Thus to insert the Fsquare reflection data, select X-ray Data, Reflection Data to import the HKL Intensity file. However, If the connectivity was not as it should be, this would be a good time to relabel the atoms if you know the connectivity. To zoom in or out of the structure. Select Refinement, Guided Automatic to start the refinement. Crystals will do a few cycles of refinement, then the Supervisor Dialog will then come up to guide you through the refinement.
Crystals recommends going straight to adding hydrogens.
Crystals now recommends that you continue on with anisotropic refinement but before doing this, it would be best to check out the thermals and other nuances in the Cameron Structure Viewing program as blown up thermals may reveal spurious peaks that were assigned as atoms. Close the Guided Refinement dialog and select Cameron from the top menu. Selecting Ellipses shows that things do look OK here at the moment. Exit Cameron using File, Exit Cameron . Crystals will prompt whether you wish to apply the changes performed by Cameron.