## 3 Results
### Volatile Organic Compounds
\begin{table}
\begin{tabular}{c c c c c c c c c c} \hline \hline \multicolumn{1}{c}{} & \multicolumn{6}{c}{**25 \({}^{\circ}\)C**} & \multicolumn{6}{c}{**40 \({}^{\circ}\)C**} \\ \hline  & **Time 0** & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} \\ \hline
**Compound** & & **STD** & **ALT** & **STD** & **ALT** & **STD** & **ALT** & **STD** & **ALT** & **STD** & **ALT** \\ \hline
5-methyl-Fururral & 1.35 \(\pm\) 0.28 & 1.62 \(\pm\) 0.02\({}^{\rm a}\) & 1.78 \(\pm\) 0.08\({}^{\rm a}\) & 1.8  
\begin{table}
\begin{tabular}{c c c c c c c c c c} \hline \hline  & \multicolumn{4}{c}{**25 \({}^{\circ}\)C**} & \multicolumn{4}{c}{**40 \({}^{\circ}\)C**} \\ \hline  & \multicolumn{2}{c}{**Time 0**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} & \multicolumn{2}{c}{**90 Days**} & \multicolumn{2}{c}{**180 Days**} \\ \hline
**Compound** & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} & \multicolumn{2}{c}{**STD**} & \multicolumn{2}{c}{**ALT**} \\ \hline Acetone & 1.04 \(\pm\) 0.14 & 0.98 \(\pm\) 0.04 \({}^{\circ}\) & 0.96 \(\pm\) 0.03 \({}^{\circ}\) & 1.06 \(\pm\) 0.05 \({}^{\circ}\) & 0.99 \(\pm\) 0.16 \({}^{\circ}\) & 0.78 \(\pm\) 0.03 \({}^{\circ}\) & 1.09 \(\pm\) 0.09 \({}^{\circ}\) \({}^{\circ}\) & 1.06 \(\pm\) 0.05 \({}^{\circ}\) & 0.73 \(\pm\) 0.04 \({}^{\circ}\) \({}^{\circ}\) \\ \hline
3-Hydroxy-2-butanone & 0.47 \(\pm\) 0.13 & 0.63 \(\pm\) 0.05 \({}^{\circ}\) & 0.60 \(\pm\) 0.02 \({}^{\circ}\) & 0.46 \(\pm\) 0.02 \({}^{\circ}\) & 0.69 \(\pm\) 0.05 \({}^{\circ}\) & 0.32 \(\pm\) 0.03 \({}^{\circ}\) & 0.37 \(\pm\) 0.02 \({}^{\circ}\) & 0.46 \(\pm\) 0.02 \({}^{\circ}\) \({}^{\circ}\) & 0.19 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline
2-Hydroxy-3-methyl-2- & 0.40 \(\pm\) 0.01 & 0.61 \(\pm\) 0.05 \({}^{\circ}\) & 0.57 \(\pm\) 0.03 \({}^{\circ}\) & 0.47 \(\pm\) 0.03 \({}^{\circ}\) & 0.54 \(\pm\) 0.03 \({}^{\circ}\) & 0.38 \(\pm\) 0.02 \({}^{\circ}\) & 0.38 \(\pm\) 0.01 \({}^{\circ}\) & 0.47 \(\pm\) 0.03 \({}^{\circ}\) & 0.26 \(\pm\) 0.02 \({}^{\circ}\) \({}^{\circ}\) \\ \hline
3-Ethyl-2-hydroxy-2- & 0.19 \(\pm\) 0.01 & 0.38 \(\pm\) 0.01 \({}^{\circ}\) & 0.35 \(\pm\) 0.02 \({}^{\circ}\) & 0.30 \(\pm\) 0.01 \({}^{\circ}\) & 0.24 \(\pm\) 0.01 \({}^{\circ}\) & n.d. & 0.20 \(\pm\) 0.04 \({}^{\circ}\) & 0.30 \(\pm\) 0.01 \({}^{\circ}\) & 0.20 \(\pm\) 0.02 \({}^{\circ}\) \\ cyclopentometone & & & & & & & & & \\ \hline \(\Sigma\) Phenols & 5.46 \(\pm\) 1.68 & 8.03 \(\pm\) 0.07 \({}^{\circ}\) & 7.71 \(\pm\) 0.02 \({}^{\circ}\) & 8.27 \(\pm\) 0.05 \({}^{\circ}\) & 7.29 \(\pm\) 0.04 \({}^{\circ}\) & 4.52 \(\pm\) 0.02 \({}^{\circ}\) & 4.01 \(\pm\) 0.03 \({}^{\circ}\) & 8.27 \(\pm\) 0.05 \({}^{\circ}\) \({}^{\circ}\) & 3.83 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline Gaisacol & 2.28 \(\pm\) 0.05 & 2.62 \(\pm\) 0.12 \({}^{\circ}\) & 2.54 \(\pm\) 0.02 \({}^{\circ}\) & 2.16 \({}^{\circ}\) & 2.21 \(\pm\) 0.06 \({}^{\circ}\) & 1.91 \(\pm\) 0.03 \({}^{\circ}\) & 1.97 \(\pm\) 0.06 \({}^{\circ}\) & 2.16 \(\pm\) 0.06 \({}^{\circ}\) & 1.88 \(\pm\) 0.02 \({}^{\circ}\) \\ \hline
4-Vinylphenol & 1.47 \(\pm\) 0.03 & 2.89 \(\pm\) 0.07 \({}^{\circ}\) & 2.86 \(\pm\) 0.02 \({}^{\circ}\) & 3.90 \(\pm\) 0.02 \({}^{\circ}\) & 3.40 \(\pm\) 0.06 \({}^{\circ}\) & 0.76 \(\pm\) 0.02 \({}^{\circ}\) & 0.47 \(\pm\) 0.03 \({}^{\circ}\) & 3.90 \(\pm\) 0.02 \({}^{\circ}\) & 0.59 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline
4-ethyl-2-methoxyphenol & 0.95 \(\pm\) 0.21 & 1.91 \(\pm\) 0.05 \({}^{\circ}\) & 1.69 \(\pm\) 0.01 \({}^{\circ}\) & 1.87 \(\pm\) 0.07 \({}^{\circ}\) & 1.20 \(\pm\) 0.03 \({}^{\circ}\) & 1.50 \(\pm\) 0.04 \({}^{\circ}\) & 1.05 \(\pm\) 0.01 \({}^{\circ}\) & 1.87 \(\pm\) 0.07 \({}^{\circ}\) & 0.83 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline Phenol & 0.77 \(\pm\) 0.19 & 0.61 \(\pm\) 0.06 \({}^{\circ}\) & 0.62 \(\pm\) 0.02 \({}^{\circ}\) & 0.34 \(\pm\) 0.03 \({}^{\circ}\) & 0.48 \(\pm\) 0.02 \({}^{\circ}\) & 0.35 \(\pm\) 0.01 \({}^{\circ}\) & 0.52 \(\pm\) 0.01 \({}^{\circ}\) & 0.34 \(\pm\) 0.03 \({}^{\circ}\) & 0.53 \(\pm\) 0.01 \({}^{\circ}\) \\ \hline \(\Sigma\) Pyroles & 3.13 \(\pm\) 0.16 & 3.17 \(\pm\) 0.02 \({}^{\circ}\) & 2.71 \(\pm\) 0.02 \({}^{\circ}\) & 3.05 \(\pm\) 0.04 \({}^{\circ}\) & 2.96 \(\pm\) 0.04 \({}^{\circ}\) & 3.18 \(\pm\) 0.02 \({}^{\circ}\) & 3.06 \(\pm\) 0.02 \({}^{\circ}\) & 3.05 \(\pm\) 0.04 \({}^{\circ}\) \({}^{\circ}\) & 3.23 \(\pm\) 0.