## 2 Results and Discussion
### The Chemical Composition of the Content of Honey-Sac Headspace, Volatiles and Semi-Volatiles
\begin{table}
\begin{tabular}{c c c c c c c c c c c} \hline \hline \multirow{2}{*}{**No.**} & \multirow{2}{*}{**Compound**} & \multirow{2}{*}{**RI**} & \multicolumn{3}{c}{**Area (%) USE (Pentane/El\_0 12 (\(\
u\)/\(\
u\)))**} & \multicolumn{3}{c}{**Area (%) USE (CH\({}_{4}\)Cl\({}_{4}\))**} \\ \cline{3-10}  & & & **Min.** & **Max.** & **Av.** & **SD.** & **Min.** & **Max.** & **Av.** & **SD.** \\ \hline
1 & Ethylbenzene & \textless{}900 & 0.1 & 0.8 & 0.24 & 0.31 & 0.0 & 0.1 & 0.03 & 0.05 \\
2 & 1,3-Dimethylbenzene ** & \textless{}900 & 0.2 & 3.1 & 0.88 & 1.25 & 0.0 & 0.1 & 0.03 & 0.05 \\
3 & 1,4-Dimethylbenzene ** & \textless{}900 & 0.1 & 0.8 & 0.34 & 0.34 & 0.0 & 0.1 & 0.03 & 0.05 \\
4 & Benzyl alcohol & 1038 & 0.1 & 0.6 & 0.22 & 0.22 & 0.0 & 0.1 & 0.05 & 0.06 \\
5 & Phenycatechhyde & 1048 & 0.0 & 1.2 & 0.38 & 0.48 & 0.0 & 0.5 & 0.20 & 0.24 \\
6 & 2-Phenycethanol & 1118 & 0.0 & 0.3 & 0.12 & 0.11 & 0.0 & 0.1 & 0.05 & 0.06 \\
7 & Benzoic acid & 1166 & 0.1 & 0.3 & 0.14 & 0.09 & 0.0 & 0.2 & 0.08 & 0.10 \\
8 & Decanal & 1207 & 0.0 & 0.1 & 0.02 & 0.04 & 0.0 & 0.0 & 0.00 & 0.00 \\
9 & 2,3-Dihydrobenzofuran & 1222 & 0.0 & 0.0 & 0.00 & 0.00 & 0.0 & 0.1 & 0.05 & 0.06 \\
10 & Phenyclectic acid & 1262 & 0.1 & 0.3 & 0.18 & 0.08 & 0.1 & 0.2 & 0.15 & 0.06 \\
11 & 1-H-Indole & 1295 & 0.1 & 0.3 & 0.14 & 0.09 & 0.1 & 2.6 & 0.90 & 1.16 \\
12 & 1-Hydroxylinol ** & 1366 & 0.5 & 6.5 & 2.16 & 2.58 & 0.2 & 2.0 & 1.25 & 0.79 \\
13 & 4-Hydrox-2-phenylphenylethanol & 1425 & 0.1 & 0.3 & 0.20 & 0.07 & 0.0 & 0.5 & 0.25 & 0.29 \\
14 & 1,3-Dihydro-2-\(H\)-indol-2-one & 1471 & 0.2 & 1.7 & 0.74 & 0.60 & 0.1 & 1.3 & 0.53 & 0.57 \\
15 & Tetadecan-1-ol & 1676 & 0.5 & 1.3 & 0.72 & 0.33 & 0.0 & 0.4 & 0.10 & 0.20 \\
16 & 1-H-indole-2-3-dione * & 1698 & 0.0 & 0.1 & 0.02 & 0.04 & 0.0 & 0.9 & 0.45 & 0.37 \\
17 & Hepatocellular & 1700 & 0.0 & 1.0 & 0.30 & 0.42 & 0.0 & 0.0 & 0.0 & 0.00 \\
18 & Methyl syringae & 1744 & 0.0 & 0.4 & 0.10 & 0.17 & 0.0 & 1.3 & 0.33 & 0.65 \\
19 & 4-Hydrox-3,5,6-trimethyl-4(3-oxo-1-b)utenyl & 1796 & 0.2 & 2.0 & 0.84 & 0.81 & 0.2 & 2.4 & 1.53 & 1.04 \\ cyclohex-2-en-neo (Vomifoliol) & Octadecan & 1800 & 0.0 & 0.1 & 0.04 & 0.05 & 0.0 & 0.5 & 0.13 & 0.25 \\
20 & 21 & Caffe & 0.3 & 0.8 & 0.56 & 0.21 & 1.2 & 7.1 & 3.15 & 2.71 \\
22 & 4-(1-Methyl-1-phenylethyl)phenol & 1858 & 0.0 & 0.0 & 0.00 & 0.00 & 0.0 & 0.2 & 0.05 & 0.10 \\
23 & Hexadecan-1-ol & 1882 & 5.8 & 15.3 & 10.14 & 3.51 & 2.4 & 5.4 & 3.38 & 1.38 \\
24 & Nonadecane & 1900 & 0.0 & 1.3 & 0.26 & 0.58 & 0.0 & 0.0 & 0.00 & 0.00 \\
25 & Hexadecan acid & 1963 & 0.5 & 6.6 & 4.02 & 2.88 & 7.3 & 33.8 & 14.90 & 12.71 \\
26 & Methyl 11-indole-3-acetate & 1980 & 0.0 & 0.2 & 0.04 & 0.09 & 0.0 & 5.6 & 1.95 & 2.62 \\
27 & 27 & Hexosine & 2000 & 0.0 & 0.4 & 0.12 & 0.18 & 0.1 & 0.9 & 0.45 & 0.37 \\
28 & 2,3-Dihydro-5,7-dihydroxy-2-one & 2010 & 0.0 & 0.0 & 0.00 & 0.00 & 1.0 & 19.6 & 8.48 & 8.22 \\
29 & (2)-Octadec-9-en-1-ol & 2059 & 20.5 & 49.1 & 36.54 & 10.88 & 11.8 & 22.8 & 18.73 & 5.18 \\
30 & Octadecan-1-ol & 2084 & 4.5 & 11.4 & 7.70 & 2.97 & 3.8 & 5.4 & 4.80 & 0.70 \\
31 & Pheniconsane & 2100 & 0.0 & 3.7 & 0.78 & 1.63 & 0.0 & 3.0 & 0.75 & 1.50 \\
32 & (2)-Octadec-9-enoic acid & 2142 & 0.0 & 0.0 & 0.00 & 0.00 & 0.0 & 15.7 & 5.65 & 7.26 \\
33 & Decouse & 2200 & 0.2 & 15.7 & 7.34 & 7.73 & 0.0 & 8.5 & 3.30 & 3.76 \\
34 & (2)-Tricos-9-ene & 2264 & 0.0 & 1.6 & 0.50 & 0.73 & 0.0 & 2.3 & 0.58 & 1.15 \\
35 & Titosane & 2300 & 0.3 & 26.4 & 7.54 & 10.93 & 1.5 & 8.9 & 3.80 & 3.43 \\
36 & Tetecrossane & 2400 & 1.1 & 20.8 & 9.50 & 8.38 & 0.1 & 29.7 & 16.05 & 12.75 \\ \hline \hline \end{tabular}
\end{table} 
Table 4: The results of GC-FID and GC-MS analysis of C. _unshitu_ honey (\(n=12\)) ultrasonic solvent extracts. \begin{table}
\begin{tabular}{c c c c c c c c c} \hline \hline \multirow{2}{*}{**No. **} & \multirow{2}{*}{**Compound**} & \multirow{2}{*}{**RI**} & \multicolumn{3}{c}{**Area (%) Fibre PDMS/DVB**} & \multicolumn{3}{c}{**Area (%) Fibre DVB/CAR/PDMS**} \\ \cline{3-10}  & & & **Min. ** & **Max. ** & **Av. ** & **SD. ** & **Min. ** & **Max. ** & **Av. ** & **SD.