Document ID: EPA-HQ-OW-2003-0003-0011
Agency: epa
Document Type: Supporting & Related Material
Title: 
Posted Date: 2003-03-12T05:00Z

Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.00
10.00
1.00
0.10
0.01
10^­
4
100.0
10.0
1.0
0.1
10^­
4
100.0
10.0
1.0
0.1
10^­
4
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
GHI)
PERYLENE,
NG/
ULBENZO(
UL
100.0
10.0
1.0
0.1
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
Organics,
Method
1625:
T=
0Organics,
0
BIPHENYL,
NG/
ULBIPHENYL,
UL
100.00
10.00
1.00
0.10
0.01
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
CHLOROISOPROPYL)
ETHER,
NG/
ULBIS(
UL
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
Organics,
Method
1625:
T=
0Organics,
0
CARBAZOLE,
NG/
ULCARBAZOLE,
UL
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
100.00
10.00
1.00
0.10
0.01
0.50
5.00
50.00
10^­
4
100.00
10.00
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
CHLOROETHOXY)
METHANE,
NG/
ULBIS(
UL
1.00
0.10
0.01
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
ETHYLHEXYL)
PHTHALATE,
NG/
ULBIS(
UL
100.0
10.0
1.0
0.1
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
Organics,
Method
1625:
T=
0Organics,
0
CHRYSENE,
NG/
ULCHRYSENE,
UL
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.50
5.00
50.00
0.05
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
K)
FLUORANTHENE,
NG/
ULBENZO(
UL
Page
21
of
32
Organics,
Method
1625:
T=
0Organics,
0
BETA­
NAPHTHYLAMINE,
NG/
ULBETA­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
CHLOROETHYL)
ETHER,
NG/
ULBIS(
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
BUTYL
BENZYL
PHTHALATE,
NG/
ULBUTYL
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
DI­
N­
BUTYL
PHTHALATE,
NG/
ULDI­
UL
0.50
5.00
50.00
Log­
10
of
Measured
Concentration
Mon
Mar
18
16:
44:
28
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
DI­
N­
OCTYL
PHTHALATE,
NG/
ULDI­
UL
100.0
10.0
1.0
0.1
Organics,
Method
1625:
T=
0Organics,
0
DIBENZOFURAN,
NG/
ULDIBENZOFURAN,
UL
0.05
0.50
5.00
50.00
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
DIMETHYL
PHTHALATE,
NG/
ULDIMETHYL
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
FLUORANTHENE,
NG/
ULFLUORANTHENE,
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Mon
Mar
18
16:
44:
43
2002
100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
DI­
N­
PROPYLNITROSAMINE,
NG/
ULDI­
UL
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
DIBENZOTHIOPHENE,
NG/
ULDIBENZOTHIOPHENE,
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
DIPHENYL
ETHER,
NG/
ULDIPHENYL
UL
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
FLUORENE,
NG/
ULFLUORENE,
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Log­
10
of
Spike
Concentration
100.0
10.0
1.0
0.1
0.05
100.0
10.0
1.0
0.1
10^­
4
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
10.00
1.00
0.10
0.01
Page
22
of
32
Organics,
Method
1625:
T=
0Organics,
0
DIBENZO(
A,
H)
ANTHRACENE,
NG/
ULDIBENZO(
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
DIETHYL
PHTHALATE,
NG/
ULDIETHYL
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
DIPHENYLAMINE,
NG/
ULDIPHENYLAMINE,
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROBENZENE,
NG/
ULHEXACHLOROBENZENE,
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­
10
of
Measured
Concentration
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROBUTADIENE,
NG/
ULHEXACHLOROBUTADIENE,
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
INDENO(
1,2,3­
CD)
PYRENE,
NG/
ULINDENO(
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
N­
DOCOSANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
HEXACOSANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROCYCLOPENTADIENE,
NG/
ULHEXACHLOROCYCLOPENTADIENE,
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
ISOPHORONE,
NG/
ULISOPHORONE,
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
N­
DODECANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
HEXADECANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Page
23
of
32
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROETHANE,
NG/
ULHEXACHLOROETHANE,
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
DECANE,
NG/
ULN­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
N­
EICOSANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
NITROSODIMETHYLAMINE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
c:/
pw/
ostmdl/
req004/
r004sd1.
s
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
10.00
1.00
0.10
0.01
10^­
4
100.0
10.0
1.0
0.1
100.0
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
10.00
1.00
0.10
0.01
10.0
1.0
0.1
10^­
4
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
10.00
1.00
0.10
0.01
Log­
10
of
Measured
Concentration
Log­
10
of
Spike
Concentration
Mon
Mar
18
16:
44:
57
2002
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
NITROSODIPHENYLAMINE,
NG/
ULN­
UL
50.0
10.0
5.0
1.0
0.5
Organics,
Method
1625:
T=
0Organics,
0
N­
TETRACOSANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
NAPHTHALENE,
NG/
ULNAPHTHALENE,
UL
100.0
10.0
1.0
0.1
Organics,
Method
1625:
T=
0Organics,
0
PENTACHLOROPHENOL,
NG/
ULPENTACHLOROPHENOL,
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Mon
Mar
18
16:
45:
11
2002
100.0
10.0
1.0
0.1
Organics,
Method
1625:
T=
0Organics,
0
N­
OCTACOSANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
TETRADECANE,
NG/
ULN­
UL
100.00
10.00
1.00
0.10
0.01
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
NITROBENZENE,
NG/
ULNITROBENZENE,
UL
100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
PHENANTHRENE,
NG/
ULPHENANTHRENE,
UL
Log­
10
of
Spike
Concentration
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
Page
24
of
32
Organics,
Method
1625:
T=
0Organics,
0
N­
OCTADECANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
N­
TRIACONTANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
P­
CYMENE,
NG/
ULP­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
0Organics,
0
PHENOL,
NG/
ULPHENOL,
UL
0.05
0.50
5.00
50.00
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­
10
of
Measured
Concentration
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
PHENOL,
2­
METHYL­
4,6­
DINITRO­,
NG/
ULPHENOL,
UL
10.0
1.0
0.1
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
1,2,3­
TRICHLOROBENZENE,
NG/
UL1,2,3­
UL
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
1,2­
DIPHENYLHYDRAZINE,
NG/
UL1,2­
UL
100.0
10.0
1.0
0.1
Organics,
Method
1625:
T=
1000Organics,
1000
2,3,6­
TRICHLOROPHENOL,
NG/
UL2,3,6­
UL
0.05
0.50
5.00
50.00
Mon
Mar
18
16:
45:
25
2002
100.0
100.00
Organics,
Method
1625:
T=
0Organics,
0
PYRENE,
NG/
ULPYRENE,
UL
10.00
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
1,2,4­
TRICHLOROBENZENE,
NG/
UL1,2,4­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
1,3­
DICHLOROBENZENE,
NG/
UL1,3­
UL
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
2,4,5­
TRICHLOROPHENOL,
NG/
UL2,4,5­
UL
Log­
10
of
Spike
Concentration
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
10^­
4
100.0
10.0
1.0
0.1
Page
25
of
32
Organics,
Method
1625:
T=
0Organics,
0
STYRENE,
NG/
ULSTYRENE,
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
1,2­
DICHLOROBENZENE,
NG/
UL1,2­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
1,4­
DICHLOROBENZENE,
NG/
UL1,4­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
2,4,6­
TRICHLOROPHENOL,
NG/
UL2,4,6­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­
10
of
Measured
Concentration
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Measured
Concentration
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DICHLOROPHENOL,
NG/
UL2,4­
UL
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DIMETHYLPHENOL,
NG/
UL2,4­
UL
100.0
50.0
50.00
10.00
10.0
10.0
5.00
5.0
1.00
1.0
1.0
0.50
0.5
0.10.10
0.1
0.05
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
Page
26
of
32
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DINITROPHENOL,
NG/
UL2,4­
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DINITROTOLUENE,
NG/
UL2,4­
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
2,6­
DINITROTOLUENE,
NG/
UL2,6­
UL
100.00
50.0
50.00
10.0
10.0
10.00
5.0
5.00
1.0
1.001.0
0.50
0.5
0.1
0.10
0.1
0.05
Organics,
Method
1625:
T=
1000Organics,
1000
2­
CHLORONAPHTHALENE,
NG/
UL2­
UL
0.05
0.50
5.00
50.00
0.1
0.5
5.0
50.0
0.05
0.50
5.00
50.00
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
2­
CHLOROPHENOL,
NG/
UL2­
UL
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
2­
NITROPHENOL,
NG/
UL2­
UL
100.0
50.00
50.0
Organics,
Method
1625:
T=
1000Organics,
1000
2­
PICOLINE,
NG/
UL2­
UL
10.0
10.00
10.0
5.00
5.0
1.0
1.00
0.50
1.0
0.5
0.1
0.10
0.05
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
0.5
1.0
5.0
10.0
50.0
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
3,3'­
DICHLOROBENZIDINE,
NG/
UL3,3'­
UL
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
4­
BROMOPHENYL
PHENYL
ETHER,
NG/
UL4­
UL
100.0
10.00
10.0
10.0
1.00
1.0
1.0
0.10
0.1
0.1
0.01
0.05
0.50
5.00
50.00
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
4­
CHLORO­
3­
METHYLPHENOL,
NG/
UL4­
UL
Mon
Mar
18
16:
45:
39
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­
10
of
Measured
Concentration
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.00
Organics,
Method
1625:
T=
1000Organics,
1000
4­
CHLOROPHENYLPHENYL
ETHER,
NG/
UL4­
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
4­
NITROPHENOL,
NG/
UL4­
UL
100.00
50.00
50.0
10.00
10.00
10.0
5.00
1.00
5.0
1.00
0.10
0.50
1.0
0.01
0.5
0.10
0.05
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
1
5
10
50
100
0.05
0.50
5.00
50.00
Page
27
of
32
Organics,
Method
1625:
T=
1000Organics,
1000
ACENAPHTHENE,
NG/
ULACENAPHTHENE,
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
ACENAPHTHYLENE,
NG/
ULACENAPHTHYLENE,
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
ALPHA­
TERPINEOL,
NG/
ULALPHA­
UL
100.00
50.00
10.0
10.0
10.00
5.00
1.0
1.0
1.00
0.50
0.1
0.1
0.10
0.05
Organics,
Method
1625:
T=
1000Organics,
1000
ANTHRACENE,
NG/
ULANTHRACENE,
UL
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
A)
PYRENE,
NG/
ULBENZO(
UL
100.00
100.00
100.00
50.00
50.00
10.00
10.00
10.00
5.00
5.00
1.00
1.00
Organics,
Method
1625:
T=
1000Organics,
1000
BENZIDINE,
NG/
ULBENZIDINE,
UL
1.00
0.50
0.50
0.10
0.10
0.10
0.05
0.05
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
A)
ANTHRACENE,
NG/
ULBENZO(
UL
0.01
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
B)
FLUORANTHENE,
NG/
ULBENZO(
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
GHI)
PERYLENE,
NG/
ULBENZO(
UL
100.0
10.0
10.0
10.0
1.0
1.0
1.0
0.1
0.1
0.1
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
K)
FLUORANTHENE,
NG/
ULBENZO(
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
0.50
5.00
50.00
Mon
Mar
18
16:
45:
52
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
BIS(
2­
CHLOROETHOXY)
METHANE,
NG/
ULBIS(
UL
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.0
100.0
100.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
BETA­
NAPHTHYLAMINE,
NG/
ULBETA­
UL
Organics,
Method
1625:
T=
1000Organics,
1000
BIPHENYL,
NG/
ULBIPHENYL,
UL
Page
28
of
32
Organics,
Method
1625:
T=
1000Organics,
1000
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
BIS(
2­
ETHYLHEXYL)
PHTHALATE,
NG/
ULBIS(
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
CHRYSENE,
NG/
ULCHRYSENE,
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
DI­
N­
PROPYLNITROSAMINE,
NG/
ULDI­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10.0
1.0
0.1
0.05
100.00
10.00
1.00
0.10
0.01
10^­
4
100.0
10.0
1.0
0.1
10^­
4
100.00
10.00
1.00
0.10
0.01
10.0
10.00
5.00
1.0
1.00
0.50
0.1
0.10
0.05
0.50
5.00
50.00
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
Organics,
Method
1625:
T=
1000Organics,
1000
BIS(
2­
CHLOROETHYL)
ETHER,
NG/
ULBIS(
UL
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
BIS(
2­
CHLOROISOPROPYL)
ETHER,
NG/
ULBIS(
UL
100.0
50.00
10.00
10.0
5.00
1.0
1.00
0.50
0.1
0.10
0.05
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.1
0.5
5.0
50.0
10^­
4
Organics,
Method
1625:
T=
1000Organics,
1000
BUTYL
BENZYL
PHTHALATE,
NG/
ULBUTYL
UL
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
CARBAZOLE,
NG/
ULCARBAZOLE,
UL
100.00
50.00
10.00
10.00
5.00
1.00
1.00
0.10
0.50
0.01
0.10
0.05
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
0.50
5.00
50.00
10^­
4
Organics,
Method
1625:
T=
1000Organics,
1000
DI­
N­
BUTYL
PHTHALATE,
NG/
ULDI­
UL
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
DI­
N­
OCTYL
PHTHALATE,
NG/
ULDI­
UL
100.00
10.0
10.00
1.00
1.0
0.10
0.1
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
0.05
0.50
5.00
50.00
10^­
4
Log­
10
of
Measured
Concentration
Mon
Mar
18
16:
46:
06
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
0.050.505.0050.00
0.1
0.5
1.0
5.0
10.0
50.0
100.0Organics,
Method
1625:
T=
1000Organics,
1000
DIBENZO(
A,
H)
ANTHRACENE,
NG/
ULDIBENZO(
UL
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)
Episode
6000
DataPage
29
of
32
Log­
10
of
Measured
Concentration
Log­
10
of
Spike
Concentrationc:/
pw/
ostmdl/
req004/
r004sd1.
sMon
Mar
18
16:
46:
20
2002
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
DIBENZOFURAN,
NG/
ULDIBENZOFURAN,
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
DIBENZOTHIOPHENE,
NG/
ULDIBENZOTHIOPHENE,
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
DIETHYL
PHTHALATE,
NG/
ULDIETHYL
UL
0.050.505.0050.00
0.1
0.5
1.0
5.0
10.0
50.0
100.0Organics,
Method
1625:
T=
1000Organics,
1000
DIMETHYL
PHTHALATE,
NG/
ULDIMETHYL
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
DIPHENYL
ETHER,
NG/
ULDIPHENYL
UL
10^­
410^­
310^­
210^­
110^
010^
110^
2
0.1
0.5
1.0
5.0
10.0
50.0
100.0Organics,
Method
1625:
T=
1000Organics,
1000
DIPHENYLAMINE,
NG/
ULDIPHENYLAMINE,
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
FLUORANTHENE,
NG/
ULFLUORANTHENE,
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
FLUORENE,
NG/
ULFLUORENE,
UL
10^­
410^­
310^­
210^­
110^
010^
110^
2
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
HEXACHLOROBENZENE,
NG/
ULHEXACHLOROBENZENE,
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
HEXACHLOROBUTADIENE,
NG/
ULHEXACHLOROBUTADIENE,
UL
0.050.505.0050.00
0.05
0.10
0.50
1.00
5.00
10.00
50.00
100.00Organics,
Method
1625:
T=
1000Organics,
1000
HEXACHLOROCYCLOPENTADIENE,
NG/
ULHEXACHLOROCYCLOPENTADIENE,
UL
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.0
50.0
10.0
5.0
1.0
0.5
0.1
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
HEXACHLOROETHANE,
NG/
ULHEXACHLOROETHANE,
UL
100.0
50.0
10.0
5.0
1.0
0.5
0.1
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
N­
DECANE,
NG/
ULN­
UL
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
N­
EICOSANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
N­
NITROSODIMETHYLAMINE,
NG/
ULN­
UL
Mon
Mar
18
16:
46:
33
2002
100.0
50.0
10.0
5.0
1.0
0.5
0.1
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
INDENO(
1,2,3­
CD)
PYRENE,
NG/
ULINDENO(
UL
100.000
10.000
1.000
0.100
0.010
0.001
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
N­
DOCOSANE,
NG/
ULN­
UL
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
N­
HEXACOSANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.0
50.0
10.0
5.0
1.0
0.5
0.1
Organics,
Method
1625:
T=
1000Organics,
1000
N­
NITROSODIPHENYLAMINE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Log­
10
of
Spike
Concentration
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Page
30
of
32
Organics,
Method
1625:
T=
1000Organics,
1000
ISOPHORONE,
NG/
ULISOPHORONE,
UL
100.0
10.0
1.0
0.1
Organics,
Method
1625:
T=
1000Organics,
1000
N­
DODECANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
N­
HEXADECANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
100.0
10.0
1.0
0.1
Organics,
Method
1625:
T=
1000Organics,
1000
N­
OCTACOSANE,
NG/
ULN­
UL
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­
10
of
Measured
Concentration
Episode
6000
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.000
10.000
1.000
0.100
0.010
0.001
10^­
4
100.00
10.00
1.00
0.10
0.01
10^­
4
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
0.05
100.00
50.00
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
1625:
T=
1000Organics,
1000
N­
OCTADECANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
N­
TRIACONTANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
P­
CYMENE,
NG/
ULP­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
PHENOL,
NG/
ULPHENOL,
UL
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
N­
TETRACOSANE,
NG/
ULN­
UL
100.0
50.0
10.0
10.0
5.0
1.0
1.0
0.1
0.5
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
NAPHTHALENE,
NG/
ULNAPHTHALENE,
UL
100.0
10.00
10.0
1.00
1.0
0.10
0.1
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
10^­
4
100.0
Organics,
Method
1625:
T=
1000Organics,
1000
PENTACHLOROPHENOL,
NG/
ULPENTACHLOROPHENOL,
UL
100.00
50.0
50.00
10.0
10.00
5.0
5.00
1.00
1.0
0.50
0.5
0.10
0.1
0.05
0.05
0.50
5.00
50.00
0.05
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
PHENOL,
2­
METHYL­
4,6­
DINITRO­,
NG/
ULPHENOL,
UL
100.00
50.00
10.00
10.00
5.00
1.00
1.00
0.10
0.50
0.010.10
0.05
0.05
0.50
5.00
50.00
10^­
4
Log­
10
of
Spike
Concentration
Page
31
of
32
Organics,
Method
1625:
T=
1000Organics,
1000
N­
TETRADECANE,
NG/
ULN­
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
NITROBENZENE,
NG/
ULNITROBENZENE,
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Organics,
Method
1625:
T=
1000Organics,
1000
PHENANTHRENE,
NG/
ULPHENANTHRENE,
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
PYRENE,
NG/
ULPYRENE,
UL
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­
10
of
Measured
Concentration
Mon
Mar
18
16:
46:
47
2002
Episode
6000
Data
Page
32
of
32
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

100.00
10.00
Organics,
Method
1625:
T=
1000Organics,
1000
STYRENE,
NG/
ULSTYRENE,
UL
1.00
0.10
0.01
10^­
4
10^­
3
10^­
2
10^­
1
10^
0
10^
1
10^
2
Log­
10
of
Measured
Concentration
Mon
Mar
18
16:
47:
01
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
APPENDIX
B
­
2
­
2
Page
1
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)
500.0500
500
100.0
50.0
100
Lab:
1Lab:
1
ALUMINUM,
UG/

LALUMINUM,
L
100
10.0
50
Lab:
2Lab:
2
ALUMINUM,
UG/

LALUMINUM,
L
5.0
50
1.0
10
0.5
Lab:
3Lab:
3
ALUMINUM,
UG/

LALUMINUM,
L
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
600
1000
500
Lab:
5Lab:
5
ALUMINUM,
UG/

LALUMINUM,
L
500
500
Lab:
4Lab:
4
ALUMINUM,
UG/

LALUMINUM,
L
400
300
200
100
100
50
50
100
90
Lab:
6Lab:
6
ALUMINUM,
UG/

LALUMINUM,
L
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
500
Lab:
7Lab:
7
ALUMINUM,
UG/

LALUMINUM,
L
500
500
100
50
Lab:
8Lab:
8
ALUMINUM,
UG/

LALUMINUM,
L
100
50
100
10
5
5
50
10
Lab:
9Lab:
9
ALUMINUM,
UG/

LALUMINUM,
L
50
100
500
5
10
50
100
500
0.1
1.0
10.0
100.0
Log­
10
of
Spike
Concentration
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
2
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

500
Lab:
1Lab:
1
ARSENIC,
UG/

LARSENIC,
L
Lab:
2Lab:
2
ARSENIC,
UG/

LARSENIC,
L
500
500
100
100
50
50
100
10
50
5
10
5
1
Lab:
3Lab:
3
ARSENIC,
UG/

LARSENIC,
L
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
500
Lab:
4Lab:
4
ARSENIC,
UG/

LARSENIC,
L
Lab:
5Lab:
5
ARSENIC,
UG/

LARSENIC,
L
500
100.0
100
100
5010.0
50
Lab:
6Lab:
6
ARSENIC,
UG/

LARSENIC,
L
1.0
10
10
5
5
0.1
5
10
50
100
500
5
10
50
100
500
0.1
1.0
10.0
100.0
500
Lab:
7Lab:
7
ARSENIC,
UG/

LARSENIC,
L
500
100.0
100
50
100
10.0
50
10
5
Lab:
8Lab:
8
ARSENIC,
UG/

LARSENIC,
L
1.0
10
1
5
0.1
Lab:
9Lab:
9
ARSENIC,
UG/

LARSENIC,
L
5
10
50100
500
5
10
50100
500
5
10
50100
500
Tue
Mar
26
17:
16:
51
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
3
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)
100100
Lab:
1Lab:
1
CADMIUM,
UG/

LCADMIUM,
L
100
50
Lab:
2Lab:
2
CADMIUM,
UG/

LCADMIUM,
L
50
50
10
10
10
55
5
11
1
5
10
50100
1
5
10
50100
1
5
10
50100
Lab:
3Lab:
3
CADMIUM,
UG/

LCADMIUM,
L
100.0
Lab:
4Lab:
4
CADMIUM,
UG/

LCADMIUM,
L
100.0
Lab:
5Lab:
5
CADMIUM,
UG/

LCADMIUM,
L
100
50.0
50.0
50
10.0
10.0
10
5.0
5.0
5
1.0
1.0
0.5
0.5
1
1
5
10
50
100
1
5
10
50
100
0.1
0.5
1.0
5.0
10.0
50.0
Lab:
6Lab:
6
CADMIUM,
UG/

LCADMIUM,
L
100
Lab:
7Lab:
7
CADMIUM,
UG/

LCADMIUM,
L
100
Lab:
8Lab:
8
CADMIUM,
UG/

LCADMIUM,
L
100
50
50
50
10
10
10
55
5
111
0.1
0.5
1.0
5.010.0
50.0
1
5
10
50
100
1
5
10
50
100
Lab:
9Lab:
9
CADMIUM,
UG/

LCADMIUM,
L
Tue
Mar
26
17:
16:
54
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
4
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

Lab:
1Lab:
1
CHROMIUM,
UG/

LCHROMIUM,
L
100.0
Lab:
2Lab:
2
CHROMIUM,
UG/

LCHROMIUM,
L
100
100
50.0
50
50
10.0
5.0
10
10
5
1.0
5
0.5
1
Lab:
3Lab:
3
CHROMIUM,
UG/

LCHROMIUM,
L
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
5
10
50
100
100
Lab:
5Lab:
5
CHROMIUM,
UG/

LCHROMIUM,
L
100
100
50
50
50
10
10
5
10
Lab:
4Lab:
4
CHROMIUM,
UG/

LCHROMIUM,
L
5
51
Lab:
6Lab:
6
CHROMIUM,
UG/

LCHROMIUM,
L
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
100
Lab:
7Lab:
7
CHROMIUM,
UG/

LCHROMIUM,
L
100
Lab:
8Lab:
8
CHROMIUM,
UG/

LCHROMIUM,
L
100
50
50
50
10
10
10
5
5
5
Lab:
9Lab:
9
CHROMIUM,
UG/

LCHROMIUM,
L
5
10
50100
5
10
50100
5
10
50100
Tue
Mar
26
17:
16:
56
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
5
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

100.0
100.0
100
50.0
50.0
50
10.0
10.0
5.0
5.0
10
5
1.0
1.0
0.5
0.5
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
Lab:
2Lab:
2
COPPER,
UG/
LCOPPER,
L
Lab:
3Lab:
3
COPPER,
UG/
LCOPPER,
L
Lab:
1Lab:
1
COPPER,
UG/
LCOPPER,
L
100
Lab:
5Lab:
5
COPPER,
UG/
LCOPPER,
L
100
100
50
50
50
10
10
Lab:
4Lab:
4
COPPER,
UG/
LCOPPER,
L
10
5
55
1
Lab:
6Lab:
6
COPPER,
UG/
LCOPPER,
L
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
100
Lab:
7Lab:
7
COPPER,
UG/
LCOPPER,
L
100
Lab:
8Lab:
8
COPPER,
UG/
LCOPPER,
L
100
50
50
50
10
10
10
55
5
1
5
10
50
100
5
10
50
100
0.1
0.5
1.0
5.0
50.0
Lab:
9Lab:
9
COPPER,
UG/
LCOPPER,
L
Tue
Mar
26
17:
16:
59
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
6
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

500
Lab:
1Lab:
1
LEAD,
UG/
LLEAD,
L
500
Lab:
2Lab:
2
LEAD,
UG/
LLEAD,
L
500
100
100
100
50
50
50
10
10
55
10
15
1
Lab:
3Lab:
3
LEAD,
UG/
LLEAD,
L
5
10
50
100
500
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
500
Lab:
5Lab:
5
LEAD,
UG/
LLEAD,
L
500
500
100
100
100
Lab:
4Lab:
4
LEAD,
UG/
LLEAD,
L
50
50
50
Lab:
6Lab:
6
LEAD,
UG/
LLEAD,
L
10
10
10
5
5
5
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
0.1
1.0
10.0
100.0
500
Lab:
7Lab:
7
LEAD,
UG/
LLEAD,
L
500
Lab:
8Lab:
8
LEAD,
UG/
LLEAD,
L
500
100
100
100
50
50
50
10
10
10
55
5
Lab:
9Lab:
9
LEAD,
UG/
LLEAD,
L
0.1
1.0
10.0
100.0
5
10
50
100
500
0.1
1.0
10.0
100.0
Tue
Mar
26
17:
17:
01
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Lab:
4Lab:
4
MANGANESE,
UG/
LMANGANESE,
L
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
7
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

50
Lab:
1Lab:
1
MANGANESE,
UG/
LMANGANESE,
L
50
Lab:
2Lab:
2
MANGANESE,
UG/
LMANGANESE,
L
50.0
Lab:
3Lab:
3
MANGANESE,
UG/
LMANGANESE,
L
10.0
10
5.0
10
5
1.0
5
0.5
1
0.1
0.5
1.0
5.0
10.0
50.0
5
10
50
0.5
1.0
5.0
10.0
50.0
50.0
50.0
Lab:
5Lab:
5
MANGANESE,
UG/
LMANGANESE,
L
50.0
10.0
10.0
10.0
5.05.0
5.0
1.0
1.0
1.0
0.5
0.5
0.5
Lab:
6Lab:
6
MANGANESE,
UG/
LMANGANESE,
L
0.1
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
50.0
Lab:
7Lab:
7
MANGANESE,
UG/
LMANGANESE,
L
50.0
10.00
10.0
10.0
1.00
5.0
5.0
0.10
1.0
1.0
0.5
Lab:
8Lab:
8
MANGANESE,
UG/
LMANGANESE,
L
0.01
0.5
0.5
1.0
5.0
10.0
50.0
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
Lab:
9Lab:
9
MANGANESE,
UG/
LMANGANESE,
L
Tue
Mar
26
17:
17:
04
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
8
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
245
CVA)

1.00
Lab:
1Lab:
1
MERCURY,
UG/

LMERCURY,
L
1.00
Lab:
2Lab:
2
MERCURY,
UG/

LMERCURY,
L
1.00
0.50
0.50
0.50
0.10
0.10
0.10
0.050.05
0.05
0.01
0.01
Lab:
3Lab:
3
MERCURY,
UG/

LMERCURY,
L
0.01
0.05
0.10
0.50
1.00
0.01
0.05
0.10
0.50
1.00
0.01
0.05
0.10
0.50
1.00
10.00
1.00
Lab:
4Lab:
4
MERCURY,
UG/

LMERCURY,
L
1.00
Lab:
5Lab:
5
MERCURY,
UG/

LMERCURY,
L
5.00
0.50
0.50
1.00
Lab:
6Lab:
6
MERCURY,
UG/

LMERCURY,
L
0.10
0.10
0.50
0.05
0.05
0.10
0.01
0.01
0.05
0.001
0.005
0.050
0.500
0.001
0.005
0.050
0.500
0.001
0.005
0.050
0.500
1.000
1.00
Lab:
8Lab:
8
MERCURY,
UG/

LMERCURY,
L
1.00
0.500
0.50
0.50
0.100
0.050
Lab:
7Lab:
7
MERCURY,
UG/

LMERCURY,
L
0.10
0.10
0.05
0.010
0.05
0.005
0.01
0.05
0.10
0.50
1.00
0.01
0.05
0.10
0.50
1.00
0.001
0.005
0.050
0.500
Lab:
9Lab:
9
MERCURY,
UG/

LMERCURY,
L
Tue
Mar
26
17:
17:
07
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Page
9
of
13
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

100
100
50
50
10
Lab:
1Lab:
1
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
Lab:
2Lab:
2
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
5.0
5
1.0
10
0.5
0.1
0.5
1.0
5.0
50.0
5
10
50
100
0.1
0.5
1.0
5.0
50.0
10.0
50.0
100.0
Lab:
3Lab:
3
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
100
50
50
10
10.0
50.0
100.0
Lab:
4Lab:
4
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
5.0
10
5
Lab:
5Lab:
5
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
5
1.0
0.5
1
100
Lab:
6Lab:
6
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
5
10
50
100
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
Lab:
7Lab:
7
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
100
100
50
Lab:
8Lab:
8
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
50
50
10
10
10
5
5
5
11
100
Lab:
9Lab:
9
MOLYBDENUM,
UG/

LMOLYBDENUM,
L
5
10
50
100
5
10
50
100
0.1
0.5
1.0
5.0
50.0
Tue
Mar
26
17:
17:
10
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

Lab:
1Lab:
1
NICKEL,
UG/

LNICKEL,
L
100
100
50
50
10
5.0
5
10
1.0
5
1
Lab:
2Lab:
2
NICKEL,
UG/

LNICKEL,
L
0.5
Page
10
of
13
10.0
50.0
100.0
Lab:
3Lab:
3
NICKEL,
UG/

LNICKEL,
L
5
10
50
100
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
100
100
50
50
Lab:
4Lab:
4
NICKEL,
UG/

LNICKEL,
L
Lab:
5Lab:
5
NICKEL,
UG/

LNICKEL,
L
50
10
10
5
5
100
500
1000
Lab:
6Lab:
6
NICKEL,
UG/

LNICKEL,
L
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
100
Lab:
7Lab:
7
NICKEL,
UG/

LNICKEL,
L
100
50
50
50
10
5
10
10
5
1
Lab:
8Lab:
8
NICKEL,
UG/

LNICKEL,
L
5
100
Lab:
9Lab:
9
NICKEL,
UG/

LNICKEL,
L
5
10
50100
5
10
50100
5
10
50100
Tue
Mar
26
17:
17:
13
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

1000
Lab:
1Lab:
1
SELENIUM,
UG/

LSELENIUM,
L
1000
Lab:
2Lab:
2
SELENIUM,
UG/

LSELENIUM,
L
1000.0
500
500.0
500
100.0
100
50.0
50100
Page
11
of
13
Lab:
3Lab:
3
SELENIUM,
UG/

LSELENIUM,
L
50
10.0
10
5.0
5
10
1.0
1
0.5
10
50
100
500
1000
10
50
100
500
1000
0.1
1.0
10.0
100.0
1000.0
1000
Lab:
4Lab:
4
SELENIUM,
UG/

LSELENIUM,
L
1000
Lab:
5Lab:
5
SELENIUM,
UG/

LSELENIUM,
L
1000
500
500
100
100
50
100
10
50
10
5
1
10
1
10
50
100
500
1000
0.1
1.0
10.0
100.0
1000.0
0.1
1.0
10.0
100.0
1000.0
Lab:
6Lab:
6
SELENIUM,
UG/

LSELENIUM,
L
1000
Lab:
7Lab:
7
SELENIUM,
UG/

LSELENIUM,
L
1000
1000
500
500
500
100
100
50
50
Lab:
8Lab:
8
SELENIUM,
UG/

LSELENIUM,
L
100
50
10
10
55
10
10
50
100
500
1000
0.1
1.0
10.0
100.0
1000.0
0.1
1.0
10.0
100.0
1000.0
Lab:
9Lab:
9
SELENIUM,
UG/

LSELENIUM,
L
Tue
Mar
26
17:
17:
16
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

100
Lab:
1Lab:
1
SILVER,
UG/
LSILVER,
L
100.0
Lab:
2Lab:
2
SILVER,
UG/
LSILVER,
L
100.0
50.0
50.0
50
10.0
10.0
5.0
10
5.0
5
1.0
1.0
0.5
0.5
1
Page
12
of
13
Lab:
3Lab:
3
SILVER,
UG/
LSILVER,
L
0.1
0.5
1.0
5.0
10.0
50.0
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
100.0
50.0
100.0
100
50.0
50
Lab:
4Lab:
4
SILVER,
UG/
LSILVER,
L
10.0
5.0
Lab:
5Lab:
5
SILVER,
UG/
LSILVER,
L
10.0
5.0
1.0
10
0.5
1.0
0.5
5
0.1
0.1
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
Lab:
6Lab:
6
SILVER,
UG/
LSILVER,
L
100
Lab:
7Lab:
7
SILVER,
UG/
LSILVER,
L
100
Lab:
8Lab:
8
SILVER,
UG/
LSILVER,
L
100.00
50
50
10.00
1.00
10
10
5
5
0.10
0.01
11
0.1
0.5
1.0
5.0
10.0
50.0
0.5
1.0
5.0
10.0
50.0
0.1
0.5
1.0
5.0
10.0
50.0
Lab:
9Lab:
9
SILVER,
UG/
LSILVER,
L
Tue
Mar
26
17:
17:
19
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s
Log­

10
of
Measured
Concentration
AAMA
Metals
Data
Measurement
Results
vs
Spike
Concentrations
(
Log­
10
Scale)

(
Matrix
A,
Method
EPA
200.7
ICP/
AES)

100
Lab:
2Lab:
2
ZINC,
UG/
LZINC,
L
100
100
50
50
50
10
10
10
Lab:
1Lab:
1
ZINC,
UG/
LZINC,
L
5
5
5
1
Page
13
of
13
Lab:
3Lab:
3
ZINC,
UG/
LZINC,
L
0.1
0.5
1.0
5.0
50.0
5
10
50
100
0.1
0.5
1.0
5.0
50.0
100
Lab:
5Lab:
5
ZINC,
UG/
LZINC,
L
100
100
Lab:
4Lab:
4
ZINC,
UG/
LZINC,
L
50
50
50
10
10
5
10
5
5
Lab:
6Lab:
6
ZINC,
UG/
LZINC,
L
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
100.0
100
50.0
100
Lab:
7Lab:
7
ZINC,
UG/
LZINC,
L
50
10.0
5.0
50
10
1.0
5
Lab:
8Lab:
8
ZINC,
UG/
LZINC,
L
0.5
0.1
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
0.1
0.5
1.0
5.0
50.0
Lab:
9Lab:
9
ZINC,
UG/
LZINC,
L
Tue
Mar
26
17:
17:
21
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req005/
r005sd1.
s