h}\) & 0.00 \(\pm\) 0.00\({}^{\rm a}\) & MS, RI \\  & 713 & BF & 1.88 \(\pm\) 0.35\({}^{\rm h}\) & 2.57 \(\pm\) 0.48\({}^{\rm h}\) & 1.55 \(\pm\) 0.14\({}^{\rm h}\) & 1.49 \(\pm\) 0.10\({}^{\rm h}\) & 0.89 \(\pm\) 0.16\({}^{\rm h}\) & MS, RI \\  & & SM & 1.23 \(\pm\) 0.59\({}^{\rm h}\) & 1.98 \(\pm\) 0.22\({}^{\rm h}\) & 1.08 \(\pm\) 0.21\({}^{\rm h}\) & 2.07 \(\pm\) 0.4\({}^{\rm h}\) & 0.17 \(\pm\) 0.03\({}^{\rm a,1}\) & MS, RI \\  & 799 & BF & 447 \(\pm\) 3.18\({}^{\rm h}\) & 544 \(\pm\) 4.49\({}^{\rm h}\) & 4.30 \(\pm\) 0.36\({}^{\rm h}\) & 39.22 \(\pm\) 0.25\({}^{\rm h}\) & 0.109 \(\pm\) 0.04\({}^{\rm a,2}\) & MS, RI \\  & & SM & 48.85 \(\pm\) 3.16\({}^{\rm h}\) & 55.83 \(\pm\) 1.16\({}^{\rm h}\) & 4.37 \(\pm\) 1.40\({}^{\rm h}\) & 7.26 \(\pm\) 0.67\({}^{\rm h}\) & 1.62 \(\pm\) 0.07\({}^{\rm a,1}\) & MS, RI \\  & 903 & BF & 0.30 \(\pm\) 0.13\({}^{\rm h}\) & 1.08 \(\pm\) 0.14\({}^{  
\begin{table}
\begin{tabular}{c c c c c c c c c} \hline
**Volatile Compounds** & **RI** & **Muscle** & **Raw Ham** & **After Salting** & **After Smoking** & **After Drying** & **After Tipening** & **Identification** \\ \hline
1-Octanol & 1076 & BF & 7.62 \(\pm\) 0.82 b\({}^{2}\) & 1.26 \(\pm\) 0.10 a & 1.56 \(\pm\) 0.19 a\({}^{1.1}\) & 1.35 \(\pm\) 0.26 a & 2.88 \(\pm\) 0.42 a\({}^{2.2}\) & MS, RI \\  & SM & 4.94 \(\pm\) 0.26 c\({}^{1.1}\) & 1.42 \(\pm\) 0.11 a & 2.03 \(\pm\) 0.11 b\({}^{2.1}\) & 1.42 \(\pm\) 0.09 a & 1.01 \(\pm\) 0.07 a\({}^{1.1}\) & MS, RI \\ Phenylethyl alcohol & 1113 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.12 \(\pm\) 0.01 a & 0.11 \(\pm\) 0.01 a & 0.96 \(\pm\) 0.12 b\({}^{2.1}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.14 \(\pm\) 0.02 b & 0.11 \(\pm\) 0.01 a & 0.38 \(\pm\) 0.06 c\({}^{1.1}\) & MS, RI \\
1-Undecanol & 1174 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.09 \(\pm\) 0.02 b\({}^{1.1}\) & 0.07 \(\pm\) 0.00 b\({}^{1.1}\) & 0.00 \(\pm\) 0.00 a & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.18 \(\pm\) 0.02 b & 0.19 \(\pm\) 0.03 b\({}^{1.2}\) & 0.00 \(\pm\) 0.00 a & MS, RI \\
2-Cydebeen-1-ol & 1366 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.51 \(\pm\) 0.14 b & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.34 \(\pm\) 0.05 b & MS, RI \\  & & BF 19.97 \(\pm\) 1.62 b & 16.25 \(\pm\) 0.98 b & 16.13 \(\pm\) 0.06 b\({}^{2.0}\) & 14.91 \(\pm\) 0.53 b\({}^{2.5}\) & 1.595 \(\pm\) 0.90 b\({}^{2.0}\) & MS, RI \\  & & SM & 21.23 \(\pm\) 1.13 a & 16.42 \(\pm\) 0.71 a & 14.12 \(\pm\) 0.64 b\({}^{2.0}\) & 12.56 \(\pm\) 0.72 a\({}^{2.1}\) & 6.46 \(\pm\) 0.10 a\({}^{1.1}\) & MS, RI \\  & & & & & & & & \\
2-Methylphenol & 1061 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 2.07 \(\pm\) 0.36 b\({}^{1.1}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 4.58 \(\pm\) 0.26 b\({}^{1.2}\) & 6.05 \(\pm\) 0.23 c\({}^{1.2}\) & MS, RI \\
4-Methylphenol & 1080 & BF & 0.00 \(\pm\) 0.00 a & 0.64 \(\pm\) 0.11 a & 0.87 \(\pm\) 0.17 a & 0.83 \(\pm\) 0.09 a & 5.13 \(\pm\) 0.54 b\({}^{1.1}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.30 \(\pm\) 0.04 b\({}^{1.2}\) & 1.25 \(\pm\) 0.15 b\({}^{1.5}\) & 5.87 \(\pm\) 0.57 a\({}^{2.2}\) & 7.22 \(\pm\) 0.24 c\({}^{2.2}\) & MS, RI \\
2-Metchoxyphenylend & 1090 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.98 \(\pm\) 0.12 a\({}^{3.1}\) & 2.08 \(\pm\) 0.09 b\({}^{1.1}\) & 9.32 \(\pm\) 0.08 c\({}^{1.2}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.82 b\({}^{2.2}\) b\({}^{2.1}\) & 8.25 \(\pm\) 0.11 b\({}^{1.2}\) & 10.08 \(\pm\) 0.12 c\({}^{1.2}\) & MS, RI \\
4-Metchoxyphenylend & 1098 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.38 \(\pm\) 0.03 b\({}^{1.3}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.04 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.38 \(\pm\) 0.03 b & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.04 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.03 b & 0.42 \(\pm\) 0.02 b & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.18 \(\pm\) 0.02 b\({}^{1.1}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.33 \(\pm\) 0.07 b\({}^{1.2}\) & 0.68 \(\pm\) 0.04 c\({}^{2.2}\) & MS, RI \\  & & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.33 \(\pm\) 0.06 b\({}^{1.1}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 2.85 \(\pm\) 0.20 b\({}^{1.2}\) & MS, RI \\  & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 2.85 \(\pm\) 0.20 b\({}^{1.2}\) & MS, RI \\  & & SM & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & MS, RI \\
3-Ethylphenol & 1169 & BF & 0.00 \(\pm\) 0.00 a & 0.00 \(\pm\) 0.00 a & 0.