It is not normally necessary to make nickel in the laboratory as it is available readily commercially. Small amounts of pure nickel can be islated in the laborotory through the purification of crude nickel with carbon monoxide. 4 is a volatile complex which is easily flushed from the reaction vessel as a gas leaving the impurities behind. Industrially, the Mond process uses the same chemistry. Reduction of the oxide with the hydrogen results in impure nickel.
Thermal decomposition leaves pure nickel metal.
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