Document ID: EPA-HQ-OW-2003-0003-0014
Agency: epa
Document Type: Supporting & Related Material
Title: 
Posted Date: 2003-03-12T05:00Z

Episode
6000
Data
APPENDIX
B
­
4
­
1
Page
1
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

0.40Classicals,
Method
130.2Classicals,
130.2
HARDNESS,
MG/
LHARDNESS,
L
5
10
50
100
0.005
0.050
0.500
0.1
1.0
10.0
100.0
1000.0
0.1
1.0
10.0
100.0
1000.0
Classicals,
Method
350.3Classicals,
350.3
AMMONIA
AS
NITROGEN,
MG/
LAMMONIA
L
Metals,
Method
ICP/
MSMetals,
MS
Cd
111,
pptCd
ppt
Metals,
Method
ICP/
MSMetals,
MS
Pb
206,
pptPb
ppt
Classicals,
Method
160.2Classicals,
160.2
TOTAL
SUSPENDED
SOLIDS,
MG/
LTOTAL
L
0.5
5.0
50.0
0.050
0.500
0.1
1.0
10.0
100.0
1000.0
0.1
1.0
10.0
100.0
1000.0
Classicals,
Method
365.2Classicals,
365.2
TOTAL
PHOSPHORUS,
MG/
LTOTAL
L
Metals,
Method
ICP/
MSMetals,
MS
Cu
63,
pptCu
ppt
Metals,
Method
ICP/
MSMetals,
MS
Pb
207,
pptPb
ppt
Classicals,
Method
1677Classicals,
1677
WAD
CYANIDE,
UG/
LWAD
L
0.5
1.0
5.0
10.0
Metals,
Method
ICP/
MSMetals,
MS
Ag
107,
pptAg
ppt
0.1
1.0
10.0
100.0
1000.0
Metals,
Method
ICP/
MSMetals,
MS
Ni
60,
pptNi
ppt
0.1
1.0
10.0
100.0
1000.0
Metals,
Method
ICP/
MSMetals,
MS
Pb
208,
pptPb
ppt
0.1
1.0
10.0
100.0
1000.0
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.050
0.010
0.005
0.001
100.0
50.0
10.0
5.0
1.0
0.5
100.0
50.0
10.0
5.0
1.0
0.5
0.30
0.20
0.10
0.09
0.08
0.07
0.06
100.0
50.0
10.0
5.0
1.0
0.5
100
50
10
5
100
50
10
5
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.006
0.005
0.004
0.003
0.002
0.005
100
50
10
5
100
50
10
5
1
Log­
10
of
Observed
Standard
Deviation
Log­
10
of
Spike
Concentration
50.0
Episode
6000
Data
Page
2
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

500
Log­
10
of
Observed
Standard
Deviation
100.0
100
50.0
Metals,
Method
ICP/
MSMetals,
MS
Sb
123,
pptSb
ppt
50
Metals,
Method
ICP/
MSMetals,
MS
Se
82,
pptSe
ppt
Metals,
Method
ICP/
MSMetals,
MS
Tl
205,
pptTl
ppt
10.0
5.0
100
10
5
1.0
50
0.5
1
0.1
1.0
10.0
100.0
1000.0
0.1
1.0
10.0
100.0
1000.0
0.1
1.0
10.0
100.0
1000.0
Metals,
Method
ICP/
MSMetals,
MS
Zn
66,
pptZn
ppt
100
Metals,
Method
1620Metals,
1620
ANTIMONY,
UG/
LANTIMONY,
L
100
1.0
50
0.9
50
0.8
0.7
0.6
10
10
Metals,
Method
1620Metals,
1620
ALUMINUM,
UG/
LALUMINUM,
L
0.5
5
5
0.4
0.1
1.0
10.0
100.0
1000.0
1
5
10
50
100
500
0.1
0.5
5.0
50.0
Metals,
Method
1620Metals,
1620
BERYLLIUM,
UG/
LBERYLLIUM,
L
1.0
1.0
0.9
1.0
0.8
0.7
0.5
0.6
0.5
0.5
0.4
0.3
Metals,
Method
1620Metals,
1620
ARSENIC,
UG/
LARSENIC,
L
Metals,
Method
1620Metals,
1620
BARIUM,
UG/
LBARIUM,
L
0.1
0.5
1.0
5.0
10.0
50.0
0.1
0.5
5.0
50.0
0.05
0.50
5.00
50.00
0.10
10
Metals,
Method
1620Metals,
1620
BORON,
UG/
LBORON,
L
Metals,
Method
1620Metals,
1620
CADMIUM,
UG/
LCADMIUM,
L
10
0.05
55
Metals,
Method
1620Metals,
1620
CALCIUM,
UG/
LCALCIUM,
L
5
10
50
100
500
0.05
0.50
5.00
5
10
50
100
500
Mon
Mar
18
16:
24:
15
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
3
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

10
Metals,
Method
1620Metals,
1620
CHROMIUM,
UG/
LCHROMIUM,
L
0.5
0.1
0.1
0.5
5.0
50.0
100
50
10
5
1
5
10
50
100
500
Metals,
Method
1620Metals,
1620
IRON,
UG/
LIRON,
L
1.0
0.5
Metals,
Method
1620Metals,
1620
MANGANESE,
UG/
LMANGANESE,
L
0.1
0.5
5.0
50.0
1.0
0.5
Metals,
Method
1620Metals,
1620
SELENIUM,
UG/
LSELENIUM,
L
0.5
1.0
5.0
10.0
50.0
Metals,
Method
1620Metals,
1620
COBALT,
UG/
LCOBALT,
L
10
5
1
5
10
50
100
500
1.0
0.5
Metals,
Method
1620Metals,
1620
LEAD,
UG/
LLEAD,
L
0.5
5.0
50.0
2.0
1.0
0.9
0.8
0.7
0.6
0.5
0.4
Metals,
Method
1620Metals,
1620
MOLYBDENUM,
UG/
LMOLYBDENUM,
L
0.5
5.0
50.0
6
5
4
3
2
Metals,
Method
1620Metals,
1620
SILVER,
UG/
LSILVER,
L
0.5
5.0
50.0
500.0
Metals,
Method
1620Metals,
1620
COPPER,
UG/
LCOPPER,
L
5
0.5
5.0
50.0
60
50
40
30
20
Metals,
Method
1620Metals,
1620
MAGNESIUM,
UG/
LMAGNESIUM,
L
5
10
50
100
500
5000
10
5
Metals,
Method
1620Metals,
1620
NICKEL,
UG/
LNICKEL,
L
5
10
50
100
500
70
60
50
40
30
20
5
10
50
100
500
5000
Metals,
Method
1620Metals,
1620
SODIUM,
UG/
LSODIUM,
L
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
24:
28
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
4
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
0.7
0.6
0.5
0.4
0.3
0.2
Metals,
Method
1620Metals,
1620
THALLIUM,
UG/
LTHALLIUM,
L
0.1
0.5
5.0
50.0
10
5
Metals,
Method
1620Metals,
1620
VANADIUM,
UG/
LVANADIUM,
L
1
5
10
50
100
500
10
5
1
0.5
5.0
50.0
500.0
Metals,
Method
200.8Metals,
200.8
ALUMINUM,
UG/
LALUMINUM,
L
0.100
0.050
0.010
0.005
0.01
0.10
1.00
10.00
Metals,
Method
200.8Metals,
200.8
BARIUM,
UG/
LBARIUM,
L
4.0
3.0
3.0
2.0
2.0
1.0
Metals,
Method
1620Metals,
1620
TIN,
UG/
LTIN,
L
1.0
0.9
0.9
0.8
0.8
0.7
0.7
0.6
0.6
Metals,
Method
1620Metals,
1620
TITANIUM,
UG/
LTITANIUM,
L
0.5
5.0
50.0
0.5
5.0
50.0
10.0
5.0
1.0
0.5
Metals,
Method
1620Metals,
1620
YTTRIUM,
UG/
LYTTRIUM,
L
1.0
0.5
Metals,
Method
1620Metals,
1620
ZINC,
UG/
LZINC,
L
0.1
0.5
5.0
50.0
0.5
5.0
50.0
0.100
Metals,
Method
200.8Metals,
200.8
ANTIMONY,
UG/
LANTIMONY,
L
1.00
0.050
0.50
0.010
0.005
0.10
0.05
0.001
0.01
0.10
1.00
10.00
0.1
1.0
10.0
100.0
Metals,
Method
200.8Metals,
200.8
ARSENIC,
UG/
LARSENIC,
L
0.100
0.050
Metals,
Method
200.8Metals,
200.8
BERYLLIUM,
UG/
LBERYLLIUM,
L
0.010
0.005
0.010
0.005
0.001
0.005
0.050
0.500
5.000
0.001
0.005
0.050
0.500
Metals,
Method
200.8Metals,
200.8
CADMIUM,
UG/
LCADMIUM,
L
Mon
Mar
18
16:
24:
42
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
5
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

0.50
Metals,
Method
200.8Metals,
200.8
CHROMIUM,
UG/
LCHROMIUM,
L
Metals,
Method
200.8Metals,
200.8
COBALT,
UG/
LCOBALT,
L
Metals,
Method
200.8Metals,
200.8
COPPER,
UG/
LCOPPER,
L
0.0100
0.0050
0.10
0.10
0.05
0.05
0.0010
0.0005
0.01
0.05
0.50
5.00
0.0005
0.0050
0.0500
0.5000
0.01
0.05
0.50
5.00
0.50
Metals,
Method
200.8Metals,
200.8
LEAD,
UG/
LLEAD,
L
0.050
Metals,
Method
200.8Metals,
200.8
MANGANESE,
UG/
LMANGANESE,
L
0.100
0.050
0.10
0.010
0.05
0.010
0.005
0.005
0.01
0.05
0.50
5.00
50.00
0.001
0.005
0.050
0.500
0.005
0.050
0.500
5.000
Metals,
Method
200.8Metals,
200.8
MERCURY,
UG/
LMERCURY,
L
Log­
10
of
Observed
Standard
Deviation
0.1000
0.0500
0.0100
0.0050
0.0010
0.0005
0.0005
0.0050
0.0500
0.5000
Metals,
Method
200.8Metals,
200.8
MOLYBDENUM,
UG/
LMOLYBDENUM,
L
0.010
0.005
0.001
0.0005
0.0050
0.0500
0.5000
Metals,
Method
200.8Metals,
200.8
SILVER,
UG/
LSILVER,
L
Mon
Mar
18
16:
24:
55
2002
1.000
0.500
Metals,
Method
200.8Metals,
200.8
NICKEL,
UG/
LNICKEL,
L
1.00
0.50
0.100
0.050
0.10
0.010
0.05
0.005
0.01
0.10
1.00
10.00
0.05
0.50
5.00
50.00
Metals,
Method
200.8Metals,
200.8
SELENIUM,
UG/
LSELENIUM,
L
Metals,
Method
200.8Metals,
200.8
THALLIUM,
UG/
LTHALLIUM,
L
0.0100
0.0010
0.0050
0.0005
0.0010
0.0005
Metals,
Method
200.8Metals,
200.8
THORIUM,
UG/
LTHORIUM,
L
0.0001
0.0005
0.0050
0.0500
0.001
0.010
0.100
1.000
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
6
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

5.0
0.00100
0.00050
0.00010
0.00005
0.500
0.100
0.050
0.010
0.005
0.05
0.100
0.050
0.010
0.005
0.05
0.50
0.10
0.05
0.01
Metals,
Method
200.8Metals,
200.8
URANIUM,
UG/
LURANIUM,
L
0.0001
0.0010
0.0100
0.1000
0.50
5.00
0.50
5.00
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,1,1,2­
TETRACHLOROETHANE,
UG/
L1,1,1,2­
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,1,2­
TRICHLOROETHANE,
UG/
L1,1,2­
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,2,3­
TRICHLOROBENZENE,
UG/
L1,2,3­
L
1.0
0.5
0.1
0.500
0.100
0.050
0.010
0.005
0.05
0.500
0.100
0.050
0.010
0.005
0.05
0.50
0.10
0.05
0.01
Metals,
Method
200.8Metals,
200.8
VANADIUM,
UG/
LVANADIUM,
L
0.1
1.0
10.0
100.0
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,1,1­
TRICHLOROETHANE,
UG/
L1,1,1­
L
0.50
5.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,1­
DICHLOROETHANE,
UG/
L1,1­
L
0.50
5.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,2,4­
TRICHLOROBENZENE,
UG/
L1,2,4­
L
0.001
0.010
0.100
1.000
10.000
Metals,
Method
200.8Metals,
200.8
ZINC,
UG/
LZINC,
L
1.0
0.5
0.1
0.5
5.0
50.0
1.00
0.50
0.10
0.05
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,1,2,2­
TCE+
1,2,3­
TCP,
UG/
L1,1,2,2­
L
1
510
0.500
0.100
0.050
0.010
0.005
0.1
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,1­
DICHLOROETHENE,
UG/
L1,1­
L
0.100
0.050
0.010
0.005
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,2­
DIBROMOETHANE,
UG/
L1,2­
L
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
25:
09
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
7
of
32
Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)
1.000
0.500
0.500
0.500
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,2­
DICHLOROBENZENE,
UG/
L1,2­
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,2­
DICHLOROETHANE,
UG/
L1,2­
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,2­
DICHLOROPROPANE,
UG/
L1,2­
L
0.100
0.100
0.100
0.050
0.050
0.050
0.010
0.010
0.010
0.005
0.005
0.005
0.05
0.50
5.00
0.05
0.50
5.00
0.05
0.50
5.00
0.500
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,3­
DICHLOROBENZENE,
UG/
L1,3­
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,3­
DICHLOROPROPANE,
UG/
L1,3­
L
0.500
0.100
0.100
0.100
0.050
0.050
0.050
0.010
0.010
0.010
0.005
0.005
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
1,4­
DICHLOROBENZENE,
UG/
L1,4­
L
0.01
0.05
0.50
5.00
0.1
0.5
1.0
5.0
10.0
0.05
0.50
5.00
1.00
1.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
4­
CHLOROTOLUENE,
UG/
L4­
L
0.50
0.50
Organics,
Method
502.2­
ELCDOrganics,
ELCD
2­
CHLOROTOLUENE,
UG/
L2­
L
0.50
0.10
0.10
0.10
0.05
0.05
0.05
0.01
Organics,
Method
502.2­
ELCDOrganics,
ELCD
BROMOBENZENE,
UG/
LBROMOBENZENE,
L
0.05
0.50
5.00
0.05
0.50
5.00
0.5
1.0
5.0
10.0
0.500
Organics,
Method
502.2­
ELCDOrganics,
ELCD
BROMOCHLOROMETHANE,
UG/
LBROMOCHLOROMETHANE,
L
0.500
0.100
Organics,
Method
502.2­
ELCDOrganics,
ELCD
BROMODICHLOROMETHANE,
UG/
LBROMODICHLOROMETHANE,
L
0.100
0.100
0.050
0.050
0.050
0.010
0.010
0.010
0.005
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
BROMOFORM,
UG/
LBROMOFORM,
L
Log­
10
of
Observed
Standard
Deviation
0.005
0.1
0.5
1.0
5.0
10.0
0.05
0.50
5.00
0.5
1.0
5.0
10.0
Mon
Mar
18
16:
25:
23
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
8
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

0.500
0.20
0.10
0.09
0.08
0.07
Organics,
Method
502.2­
ELCDOrganics,
ELCD
BROMOMETHANE,
UG/
LBROMOMETHANE,
L
1
510
0.100
0.050
0.010
0.005
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CHLOROETHANE,
UG/
LCHLOROETHANE,
L
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CIS­
1,2­
DCE+
2,2­
DCP,
UG/
LCIS­
L
0.1
0.5
1.0
5.0
10.0
0.500
0.100
0.050
0.010
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
DIBROMOMETHANE,
UG/
LDIBROMOMETHANE,
L
0.1
0.5
1.0
5.0
10.0
1.000
0.500
0.100
0.050
0.010
0.005
0.500
0.100
0.050
0.010
0.005
0.05
0.500
0.100
0.050
0.010
0.005
0.001
0.05
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CARBONTET+
1,1­
DCP,
UG/
LCARBONTET+
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CHLOROBENZENE,
UG/
LCHLOROBENZENE,
L
0.100
0.050
0.010
0.005
0.1
0.5
1.0
5.0
10.0
0.1
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CHLOROFORM,
UG/
LCHLOROFORM,
L
0.10
0.05
0.01
0.50
5.00
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CHLOROMETHANE,
UG/
LCHLOROMETHANE,
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
CIS­
1,3­
DICHLOROPROPENE,
UG/
LCIS­
L
0.100
0.050
0.010
0.005
0.001
0.50
5.00
0.1
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
ELCDOrganics,
ELCD
DIBROMOCHLOROMETHANE,
UG/
LDIBROMOCHLOROMETHANE,
L
Organics,
Method
502.2­
ELCDOrganics,
ELCD
DICHLORODIFLUOROMETHANE,
UG/
LDICHLORODIFLUOROMETHANE,
L
0.500
0.100
0.050
0.010
0.005
0.05
0.50
5.00
0.001
0.010
0.100
1.000
10.000
Organics,
Method
502.2­
ELCDOrganics,
ELCD
HEXACHLOROBUTADIENE,
UG/
LHEXACHLOROBUTADIENE,
L
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
25:
36
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
Page
9
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
1.00
0.50
0.10
0.05
Organics,
Method
502.2­
ELCDOrganics,
ELCD
METHYLENE
CHLORIDE,
UG/
LMETHYLENE
L
0.05
0.50
5.00
0.500
0.100
0.050
0.010
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
TRANS­
1,3­
DICHLOROPROPENE,
UG/
LTRANS­
L
0.05
0.50
5.00
0.10
0.05
Organics,
Method
502.2­
ELCDOrganics,
ELCD
VINYL
CHLORIDE,
UG/
LVINYL
L
0.5
1.0
5.0
10.0
0.50
0.10
0.05
0.01
Organics,
Method
502.2­
PIDOrganics,
PID
1,2,4­
TRIMETHYLBENZENE,
UG/
L1,2,4­
L
0.05
0.50
5.00
0.500
0.100
0.050
0.010
0.005
0.05
0.50
5.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
TETRACHLOROETHENE,
UG/
LTETRACHLOROETHENE,
L
0.500
0.100
0.050
0.010
0.005
0.001
0.05
0.50
5.00
Organics,
Method
502.2­
ELCDOrganics,
ELCD
TRICHLOROETHENE,
UG/
LTRICHLOROETHENE,
L
0.10
0.05
0.01
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
1,2,3­
TRICHLOROBENZENE,
UG/
L1,2,3­
L
0.50
0.10
0.05
0.01
0.1
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
PIDOrganics,
PID
1,2­
DICHLOROBENZENE,
UG/
L1,2­
L
0.500
0.100
0.050
0.010
0.005
Organics,
Method
502.2­
ELCDOrganics,
ELCD
TRANS­
1,2­
DICHLOROETHENE,
UG/
LTRANS­
L
0.05
0.50
5.00
0.50
0.10
0.05
Organics,
Method
502.2­
ELCDOrganics,
ELCD
TRICHLOROFLUOROMETHANE,
UG/
LTRICHLOROFLUOROMETHANE,
L
0.5
1.0
5.0
10.0
0.50
0.10
0.05
Organics,
Method
502.2­
PIDOrganics,
PID
1,2,4­
TRICHLOROBENZENE,
UG/
L1,2,4­
L
0.05
0.50
5.00
1.00
0.50
0.10
0.05
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
1,3,5­
TMB+
4­
CHLOROTOLUENE,
UG/
L1,3,5­
L
Mon
Mar
18
16:
25:
49
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
0.50
0.50
0.500
0.100
Log­
10
of
Observed
Standard
Deviation
Organics,
Method
502.2­
PIDOrganics,
PID
1,3­
DICHLOROBENZENE,
UG/
L1,3­
L
0.10
0.05
0.01
0.05
0.50
5.00
0.100
0.050
0.010
0.005
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
BROMOBENZENE,
UG/
LBROMOBENZENE,
L
0.50
0.10
0.05
0.01
Organics,
Method
502.2­
PIDOrganics,
PID
ETHYLBENZENE,
UG/
LETHYLBENZENE,
L
0.05
0.50
5.00
1.000
0.500
0.100
0.050
0.010
0.005
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
M+
P
XYLENE,
UG/
LM+
L
Organics,
Method
502.2­
PIDOrganics,
PID
2­
CHLOROTOLUENE,
UG/
L2­
L
Page
10
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
502.2­
PIDOrganics,
PID
BENZENE,
UG/
LBENZENE,
L
0.050
0.10
0.05
0.010
0.005
0.05
0.50
5.00
0.05
0.50
5.00
0.50
0.50
0.10
Organics,
Method
502.2­
PIDOrganics,
PID
CHLOROBENZENE,
UG/
LCHLOROBENZENE,
L
0.10
0.05
0.05
0.01
0.05
0.50
5.00
0.1
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
PIDOrganics,
PID
CIS­
1,3­
DICHLOROPROPENE,
UG/
LCIS­
L
0.5000.50
0.100
0.050
0.10
0.010
0.005
0.05
0.01
0.05
0.50
5.00
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
HEXCHLOBUTADIENE+
NAPHTHALENE,
UG/
LHEXCHLOBUTADIENE+
L
Organics,
Method
502.2­
PIDOrganics,
PID
ISOPROPYLBENZENE,
UG/
LISOPROPYLBENZENE,
L
0.50
Organics,
Method
502.2­
PIDOrganics,
PID
N­
BUTYLBENZENE,
UG/
LN­
L
0.50
0.10
0.10
0.05
0.05
0.01
0.01
0.05
0.50
5.00
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
N­
PROPYLBENZENE,
UG/
LN­
L
Mon
Mar
18
16:
26:
02
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
1.00
0.50
0.10
0.05
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
O­
XYLENE+
STYRENE,
UG/
LO­
L
0.50
0.10
0.05
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
TERT­
BUTYLBENZENE,
UG/
LTERT­
L
0.50
0.10
0.05
Organics,
Method
502.2­
PIDOrganics,
PID
TRANS­
1,3­
DICHLOROPROPENE,
UG/
LTRANS­
L
0.1
0.5
1.0
5.0
10.0
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,1,1­
TRICHLOROETHANE,
UG/
L1,1,1­
L
1.00
0.50
0.10
0.05
0.01
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
P­
ISOPROPTOL+
1,4­
DCB,
UG/
LP­
L
0.50
0.10
0.05
Organics,
Method
502.2­
PIDOrganics,
PID
TETRACHLOROETHENE,
UG/
LTETRACHLOROETHENE,
L
0.5
1.0
5.0
10.0
0.50
0.10
0.05
0.01
0.1
0.5
1.0
5.0
10.0
Organics,
Method
502.2­
PIDOrganics,
PID
TRICHLOROETHENE,
UG/
LTRICHLOROETHENE,
L
10.00
5.00
1.00
0.50
0.10
0.05
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,1,2,2­
TETRACHLOROETHANE,
UG/
L1,1,2,2­
L
0.50
0.10
0.05
0.01
0.05
0.50
5.00
Page
11
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
Organics,
Method
502.2­
PIDOrganics,
PID
SEC­
BUTYLBENZENE,
UG/
LSEC­
L
0.500
0.100
0.050
0.010
0.005
0.05
0.50
5.00
Organics,
Method
502.2­
PIDOrganics,
PID
TOLUENE,
UG/
LTOLUENE,
L
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,1,1,2­
TETRACHLOROETHANE,
UG/
L1,1,1,2­
L
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
1,1,2­
TRICHLOROETHANE,
UG/
L1,1,2­
L
0.5
1.0
5.0
50.0
Mon
Mar
18
16:
26:
16
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,1­
DICHLOROETHANE,
UG/
L1,1­
L
10.000
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,1­
DICHLOROPROPENE,
UG/
L1,1­
L
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,2,4­
TRICHLOROBENZENE,
UG/
L1,2,4­
L
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
1,2­
DIBROMOETHANE,
UG/
L1,2­
L
0.5
1.0
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
1,1­
DICHLOROETHENE,
UG/
L1,1­
L
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
1,2,3­
TRICHLOROBENZENE,
UG/
L1,2,3­
L
0.5
5.0
50.0
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
524.2Organics,
524.2
1,2,4­
TRIMETHYLBENZENE,
UG/
L1,2,4­
L
0.1
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.1
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,2­
DICHLOROBENZENE,
UG/
L1,2­
L
5
4
3
2
Page
12
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
Organics,
Method
524.2Organics,
524.2
1,1­
DICHLOROPROPANONE,
UG/
L1,1­
L
50
100
5.00
1.00
0.50
0.10
0.05
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,2,3­
TRICHLOROPROPANE,
UG/
L1,2,3­
L
10.0
5.0
1.0
0.5
Organics,
Method
524.2Organics,
524.2
1,2­
DIBROMO­
3­
CHLOROPROPANE,
UG/
L1,2­
L
5
10
50
100
5.00
1.00
0.50
0.10
0.05
0.01
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,2­
DICHLOROETHANE,
UG/
L1,2­
L
Mon
Mar
18
16:
26:
29
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.000
Log­
10
of
Observed
Standard
Deviation
5.00
Organics,
Method
524.2Organics,
524.2
1,2­
DICHLOROPROPANE,
UG/
L1,2­
L
5.000
1.000
1.00
0.500
0.50
0.100
0.050
0.10
0.05
0.010
0.005
Organics,
Method
524.2Organics,
524.2
1,3,5­
TRIMETHYLBENZENE,
UG/
L1,3,5­
L
0.5
1.0
5.0
50.0
0.1
0.5
5.0
50.0
5.00
Organics,
Method
524.2Organics,
524.2
1,3­
DICHLOROPROPANE,
UG/
L1,3­
L
10.000
5.000
1.00
1.000
0.50
0.500
0.100
0.10
0.050
0.05
0.010
0.005
0.01
0.5
5.0
50.0
0.1
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
1,4­
DICHLOROBENZENE,
UG/
L1,4­
L
10.00
5.00
Organics,
Method
524.2Organics,
524.2
2,2­
DICHLOROPROPANE,
UG/
L2,2­
L
5.0
1.00
1.0
0.50
0.5
0.10
0.05
1
5
10
50100
5
10
50
100
Organics,
Method
524.2Organics,
524.2
2­
BUTANONE,
UG/
L2­
L
Organics,
Method
524.2Organics,
524.2
2­
HEXANONE,
UG/
L2­
L
10.0
10.0
5.0
5.0
1.0
1.0
0.5
0.5
0.1
Organics,
Method
524.2Organics,
524.2
2­
NITROPROPANE,
UG/
L2­
L
5
10
50100
5
10
50
100
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.1
0.5
5.0
50.0
Page
13
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
524.2Organics,
524.2
1,3­
DICHLOROBENZENE,
UG/
L1,3­
L
100.00
10.00
1.00
0.10
0.01
Organics,
Method
524.2Organics,
524.2
1­
CHLOROBUTANE,
UG/
L1­
L
0.1
0.5
5.0
50.0
10.000
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.1
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
2­
CHLOROTOLUENE,
UG/
L2­
L
10.00
1.00
0.10
0.01
Organics,
Method
524.2Organics,
524.2
4­
CHLOROTOLUENE,
UG/
L4­
L
0.1
0.5
5.0
50.0
Mon
Mar
18
16:
26:
42
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
524.2Organics,
524.2
4­
ISOPROPYLTOLUENE,
UG/
L4­
L
0.1
0.5
5.0
50.0
5.0
1.0
0.5
Organics,
Method
524.2Organics,
524.2
ACRYLONITRILE,
UG/
LACRYLONITRILE,
L
5
10
50
100
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
BROMOBENZENE,
UG/
LBROMOBENZENE,
L
0.5
5.0
50.0
5.00
1.00
0.50
0.10
0.05
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
BROMOFORM,
UG/
LBROMOFORM,
L
10.0
5.0
1.0
0.5
Organics,
Method
524.2Organics,
524.2
4­
METHYL­
2­
PENTANONE,
UG/
L4­
L
5
10
50
100
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
ALLYL
CHLORIDE,
UG/
LALLYL
L
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
BROMOCHLOROMETHANE,
UG/
LBROMOCHLOROMETHANE,
L
0.5
1.0
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
BROMOMETHANE,
UG/
LBROMOMETHANE,
L
0.5
5.0
50.0
10.0
5.0
1.0
0.5
Page
14
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
Organics,
Method
524.2Organics,
524.2
ACETONE,
UG/
LACETONE,
L
5
10
50
100
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
524.2Organics,
524.2
BENZENE,
UG/
LBENZENE,
L
0.1
1.0
10.0
100.0
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
BROMODICHLOROMETHANE,
UG/
LBROMODICHLOROMETHANE,
L
10.00
5.00
1.00
0.50
0.10
0.05
0.01
Organics,
Method
524.2Organics,
524.2
CARBON
DISULFIDE,
UG/
LCARBON
L
0.1
0.5
5.0
50.0
Mon
Mar
18
16:
26:
55
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.00
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
CARBON
TETRACHLORIDE,
UG/
LCARBON
L
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
CHLOROETHANE,
UG/
LCHLOROETHANE,
L
0.5
1.0
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
CIS­
1,2­
DICHLOROETHENE,
UG/
LCIS­
L
0.5
1.0
5.0
50.0
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
DIBROMOMETHANE,
UG/
LDIBROMOMETHANE,
L
0.5
1.0
5.0
50.0
5.0
1.0
0.5
Organics,
Method
524.2Organics,
524.2
CHLOROACETONITRILE,
UG/
LCHLOROACETONITRILE,
L
10
50
100
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
CHLOROFORM,
UG/
LCHLOROFORM,
L
0.5
5.0
50.0
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
CIS­
1,3­
DICHLOROPROPENE,
UG/
LCIS­
L
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
DICHLORODIFLUOROMETHANE,
UG/
LDICHLORODIFLUOROMETHANE,
L
0.5
1.0
5.0
50.0
Page
15
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
524.2Organics,
524.2
CHLOROBENZENE,
UG/
LCHLOROBENZENE,
L
1.00
0.10
0.01
0.1
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
CHLOROMETHANE,
UG/
LCHLOROMETHANE,
L
0.5
5.0
50.0
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
DIBROMOCHLOROMETHANE,
UG/
LDIBROMOCHLOROMETHANE,
L
0.5
1.0
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
DIETHYL
ETHER,
UG/
LDIETHYL
L
0.5
1.0
5.0
50.0
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
27:
09
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
ETHYL
METHACRYLATE,
UG/
LETHYL
L
0.5
1.0
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
HEXACHLOROETHANE,
UG/
LHEXACHLOROETHANE,
L
0.5
5.0
50.0
5.0
1.0
0.5
Organics,
Method
524.2Organics,
524.2
METHACRYLONITRILE,
UG/
LMETHACRYLONITRILE,
L
5
10
50
100
10.00
5.00
1.00
0.50
0.10
0.05
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
METHYLACRYLATE,
UG/
LMETHYLACRYLATE,
L
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
ETHYLBENZENE,
UG/
LETHYLBENZENE,
L
10.00
1.00
0.10
0.01
Organics,
Method
524.2Organics,
524.2
ISOPROPYLBENZENE,
UG/
LISOPROPYLBENZENE,
L
0.1
0.5
5.0
50.0
10.000
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
METHYL
IODIDE,
UG/
LMETHYL
L
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
METHYLENE
CHLORIDE,
UG/
LMETHYLENE
L
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
Page
16
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
524.2Organics,
524.2
HEXACHLOROBUTADIENE,
UG/
LHEXACHLOROBUTADIENE,
L
0.5
5.0
50.0
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
524.2Organics,
524.2
M+
P
XYLENE,
UG/
LM+
L
0.1
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
METHYL
TERT­
BUTYL
ETHER,
UG/
LMETHYL
L
5.00
1.00
0.50
0.10
0.05
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
METHYLMETHACRYLATE,
UG/
LMETHYLMETHACRYLATE,
L
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
27:
22
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
524.2Organics,
524.2
N­
BUTYLBENZENE,
UG/
LN­
L
0.1
0.5
5.0
50.0
10.000
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
O­
XYLENE,
UG/
LO­
L
10.000
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.1
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
STYRENE,
UG/
LSTYRENE,
L
10.00
1.00
0.10
0.01
Organics,
Method
524.2Organics,
524.2
TOLUENE,
UG/
LTOLUENE,
L
0.1
0.5
5.0
50.0
Mon
Mar
18
16:
27:
36
2002
10.00
5.00
1.00
0.50
0.10
0.05
Organics,
Method
524.2Organics,
524.2
N­
PROPYLBENZENE,
UG/
LN­
L
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
PENTACHLOROETHANE,
UG/
LPENTACHLOROETHANE,
L
10.000
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.1
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
TERT­
BUTYLBENZENE,
UG/
LTERT­
L
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
TRANS­
1,2­
DICHLOROETHENE,
UG/
LTRANS­
L
Log­
10
of
Spike
Concentration
10.00
5.00
1.00
0.50
0.10
0.05
Page
17
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
Organics,
Method
524.2Organics,
524.2
NAPHTHALENE,
UG/
LNAPHTHALENE,
L
0.5
5.0
50.0
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
524.2Organics,
524.2
SEC­
BUTYLBENZENE,
UG/
LSEC­
L
0.1
0.5
5.0
50.0
10.00
5.00
1.00
0.50
0.10
0.05
0.01
0.5
5.0
50.0
Organics,
Method
524.2Organics,
524.2
TETRACHLOROETHENE,
UG/
LTETRACHLOROETHENE,
L
5.00
1.00
0.50
0.10
0.05
0.01
0.5
1.0
5.0
50.0
Organics,
Method
524.2Organics,
524.2
TRANS­
1,3­
DICHLOROPROPENE,
UG/
LTRANS­
L
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.00
Log­
10
of
Observed
Standard
Deviation
5.0
Organics,
Method
524.2Organics,
524.2
TRANS­
1,4­
DICHLORO­
2­
BUTENE,
UG/
LTRANS­
L
5.00
Organics,
Method
524.2Organics,
524.2
TRICHLOROETHENE,
UG/
LTRICHLOROETHENE,
L
10.00
5.00
1.00
0.50
1.00
1.0
0.50
0.10
0.5
0.05
0.10
0.05
0.01
Page
18
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
524.2Organics,
524.2
TRICHLOROFLUOROMETHANE,
UG/
LTRICHLOROFLUOROMETHANE,
L
5
10
50
100
0.5
5.0
50.0
0.5
1.0
5.0
50.0
10.00
Organics,
Method
524.2Organics,
524.2
XYLENE
(
TOTAL),
UG/
LXYLENE
L
5.000
10.00
5.00
Organics,
Method
524.2Organics,
524.2
VINYL
CHLORIDE,
UG/
LVINYL
L
1.000
1.00
0.500
1.00
0.100
0.50
0.10
0.050
0.10
0.010
0.05
0.01
0.005
Organics,
Method
1625:
T=
0Organics,
0
1,2,3­
TRICHLOROBENZENE,
NG/
UL1,2,3­
UL
0.5
5.0
50.0
0.1
0.5
5.0
50.0
0.01
0.10
1.00
10.00
100.00
1.000
Organics,
Method
1625:
T=
0Organics,
0
1,2­
DICHLOROBENZENE,
NG/
UL1,2­
UL
10.000
1.000
Organics,
Method
1625:
T=
0Organics,
0
1,2,4­
TRICHLOROBENZENE,
NG/
UL1,2,4­
UL
0.500
0.500
1.000
0.100
0.100
0.050
0.100
0.050
0.010
0.010
0.010
0.005
0.005
0.001
Organics,
Method
1625:
T=
0Organics,
0
1,2­
DIPHENYLHYDRAZINE,
NG/
UL1,2­
UL
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
5.000
1.000
1.00
0.500
Organics,
Method
1625:
T=
0Organics,
0
1,3­
DICHLOROBENZENE,
NG/
UL1,3­
UL
Organics,
Method
1625:
T=
0Organics,
0
1,4­
DICHLOROBENZENE,
NG/
UL1,4­
UL
1.000
0.50
0.500
0.100
0.050
0.10
0.100
0.050
0.05
0.010
0.005
0.010
0.01
0.005
Organics,
Method
1625:
T=
0Organics,
0
2,3,6­
TRICHLOROPHENOL,
NG/
UL2,3,6­
UL
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
Mon
Mar
18
16:
27:
49
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.01
1.000
0.500
0.100
0.050
0.010
0.005
0.001
0.01
1.00
0.50
0.10
0.05
0.01
0.01
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
1625:
T=
0Organics,
0
2,4,5­
TRICHLOROPHENOL,
NG/
UL2,4,5­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
2,4­
DIMETHYLPHENOL,
NG/
UL2,4­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
2,6­
DINITROTOLUENE,
NG/
UL2,6­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
2­
NITROPHENOL,
NG/
UL2­
UL
0.01
0.10
1.00
10.00
100.00
10.000
1.000
0.100
0.010
0.001
0.01
1.00
0.50
0.10
0.05
0.01
0.01
1.000
0.500
0.100
0.050
0.010
0.005
0.001
0.01
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
0Organics,
0
2,4,6­
TRICHLOROPHENOL,
NG/
UL2,4,6­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
2,4­
DINITROPHENOL,
NG/
UL2,4­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
2­
CHLORONAPHTHALENE,
NG/
UL2­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
2­
PICOLINE,
NG/
UL2­
UL
0.01
0.10
1.00
10.00
100.00
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.01
10.00
1.00
0.10
0.01
0.01
0.500
0.100
0.050
0.010
0.005
0.01
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Page
19
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
2,4­
DICHLOROPHENOL,
NG/
UL2,4­
UL
0.10
1.00
10.00
100.00
0.10
1.00
10.00
100.00
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
2,4­
DINITROTOLUENE,
NG/
UL2,4­
UL
Organics,
Method
1625:
T=
0Organics,
0
2­
CHLOROPHENOL,
NG/
UL2­
UL
Organics,
Method
1625:
T=
0Organics,
0
3,3'­
DICHLOROBENZIDINE,
NG/
UL3,3'­
UL
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
28:
03
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
1.000
0.500
0.100
0.050
0.010
0.005
0.001
0.01
0.10
1.00
10.00
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
4­
NITROPHENOL,
NG/
UL4­
UL
0.01
0.10
1.00
10.00
100.00
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
0Organics,
0
ALPHA­
TERPINEOL,
NG/
ULALPHA­
UL
0.01
0.10
1.00
10.00
100.00
1.00
0.50
0.10
0.05
0.01
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
A)
ANTHRACENE,
NG/
ULBENZO(
UL
0.05
0.50
5.00
50.00
5.000
Organics,
Method
1625:
T=
0Organics,
0
4­
BROMOPHENYL
PHENYL
ETHER,
NG/
UL4­
UL
1.000
0.500
0.100
0.050
0.010
0.005
0.01
10.000
1.000
0.100
0.010
0.001
0.01
1.000
0.100
0.010
0.001
0.01
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
1625:
T=
0Organics,
0
4­
CHLORO­
3­
METHYLPHENOL,
NG/
UL4­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
ACENAPHTHENE,
NG/
ULACENAPHTHENE,
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
ANTHRACENE,
NG/
ULANTHRACENE,
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
A)
PYRENE,
NG/
ULBENZO(
UL
0.05
0.50
5.00
50.00
1.000
0.500
0.100
0.050
0.010
0.005
Page
20
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
4­
CHLOROPHENYLPHENYL
ETHER,
NG/
UL4­
UL
0.05
0.50
5.00
50.00
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
0Organics,
0
ACENAPHTHYLENE,
NG/
ULACENAPHTHYLENE,
UL
0.01
0.10
1.00
10.00
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
0Organics,
0
BENZIDINE,
NG/
ULBENZIDINE,
UL
0.01
0.10
1.00
10.00
100.00
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
B)
FLUORANTHENE,
NG/
ULBENZO(
UL
0.01
0.10
1.00
10.00
100.00
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
28:
17
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
1.000
0.500
0.100
0.050
0.010
0.005
0.01
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.01
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.01
5.000
1.000
0.500
0.100
0.050
0.010
0.005
10.00
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
K)
FLUORANTHENE,
NG/
ULBENZO(
UL
10.00
1.00
1.00
0.10
0.10
0.01
0.01
Page
21
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
BETA­
NAPHTHYLAMINE,
NG/
ULBETA­
UL
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
BIPHENYL,
NG/
ULBIPHENYL,
UL
5.000
1.0001.000
0.500
0.100
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
CHLOROETHOXY)
METHANE,
NG/
ULBIS(
UL
0.100
0.050
0.010
0.010
0.005
0.001
0.001
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
CHLOROETHYL)
ETHER,
NG/
ULBIS(
UL
1.000
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
ETHYLHEXYL)
PHTHALATE,
NG/
ULBIS(
UL
1.000
0.500
0.500
0.100
0.100
0.050
0.050
0.010
0.010
0.005
0.005
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
BIS(
2­
CHLOROISOPROPYL)
ETHER,
NG/
ULBIS(
UL
Organics,
Method
1625:
T=
0Organics,
0
BUTYL
BENZYL
PHTHALATE,
NG/
ULBUTYL
UL
Organics,
Method
1625:
T=
0Organics,
0
CARBAZOLE,
NG/
ULCARBAZOLE,
UL
1.000
1.000
0.500
0.100
Organics,
Method
1625:
T=
0Organics,
0
CHRYSENE,
NG/
ULCHRYSENE,
UL
0.100
0.050
0.010
0.010
0.005
0.001
Organics,
Method
1625:
T=
0Organics,
0
DI­
N­
BUTYL
PHTHALATE,
NG/
ULDI­
UL
0.01
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
BENZO(
GHI)
PERYLENE,
NG/
ULBENZO(
UL
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
28:
30
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.00
1.000
0.500
0.100
0.050
0.010
0.005
0.05
1.000
0.100
0.010
0.001
0.05
1.000
0.500
0.100
0.050
0.010
0.005
0.01
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
0Organics,
0
DI­
N­
OCTYL
PHTHALATE,
NG/
ULDI­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
DIBENZOFURAN,
NG/
ULDIBENZOFURAN,
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
DIMETHYL
PHTHALATE,
NG/
ULDIMETHYL
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
FLUORANTHENE,
NG/
ULFLUORANTHENE,
UL
0.01
0.10
1.00
10.00
100.00
1.00
0.10
0.01
0.01
1.000
0.100
0.010
0.001
0.01
1.000
0.100
0.010
0.001
0.01
10.000
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
0Organics,
0
DI­
N­
PROPYLNITROSAMINE,
NG/
ULDI­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
DIBENZOTHIOPHENE,
NG/
ULDIBENZOTHIOPHENE,
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
DIPHENYL
ETHER,
NG/
ULDIPHENYL
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
FLUORENE,
NG/
ULFLUORENE,
UL
0.01
0.10
1.00
10.00
100.00
1.000
0.500
0.100
0.050
0.010
0.005
0.05
1.000
0.500
0.100
0.050
0.010
0.005
0.01
10.00
1.00
0.10
0.01
0.01
1.000
0.100
0.010
0.001
Page
22
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
DIBENZO(
A,
H)
ANTHRACENE,
NG/
ULDIBENZO(
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
DIETHYL
PHTHALATE,
NG/
ULDIETHYL
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
DIPHENYLAMINE,
NG/
ULDIPHENYLAMINE,
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROBENZENE,
NG/
ULHEXACHLOROBENZENE,
UL
0.01
0.10
1.00
10.00
100.00
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
28:
44
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
0.500
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROBUTADIENE,
NG/
ULHEXACHLOROBUTADIENE,
UL
5.000
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROCYCLOPENTADIENE,
NG/
ULHEXACHLOROCYCLOPENTADIENE,
UL
1.00
1.000
0.500
0.50
0.100
0.050
0.100
0.050
0.10
0.010
0.05
0.010
0.005
0.005
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
0.01
0.10
1.00
10.00
100.00
Page
23
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Log­
10
of
Observed
Standard
Deviation
Organics,
Method
1625:
T=
0Organics,
0
HEXACHLOROETHANE,
NG/
ULHEXACHLOROETHANE,
UL
10.00
Organics,
Method
1625:
T=
0Organics,
0
INDENO(
1,2,3­
CD)
PYRENE,
NG/
ULINDENO(
UL
1.000
Organics,
Method
1625:
T=
0Organics,
0
ISOPHORONE,
NG/
ULISOPHORONE,
UL
10.00
0.500
1.001.00
0.100
0.050
0.10
0.10
0.010
0.005
0.01
0.01
0.001
Organics,
Method
1625:
T=
0Organics,
0
N­
DECANE,
NG/
ULN­
UL
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
0Organics,
0
N­
DOCOSANE,
NG/
ULN­
UL
10.000
10.00
1.000
1.000
1.00
0.100
Organics,
Method
1625:
T=
0Organics,
0
N­
DODECANE,
NG/
ULN­
UL
0.100
0.10
0.010
0.010
0.01
0.001
0.001
Organics,
Method
1625:
T=
0Organics,
0
N­
EICOSANE,
NG/
ULN­
UL
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
10.000
Organics,
Method
1625:
T=
0Organics,
0
N­
HEXADECANE,
NG/
ULN­
UL
10.00
10.00
1.000
1.001.00
0.100
0.10
Organics,
Method
1625:
T=
0Organics,
0
N­
HEXACOSANE,
NG/
ULN­
UL
0.10
0.010
0.01
0.01
0.001
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
N­
NITROSODIMETHYLAMINE,
NG/
ULN­
UL
Mon
Mar
18
16:
28:
58
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
10.000
Log­
10
of
Observed
Standard
Deviation
1.000
Organics,
Method
1625:
T=
0Organics,
0
N­
NITROSODIPHENYLAMINE,
NG/
ULN­
UL
10.00
0.500
1.000
1.00
0.100
0.050
Organics,
Method
1625:
T=
0Organics,
0
N­
OCTACOSANE,
NG/
ULN­
UL
0.100
0.10
0.010
0.010
0.005
0.01
0.001
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
Page
24
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
N­
OCTADECANE,
NG/
ULN­
UL
10.00
10.000
1.000
0.500
Organics,
Method
1625:
T=
0Organics,
0
N­
TETRACOSANE,
NG/
ULN­
UL
1.000
Organics,
Method
1625:
T=
0Organics,
0
N­
TETRADECANE,
NG/
ULN­
UL
1.00
0.100
0.100
0.10
0.050
Organics,
Method
1625:
T=
0Organics,
0
N­
TRIACONTANE,
NG/
ULN­
UL
0.010
0.010
0.01
0.005
0.001
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
10.000
1.000
0.500
Organics,
Method
1625:
T=
0Organics,
0
NAPHTHALENE,
NG/
ULNAPHTHALENE,
UL
1.000
1.000
0.500
0.100
0.050
Organics,
Method
1625:
T=
0Organics,
0
NITROBENZENE,
NG/
ULNITROBENZENE,
UL
0.100
0.100
0.050
0.010
0.010
0.005
0.010
0.001
0.005
0.001
0.01
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
P­
CYMENE,
NG/
ULP­
UL
10.00
0.500
1.000
1.00
0.100
Organics,
Method
1625:
T=
0Organics,
0
PENTACHLOROPHENOL,
NG/
ULPENTACHLOROPHENOL,
UL
0.100
0.050
Organics,
Method
1625:
T=
0Organics,
0
PHENANTHRENE,
NG/
ULPHENANTHRENE,
UL
0.10
0.010
0.010.010
0.001
0.005
Organics,
Method
1625:
T=
0Organics,
0
PHENOL,
NG/
ULPHENOL,
UL
0.01
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
Mon
Mar
18
16:
29:
11
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Episode
6000
Data
1.00
0.50
0.10
0.05
Organics,
Method
1625:
T=
0Organics,
0
PHENOL,
2­
METHYL­
4,6­
DINITRO­,
NG/
ULPHENOL,
UL
0.01
0.10
1.00
10.00
100.00
1.000
0.500
0.100
0.050
0.010
0.005
0.001
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
1,2,3­
TRICHLOROBENZENE,
NG/
UL1,2,3­
UL
10.000
1.000
0.100
0.010
0.001
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
1,2­
DIPHENYLHYDRAZINE,
NG/
UL1,2­
UL
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
2,3,6­
TRICHLOROPHENOL,
NG/
UL2,3,6­
UL
Mon
Mar
18
16:
29:
25
2002
1.000
0.100
0.010
0.001
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
0Organics,
0
PYRENE,
NG/
ULPYRENE,
UL
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
1625:
T=
1000Organics,
1000
1,2,4­
TRICHLOROBENZENE,
NG/
UL1,2,4­
UL
0.01
0.10
1.00
10.00
100.00
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
1000Organics,
1000
1,3­
DICHLOROBENZENE,
NG/
UL1,3­
UL
0.05
0.50
5.00
50.00
5.00
1.00
0.50
0.10
0.05
0.01
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
2,4,5­
TRICHLOROPHENOL,
NG/
UL2,4,5­
UL
Log­
10
of
Spike
Concentration
5.000
1.000
0.500
0.100
0.050
0.010
0.005
0.01
1.000
0.500
0.100
0.050
0.010
0.005
0.05
1.000
0.500
0.100
0.050
0.010
0.005
0.01
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Page
25
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
0Organics,
0
STYRENE,
NG/
ULSTYRENE,
UL
0.10
1.00
10.00
100.00
0.50
5.00
50.00
0.10
1.00
10.00
100.00
0.01
0.10
1.00
10.00
100.00
c:/
pw/
ostmdl/
req004/
r004sd1.
s
Organics,
Method
1625:
T=
1000Organics,
1000
1,2­
DICHLOROBENZENE,
NG/
UL1,2­
UL
Organics,
Method
1625:
T=
1000Organics,
1000
1,4­
DICHLOROBENZENE,
NG/
UL1,4­
UL
Organics,
Method
1625:
T=
1000Organics,
1000
2,4,6­
TRICHLOROPHENOL,
NG/
UL2,4,6­
UL
Log­
10
of
Observed
Standard
Deviation
Episode
6000
Data
1.00
0.50
0.10
0.05
0.01
0.01
1.000
0.100
0.010
0.001
0.05
1.000
0.500
0.100
0.050
0.010
0.005
0.05
1.000
0.500
0.100
0.050
0.010
0.005
0.001
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DICHLOROPHENOL,
NG/
UL2,4­
UL
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DINITROTOLUENE,
NG/
UL2,4­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
2­
CHLOROPHENOL,
NG/
UL2­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
3,3'­
DICHLOROBENZIDINE,
NG/
UL3,3'­
UL
0.05
0.50
5.00
50.00
1.000
0.500
0.100
0.050
0.010
0.005
0.05
5.000
1.000
0.500
0.100
0.050
0.010
0.005
1.000
0.500
0.100
0.050
0.010
0.005
0.05
1.00
0.50
0.10
0.05
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DIMETHYLPHENOL,
NG/
UL2,4­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
2,6­
DINITROTOLUENE,
NG/
UL2,6­
UL
0.1
0.5
5.0
50.0
Organics,
Method
1625:
T=
1000Organics,
1000
2­
NITROPHENOL,
NG/
UL2­
UL
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
4­
BROMOPHENYL
PHENYL
ETHER,
NG/
UL4­
UL
0.01
0.10
1.00
10.00
100.00
1.00
0.50
0.10
0.05
0.05
0.50
5.00
50.00
Page
26
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
1000Organics,
1000
2,4­
DINITROPHENOL,
NG/
UL2,4­
UL
5.00
1.00
0.50
0.10
0.05
0.01
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
2­
CHLORONAPHTHALENE,
NG/
UL2­
UL
5.00
1.00
0.50
0.10
0.05
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
2­
PICOLINE,
NG/
UL2­
UL
0.5
1.0
5.0
10.0
50.0
1.000
0.500
0.100
0.050
0.010
0.005
0.001
0.01
0.10
1.00
10.00
100.00
Organics,
Method
1625:
T=
1000Organics,
1000
4­
CHLORO­
3­
METHYLPHENOL,
NG/
UL4­
UL
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
29:
39
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s
4­
CHLOROPHENYLPHENYL
ETHER,
NG/
UL4­
UL
Episode
6000
Data
Organics,
Method
1625:
T=
1000Organics,
1000
0.500
0.100
0.050
0.010
0.005
0.01
0.10
1.00
10.00
100.00
10.00
1.00
0.10
0.01
Organics,
Method
1625:
T=
1000Organics,
1000
ACENAPHTHYLENE,
NG/
ULACENAPHTHYLENE,
UL
0.05
0.50
5.00
50.00
1.000
0.100
0.010
0.001
Organics,
Method
1625:
T=
1000Organics,
1000
BENZIDINE,
NG/
ULBENZIDINE,
UL
0.05
0.50
5.00
50.00
5.000
1.000
0.500
0.100
0.050
0.010
0.005
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
B)
FLUORANTHENE,
NG/
ULBENZO(
UL
0.01
0.10
1.00
10.00
100.00
10.00
5.00
Organics,
Method
1625:
T=
1000Organics,
1000
4­
NITROPHENOL,
NG/
UL4­
UL
Page
27
of
32Standard
Deviations
vs
Spike
Concentrations
(
Log­
10
Scale)

Organics,
Method
1625:
T=
1000Organics,
1000
ACENAPHTHENE,
NG/
ULACENAPHTHENE,
UL
1.000
1.00
0.500
0.50
0.100
0.050
0.10
0.05
0.010
0.005
1
5
10
50
100
0.05
0.50
5.00
50.00
1.000
0.500
Organics,
Method
1625:
T=
1000Organics,
1000
ALPHA­
TERPINEOL,
NG/
ULALPHA­
UL
1.000
0.100
0.100
0.050
0.010
0.010
0.005
0.001
0.05
0.50
5.00
50.00
0.05
0.50
5.00
50.00
Organics,
Method
1625:
T=
1000Organics,
1000
ANTHRACENE,
NG/
ULANTHRACENE,
UL
5.000
1.000
1.000
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
A)
ANTHRACENE,
NG/
ULBENZO(
UL
0.500
0.500
0.100
0.100
0.050
0.050
0.010
0.010
0.005
0.005
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
A)
PYRENE,
NG/
ULBENZO(
UL
0.05
0.50
5.00
50.00
0.01
0.10
1.00
10.00
100.00
10.00
1.000
1.00
0.500
0.100
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
GHI)
PERYLENE,
NG/
ULBENZO(
UL
0.10
0.050
0.01
0.010
0.005
Organics,
Method
1625:
T=
1000Organics,
1000
BENZO(
K)
FLUORANTHENE,
NG/
ULBENZO(
UL
0.01
0.10
1.00
10.00
100.00
0.05
0.50
5.00
50.00
5.000
1.000
Log­
10
of
Observed
Standard
Deviation
Mon
Mar
18
16:
29:
53
2002
Log­
10
of
Spike
Concentration
c:/
pw/
ostmdl/
req004/
r004sd1.
s