## 1 Introduction  
As broad-spectrum systemic insecticides, neonicotinoid insecticides have been authorized for use and operation on hundreds of farmland plants in more than 120 countries with the fastest-growing speed worldwide [1, 2]. These pesticides are used to control aphids and other sap-sucking insects that can easily cause behavioral problems [3]. They selectively act on the nicotinic acetylcholine receptors of insects and cause the overexcitement of acetylcholine receptors. Neonicotinoids are nicotinic acetylcholine receptor agonists. They bind tightly to acetylcholine receptors in the central nervous system of insects, causing death at higher levels [4]. Neonicotinoids can penetrate into plant tissues and protect the entire crop. These neonicotinoids are also widely used in seed dressing [5]. However, recent studies have shown that these pesticides can cause a decline in pollen-transmitting organisms (e.g., the colony collapse of bees) and threaten human health [6]. Therefore, the use of neonicotinoids in the environment has been controlled by authorities to prevent the extinction of beneficial insects and guarantee human health [7]. The maximum residue limit (MRL) (50-200 \(\mu\)g/kg) of these substances in honey has been set up by the European Union and other international authorities [8]. In China, the detection of pesticide residues in honey usually follows the national standard GB23200.7-2016 [9]. Similar to this standard, other methods also involve careful sample preparation procedures, including analyte enrichment and cleanup of the extract [10]. A simple and fast method for the multiresidue detection of pesticides in honey with low cost and reusable materials is always preferable. This is also the goal of our study. Many studies reported the residue of neonicotinoids in surface waters and honey [1; 5]. Previous literature has reported possible pharmaceutical and personal-care residues in bottled water [11; 12; 13]. The surface water is often contaminated by the use of pesticides in agricultural activities. As most of the bottled water is produced from the surface water, it probably contains these contaminants if the processing step is not performed well. Therefore, pesticide residue in bottled water produced from surface water and in honey products needs to be examined. Solid-phase extraction (SPE) [14; 15] and liquid-liquid extraction (LLE) [16; 17] coupled with liquid chromatography (LC) [18; 19; 20], gas chromatography-mass spectrometry (GC-MS) [21], and liquid chromatography-tandem mass spectrometry (LC-MS/MS) [22; 23] are frequently used to detect the residues of neonicotinoid insecticides in food, e.g., fruit, honey, milk, and vegetables. The SPE procedure includes conditioning, sample loading, rinsing, and elution, and the LLE procedures involve a large volume of organic solvents and often have low processing efficiency. Both of these methods are time-consuming and laborious. Dispersive solid-phase extraction (DSPE) is a part of the QuEChERS (quick, easy, cheap, effective, rugged and safe) procedure proposed by [PERSON] et al. in 2003 [24]. DSPE can also be independently used in sample extraction and cleanup, and it has been widely applied due to its simple procedure and low cost [25; 26]. A large number of sorbents have been commercialized for testing in water or food [27; 28], and there is still a demand for high-efficiency and low-cost sorbents. The research is challenging not only for adsorption but also for separation technology. Zeolites, including natural minerals (such as natrolite, scolecite, clinoptilolite) and synthetic zeolites (such as A, X, ZSM-5, Beta), have been widely used as desiccants, catalysts, and soil amendments [29; 30]. Its open frame is filled with crystalline aluminosilicate, which contains silica and alumina tetrahedrons connected by oxygen bridges [31; 32].