## 3 Results
\begin{table}
\begin{tabular}{c c c c c c c c c c} \hline \multicolumn{6}{c}{**Freezing WSL + F WSL + BZT**} & \multicolumn{6}{c}{**Thawing WSL + F WSL + BZT**} \\ \hline  & **DOC** & **Na** & **Al** & **Fe** & & **DOC** & **Na** & **Al** & **Fe** \\ \hline DOC & \(1\) & \(-\)0.0584 & 0.9752 * & 0.9537 * & DOC & \(1\) & 0.1815 & 0.9320 * & 0.9695 * \\ Li & 0.2841 & 0.6957 & 0.4028 & 0.4249 & Li & 0.9149 * & 0.3597 & 0.9141 * & 0.9396 * \\ B & 0.0137 & 0.9399 * & 0.0984 & 0.1099 & B & 0.2050 & 0.9889 * & 0.1702 & 0.2581 \\ Na & \(-\)0.0584 & \(1\) & 0.0585 & 0.0556 & Na & \(-\)0.4262 & \(1\) & 0.1483 & 0.2255 \\ Mg & 0.2708 & 0.7249 * & 0.3661 & 0.3465 & Mg & 0.6507 & 0.5771 & 0.6468 & 0.6935 \\ Al & 0.9752 * & 0.0585 & \(1\) & 0.9714 * & Al & 0.9320 * & 0.1483 & \(1\) & 0.9684 * \\ Si & 0.9433 * & 0.0777 & 0.9784 * & 0.9533 * & Si & 0.9032 * & 0.2209 & 0.9686 * & 0.9516 * \\ P & 0.8843 * & 0.2769 & 0.9342 * & 0.9110 * & P & 0.9797 * & 0.1920 & 0.9584 * & 0.9802 * \\ K & 0.8286 * & 0.0625 & 0.8723 * & 0.8240 * & K & 0.8810 * & 0.1027 & 0.9076 * & 0.8650 * \\ Ca & 0.2949 & 0.7511 * & 0.3536 & 0.4123 & Ca & 0.6472 & 0.7605 * & 0.6221 & 0.6901 \\ Ti & 0.9329 * & 0.1386 & 0.9767 * & 0.9448 * & Ti & 0.9463 * & 0.3545 & 0.8872 * & 0.9503 * \\ V & \(-\)0.0965 & \(-\)0.0566 & \(-\)0.1673 & 0.0424 & V & 0.2062 & \(-\)0.0739 & 0.2954 & 0.3317 \\ Cr & 0.7382 * & \(-\)0.0688 & 0.7430 * & 0.6332 & Cr & 0.8028 * & 0.5378 & 0.7283 * & 0.7761 * \\ Mn & \(-\)0.3950 & \(-\)0.2971 & \(-\)0.4310 & \(-\)0.3443 & Mn & \(-\)0.4973 & \(-\)0.2645 & \(-\)0.3969 & \(-\)0.4086 * \\ Fe & 0.9537 * & 0.0556 & 0.9714 * & 1 Fe & 0.9695 * & 0.2254 & 0.9684 * & \\ Co & 0.5802 & 0.2920 & 0.6675 & 0.6908 & Co & 0.8884 * & 0.1750 & 0.9240 * & 0.9248 * \\ Ni & 0.7402 * & \(-\)0.1376 & 0.7681 * & 0.7031 * & Ni & 0.9220 * & 0.2549 & 0.9012 * & 0.9375 * \\ Cu & 0.9422 * & 0.0668 & 0.9787 * & 0.9200 * & Cu & 0.9824 * & 0.2509 & 0.9490 * & 0.9864 * \\ Zn & 0.3588 & 0.3950 & 0.3647 & 0.3455 & Zn & 0.2217 & 0.8124 * & 0.1310 & 0.2148 * \\ Ga & 0.9447 * & \(-\)0.0082 & 0.9617 * & 0.8982 * & Ga & 0.8970 * & 0.1903 & 0.9884 * & 0.9363 * \\ As & 0.7844 * & \(-\)0.0093 & 0.7550 * & 0.8698 * & As & 0.9210 * & 0.2233 & 0.9128 * & 0.9598 * \\ Rb & 0.7832 * & \(-\)0.1507 & 0.8052 * & 0.7907 * & Rb & 0.7769 * & \(-\)0.1060 & 0.9331 * & 0.8367 * \\ Sr & \(-\)0.1877 & 0.5511 & \(-\)0.1361 & \(-\)0.0676 & Sr & \(-\)0.0097 & \(-\)0.1975 & \(-\)0.0006 & \(-\)0.0264 * \\ Y & 0.8549 * & 0.0521 & 0.8609 * & 0.8934 * & Y & 0.9522 * & 0.3111 & 0.9301 * & 0.9605 * \\ Zr & 0.8053 * & 0.0260 & 0.8602 * & 0.7922 * & Zr & 0.9661 * & 0.2834 & 0.9565 * & 0.9804 * \\ Nb & 0.9546 * & 0.1243 & 0.9925 * & 0.9635 * & Nb & 0.9577 * & 0.3725 & 0.8911 * & 0.9628 * \\ Mo & \(-\)0.5612 & 0.2892 & \(-\)0.4798 & \(-\)0.5046 & Mo & \(-\)0.4110 & \(-\)0.2568 & \(-\)0.3710 & \(-\)0.4251 \\ Cd & \(-\)0.3985 & \(-\)0.1202 & \(-\)0.3732 & \(-\)0.3835 & Cd & \(-\)0.5188 & \(-\)0.3213 & \(-\)0.4304 & \(-\)0.4827 * \\ Sb & \(-\)0.5286 & 0.1542 & \(-\)0.4595 & \(-\)0.4747 & Sb & \(-\)0.3971 & \(-\)0.2852 & \(-\)0.3401 & \(-\)0.3979 * \\ Cs & 0.6519 & \(-\)0.1790 & 0.6329 & 0.6351 & Cs & 0.6829 & \(-\)0.0942 & 0.8846 * & 0.7569 * \\ Ba & 0.4225 & \(-\)0.1811 & 0.4279 & 0.4552 & Ba & 0.7095 * & \(-\)0.0895 & 0.7918 * & 0.7180 * \\ La & 0.6586 & \(-\)0.0468 & 0.6731 & 0.6531 & La & 0.9526 * & 0.1168 & 0.9755 * & 0.9722 * \\ Ce & 0.6706 & \(-\)0.0138 & 0.6699 & 0.6963 & Ce & 0.9631 * & 0.1622 & 0.9812 * & 0.9906 * \\ Nd & 0.9474 * & 0.0619 & 0.9602 * & 0.9655 * & Nd & 0.9643 * & 0.2661 & 0.9659 * & 0.9818 * \\ Hf & 0.7619 * & 0.0501 & 0.8238 * & 0.7434 * & Hf & 0.9608 * & 0.3444 & 0.9306 * & 0.9613 * \\ Pb & 0.9462 * & 0.0543 & 0.9799 * &