Document ID: EPA-HQ-RCRA-2002-0028-0019
Agency: epa
Document Type: Supporting & Related Material
Title: 
Posted Date: 2002-12-24T05:00Z

CAS
Number
Chemical
Name
Sludge
WO/
Grit
PQL
Non
wastewaters
MDL
Non
wastewaters
UTS
Non
Wastewater
Units
mg/
kg
mg/
kg
mg/
kg
mg/
kg
SEMIVOLATILE
ORGANICS
82329
Acenaphthene
0.5
0.1
3.4
208986
Acenaphthylene
0.5
0.1
3.4
96862
Acetophenone
0.5
0.1
9.7
53963
2­
Acetylaminofluorene
0.5
0.1
140
309002
Aldrin
0.5
0.1
0.066
92671
4­
Aminobiphenyl
2
0.4
NA
62533
Aniline
3.52
0.5
0.1
14
120127
Anthracene
0.5
0.1
3.4
140578
Aramite
0.5
0.1
NA
319846
alpha­
BHC
0.5
0.1
0.066
319857
beta­
BHC
0.5
0.1
0.066
319868
delta­
BHC
0.5
0.1
0.066
58899
gamma­
BHC
0.5
0.1
0.066
98873
Benzal
chloride
1
0.2
6
56553
Benzo(
a)
anthracene
0.5
0.1
3.4
205992
Benzo(
b)
fluoranthene
0.5
0.1
6.8
207089
Benzo(
k)
fluoranthene
0.5
0.1
6.8
191242
Benzo(
g,
h,
i)
perylene
0.5
0.1
1.8
50328
Benze(
a)
pyrene
0.5
0.1
3.4
111911
Bis(
2­
chloroethoxy)
methane
0.5
0.1
7.2
111444
Bis(
2­
chloroethyl)
ether
0.5
0.1
6
108601
Bis(
2­
chloro­
1­
methylethyl)
ether
0.5
0.1
7.2
117817
Bis(
2­
ethylhexyl)
phthalate
3.11
1.5
0.3
28
101553
4­
Bromophenyl
phenyl
ether
0.5
0.1
15
85687
Butyl
benzyl
phthalate
2.5
0.5
28
88857
2­
s­
Butyl­
4,6­
dinitrophenol
0.5
0.1
2.5
106478
p­
Chloroaniline
0.5
0.1
16
510156
Chlorobenzilate
0.5
0.1
NA
59507
p­
Chloro­
m­
cresol
0.5
0.1
14
91587
2­
Chloronaphthalene
0.5
0.1
5.6
95578
2­
Chlorophenol
0.5
0.1
5.7
218019
Chrysene
0.5
0.1
3.4
108394
&
106445
m
&
p
­
Cresol
0.5
0.1
5.6
95487
o­
Cresol
0.5
0.1
5.6
72548
4,4'­
DDD
0.5
0.1
0.087
72559
4,4'­
DDE
0.5
0.1
0.087
50293
4,4'­
DDT
1
0.2
0.087
53703
Dibenz(
a,
h)
anthracene
0.5
0.1
8.2
192654
Dibenz(
a,
e)
pyrene
0.5
0.1
NA
60571
Dieldrin
0.5
0.1
0.13
84742
Di­
n­
butyl
phthalate
1.05
1
0.2
28
541731
m­
Dichlorobenzene
0.5
0.1
6
95501
o­
Dichlorobenzene
0.5
0.1
6
106467
p­
Dichlorobenzene
0.5
0.1
6
120832
2,4­
Dichlorophenol
0.5
0.1
14
87650
2,6­
Dichlorophenol
0.5
0.1
14
84662
Diethyl
phthalate
0.823
0.5
0.1
28
60117
p­(
Dimethylamino)
azobenzene
2
0.4
NA
105679
2,4­
Dimethylphenol
0.5
0.1
14
131113
Dimethyl
phthalate
0.5
0.1
28
100254
1,4­
Dinitrobenzene
1
0.2
2.3
534521
4,6­
Dinitro­
o­
cresol
0.5
0.1
160
51285
2,4­
Dinitrophenol
4
0.8
160
Sludge
Data
Without
Grit
­
Samples
Collected
May
1,
2000
Page
1
CAS
Number
Chemical
Name
Sludge
WO/
Grit
PQL
Non
wastewaters
MDL
Non
wastewaters
UTS
Non
Wastewater
Units
mg/
kg
mg/
kg
mg/
kg
mg/
kg
Sludge
Data
Without
Grit
­
Samples
Collected
May
1,
2000
121142
2,4­
Dinitrotoluene
0.5
0.1
140
606202
2,6­
Dinitrotoluene
0.5
0.1
28
117840
Di­
n­
octyl
phthalate
0.5
0.1
28
122394
Diphenylamine
0.5
0.1
13
86306
Diphenylnitrosoamine
0.5
0.1
13
122667
1,2­
Diphenyl
hydrazine
12.5
2.5
NA
298044
Disulfoton
0.5
0.1
6.2
959988
Endosulfan
I
0.5
0.1
0.066
33213659
Endosulfan
II
2.5
0.5
0.13
1031078
Endosulfan
sulfate
0.5
0.1
0.13
72208
Endrin
1
0.2
0.13
7421934
Endrin
aldehyde
0.5
0.1
0.13
52857
Famphur
1
0.2
15
206440
Fluoranthene
0.5
0.1
3.4
86737
Fluorene
0.5
0.1
3.4
76448
Heptachlor
1
0.2
0.066
1024573
Heptachlor
epoxide
0.5
0.1
0.066
118741
Hexachlorobenzene
0.5
0.1
10
87683
Hexachlorobutadiene
3.5
0.7
5.6
77474
Hexachlorocyclopentadiene
7
1.4
2.4
67721
Hexachloroethane
4
0.8
30
1888717
Hexachloropropene
4
0.8
30
193395
Indeno
(
1,2,3­
cd)
pyrene
0.5
0.1
3.4
465736
Isodrin
0.5
0.1
0.066
120581
Isosafrole
0.5
0.1
2.6
143500
Kepone
20
4
0.13
91805
Methapyrilene
2.5
0.5
1.5
72435
Methoxychlor
0.5
0.1
0.18
56495
3­
Methylcholanthrene
0.5
0.1
15
101144
4,4­
Methylene­
bis­(
2­
chloroaniline)
1
0.2
30
66273
Methyl
methanesulonate
0.5
0.1
NA
298000
Methyl
parathion
1
0.2
4.6
91203
Naphthalene
0.5
0.1
5.6
91598
2­
Naphthylamine
1.5
0.3
NA
88744
o­
Nitroaniline
0.5
0.1
14
100016
p­
Nitroaniline
1
0.2
28
98953
Nitrobenzene
0.5
0.1
14
88755
o­
Nitrophenol
0.5
0.1
13
100027
p­
Nitrophenol
0.5
0.1
29
924163
N­
Nitrosodi­
n­
butylamine
0.5
0.1
17
55185
N­
Nitrosodiethylamine
0.5
0.1
28
62759
N­
Nitrosodimethylamine
0.5
0.1
2.3
621647
N­
Nitroso­
di­
n­
propylamine
0.5
0.1
14
10595956
N­
Nitrosomethylethylamine
0.5
0.1
2.3
59892
N­
Nitrosomorpholine
0.5
0.1
2.3
100754
N­
Nitrosopiperidine
0.5
0.1
35
930552
N­
Nitrosopyrrolidine
0.5
0.1
35
99558
5­
Nitro­
o­
toluidine
3
0.6
28
56382
Parathion
1
0.2
4.6
608935
Pentachlorobenzene
0.5
0.1
10
82688
Pentachloronitrobenzene
0.5
0.1
4.8
87865
Pentachlorophenol
1
0.2
7.4
62442
Phenacetin
0.5
0.1
16
85018
Phenanthrene
0.5
0.1
5.6
Page
2
CAS
Number
Chemical
Name
Sludge
WO/
Grit
PQL
Non
wastewaters
MDL
Non
wastewaters
UTS
Non
Wastewater
Units
mg/
kg
mg/
kg
mg/
kg
mg/
kg
Sludge
Data
Without
Grit
­
Samples
Collected
May
1,
2000
108952
Phenol
0.5
0.1
6.2
298022
Phorate
0.5
0.1
4.6
100210
Phthalic
Acid/
wastewater
NA
NA
28
85449
Phthalic
Anhydride/
non
wastewater
1.5
0.3
28
23950585
Pronamide
0.5
0.1
1.5
129000
Pyrene
0.5
0.1
8.2
110861
Pyridine
4.5
0.9
16
94597
Safrole
0.5
0.1
22
85943
1,2,4,5­
Tetrachlorobenzene
0.5
0.1
14
58902
2,3,4,6­
Tetrachlorophenol
0.5
0.1
7.4
120821
1,2,4­
Trichlorobenene
0.5
0.1
19
95954
2,4,5­
Trichlorophenol
0.5
0.1
7.4
88062
2,4,6­
Trichlorophenol
0.5
0.1
7.4
126727
tris(
2,3­
Dibromopropyl)
phosphate
0.5
0.1
0.1
VOLATILE
ORGANICS
67641
Acetone
6.25
1.25
160
75058
Acetonitrile
1.25
0.25
38
107028
Acrolein
6.88
1.38
NA
107131
Acrylonitrile
0.625
0.125
84
71432
Benzene
0.625
0.125
10
75274
Bromodichloromethane
0.625
0.125
15
75252
Bromoform
0.625
0.125
15
74839
Bromomethane
0.625
0.125
15
71363
n­
Butyl
alcohol
5
1
2.6
75150
Carbon
Disulfide
0.625
0.125
4.8
TCLP
56235
Carbon
Tetrachloride
0.625
0.125
6
108907
Chlorobenzene
0.625
0.125
6
126998
2­
Chloro­
1,3­
butadiene
0.625
0.125
0.28
124481
Chlorodibromomethane
0.625
0.125
15
75003
Chloroethane
0.625
0.125
6
110758
2­
Chloroethyl
vinyl
ether
0.625
0.125
NA
67663
Chloroform
0.625
0.125
6
74873
Chloromethane
0.625
0.125
30
107051
3­
Chloropropene
0.625
0.125
30
108941
Cyclohexanone
4.38
(
Divided
by
20
is
0.21
TCLP)
0.88
0.75
TCLP
96128
1,2­
Dibromo­
3­
chloropropane
0.625
0.125
15
106934
1,2­
Dibromoethane
0.625
0.125
15
74953
Dibromomethane
0.625
0.125
15
75718
Dichlorodifluoromethane
0.625
0.125
7.2
75343
1,1­
Dichloroethane
0.625
0.125
6
107062
1,2­
Dichloroethane
0.625
0.125
6
75354
1,1­
Dichloroethylene
0.625
0.125
6
156605
trans­
1,2­
Dichloroethene
0.625
0.125
30
78875
1,2­
Dichloropropane
0.625
0.125
18
10061015
cis­
1,3­
Dichloropropene
0.625
0.125
18
10061026
trans­
1,3­
Dichloropropene
0.625
0.125
18
123911
1,4­
Dioxane
12.5
2.5
170
141786
Ethyl
acetate
1.25
0.25
33
100414
Ethyl
benzene
0.334
0.625
0.125
10
107120
Ethyl
cyanide
1.25
0.25
360
Page
3
CAS
Number
Chemical
Name
Sludge
WO/
Grit
PQL
Non
wastewaters
MDL
Non
wastewaters
UTS
Non
Wastewater
Units
mg/
kg
mg/
kg
mg/
kg
mg/
kg
Sludge
Data
Without
Grit
­
Samples
Collected
May
1,
2000
60297
Ethyl
ether
0.625
0.125
160
97632
Ethyl
methacrylate
0.625
0.125
160
75218
Ethylene
oxide
1.25
0.25
NA
75694
Fluorotrichloromethane
0.625
0.125
30
74884
Iodomethane
0.625
0.125
65
78831
Isobutanol
12.5
2.5
170
126987
Methacrylonitrile
0.625
0.125
84
67561
Methanol
0.5
0.5
0.75
TCLP
75092
Methylene
Chloride
0.625
0.125
30
78933
Methyl
ethyl
ketone
4.73
1/
6.25
1.25
36
108101
Methyl
isobutyl
ketone
0.625
0.125
33
80626
Methyl
methacrylate
0.625
0.125
160
76017
Pentachloroethane
0.625
0.125
6
630206
1,1,1,2­
Tetrachloroethane
0.625
0.125
6
79345
1,1,2,2­
Tetrachloroethane
0.625
0.125
6
127184
Tetrachloroethene
0.625
0.125
6
8001352
Toluene
0.964
0.625
0.125
10
71556
1,1,1­
Trichloroethane
0.625
0.125
6
79005
1,1,2­
Trichloroethane
0.625
0.125
6
79016
Trichloroethene
0.625
0.125
6
96184
1,2,3­
Trichloropropane
0.625
0.125
30
76131
1,1,2­
Trichloro­
1,2,2­
trifluoroethane
0.625
0.125
30
75014
Vinyl
chloride
0.625
0.125
6
1330207
m
&
p
 
Xylene
1.87
0.625
0.125
30
o
­
Xylene
0.545
0.625
0.125
30
1/
Method
blank
had
4
mg/
kg
INORGANICS
57­
12­
5
Cyanide
0.5
0.5
590
Total/
30
Amenable
TCLP
(
mg/
L)
TCLP
(
mg/
L)
TCLP
(
mg/
L)
TCLP
(
mg/
L)
7439­
97­
6
Mercury
0.001
0.0001
0.025
7440­
36­
0
Antimony
0.0172
0.02
0.002
1.15
7440­
38­
2
Arsenic
0.0343
0.02
0.002
5
7440­
39­
3
Barium
0.587
0.001
0.0001
21
7440­
41­
7
Beryllium
0.001
0.0001
1.22
7440­
43­
9
Cadmium
0.00392
0.003
0.0003
0.11
7440­
47­
3
Chromium
0.0258
0.006
0.0006
0.6
7439­
92­
1
Lead
0.0039
0.02
0.002
0.75
7440­
02­
0
Nickel
0.318
0.009
0.0009
11
7782­
49­
2
Selenium
0.00432
0.02
0.002
5.7
7440­
22­
4
Silver
0.000734
0.004
0.0004
0.14
7440­
28­
0
Thallium
0.0147
0.02
0.002
0.2
7440­
62­
2
Vanadium*
0.00845
0.006
0.0006
1.6
7440­
66­
6
Zinc*
2.6
0.009
0.0009
4.3
*
These
constituents
are
not
underlying
hazardous
constituents.
Page
4
INORGANICS
PQL
TCLP
MDL
TCLP
UTS
Non
Wastewater
TCLP
PQL
MDL
UTS
Wastewater
mg/
L
mg/
L
mg/
L
mg/
L
mg/
L
mg/
L
7439976
Mercury
0.001
0.0001
0.025
0.001
0.0001
0.15
7440360
Antimony
0.02
0.002
1.15
0.02
0.002
1.9
7440382
Arsenic
0.02
0.002
5
0.02
0.002
1.4
7440393
Barium
0.001
0.0001
21
0.001
0.0001
1.2
7440417
Berillium
0.001
0.0001
1.22
0.001
0.0001
0.82
7440439
Cadmium
0.003
0.0003
0.11
0.003
0.0003
0.69
7440473
Chromium
0.006
0.0006
0.6
0.006
0.0006
2.77
7439921
Lead
0.02
0.002
0.75
0.02
0.002
0.69
7440020
Nickel
0.009
0.0009
11
0.009
3.98
7782492
Selenium
0.02
0.002
5.7
0.009
0.0009
0.82
7440224
Silver
0.004
0.0004
0.014
0.004
0.0004
0.43
7440280
Thallium
0.02
0.002
0.2
0.02
0.002
1.4
Cyanides
(
Total)
5
TCA
mg/
kg
0.5
TCA
mg/
kg
590
0.1
0.01
1.2
ATTACHMENT
2
ENVIRONMENTAL
SERVICES
LABORATORY
ANALYTICAL
QUANTIFICATION
AND
METHOD
DETECTION
LIMITS
Page
7