Document ID: EPA-HQ-OW-2003-0002-0135
Agency: epa
Document Type: Supporting & Related Material
Title: 
Posted Date: 2003-03-12T05:00Z

Table
2:
Two­
Component
Model
Estimates
and
Diagnostics
(
EPA,
Calibration
Indicator)

Source
Method
Technique
Analyte
Calibration
Number
of
Error
Alpha
Beta
Eta
Epsilon
Order
Spike
Conc.

CL6000
365.2
.
TOTAL
PHOSPHORUS
3
12
NO
0.0000
1.0037
0.0275
0.0025
MT6000
1620
Axial
ICP
CADMIUM
1
5
NO
­
0.3740
1.1737
0.0154
0.0770
MT6000
1620
Axial
ICP
CADMIUM
3
7
NO
.
.
.
.

MT6000
1620
Axial
ICP
CHROMIUM
1
5
NO
0.0700
1.3143
0.0097
0.2484
MT6000
1620
Axial
ICP
CHROMIUM
3
7
NO
0.0440
1.2646
0.0014
0.1428
MT6000
1620
Axial
ICP
LEAD
1
5
NO
­
0.4060
1.2072
0.0080
0.8147
MT6000
1620
Axial
ICP
LEAD
3
7
NO
0.7360
1.1158
0.0026
0.5874
MT6000
1620
Axial
ICP
MOLYBDENUM
1
5
NO
­
1.6060
0.9007
0.0106
0.7892
MT6000
1620
Axial
ICP
MOLYBDENUM
3
7
YES
.
.
.
.

MT6000
1620
Axial
ICP
TIN
1
5
NO
0.7310
1.1835
0.0003
4.8290
MT6000
1620
Axial
ICP
TIN
3
7
NO
­
2.5760
1.2376
0.0127
0.8768
MT6000
200.8
ICP/
MS
ALUMINUM
1
5
NO
­
0.5620
0.9628
0.0265
1.4239
MT6000
200.8
ICP/
MS
ALUMINUM
3
8
NO
7.2920
0.8241
0.2797
4.8361
MT6000
200.8
ICP/
MS
ANTIMONY
1
8
NO
0.0096
0.9595
0.0191
0.0094
MT6000
200.8
ICP/
MS
ANTIMONY
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
ARSENIC
1
8
NO
­
1.0278
1.0257
0.0202
0.0030
MT6000
200.8
ICP/
MS
ARSENIC
2
8
NO
­
0.2266
0.9598
0.0067
0.0838
MT6000
200.8
ICP/
MS
BARIUM
1
8
NO
­
0.0746
0.9585
0.0148
0.0210
MT6000
200.8
ICP/
MS
BARIUM
2
8
NO
0.0151
1.1457
0.0044
0.0412
MT6000
200.8
ICP/
MS
BERYLLIUM
1
8
NO
­
0.0843
1.1362
0.0445
0.0059
MT6000
200.8
ICP/
MS
BERYLLIUM
2
8
NO
0.0038
1.1445
0.0115
0.0042
MT6000
200.8
ICP/
MS
CADMIUM
1
8
YES
­
0.2108
1.0146
0.0140
0.0050
MT6000
200.8
ICP/
MS
CADMIUM
2
8
YES
­
0.0077
1.1520
0.0306
0.0020
MT6000
200.8
ICP/
MS
CHROMIUM
1
8
NO
0.7191
0.9945
0.0128
0.0902
MT6000
200.8
ICP/
MS
CHROMIUM
2
8
NO
0.8095
1.6052
0.0279
0.1655
MT6000
200.8
ICP/
MS
COBALT
1
8
NO
­
0.3699
1.0111
0.0221
0.0116
MT6000
200.8
ICP/
MS
COBALT
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
COPPER
1
8
NO
0.0071
1.0200
0.0228
0.0187
MT6000
200.8
ICP/
MS
LEAD
1
8
NO
0.0509
1.0295
0.0180
0.0204
MT6000
200.8
ICP/
MS
LEAD
2
8
NO
0.0770
0.7867
0.0777
0.1020
Table
2:
Two­
Component
Model
Estimates
and
Diagnostics
(
EPA,
Calibration
Indicator)

Source
Method
Technique
Analyte
Calibration
Number
of
Error
Alpha
Beta
Eta
Epsilon
Order
Spike
Conc.

MT6000
200.8
ICP/
MS
MANGANESE
1
8
YES
0.1654
1.1744
0.0578
0.0002
MT6000
200.8
ICP/
MS
MANGANESE
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
MERCURY
1
5
NO
0.8399
0.3397
0.0734
0.0200
MT6000
200.8
ICP/
MS
MOLYBDENUM
1
8
YES
­
0.1492
1.0249
0.0326
0.0018
MT6000
200.8
ICP/
MS
MOLYBDENUM
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
NICKEL
1
8
NO
­
0.0653
1.0783
0.0804
0.0649
MT6000
200.8
ICP/
MS
NICKEL
2
8
NO
0.0296
1.2423
0.1614
0.0064
MT6000
200.8
ICP/
MS
SELENIUM
1
8
NO
­
0.9597
1.0555
0.0383
0.0263
MT6000
200.8
ICP/
MS
SELENIUM
2
8
NO
­
0.5236
1.0048
0.0012
0.0876
MT6000
200.8
ICP/
MS
SILVER
1
8
YES
­
0.0036
0.8810
0.1066
0.0004
MT6000
200.8
ICP/
MS
SILVER
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
THALLIUM
1
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
THALLIUM
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
THORIUM
1
8
YES
0.2518
0.8373
0.0436
0.0060
MT6000
200.8
ICP/
MS
THORIUM
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
URANIUM
1
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
URANIUM
2
8
YES
.
.
.
.

MT6000
200.8
ICP/
MS
VANADIUM
1
8
NO
­
0.8290
1.0528
0.0223
0.1028
MT6000
200.8
ICP/
MS
VANADIUM
2
8
NO
­
0.6076
1.0102
0.0338
0.2259
MT6000
200.8
ICP/
MS
ZINC
1
8
NO
­
1.2452
1.1568
0.0515
0.4403
MT6000
200.8
ICP/
MS
ZINC
2
8
NO
1.2179
0.6351
0.0096
1.3254