Document ID: EPA-HQ-OAR-2005-0135-0007
Agency: epa
Document Type: Supporting & Related Material
Title: 
Posted Date: 2005-09-29T04:00Z

Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:

Laboratory
Contact
Person:

Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
Is
15
ppm
Sulfur
Precision
Criterion
Met?
standard
deviation
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
15
ppm
Diesel
Sulfur
Precision
Demonstration
[
DLQ001:
OMB
#
2060­
0566
Ex
REQUIRED
DATA
MISSING
Test
Method
Laboratory
Identification
REQUIRED
DATA
MISSING
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confidentiality
claim
covering
the
information
contained
in
this
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
public
by
EPA
without
further
notice.
All
questions
of
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
for
the
information
in
this
submission?
(
Note:
Please
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)

15
ppm
Sulfur
Precision
Criterion
­
a
standard
deviation
less
than
0.72
ppm,
computed
from
the
r
tests
made
over
20
days
on
samples
taken
from
a
single
homogenous
commerically
available
diese
15
ppm.
The
20
results
must
be
a
series
of
tests
with
a
sequential
record
of
the
analyses
and
no
om
exclude
a
given
sample
or
test
result
only
if
the
exclusion
is
for
a
valid
reason
under
good
laboratory
records
regarding
the
sample
and
test
results
and
the
reason
for
excluding
them.
Data
Entry
QC
Check
on
Test
Result
DATA
REQUIRED
IN
CELL
D20
DATA
REQUIRED
IN
CELL
D21
DATA
REQUIRED
IN
CELL
D22
DATA
REQUIRED
IN
CELL
D23
DATA
REQUIRED
IN
CELL
D24
DATA
REQUIRED
IN
CELL
D25
DATA
REQUIRED
IN
CELL
D26
DATA
REQUIRED
IN
CELL
D27
DATA
REQUIRED
IN
CELL
D28
DATA
REQUIRED
IN
CELL
D29
DATA
REQUIRED
IN
CELL
D30
DATA
REQUIRED
IN
CELL
D31
DATA
REQUIRED
IN
CELL
D32
DATA
REQUIRED
IN
CELL
D33
DATA
REQUIRED
IN
CELL
D34
Expires
9/
30/
2005]

e
results
of
a
minimum
of
20
repeat
sel
fuel
with
a
sulfur
range
of
5
to
omissions.
A
lab
facility
may
ory
practices
and
it
maintains
DATA
REQUIRED
IN
CELL
D35
DATA
REQUIRED
IN
CELL
D36
DATA
REQUIRED
IN
CELL
D37
DATA
REQUIRED
IN
CELL
D38
DATA
REQUIRED
IN
CELL
D39
15
ppm
Diesel
Sulfur
Accura
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:

Laboratory
Contact
Person:
Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
Is
1­
10
ppm
Sulfur
Accuracy
Criterion
Met?
Arithmetic
Average
(
ppm)

Vendor
Name
of
Gravimetric
Standard
Lot
Identification
Number
of
Gravimetric
Standard
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm)

Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
0
REQUIRED
DATA
MISSING
0
0
0
0
gravimetric
sulfur
standard
Accuracy
Criterion
for
1­
10
ppm
Test
Method
0
0
Laboratory
Identification
0
0
0
0
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
con
such
claim
is
made
the
information
may
be
made
available
to
the
public
by
EPA
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
for
the
information
in
this
s
cell.)

1
to
10
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
continuous
series
commercially
available
gravimetric
sulfur
standard
in
the
range
of
1
to
10
ppm
s
reference
value
(
ARV)
of
that
standard
by
more
than
0.54
ppm.
Individual
test
r
known
chemical
interferences.

REQUIRED
DATA
MISSING
REQUIRED
DATA
MISSING
racy
Demonstration
[
DLQ001:
OMB
#
2060­
0566
Expires
9/
30/
2005]

Is
10­
20
ppm
Sulfur
Accuracy
Criterion
Met?
Arithmetic
Average
(
ppm)
Vendor
Name
of
Gravimetric
Standard
Concentration
QC
Check
on
ARV
Lot
Identification
Number
of
Gravimetric
Standard
ARV
TOO
LOW
IN
CONCENTRATION
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm)

Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard
Data
Entry
QC
Check
on
Test
Result
Laboratory
Test
Identification
Number
Date
Time
DATA
REQUIRED
IN
CELL
D26
DATA
REQUIRED
IN
CELL
D27
DATA
REQUIRED
IN
CELL
D28
REQUIRED
DATA
MIS
gravimetric
sulfur
standard
Accuracy
Criterion
for
10­
20
ppm
confidentiality
claim
covering
the
information
contained
in
this
submission.
If
no
PA
without
further
notice.
All
questions
of
confidentiality
will
be
handled
is
submission?
(
Note:
Please
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
ies
of
at
least
10
tests
performed
on
a
sulfur
shall
not
differ
from
the
accepted
t
results
shall
be
compensated
for
any
10
to
20
ppm
Accuracy
Criterion
­
the
arithmetic
avera
performed
on
a
commercially
available
gravimetric
sulfu
shall
not
differ
from
the
accepted
reference
value
(
ARV)
Individual
test
results
shall
be
compensated
for
any
know
REQUIRED
DATA
MISS
REQUIRED
DATA
MISS
DATA
REQUIRED
IN
CELL
D29
DATA
REQUIRED
IN
CELL
D30
DATA
REQUIRED
IN
CELL
D31
DATA
REQUIRED
IN
CELL
D32
DATA
REQUIRED
IN
CELL
D33
DATA
REQUIRED
IN
CELL
D34
DATA
REQUIRED
IN
CELL
D35
Concentration
QC
Check
on
ARV
ARV
TOO
LOW
IN
CONCENTRATION
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
DATA
REQUIRED
IN
CELL
J26
DATA
REQUIRED
IN
CELL
J27
DATA
REQUIRED
IN
CELL
J28
MISSING
rage
of
a
continuous
series
of
at
least
10
tests
lfur
standard
in
the
range
of
10
to
20
ppm
sulfur
V)
of
that
standard
by
more
than
0.54
ppm.
own
chemical
interferences.

ISSING
ISSING
DATA
REQUIRED
IN
CELL
J29
DATA
REQUIRED
IN
CELL
J30
DATA
REQUIRED
IN
CELL
J31
DATA
REQUIRED
IN
CELL
J32
DATA
REQUIRED
IN
CELL
J33
DATA
REQUIRED
IN
CELL
J34
DATA
REQUIRED
IN
CELL
J35
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:

Laboratory
Contact
Person:

Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
Is
500
ppm
Sulfur
Precision
Criterion
Met?
standard
deviation
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confidentiality
claim
covering
the
information
contained
in
this
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
public
by
EPA
without
further
notice.
All
questions
of
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
for
the
information
in
this
submission?
(
Note:
Please
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)
500
ppm
Diesel
Sulfur
Precision
Demonstration
[
DLQ001:
OMB
#
2060­
0566
Ex
Test
Method
500
ppm
Sulfur
Precision
Criterion
­
a
standard
deviation
less
than
9.68
ppm,
computed
from
the
repeat
tests
made
over
20
days
on
samples
taken
from
a
single
homogenous
commerically
availabl
of
200
to
500
ppm.
The
20
results
must
be
a
series
of
tests
with
a
sequential
record
of
the
analyses
may
exclude
a
given
sample
or
test
result
only
if
the
exclusion
is
for
a
valid
reason
under
good
labo
records
regarding
the
sample
and
test
results
and
the
reason
for
excluding
them.

REQUIRED
DATA
MISSING
Laboratory
Identification
REQUIRED
DATA
MISSING
Data
Entry
QC
Check
on
Test
Result
DATA
REQUIRED
IN
CELL
D20
DATA
REQUIRED
IN
CELL
D21
DATA
REQUIRED
IN
CELL
D22
DATA
REQUIRED
IN
CELL
D23
DATA
REQUIRED
IN
CELL
D24
DATA
REQUIRED
IN
CELL
D25
DATA
REQUIRED
IN
CELL
D26
DATA
REQUIRED
IN
CELL
D27
DATA
REQUIRED
IN
CELL
D28
DATA
REQUIRED
IN
CELL
D29
DATA
REQUIRED
IN
CELL
D30
DATA
REQUIRED
IN
CELL
D31
DATA
REQUIRED
IN
CELL
D32
DATA
REQUIRED
IN
CELL
D33
DATA
REQUIRED
IN
CELL
D34
Expires
9/
30/
2005]

the
results
of
a
minimum
of
20
able
diesel
fuel
with
a
sulfur
range
es
and
no
omissions.
A
lab
facility
boratory
practices
and
it
maintains
DATA
REQUIRED
IN
CELL
D35
DATA
REQUIRED
IN
CELL
D36
DATA
REQUIRED
IN
CELL
D37
DATA
REQUIRED
IN
CELL
D38
DATA
REQUIRED
IN
CELL
D39
500
ppm
Diesel
Sulfur
Accuracy
De
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:
Laboratory
Contact
Person:
Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
Is
100­
200
ppm
Sulfur
Accuracy
Criterion
Met?

Arithmetic
Average
(
ppm):

Vendor
Name
of
Gravimetric
Standard:

Lot
Identification
Number
of
Gravimetric
Standard:

Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm):

Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard:

Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Test
Method
0
0
Laboratory
Identification
0
0
0
0
0
0
0
0
0
Accuracy
Criterion
for
100­
200
ppm
gravimetric
sulfur
standard
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confid
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)

100
to
200
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
continuous
serie
on
a
commercially
available
gravimetric
sulfur
standard
in
the
range
of
100
to
200
the
accepted
reference
value
(
ARV)
of
that
standard
by
more
than
7.26
ppm.
Indiv
compensated
for
any
known
chemical
interferences.

REQUIRED
DATA
MISSING
REQUIRED
DATA
MISSING
REQUIRED
DATA
MISSING
emonstration
[
DLQ001:
OMB
#
2060­
0566
Expires
9/
30/
2005]

Is
400­
500
ppm
Sulfur
Accuracy
Criterion
Met?

Arithmetic
Average
(
ppm)
Vendor
Name
of
Gravimetric
Standard
Concentration
QC
Check
on
ARV
Lot
Identification
Number
of
Gravimetric
Standard
ARV
TOO
LOW
IN
CONCENTRATION
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm)
Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard
Data
Entry
QC
Check
on
Test
Result
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
DATA
REQUIRED
IN
CELL
D26
DATA
REQUIRED
IN
CELL
D27
DATA
REQUIRED
IN
CELL
D28
Accuracy
Criterion
for
400­
500
ppm
gravimetric
sulfur
standard
fidentiality
claim
covering
the
information
contained
in
this
the
public
by
EPA
without
further
notice.
All
questions
of
ed
for
the
information
in
this
submission?
(
Note:
Please
answer
by
ries
of
at
least
10
tests
performed
0
ppm
sulfur
shall
not
differ
from
dividual
test
results
shall
be
400
to
500
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
c
tests
performed
on
a
commercially
available
gravimetric
sulfur
stand
ppm
sulfur
shall
not
differ
from
the
accepted
reference
value
(
ARV)
7.26
ppm.
Individual
test
results
shall
be
compensated
for
any
know
REQUIRED
DATA
MISSING
REQUIRED
DATA
MISSING
REQUIRED
DATA
MISSING
DATA
REQUIRED
IN
CELL
D29
DATA
REQUIRED
IN
CELL
D30
DATA
REQUIRED
IN
CELL
D31
DATA
REQUIRED
IN
CELL
D32
DATA
REQUIRED
IN
CELL
D33
DATA
REQUIRED
IN
CELL
D34
DATA
REQUIRED
IN
CELL
D35
Concentration
QC
Check
on
ARV
ARV
TOO
LOW
IN
CONCENTRATION
Data
Entry
QC
Check
on
Test
Result
DATA
REQUIRED
IN
CELL
J26
DATA
REQUIRED
IN
CELL
J27
DATA
REQUIRED
IN
CELL
J28
continuous
series
of
at
least
10
ndard
in
the
range
of
400
to
500
V)
of
that
standard
by
more
than
own
chemical
interferences.
DATA
REQUIRED
IN
CELL
J29
DATA
REQUIRED
IN
CELL
J30
DATA
REQUIRED
IN
CELL
J31
DATA
REQUIRED
IN
CELL
J32
DATA
REQUIRED
IN
CELL
J33
DATA
REQUIRED
IN
CELL
J34
DATA
REQUIRED
IN
CELL
J35
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:
Laboratory
Contact
Person:
Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
No
Is
15
ppm
Sulfur
Precision
Criterion
Met?
standard
deviation
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
#########
10/
26/
04
8:
00
AM
6.003
OK
#########
10/
27/
04
8:
01
AM
6.021
OK
#########
10/
28/
04
8:
20
AM
6.043
OK
#########
10/
29/
04
8:
23
AM
5.993
OK
#########
10/
30/
04
9:
00
AM
6.003
OK
#########
11/
1/
04
9:
10
AM
6.092
OK
#########
11/
2/
04
9:
20
AM
6.101
OK
#########
11/
3/
04
9:
30
AM
6.045
OK
#########
11/
5/
04
9:
40
AM
6.003
OK
#########
11/
6/
04
9:
50
AM
6.021
OK
#########
11/
7/
04
10:
00
AM
5.989
OK
#########
11/
8/
04
10:
10
AM
5.962
OK
#########
11/
9/
04
10:
20
AM
6.010
OK
#########
11/
10/
04
10:
30
AM
6.032
OK
#########
11/
11/
04
10:
40
AM
6.053
OK
15
ppm
Diesel
Sulfur
Precision
Demonstration
[
DLQ001:
OMB
#
2060­
0566
Expires
9/
30/
2005]
Test
Method
Total
Sulfur
in
Liquid
Aromatic
Hydrocarbons
and
Their
Derivatives
by
ASTM
D
6428­
99
Laboratory
Identification
USEPA
National
and
Vehicle
Fuels
Emissions
Laboratory/
OAR
2565
Plymouth
Road,
Mailcode
AATSG
Ann
Arbor
Michigan
48105
Joe
Sopata
202­
343­
9034
202­
343­
2801
sopata.
joe@
epa.
gov
PASSED
0.04
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confidentiality
claim
covering
the
information
contained
in
this
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
public
by
EPA
without
further
notice.
All
questions
of
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
for
the
information
in
this
submission?
(
Note:
Please
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)

15
ppm
Sulfur
Precision
Criterion
­
a
standard
deviation
less
than
0.72
ppm,
computed
from
the
results
of
a
minimum
of
20
repeat
tests
made
over
20
days
on
samples
taken
from
a
single
homogenous
commerically
available
diesel
fuel
with
a
sulfur
range
of
5
to
15
ppm.
The
20
results
must
be
a
series
of
tests
with
a
sequential
record
of
the
analyses
and
no
omissions.
A
lab
facility
may
exclude
a
given
sample
or
test
result
only
if
the
exclusion
is
for
a
valid
reason
under
good
laboratory
practices
and
it
maintains
records
regarding
the
sample
and
test
results
and
the
reason
for
excluding
them.
#########
11/
12/
04
10:
50
AM
6.050
OK
#########
11/
13/
04
11:
00
AM
5.989
OK
#########
11/
14/
04
11:
10
AM
6.033
OK
#########
11/
15/
04
11:
20
AM
5.939
OK
#########
11/
16/
04
11:
30
AM
6.042
OK
15
ppm
Diesel
Sulfur
Accuracy
Demonstration
[
DLQ001:
OMB
#
206
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:
Laboratory
Contact
Person:
Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
Is
1­
10
ppm
Sulfur
Accuracy
Criterion
Met?
Arithmetic
Average
(
ppm)
Vendor
Name
of
Gravimetric
Standard
Lot
Identification
Number
of
Gravimetric
Standard
Concentration
QC
Check
on
ARV
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm)
OK
Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
#########
1/
13/
05
8:
00
AM
7.341
OK
#########
1/
13/
05
8:
30
AM
7.562
OK
#########
1/
13/
05
9:
00
AM
7.894
OK
Test
Method
Total
Sulfur
in
Liquid
Aromatic
Hydrocarbons
and
Their
Derivatives
by
Oxid
ASTM
D
6428­
99
Laboratory
Identification
USEPA
National
and
Vehicle
Fuels
Emissions
Laboratory/
OAR
2565
Plymouth
Road,
Mailcode
AATSG
Ann
Arbor
Michigan
48105
Joe
Sopata
202­
343­
9034
202­
343­
2801
sopata.
joe@
epa.
gov
Accuracy
Criterion
for
1­
10
ppm
gravimetric
sulfur
standard
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confidentiality
claim
coverin
contained
in
this
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
pub
notice.
All
questions
of
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claim
this
submission?
(
Note:
Please
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)

1
to
10
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
continuous
series
of
at
least
10
tests
performed
on
a
commercially
available
gravimetric
sulfur
standard
in
the
range
of
1
to
10
ppm
sulfur
shall
not
differ
from
the
accepted
reference
value
(
ARV)
of
that
standard
by
more
than
0.54
ppm.
Individual
test
results
shall
be
compensated
for
any
known
chemical
interferences.

PASSED
7.95
NIST
ALDS45678
8.00
0.0515
#########
1/
13/
05
9:
30
AM
8.219
OK
#########
1/
13/
05
10:
00
AM
8.234
OK
#########
1/
13/
05
10:
30
AM
8.100
OK
#########
1/
13/
05
11:
00
AM
8.114
OK
#########
1/
13/
05
11:
30
AM
7.989
OK
#########
1/
13/
05
12:
00
PM
7.687
OK
#########
1/
13/
05
12:
30
PM
8.345
OK
2060­
0566
Expires
9/
30/
2005]

No
Is
10­
20
ppm
Sulfur
Accuracy
Criterion
Met?
Arithmetic
Average
(
ppm)
Vendor
Name
of
Gravimetric
Standard
Lot
Identification
Number
of
Gravimetric
Standard
Concentration
QC
Check
on
ARV
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm)
OK
Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
#########
1/
14/
05
8:
00
AM
13.239
OK
#########
1/
14/
05
8:
30
AM
14.231
OK
#########
1/
14/
05
9:
00
AM
13.899
OK
xidative
and
Electrochemical
Detection
Accuracy
Criterion
for
10­
20
ppm
gravimetric
sulfur
standard
ring
the
information
ublic
by
EPA
without
further
imed
for
the
information
in
10
to
20
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
continuous
series
of
at
least
10
tests
performed
on
a
commercially
available
gravimetric
sulfur
standard
in
the
range
of
10
to
20
ppm
sulfur
shall
not
differ
from
the
accepted
reference
value
(
ARV)
of
that
standard
by
more
than
0.54
ppm.
Individual
test
results
shall
be
compensated
for
any
known
chemical
interferences.

PASSED
13.91
NIST
ALDS53478
13.50
0.4075
#########
1/
14/
05
9:
30
AM
14.035
OK
#########
1/
14/
05
10:
00
AM
14.001
OK
#########
1/
14/
05
10:
30
AM
13.980
OK
#########
1/
14/
05
11:
00
AM
13.211
OK
#########
1/
14/
05
11:
30
AM
14.345
OK
#########
1/
14/
05
12:
00
PM
13.678
OK
#########
1/
14/
05
12:
30
PM
14.456
OK
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:

Laboratory
Contact
Person:

Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
No
Is
500
ppm
Sulfur
Precision
Criterion
Met?
standard
deviation
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
#########
10/
26/
04
8:
00
AM
330.023
OK
#########
10/
27/
04
8:
01
AM
331.234
OK
#########
10/
28/
04
8:
20
AM
332.897
OK
#########
10/
29/
04
8:
23
AM
334.598
OK
#########
10/
30/
04
9:
00
AM
335.998
OK
#########
11/
1/
04
9:
10
AM
328.359
OK
#########
11/
2/
04
9:
20
AM
329.062
OK
#########
11/
3/
04
9:
30
AM
330.108
OK
#########
11/
5/
04
9:
40
AM
333.730
OK
#########
11/
6/
04
9:
50
AM
335.092
OK
#########
11/
7/
04
10:
00
AM
326.340
OK
500
ppm
Diesel
Sulfur
Precision
Demonstration
[
DLQ001:
OMB
#
2060­
0566
Expires
9/
30/
2005]
Test
Method
Standard
Test
Method
for
Sulfur
in
Petroleum
Products
by
Wavelength
ASTM
D
2622­
03
Laboratory
Identification
USEPA
National
and
Vehicle
Fuels
Emissions
Laboratory/
OAR
2565
Plymouth
Road,
Mailcode
AATSG
Ann
Arbor
Michigan
48105
Joe
Sopata
202­
343­
9034
202­
343­
2801
sopata.
joe@
epa.
gov
PASSED
4.49
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confidentiality
claim
covering
the
information
contained
in
this
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
public
by
EPA
without
further
notice.
All
questions
of
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
for
the
information
in
this
submission?
(
Note:
Please
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)

500
ppm
Sulfur
Precision
Criterion
­
a
standard
deviation
less
than
9.68
ppm,
computed
from
the
results
of
a
minimum
of
20
repeat
tests
made
over
20
days
on
samples
taken
from
a
single
homogenous
commerically
available
diesel
fuel
with
a
sulfur
range
of
200
to
500
ppm.
The
20
results
must
be
a
series
of
tests
with
a
sequential
record
of
the
analyses
and
no
omissions.
A
lab
facility
may
exclude
a
given
sample
or
test
result
only
if
the
exclusion
is
for
a
valid
reason
under
good
laboratory
practices
and
it
maintains
records
regarding
the
sample
and
test
results
and
the
reason
for
excluding
them.
#########
11/
8/
04
10:
10
AM
328.903
OK
#########
11/
9/
04
10:
20
AM
329.863
OK
#########
11/
10/
04
10:
30
AM
332.998
OK
#########
11/
11/
04
10:
40
AM
334.001
OK
#########
11/
12/
04
10:
50
AM
340.100
OK
#########
11/
13/
04
11:
00
AM
341.102
OK
#########
11/
14/
04
11:
10
AM
339.887
OK
#########
11/
15/
04
11:
20
AM
338.776
OK
#########
11/
16/
04
11:
30
AM
340.002
OK
500
ppm
Diesel
Sulfur
Accuracy
Demonstration
[
DLQ001:
OMB
#
2060
Name
of
Method:
Organization
ID
No.:

Laboratory
Name:
Laboratory
Street
Address:
Laboratory
City:
Laboratory
State:
Laboratory
Zip
code:
Laboratory
Contact
Person:
Laboratory
Contact
Phone
Number
Laboratory
Contact
Facsimile
Number
Laboratory
Contact
E­
mail
Address
Is
100­
200
ppm
Sulfur
Accuracy
Criterion
Met?
Arithmetic
Average
(
ppm):
Vendor
Name
of
Gravimetric
Standard:
Lot
Identification
Number
of
Gravimetric
Standard:
Concentration
QC
Check
on
ARV
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm):
OK
Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard:

Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
#########
1/
13/
05
8:
00
AM
150.003
OK
#########
1/
13/
05
8:
30
AM
150.030
OK
#########
1/
13/
05
9:
00
AM
150.100
OK
USEPA
National
and
Vehicle
Fuels
Emissions
Laboratory/
OAR
2565
Plymouth
Road,
Mailcode
AATSG
Ann
Arbor
Michigan
Test
Method
Standard
Test
Method
for
Sulfur
in
Petroleum
Products
by
Wavelength
Dispersive
ASTM
D
2622­
03
Laboratory
Identification
48105
gravimetric
sulfur
standard
Accuracy
Criterion
for
100­
200
ppm
Joe
Sopata
202­
343­
9034
202­
343­
2801
sopata.
joe@
epa.
gov
Confidential
Business
Information
Claim.
A
company
may
assert
a
business
confidentiality
claim
covering
the
in
submission.
If
no
such
claim
is
made
the
information
may
be
made
available
to
the
public
by
EPA
without
furthe
confidentiality
will
be
handled
pursuant
to
40
CFR
Part
2.
Is
confidentiality
claimed
for
the
information
in
this
sub
answer
by
typing
"
Yes"
or
"
No"
in
the
adjacent
cell.)

NIST
AMD4567
151.00
0.4357
100
to
200
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
continuous
series
of
at
least
10
tests
performed
on
a
commercially
available
gravimetric
sulfur
standard
in
the
range
of
100
to
200
ppm
sulfur
shall
not
differ
from
the
accepted
reference
value
(
ARV)
of
that
standard
by
more
than
7.26
ppm.
Individual
test
results
shall
be
compensated
for
any
known
chemical
interferences.

150.56
PASSED
#########
1/
13/
05
9:
30
AM
149.650
OK
#########
1/
13/
05
10:
00
AM
148.500
OK
#########
1/
13/
05
10:
30
AM
150.000
OK
#########
1/
13/
05
11:
00
AM
150.100
OK
#########
1/
13/
05
11:
30
AM
151.910
OK
#########
1/
13/
05
12:
00
PM
152.130
OK
#########
1/
13/
05
12:
30
PM
153.220
OK
060­
0566
Expires
9/
30/
2005]

No
Is
400­
500
ppm
Sulfur
Accuracy
Criterion
Met?
Arithmetic
Average
(
ppm)
Vendor
Name
of
Gravimetric
Standard
Lot
Identification
Number
of
Gravimetric
Standard
Concentration
QC
Check
on
ARV
Accepted
Reference
Value
(
ARV)
of
Gravimetric
Standard
(
ppm)
OK
Difference
between
Arithmetic
Average
and
ARV
of
Gravimetric
Standard
Laboratory
Test
Identification
Number
Date
Time
Test
Result
(
ppm)
Data
Entry
QC
Check
on
Test
Result
#########
1/
14/
05
8:
00
AM
499.980
OK
#########
1/
14/
05
8:
30
AM
498.970
OK
#########
1/
14/
05
9:
00
AM
496.451
OK
ve
X­
ray
Fluorescence
Spectrometry
gravimetric
sulfur
standard
Accuracy
Criterion
for
400­
500
ppm
information
contained
in
this
her
notice.
All
questions
of
ubmission?
(
Note:
Please
500.00
1.6047
400
to
500
ppm
Accuracy
Criterion
­
the
arithmetic
average
of
a
continuous
series
of
at
least
10
tests
performed
on
a
commercially
available
gravimetric
sulfur
standard
in
the
range
of
400
to
500
ppm
sulfur
shall
not
differ
from
the
accepted
reference
value
(
ARV)
of
that
standard
by
more
than
7.26
ppm.
Individual
test
results
shall
be
compensated
for
any
known
chemical
interferences.

NIST
MNV5678
498.40
PASSED
#########
1/
14/
05
9:
30
AM
498.670
OK
#########
1/
14/
05
10:
00
AM
495.980
OK
#########
1/
14/
05
10:
30
AM
497.560
OK
#########
1/
14/
05
11:
00
AM
499.450
OK
#########
1/
14/
05
11:
30
AM
497.890
OK
#########
1/
14/
05
12:
00
PM
499.012
OK
#########
1/
14/
05
12:
30
PM
499.990
OK