Document ID: EPA-HQ-OW-2003-0003-0016
Agency: epa
Document Type: Supporting & Related Material
Title: 
Posted Date: 2003-03-12T05:00Z

Episode
6000
Data
50
40
30
20
10
Organics,
Method:
502.2­
PIDOrganics,
PID
O­
XYLENE+
STYRENE,
UG/
LO­
L
­
1.5
­
1.0
­
0.5
0.0
0.5
1.0
35
30
25
20
15
10
5
­
1.0
­
0.5
0.0
0.5
1.0
Organics,
Method:
502.2­
PIDOrganics,
PID
TERT­
BUTYLBENZENE,
UG/
LTERT­
L
40
30
20
10
Organics,
Method:
502.2­
PIDOrganics,
PID
TRANS­
1,3­
DICHLOROPROPENE,
UG/
LTRANS­
L
­
1.0
­
0.5
0.0
0.5
1.0
12
10
8
6
4
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
1,1,1­
TRICHLOROETHANE,
UG/
L1,1,1­
L
40
30
20
10
Organics,
Method:
502.2­
PIDOrganics,
PID
P­
ISOPROPTOL+
1,4­
DCB,
UG/
LP­
L
­
1.5
­
1.0
­
0.5
0.0
0.5
1.0
30
25
20
15
10
5
­
0.5
0.0
0.5
1.0
Organics,
Method:
502.2­
PIDOrganics,
PID
TETRACHLOROETHENE,
UG/
LTETRACHLOROETHENE,
L
20
15
10
5
Organics,
Method:
502.2­
PIDOrganics,
PID
TRICHLOROETHENE,
UG/
LTRICHLOROETHENE,
L
­
1.0
­
0.5
0.0
0.5
1.0
60
50
40
30
20
10
0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
1,1,2,2­
TETRACHLOROETHANE,
UG/
L1,1,2,2­
L
50
40
30
20
10
Page
11
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
502.2­
PIDOrganics,
PID
SEC­
BUTYLBENZENE,
UG/
LSEC­
L
­
1.0
­
0.5
0.0
0.5
1.0
80
60
40
20
0
­
1.5
­
1.0
­
0.5
0.0
0.5
1.0
Organics,
Method:
502.2­
PIDOrganics,
PID
TOLUENE,
UG/
LTOLUENE,
L
30
25
20
15
10
5
0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
1,1,1,2­
TETRACHLOROETHANE,
UG/
L1,1,1,2­
L
15
10
5
Organics,
Method:
524.2Organics,
524.2
1,1,2­
TRICHLOROETHANE,
UG/
L1,1,2­
L
­
0.5
0.0
0.5
1.0
1.5
2.0
Tue
May
7
16:
45:
27
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
20
25
20
20
15
15
10
10
5
Organics,
Method:
524.2Organics,
524.2
1,1­
DICHLOROETHANE,
UG/
L1,1­
L
5
Organics,
Method:
524.2Organics,
524.2
1,1­
DICHLOROETHENE,
UG/
L1,1­
L
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
10
20
8
15
6
Organics,
Method:
524.2Organics,
524.2
1,1­
DICHLOROPROPENE,
UG/
L1,1­
L
10
45
Organics,
Method:
524.2Organics,
524.2
1,2,3­
TRICHLOROBENZENE,
UG/
L1,2,3­
L
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
50
40
15
30
10
20
10
Organics,
Method:
524.2Organics,
524.2
1,2,4­
TRICHLOROBENZENE,
UG/
L1,2,4­
L
5
Organics,
Method:
524.2Organics,
524.2
1,2,4­
TRIMETHYLBENZENE,
UG/
L1,2,4­
L
­
0.50.0
0.5
1.0
1.5
2.0
­
1
0
1
2
60
25
50
20
40
30
Organics,
Method:
524.2Organics,
524.2
1,2­
DIBROMOETHANE,
UG/
L1,2­
L
15
20
10
10
5
0
Organics,
Method:
524.2Organics,
524.2
1,2­
DICHLOROBENZENE,
UG/
L1,2­
L
­
0.50.00.51.01.52.0
­
1
0
1
2
15
Page
12
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
524.2Organics,
524.2
1,1­
DICHLOROPROPANONE,
UG/
L1,1­
L
10
5
1.4
1.6
1.8
2.0
2.2
20
15
10
5
Organics,
Method:
524.2Organics,
524.2
1,2,3­
TRICHLOROPROPANE,
UG/
L1,2,3­
L
0.0
0.5
1.0
1.5
2.0
10
8
6
4
Organics,
Method:
524.2Organics,
524.2
1,2­
DIBROMO­
3­
CHLOROPROPANE,
UG/
L1,2­
L
1.0
1.5
2.0
6
5
4
3
2
1
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
1,2­
DICHLOROETHANE,
UG/
L1,2­
L
Relative
Standard
Deviation
Tue
May
7
16:
45:
41
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
7
6
5
4
3
2
1
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
1,2­
DICHLOROPROPANE,
UG/
L1,2­
L
15
10
5
Organics,
Method:
524.2Organics,
524.2
1,3­
DICHLOROPROPANE,
UG/
L1,3­
L
­
0.5
0.0
0.5
1.0
1.5
2.0
14
12
10
8
6
4
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
2,2­
DICHLOROPROPANE,
UG/
L2,2­
L
8
6
4
2
Organics,
Method:
524.2Organics,
524.2
2­
HEXANONE,
UG/
L2­
L
0.5
1.0
1.5
2.0
14
Organics,
Method:
524.2Organics,
524.2
1,3,5­
TRIMETHYLBENZENE,
UG/
L1,3,5­
L
60
12
50
10
40
8
30
6
20
4
10
20
­
10
1
2
­
1012
Page
13
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
524.2Organics,
524.2
1,3­
DICHLOROBENZENE,
UG/
L1,3­
L
20
300
15
200
10
Organics,
Method:
524.2Organics,
524.2
1,4­
DICHLOROBENZENE,
UG/
L1,4­
L
100
5
0
­
1012
­
1012
Organics,
Method:
524.2Organics,
524.2
1­
CHLOROBUTANE,
UG/
L1­
L
12
15
10
10
Organics,
Method:
524.2Organics,
524.2
2­
BUTANONE,
UG/
L2­
L
8
6
5
4
2
0.51.01.52.0
­
1
0
1
2
Organics,
Method:
524.2Organics,
524.2
2­
CHLOROTOLUENE,
UG/
L2­
L
5
30
4
20
3
2
Organics,
Method:
524.2Organics,
524.2
2­
NITROPROPANE,
UG/
L2­
L
10
1
1.01.52.0
­
1
0
1
2
Organics,
Method:
524.2Organics,
524.2
4­
CHLOROTOLUENE,
UG/
L4­
L
Tue
May
7
16:
45:
54
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
40
Organics,
Method:
524.2Organics,
524.2
4­
ISOPROPYLTOLUENE,
UG/
L4­
L
8
30
6
20
4
10
2
Organics,
Method:
524.2Organics,
524.2
4­
METHYL­
2­
PENTANONE,
UG/
L4­
L
­
1
0
1
2
1.01.52.0
8
15
6
Organics,
Method:
524.2Organics,
524.2
ACRYLONITRILE,
UG/
LACRYLONITRILE,
L
10
4
5
2
Organics,
Method:
524.2Organics,
524.2
ALLYL
CHLORIDE,
UG/
LALLYL
L
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
20
8
15
6
10
Organics,
Method:
524.2Organics,
524.2
BROMOBENZENE,
UG/
LBROMOBENZENE,
L
4
52
Organics,
Method:
524.2Organics,
524.2
BROMOCHLOROMETHANE,
UG/
LBROMOCHLOROMETHANE,
L
­
0.5
0.0
0.5
1.0
1.5
2.0
0.0
0.5
1.0
1.5
2.0
14
30
12
25
10
20
8
15
6
10
4
2
Organics,
Method:
524.2Organics,
524.2
BROMOFORM,
UG/
LBROMOFORM,
L
5
Organics,
Method:
524.2Organics,
524.2
BROMOMETHANE,
UG/
LBROMOMETHANE,
L
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
60
50
40
30
20
10
Page
14
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
524.2Organics,
524.2
ACETONE,
UG/
LACETONE,
L
0.5
1.0
1.5
2.0
50
40
30
20
10
0
­
10
12
Organics,
Method:
524.2Organics,
524.2
BENZENE,
UG/
LBENZENE,
L
40
30
20
10
0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
BROMODICHLOROMETHANE,
UG/
LBROMODICHLOROMETHANE,
L
20
15
10
5
Organics,
Method:
524.2Organics,
524.2
CARBON
DISULFIDE,
UG/
LCARBON
L
­
10
1
2
Tue
May
7
16:
46:
07
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
8
Organics,
Method:
524.2Organics,
524.2
CHLOROACETONITRILE,
UG/
LCHLOROACETONITRILE,
L
60
50
15
6
40
30
10
Organics,
Method:
524.2Organics,
524.2
CARBON
TETRACHLORIDE,
UG/
LCARBON
L
4
20
5
210
0
­
0.5
0.0
0.5
1.0
1.5
2.0
1.0
1.2
1.4
1.6
1.8
2.0
2.2
­
1
0
1
2
Page
15
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
524.2Organics,
524.2
CHLOROBENZENE,
UG/
LCHLOROBENZENE,
L
25
20
10
20
15
8
15
10
6
Organics,
Method:
524.2Organics,
524.2
CHLOROETHANE,
UG/
LCHLOROETHANE,
L
Organics,
Method:
524.2Organics,
524.2
CHLOROFORM,
UG/
LCHLOROFORM,
L
10
455
Organics,
Method:
524.2Organics,
524.2
CHLOROMETHANE,
UG/
LCHLOROMETHANE,
L
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
8
Organics,
Method:
524.2Organics,
524.2
CIS­
1,2­
DICHLOROETHENE,
UG/
LCIS­
L
Organics,
Method:
524.2Organics,
524.2
CIS­
1,3­
DICHLOROPROPENE,
UG/
LCIS­
L
8
15
6
6
10
4
4
5
2
2
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
DIBROMOCHLOROMETHANE,
UG/
LDIBROMOCHLOROMETHANE,
L
10
Organics,
Method:
524.2Organics,
524.2
DICHLORODIFLUOROMETHANE,
UG/
LDICHLORODIFLUOROMETHANE,
L
20
8
8
15
6
Organics,
Method:
524.2Organics,
524.2
DIBROMOMETHANE,
UG/
LDIBROMOMETHANE,
L
6
10
44
Organics,
Method:
524.2Organics,
524.2
DIETHYL
ETHER,
UG/
LDIETHYL
L
2
5
2
0
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
Tue
May
7
16:
46:
21
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
1440
40
12
30
30
Organics,
Method:
524.2Organics,
524.2
ETHYLBENZENE,
UG/
LETHYLBENZENE,
L
10
20
Organics,
Method:
524.2Organics,
524.2
ETHYL
METHACRYLATE,
UG/
LETHYL
L
8
20
6
10
10
4
02
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
Page
16
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
524.2Organics,
524.2
HEXACHLOROBUTADIENE,
UG/
LHEXACHLOROBUTADIENE,
L
40
Organics,
Method:
524.2Organics,
524.2
HEXACHLOROETHANE,
UG/
LHEXACHLOROETHANE,
L
30
Organics,
Method:
524.2Organics,
524.2
ISOPROPYLBENZENE,
UG/
LISOPROPYLBENZENE,
L
40
30
25
30
20
20
15
20
10
10
10
5
Organics,
Method:
524.2Organics,
524.2
M+
P
XYLENE,
UG/
LM+
L
­
0.50.00.51.01.52.0
­
1
0
1
2
­
1
0
1
2
12
Organics,
Method:
524.2Organics,
524.2
METHACRYLONITRILE,
UG/
LMETHACRYLONITRILE,
L
20
Organics,
Method:
524.2Organics,
524.2
METHYL
IODIDE,
UG/
LMETHYL
L
10
10
8
15
8
6
6
10
4
4
5
22
Organics,
Method:
524.2Organics,
524.2
METHYL
TERT­
BUTYL
ETHER,
UG/
LMETHYL
L
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
20
30
30
15
20
20
10
10
10
Organics,
Method:
524.2Organics,
524.2
METHYLACRYLATE,
UG/
LMETHYLACRYLATE,
L
Organics,
Method:
524.2Organics,
524.2
METHYLENE
CHLORIDE,
UG/
LMETHYLENE
L
Organics,
Method:
524.2Organics,
524.2
METHYLMETHACRYLATE,
UG/
LMETHYLMETHACRYLATE,
L
5
00
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
0.0
0.5
1.0
1.5
2.0
Tue
May
7
16:
46:
35
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
40
Organics,
Method:
524.2Organics,
524.2
N­
BUTYLBENZENE,
UG/
LN­
L
Organics,
Method:
524.2Organics,
524.2
N­
PROPYLBENZENE,
UG/
LN­
L
30
15
25
30
20
10
20
15
10
10
5
5
Page
17
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
524.2Organics,
524.2
NAPHTHALENE,
UG/
LNAPHTHALENE,
L
­
1
0
1
2
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
524.2Organics,
524.2
O­
XYLENE,
UG/
LO­
L
30
50
20
Organics,
Method:
524.2Organics,
524.2
PENTACHLOROETHANE,
UG/
LPENTACHLOROETHANE,
L
25
40
Organics,
Method:
524.2Organics,
524.2
SEC­
BUTYLBENZENE,
UG/
LSEC­
L
15
20
30
15
10
20
10
10
5
5
0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
­
1
0
1
2
35
Organics,
Method:
524.2Organics,
524.2
STYRENE,
UG/
LSTYRENE,
L
Organics,
Method:
524.2Organics,
524.2
TERT­
BUTYLBENZENE,
UG/
LTERT­
L
50
40
30
40
25
30
3020
2015
20
10
10
10
5
Organics,
Method:
524.2Organics,
524.2
TETRACHLOROETHENE,
UG/
LTETRACHLOROETHENE,
L
­
1
0
1
2
­
1
0
1
2
­
0.50.00.51.01.52.0
20
12
Organics,
Method:
524.2Organics,
524.2
TOLUENE,
UG/
LTOLUENE,
L
Organics,
Method:
524.2Organics,
524.2
TRANS­
1,2­
DICHLOROETHENE,
UG/
LTRANS­
L
8
15
10
6
8
10
64
Organics,
Method:
524.2Organics,
524.2
TRANS­
1,3­
DICHLOROPROPENE,
UG/
LTRANS­
L
4
5
2
2
­
1
0
1
2
­
0.5
0.0
0.5
1.0
1.5
2.0
­
0.5
0.0
0.5
1.0
1.5
2.0
Tue
May
7
16:
46:
48
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
TRANS­
1,4­
DICHLORO­
2­
BUTENE,
UG/
LTRANS­
L
Episode
6000
Data
35
Organics,
Method:
524.2Organics,
524.2
15
10
5
0.5
1.0
1.5
2.0
16
14
12
10
8
6
4
Organics,
Method:
524.2Organics,
524.2
VINYL
CHLORIDE,
UG/
LVINYL
L
­
0.5
0.0
0.5
1.0
1.5
2.0
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
1,2,4­
TRICHLOROBENZENE,
UG/
L1,2,4­
L
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
1,3­
DICHLOROBENZENE,
UG/
L1,3­
L
80
20
Organics,
Method:
524.2Organics,
524.2
TRICHLOROETHENE,
UG/
LTRICHLOROETHENE,
L
60
40
20
0
­
0.5
0.0
0.5
1.0
1.5
2.0
40
30
20
10
Organics,
Method:
524.2Organics,
524.2
XYLENE
(
TOTAL),
UG/
LXYLENE
L
­
10
1
2
20
15
10
5
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
1,2­
DICHLOROBENZENE,
UG/
L1,2­
L
120
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
1,4­
DICHLOROBENZENE,
UG/
L1,4­
L
30
25
20
15
10
5
­
0.5
0.0
0.5
1.0
1.5
2.0
Page
18
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
524.2Organics,
524.2
TRICHLOROFLUOROMETHANE,
UG/
LTRICHLOROFLUOROMETHANE,
L
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
1,2,3­
TRICHLOROBENZENE,
UG/
L1,2,3­
L
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
1,2­
DIPHENYLHYDRAZINE,
UG/
L1,2­
L
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
2,3,6­
TRICHLOROPHENOL,
UG/
L2,3,6­
L
Relative
Standard
Deviation
Tue
May
7
16:
47:
02
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
80
Organics,
Method:
1625:
T=
0Organics,
0
2,4,6­
TRICHLOROPHENOL,
UG/
L2,4,6­
L
25
50
20
40
Organics,
Method:
1625:
T=
0Organics,
0
2,4,5­
TRICHLOROPHENOL,
UG/
L2,4,5­
L
60
1530
40
20
10
20
10
5
000
­
2­
1012
­
2­
1012
­
2­
1012
Page
19
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
1625:
T=
0Organics,
0
2,4­
DICHLOROPHENOL,
UG/
L2,4­
L
40
80
Organics,
Method:
1625:
T=
0Organics,
0
2,4­
DINITROPHENOL,
UG/
L2,4­
L
30
30
60
20
20
40
10
10
20
0
Organics,
Method:
1625:
T=
0Organics,
0
2,4­
DIMETHYLPHENOL,
UG/
L2,4­
L
00
­
2­
1012
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
2,4­
DINITROTOLUENE,
UG/
L2,4­
L
80
Organics,
Method:
1625:
T=
0Organics,
0
2,6­
DINITROTOLUENE,
UG/
L2,6­
L
25
60
20
Organics,
Method:
1625:
T=
0Organics,
0
2­
CHLORONAPHTHALENE,
UG/
L2­
L
50
60
40
15
40
30
10
20
20
5
10
000
­
2­
1012
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
2­
CHLOROPHENOL,
UG/
L2­
L
80
80
30
60
60
20
40
40
10
20
20
Organics,
Method:
1625:
T=
0Organics,
0
2­
NITROPHENOL,
UG/
L2­
L
Organics,
Method:
1625:
T=
0Organics,
0
2­
PICOLINE,
UG/
L2­
L
Organics,
Method:
1625:
T=
0Organics,
0
3,3'­
DICHLOROBENZIDINE,
UG/
L3,3'­
L
000
­
2­
1012
­
2­
1012
­
1
0
1
2
Tue
May
7
16:
47:
16
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
20
Organics,
Method:
1625:
T=
0Organics,
0
4­
BROMOPHENYL
PHENYL
ETHER,
UG/
L4­
L
40
6
4
2
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
4­
CHLORO­
3­
METHYLPHENOL,
UG/
L4­
L
25
20
15
10
5
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
ACENAPHTHENE,
UG/
LACENAPHTHENE,
L
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
ANTHRACENE,
UG/
LANTHRACENE,
L
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BENZO(
A)
PYRENE,
UG/
LBENZO(
L
Page
20
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
0Organics,
0
4­
CHLOROPHENYLPHENYL
ETHER,
UG/
L4­
L
15
10
5
0
­
10
1
2
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
ACENAPHTHYLENE,
UG/
LACENAPHTHYLENE,
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BENZIDINE,
UG/
LBENZIDINE,
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BENZO(
B)
FLUORANTHENE,
UG/
LBENZO(
L
30
20
10
0
­
2­
10
1
2
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
4­
NITROPHENOL,
UG/
L4­
L
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
ALPHA­
TERPINEOL,
UG/
LALPHA­
L
30
25
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BENZO(
A)
ANTHRACENE,
UG/
LBENZO(
L
Relative
Standard
Deviation
Tue
May
7
16:
47:
30
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
50
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BENZO(
GHI)
PERYLENE,
UG/
LBENZO(
L
30
25
20
15
10
5
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BIPHENYL,
UG/
LBIPHENYL,
L
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
BIS(
2­
CHLOROISOPROPYL)
ETHER,
UG/
LBIS(
L
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
CARBAZOLE,
UG/
LCARBAZOLE,
L
10
Organics,
Method:
1625:
T=
0Organics,
0
BENZO(
K)
FLUORANTHENE,
UG/
LBENZO(
L
40
8
30
6
20
4
10
2
0
­
1
0
1
2
­
2­
1012
Page
21
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
0Organics,
0
BETA­
NAPHTHYLAMINE,
UG/
LBETA­
L
30
Organics,
Method:
1625:
T=
0Organics,
0
BIS(
2­
CHLOROETHOXY)
METHANE,
UG/
LBIS(
L
25
25
20
20
15
15
10
10
5
5
00
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
BIS(
2­
CHLOROETHYL)
ETHER,
UG/
LBIS(
L
20
Organics,
Method:
1625:
T=
0Organics,
0
BIS(
2­
ETHYLHEXYL)
PHTHALATE,
UG/
LBIS(
L
30
25
15
20
10
15
10
5
5
00
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
BUTYL
BENZYL
PHTHALATE,
UG/
LBUTYL
L
6
5
Organics,
Method:
1625:
T=
0Organics,
0
CHRYSENE,
UG/
LCHRYSENE,
L
6
4
4
3
2
2
1
00
­
1012
­
1012
Organics,
Method:
1625:
T=
0Organics,
0
DI­
N­
BUTYL
PHTHALATE,
UG/
LDI­
L
Relative
Standard
Deviation
Tue
May
7
16:
47:
44
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
12
2510
8
Organics,
Method:
1625:
T=
0Organics,
0
DI­
N­
OCTYL
PHTHALATE,
UG/
LDI­
L
20
6
15
4
10
25
00
­
1
0
1
2
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
DI­
N­
PROPYLNITROSAMINE,
UG/
LDI­
L
25
Organics,
Method:
1625:
T=
0Organics,
0
DIBENZOFURAN,
UG/
LDIBENZOFURAN,
L
200
20
150
15
100
10
50
5
00
­
1
0
1
2
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
DIBENZOTHIOPHENE,
UG/
LDIBENZOTHIOPHENE,
L
80
15
60
10
40
5
20
0
Organics,
Method:
1625:
T=
0Organics,
0
DIMETHYL
PHTHALATE,
UG/
LDIMETHYL
L
0
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
DIPHENYL
ETHER,
UG/
LDIPHENYL
L
20
80
15
60
10
40
20
Organics,
Method:
1625:
T=
0Organics,
0
FLUORANTHENE,
UG/
LFLUORANTHENE,
L
5
00
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
FLUORENE,
UG/
LFLUORENE,
L
40
30
20
10
0
­
10
1
2
Page
22
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
1625:
T=
0Organics,
0
DIBENZO(
A,
H)
ANTHRACENE,
UG/
LDIBENZO(
L
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
DIETHYL
PHTHALATE,
UG/
LDIETHYL
L
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
DIPHENYLAMINE,
UG/
LDIPHENYLAMINE,
L
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
HEXACHLOROBENZENE,
UG/
LHEXACHLOROBENZENE,
L
Tue
May
7
16:
47:
58
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
100
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
HEXACHLOROBUTADIENE,
UG/
LHEXACHLOROBUTADIENE,
L
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
INDENO(
1,2,3­
CD)
PYRENE,
UG/
LINDENO(
L
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
DOCOSANE,
UG/
LN­
L
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
HEXACOSANE,
UG/
LN­
L
20
15
10
5
0
­
10
1
2
6
5
4
3
2
1
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
ISOPHORONE,
UG/
LISOPHORONE,
L
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
DODECANE,
UG/
LN­
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
HEXADECANE,
UG/
LN­
L
25
Organics,
Method:
1625:
T=
0Organics,
0
HEXACHLOROCYCLOPENTADIENE,
UG/
LHEXACHLOROCYCLOPENTADIENE,
L
80
60
40
20
0
­
2­
10
1
2
Page
23
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
0Organics,
0
HEXACHLOROETHANE,
UG/
LHEXACHLOROETHANE,
L
30
25
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
DECANE,
UG/
LN­
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
EICOSANE,
UG/
LN­
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
NITROSODIMETHYLAMINE,
UG/
LN­
L
Relative
Standard
Deviation
Tue
May
7
16:
48:
12
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
80
100
80
Organics,
Method:
1625:
T=
0Organics,
0
N­
NITROSODIPHENYLAMINE,
UG/
LN­
L
60
60
40
40
20
20
00
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
N­
OCTACOSANE,
UG/
LN­
L
40
8
30
6
4
Organics,
Method:
1625:
T=
0Organics,
0
N­
TETRACOSANE,
UG/
LN­
L
20
2
10
00
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
N­
TETRADECANE,
UG/
LN­
L
30
Organics,
Method:
1625:
T=
0Organics,
0
NAPHTHALENE,
UG/
LNAPHTHALENE,
L
80
60
20
40
10
20
00
­
2­
1012
­
1
0
1
2
Organics,
Method:
1625:
T=
0Organics,
0
NITROBENZENE,
UG/
LNITROBENZENE,
L
100
40
80
30
60
20
40
1020
0
Organics,
Method:
1625:
T=
0Organics,
0
PENTACHLOROPHENOL,
UG/
LPENTACHLOROPHENOL,
L
0
­
2­
1012
­
2­
1012
Organics,
Method:
1625:
T=
0Organics,
0
PHENANTHRENE,
UG/
LPHENANTHRENE,
L
40
30
20
10
0
­
2­
10
1
2
Page
24
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
1625:
T=
0Organics,
0
N­
OCTADECANE,
UG/
LN­
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
N­
TRIACONTANE,
UG/
LN­
L
30
25
20
15
10
5
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
P­
CYMENE,
UG/
LP­
L
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
0Organics,
0
PHENOL,
UG/
LPHENOL,
L
Tue
May
7
16:
48:
26
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
PHENOL,
2­
METHYL­
4,6­
DINITRO­,
UG/
LPHENOL,
L
Episode
6000
Data
80
60
Organics,
Method:
1625:
T=
0Organics,
0
40
20
0
­
2­
10
1
2
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
1,2,3­
TRICHLOROBENZENE,
UG/
L1,2,3­
L
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
1,2­
DIPHENYLHYDRAZINE,
UG/
L1,2­
L
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
2,3,6­
TRICHLOROPHENOL,
UG/
L2,3,6­
L
80
Organics,
Method:
1625:
T=
0Organics,
0
PYRENE,
UG/
LPYRENE,
L
Page
25
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
0Organics,
0
STYRENE,
UG/
LSTYRENE,
L
25
60
20
40
15
10
20
5
00
­
2­
1012
­
2­
1012
30
Organics,
Method:
1625:
T=
1000Organics,
1000
1,2,4­
TRICHLOROBENZENE,
UG/
L1,2,4­
L
30
20
20
10
10
00
­
2­
1012
­
1
0
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
1,2­
DICHLOROBENZENE,
UG/
L1,2­
L
25
150
20
15
100
10
50
5
0
Organics,
Method:
1625:
T=
1000Organics,
1000
1,3­
DICHLOROBENZENE,
UG/
L1,3­
L
0
­
1
0
1
2
­
2­
1012
Organics,
Method:
1625:
T=
1000Organics,
1000
1,4­
DICHLOROBENZENE,
UG/
L1,4­
L
40
30
30
20
20
10
10
0
Organics,
Method:
1625:
T=
1000Organics,
1000
2,4,5­
TRICHLOROPHENOL,
UG/
L2,4,5­
L
0
­
1
0
1
2
­
2­
1012
Organics,
Method:
1625:
T=
1000Organics,
1000
2,4,6­
TRICHLOROPHENOL,
UG/
L2,4,6­
L
30
Relative
Standard
Deviation
Tue
May
7
16:
48:
40
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
2,4­
DICHLOROPHENOL,
UG/
L2,4­
L
50
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
2,4­
DINITROTOLUENE,
UG/
L2,4­
L
50
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
2­
CHLOROPHENOL,
UG/
L2­
L
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
3,3'­
DICHLOROBENZIDINE,
UG/
L3,3'­
L
Organics,
Method:
1625:
T=
1000Organics,
1000
2,4­
DIMETHYLPHENOL,
UG/
L2,4­
L
40
30
20
10
0
­
10
1
2
40
30
20
10
0
­
1.0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
1625:
T=
1000Organics,
1000
2,6­
DINITROTOLUENE,
UG/
L2,6­
L
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
2­
NITROPHENOL,
UG/
L2­
L
120
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
4­
BROMOPHENYL
PHENYL
ETHER,
UG/
L4­
L
150
100
60
50
Page
26
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Relative
Standard
Deviation
Organics,
Method:
1625:
T=
1000Organics,
1000
2,4­
DINITROPHENOL,
UG/
L2,4­
L
50
0
­
10
1
2
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
2­
CHLORONAPHTHALENE,
UG/
L2­
L
40
30
20
10
0
­
0.5
0.0
0.5
1.0
1.5
2.0
Organics,
Method:
1625:
T=
1000Organics,
1000
2­
PICOLINE,
UG/
L2­
L
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
4­
CHLORO­
3­
METHYLPHENOL,
UG/
L4­
L
Tue
May
7
16:
48:
54
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
15
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
4­
CHLOROPHENYLPHENYL
ETHER,
UG/
L4­
L
25
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
ACENAPHTHYLENE,
UG/
LACENAPHTHYLENE,
L
80
60
40
20
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BENZIDINE,
UG/
LBENZIDINE,
L
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BENZO(
B)
FLUORANTHENE,
UG/
LBENZO(
L
Organics,
Method:
1625:
T=
1000Organics,
1000
4­
NITROPHENOL,
UG/
L4­
L
10
5
0.0
0.5
1.0
1.5
2.0
60
40
20
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
ALPHA­
TERPINEOL,
UG/
LALPHA­
L
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BENZO(
A)
ANTHRACENE,
UG/
LBENZO(
L
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BENZO(
GHI)
PERYLENE,
UG/
LBENZO(
L
30
20
10
0
­
10
1
2
Page
27
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
1000Organics,
1000
ACENAPHTHENE,
UG/
LACENAPHTHENE,
L
12
10
8
6
4
2
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
ANTHRACENE,
UG/
LANTHRACENE,
L
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BENZO(
A)
PYRENE,
UG/
LBENZO(
L
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BENZO(
K)
FLUORANTHENE,
UG/
LBENZO(
L
Relative
Standard
Deviation
Tue
May
7
16:
49:
08
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
50
30
15
40
20
Organics,
Method:
1625:
T=
1000Organics,
1000
BETA­
NAPHTHYLAMINE,
UG/
LBETA­
L
10
0
­
101
2
50
40
30
20
10
Organics,
Method:
1625:
T=
1000Organics,
1000
BIS(
2­
CHLOROETHYL)
ETHER,
UG/
LBIS(
L
0
­
2­
10
1
2
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
BUTYL
BENZYL
PHTHALATE,
UG/
LBUTYL
L
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
DI­
N­
BUTYL
PHTHALATE,
UG/
LDI­
L
30
Organics,
Method:
1625:
T=
1000Organics,
1000
BIPHENYL,
UG/
LBIPHENYL,
L
10
Page
28
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
1000Organics,
1000
BIS(
2­
CHLOROETHOXY)
METHANE,
UG/
LBIS(
L
20
5
10
0
0
­
2­
1012
­
1
0
1
40
25
Relative
Standard
Deviation
30
20
Organics,
Method:
1625:
T=
1000Organics,
1000
BIS(
2­
CHLOROISOPROPYL)
ETHER,
UG/
LBIS(
L
10
0
­
1.0
­
0.5
0.0
0.5
1.0
1.5
2.0
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
CARBAZOLE,
UG/
LCARBAZOLE,
L
80
60
40
20
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
DI­
N­
OCTYL
PHTHALATE,
UG/
LDI­
L
20
15
10
5
Organics,
Method:
1625:
T=
1000Organics,
1000
BIS(
2­
ETHYLHEXYL)
PHTHALATE,
UG/
LBIS(
L
0
­
2­
10
1
2
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
CHRYSENE,
UG/
LCHRYSENE,
L
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
DI­
N­
PROPYLNITROSAMINE,
UG/
LDI­
L
Tue
May
7
16:
49:
22
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
2
Episode
6000
Data
15
20
40
Organics,
Method:
1625:
T=
1000Organics,
1000
DIBENZO(
A,
H)
ANTHRACENE,
UG/
LDIBENZO(
L
30
20
10
0
­
10
1
2
25
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
DIETHYL
PHTHALATE,
UG/
LDIETHYL
L
20
15
10
5
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
DIPHENYLAMINE,
UG/
LDIPHENYLAMINE,
L
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
HEXACHLOROBENZENE,
UG/
LHEXACHLOROBENZENE,
L
Organics,
Method:
1625:
T=
1000Organics,
1000
DIBENZOFURAN,
UG/
LDIBENZOFURAN,
L
10
5
0
­
10
1
2
14
12
10
8
6
4
2
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
DIMETHYL
PHTHALATE,
UG/
LDIMETHYL
L
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
FLUORANTHENE,
UG/
LFLUORANTHENE,
L
25
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
HEXACHLOROBUTADIENE,
UG/
LHEXACHLOROBUTADIENE,
L
Page
29
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
1000Organics,
1000
DIBENZOTHIOPHENE,
UG/
LDIBENZOTHIOPHENE,
L
15
10
5
0
­
10
1
2
15
10
5
Organics,
Method:
1625:
T=
1000Organics,
1000
DIPHENYL
ETHER,
UG/
LDIPHENYL
L
­
10
1
2
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
FLUORENE,
UG/
LFLUORENE,
L
30
25
20
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
HEXACHLOROCYCLOPENTADIENE,
UG/
LHEXACHLOROCYCLOPENTADIENE,
L
Relative
Standard
Deviation
Tue
May
7
16:
49:
36
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
12
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
HEXACHLOROETHANE,
UG/
LHEXACHLOROETHANE,
L
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
DECANE,
UG/
LN­
L
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
EICOSANE,
UG/
LN­
L
50
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
NITROSODIMETHYLAMINE,
UG/
LN­
L
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
INDENO(
1,2,3­
CD)
PYRENE,
UG/
LINDENO(
L
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
DOCOSANE,
UG/
LN­
L
60
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
HEXACOSANE,
UG/
LN­
L
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
NITROSODIPHENYLAMINE,
UG/
LN­
L
10
8
6
4
2
0
­
10
1
2
Page
30
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
1000Organics,
1000
ISOPHORONE,
UG/
LISOPHORONE,
L
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
DODECANE,
UG/
LN­
L
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
HEXADECANE,
UG/
LN­
L
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
OCTACOSANE,
UG/
LN­
L
Relative
Standard
Deviation
Tue
May
7
16:
49:
50
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
8
100
80
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
OCTADECANE,
UG/
LN­
L
60
40
20
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
TRIACONTANE,
UG/
LN­
L
15
10
5
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
P­
CYMENE,
UG/
LP­
L
14
12
10
8
6
4
2
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
PHENOL,
UG/
LPHENOL,
L
Organics,
Method:
1625:
T=
1000Organics,
1000
N­
TETRACOSANE,
UG/
LN­
L
6
4
2
0
­
2­
10
1
2
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
NAPHTHALENE,
UG/
LNAPHTHALENE,
L
50
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
PENTACHLOROPHENOL,
UG/
LPENTACHLOROPHENOL,
L
50
40
30
20
10
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
PHENOL,
2­
METHYL­
4,6­
DINITRO­,
UG/
LPHENOL,
L
80
60
40
20
0
­
2­
10
1
2
Page
31
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method:
1625:
T=
1000Organics,
1000
N­
TETRADECANE,
UG/
LN­
L
50
40
30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
NITROBENZENE,
UG/
LNITROBENZENE,
L
6
4
2
0
­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
PHENANTHRENE,
UG/
LPHENANTHRENE,
L
25
20
15
10
5
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
PYRENE,
UG/
LPYRENE,
L
Relative
Standard
Deviation
Tue
May
7
16:
50:
04
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s
Episode
6000
Data
Page
32
of
32
Relative
Standard
Deviation
vs
Spike
Concentrations
(
Log­
10
Scale)

30
20
10
0
­
2­
10
1
2
Organics,
Method:
1625:
T=
1000Organics,
1000
STYRENE,
UG/
LSTYRENE,
L
Relative
Standard
Deviation
Tue
May
7
16:
50:
18
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd3.
s