cometadata/datacite-titles-descriptions-related-identifiers huggingface dataset:
DOI: 10.21950/qqip3y
title: Exploring Adsorption Performance of Functionalized Mesoporous Silicas with a Different Pore Structure as Strong Cation-Exchange Sorbents for Solid-Phase Extraction of Atropine and Scopolamine

description: This database includes information on the optimal parameters for mass spectrometry detection in MRM mode for the analysis of atropine and scopolamine using the UHPLC-TQ-MS/MS method developed in this work. It also details the textural properties and functionalization degree of the prepared functionalized mesoporous silicas. The Extracted Ion Chromatograms (EIC) of the most intense product ions and Mass Spectra (MS2) obtained for atropine and scopolamine are presented. Additionally, results from X-ray diffraction, transmission electron microscopy, scanning electron microscopy, nitrogen adsorption–desorption, Fourier-transform infrared spectroscopy, 29Si solid-state nuclear magnetic resonance spectroscopy, and elemental analysis are included. The different types of interactions that may occur between tropane alkaloids (TAs) and the MCM-41-SO3H sorbent used for solid-phase extraction are described. Finally, these materials were evaluated as sorbents for strong cation-exchange solid-phase extraction (SPE), determining their efficiency in the adsorption and desorption of tropane alkaloids (atropine and scopolamine).
description: In this work, mesoporous silicas with two types of mesoporous structures were synthesized and functionalized with sulfonic acid groups: MCM-41-SO3H (honeycomblike hexagonal structure) and MSU-2-SO3H (three-dimensional porous structure with wormhole pores). The synthesized materials were characterized by X-ray diffraction, transmission electron microscopy, scanning electron microscopy, nitrogen adsorption–desorption, Fourier-transform infrared spectroscopy, 29Si solid-state nuclear magnetic resonance spectroscopy, and elemental analysis. The obtained functionalized materials were evaluated as sorbents for strong cation-exchange solid-phase extraction (SPE) to determine their efficiency in the adsorption and desorption of tropane alkaloids (atropine and scopolamine). The loading solvents, loading volume, analyte concentration, and elution volume were studied, using 50 mg of both materials. Analyses were carried out by ultra-high performance liquid chromatography coupled to triple quadrupole tandem mass spectrometry. The synthesized MCM-41-SO3H material presented the highest recovery efficiency and has proven to be a promising sorbent for strong cation-exchange SPE of atropine and scopolamine in aqueous media. The high degree of functionalization of MCM-41-SO3H and the high accessibility of the sulfonic groups for the target analytes, due to the regularity and uniformity of their pores, maximize the contact between the alkaloids and the sorbent, favoring efficient adsorption.
description: Excel
DOI: 10.13130/rd_unimi/qa4bro/ob383z
title: 250408_OPT1_TensileTest_1106.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1106.tif
DOI: 10.21950/vghsmk
title: Analytical Strategies for Green Extraction, Characterization, and Bioactive Evaluation of Polyphenols, Tocopherols, Carotenoids, and Fatty Acids in Agri-Food Bio-Residues

description: This database includes the results of the Figure 1. Documents by year found in Scopus
using the sequence of keywords described in the methodology (a). VOSviewer software plot showing the co-ocurrence of keywords in the 618 documents found in Scopus related to this study (2013-2024) (b); Figure 2. Classification and structure of principal phenolic families: phenolic acids (red color), flavonoids (orange color), lignans (purple color), tannins (green color) and stilbenes (yellow color); Figure 3. Classification and structure of tocopherols, carotenoids, and fatty acids; Table 1. Phenolic compounds, tocopherols, carotenoids and fatty acids from primary agri-food waste sources; Figure 4. Main extraction techniques for sustainable recovery of bioactive compounds from agri-food bio-residues; Table 2. TPC and major polyphenols or families found in agri-food bio-residues; Table 3. Mayor tocopherols, carotenoids and fatty acids found in agri-food bio-residues; Table 4. Methods and bioactive properties of agri-food bio-residues; Figure 5. Established and innovative industrial applications of polyphenols, carotenoids, tocopherols, and fatty acids
description: Recent advancements in analytical strategies have enabled the efficient extraction
and characterization of bioactive compounds from agri-food bio-residues, emphasizing
green chemistry and circular economy principles. This review highlights the valorization of several agri-food bio-residues for the extraction of high-value-added bioactive compounds, particularly polyphenols, tocopherols, carotenoids, and fatty acids, as a biorefinery approach. To this end, the adoption of environmentally friendly extraction technologies is essential to improve performance, reduce energy consumption, and minimize costs. This study therefore examines emerging methodologies such as supercritical fluid extraction, pressurized liquid extraction, pulsed electric fields, and matrix solid-phase dispersion, highlighting their advantages and limitations. Additionally, the chemical characterization of these bioactive compounds is explored through spectrophotometric and high-resolution chromatographic techniques, crucial for their accurate identification and quantification.
This is complemented by an analysis of bioactivity assays evaluating antioxidant, antimicrobial, anticancer, neuroprotective, and anti-inflammatory properties, with a focus on their applications in the food, pharmaceutical, and cosmetic industries. However, the analytical control of toxic compounds, such as alkaloids, in these bio-residues is undoubtedly needed. Ultimately, this approach not only promotes sustainability but also contributes to the development of eco-friendly solutions in various industries.
description: Excel
DOI: 10.25549/inscriptifact-ouc15256390
title: Glyptic Scarab Seal

description: [Text Description:] Two stylized clumps of papyrus flank ❧ cartouche which contains ❧ dots. ❧ [Excavation Description:] Gifted to the Los Angeles County Museum of Art by Ruth Greenberg ❧ [Medium:] Stone ❧ [Script Note:] Hieroglyphs ❧ [Physical Object Description:] Steatite w/dark turquoise glaze ❧ [Physical Object Note:] L: 1.42cm; H: .66cm; W: 1.08cm
DOI: 10.25549/inscriptifact-ouc15264606
title: Blue glass scarab with horses 2

description: [Text Description:] Blue glass scarab with horses 2 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Glass ❧ [Physical Object Description:] Blue glass scarab seal, 2.6 cm x 1.93 cm
DOI: 10.13130/rd_unimi/qa4bro/17wbc9
title: 250408_OPT1_TensileTest_1107.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1107.tif
DOI: 10.13130/rd_unimi/qa4bro/jgdqab
title: 250408_OPT1_TensileTest_1108.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1108.tif
DOI: 10.21950/9uf1eb
title: Códigos TFM e Investigación Posterior - Alejandro Redondo García

description: Códigos Deep Learning (entrenamiento y predicción) de un clasificador de la gravedad de lesiones orales - TFM Alejandro Redondo García. En los ficheros encontramos dos carpetas (si seleccionamos la visualización del árbol en la web). 

1. Codigo_InvestigacionPosteriorTFM. Esta carpeta contiene lo siguiente: archivo ClasificadorLesionesOrales_CrossValidation.py - es el código en python del clasificador de Deep Learning con cross validation, archivo GenerarCSV.py - es el código en python para generar el .csv, archivo Manual.pdf - son las instrucciones para ejecutar el código ClasificadorLesionesOrales_CrossValidation.py, archivo modelosTimm.csv - son los modelos disponibles de clasificación, archivo PrediccionClasificadorLesionesOrales.py - es el código para realizar la inferencia del modelo entrenado, carpeta DatasetCross - contiene un ejemplo del formato del dataset que necesita el código ClasificadorLesionesOrales_CrossValidation.py y carpeta Resultados - es un ejemplo de resultado que arroja del modelo entrenado, concretamente se guardan las métricas, la configuración y los pesos del modelo.

2. Codigo_TFM. Esta carpeta contiene lo siguiente: archivo ClasificadorLesionesOrales.py - es el código en python del clasificador de Deep Learning sin cross validation, archivo Manual.pdf - son las instrucciones para ejecutar el código ClasificadorLesionesOrales.py, archivo modelosTimm.csv - son los modelos disponibles de clasificación, archivo PrediccionClasificadorLesionesOrales.py - es el código para realizar la inferencia del modelo entrenado, carpeta Dataset - contiene un ejemplo del formato del dataset que necesita el código ClasificadorLesionesOrales.py, carpeta Predicciones - contiene un ejemplo de la inferencia del modelo y carpeta Resultados - es un ejemplo de resultado que arroja del modelo entrenado, concretamente se guardan las métricas, la configuración y los pesos del modelo.

Nota.: Es recomendable leer los manuales antes de utilizar los códigos.
DOI: 10.13130/rd_unimi/qa4bro/bup9sk
title: 250408_OPT1_TensileTest_1109.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1109.tif
DOI: 10.21950/opy68c
title: Barreras y oportunidades para la implementación de biorrefinerías
title: Un estudio longitudinal sobre aceptación social en la Comunidad de Madrid (España)

description: Este grupo de documentos contiene el dataset completo y materiales metodológicos del estudio longitudinal sobre aceptación social de biorrefinerías en la Comunidad de Madrid (2022-2024), desarrollado dentro del proyecto eCOMCIENCIA (PID2021-127019OB-I00) y los proyectos de la Comunidad de Madrid BIVALIA-CM (TEC-2024/BIO-177) y BIOTRES-CM (S2018/EMT-4344). Proporciona información detallada sobre actitudes públicas y aceptación de la sostenibilidad, biocombustibles y biorrefinerías en la región de Madrid. Incluye: 

1) Documento metodológico detallado con fundamentación teórica y procedimientos de análisis estadístico
2) Cuestionario completo con 22 ítems (versiones en español e inglés)
3) Dataset completo con 1.000 encuestas válidas distribuidas en dos oleadas (octubre 20-31, 2022 y noviembre 1-5, 2024) en formatos .csv y .sav
4) Libro de códigos con descripción de todas las variables
5) Ficheros .spv con las salidas de análisis estadísticos por pregunta del cuestionario
6) Informes detallados de los análisis por bloque temático (sociodemográfico, actitudes hacia sostenibilidad, percepción de separación y tratamiento de residuos, aceptación de biocombustibles y aceptación de biorrefinerías)
Los datos fueron recogidos mediante encuesta CAWI dirigida a residentes de Madrid mayores de 18 años y han sido anonimizados para garantizar el cumplimiento de las regulaciones de protección de datos. 
Este material constituye un recurso de utilidad para investigadores interesados en temas de aceptación social de tecnologías energéticas, energías renovables y transición energética sostenible.
description: SPSS
DOI: 10.25549/inscriptifact-ouc15264604
title: Ostracon 12

description: [Text Description:] Ostracon 12 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Clay ❧ [Script Note:] Hebrew or Aramaic ❧ [Physical Object Description:] Ostracon, 5.45 cm x 5.45 cm
DOI: 10.13130/rd_unimi/qa4bro/vcjvac
title: 250408_OPT1_TensileTest_111.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_111.tif
DOI: 10.25549/inscriptifact-ouc15264571
title: Ostracon 8

description: [Text Description:] Ostracon 8 ❧ [Text or Publication Number Note:] Lemaire Aramaic 1 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Clay ❧ [Script Note:] Aramaic ❧ [Physical Object Description:] Ostracon, 5.6 cm x 5.2 cm(average length and width) five-sided
DOI: 10.13130/rd_unimi/qa4bro/lmhsjx
title: 250408_OPT1_TensileTest_1110.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1110.tif
DOI: 10.21950/93syme
title: Synbiotic administration improves systemic and vascular alterations in rats with experimental microsurgical extrahepatic cholestasis: Role of perivascular mesenteric innervation

description: &lt;p&gt;Effect of synbiotic supplementation on the body alterations in a rat model of liver colestasis.&lt;/p&gt;
&lt;p&gt;This dataset is supplementary material for the paper: "Synbiotic administration improves systemic and vascular alterations in rats with experimental microsurgical extrahepatic cholestasis: role of perivascular mesenteric innervation". It contains 6 tables and 7 figures.&lt;/p&gt;
&lt;ul&gt;
&lt;p&gt;Background&lt;/p&gt;
&lt;p&gt;Liver cholestasis is marked by bile acid accumulation in the liver, along with renal issues, portal hypertension, and altered circulation. Previous studies suggest that synbiotics may improve systemic and hemodynamic conditions in liver diseases.&lt;/p&gt;

&lt;p&gt;Objective&lt;/p&gt;
&lt;p&gt;This study investigated the effects of a commercial synbiotic on gut microbiota, liver and kidney function, and vascular changes in a cholestatic rat model, focusing on nerve functions in the superior mesenteric arteries.&lt;/p&gt;

&lt;/p&gt;Methodology&lt;/p&gt;
&lt;p&gt;Adult Wistar rats were divided into three groups: Sham-operated, Cholestatic, and Cholestatic with synbiotic supplementation for 3 weeks. Liver colestasis was induced by surgical techniques. Blood pressure was measured using tail-cuff method.Liver and renal structure were determined using histological techniques (hematoxilin-eosin tinction). Liver and renal parameters in serum were measured using spectrophotometrical techniques. Short chain fatty acids were determined through liquid chromatography. Gene expression in kidney and fecal simples were determined by qRT-PCR. Vasomotor responses in superior mesenteric artery were determined by vascular reactivity techniques (organ bath).Neurotransmitter and endotoxin releases were measured using enzymeinmunoassay and fluorescence techniques. Protein expression was measured using western blot.&lt;/p&gt;
&lt;/ul&gt;
description: LabChart
description: GraphPad Prism, 8.2
DOI: 10.13130/rd_unimi/qa4bro/qdxhar
title: 250408_OPT1_TensileTest_1111.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1111.tif
DOI: 10.21950/tmowy4
title: Bird mortality on high-speed railways: Lessons from two large contrasting species

description: &lt;p&gt;Collisions are the chief effect of transport infrastructures on vertebrate populations but their relevance in high-speed railways (HSR) is largely unknown. We analyzed Great Bustard (Otis tarda) and Eurasian Eagle-owl (Bubo bubo) mortality along two 5-km stretches of a Spanish HSR. Five fresh bustard and 10 owl carcasses were collected during 40 weeks of monitoring over two years, plus older remains of 14 bustards and 17 owls more. Relevant mortalities of both bird species thus occur, and differences in local use of the infrastructure explain their spatial patterns. Bustards die at points where they fly across optimizing their local movements according to MaxEnt models, while owls die while hunting the abundant rabbits present in railway verges as pointed by camera trapping. Impact prediction, evaluation and mitigation must therefore accommodate to species’ characteristics.&lt;/p&gt;
description: Methodology:
Two types of data:

Coordinates of Great bustard observations used as input for MaxEnt models of probability of presence for the species.
Data from trainkills corresponding to great bustard (Otis tarda) and Eagle owl (Bubo bubo) collected along two years of railway monitoring.
DOI: 10.25549/inscriptifact-ouc15264572
title: Ostracon 1

description: [Text Description:] Ostracon 1 ❧ [Text or Publication Number Note:] Lemaire Aramaic 6 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Clay ❧ [Script Note:] Aramaic ❧ [Physical Object Description:] Ostracon, 5.2 cm x 6.5 cm (average length and width)
DOI: 10.25549/inscriptifact-ouc15264594
title: Blue glass scarab with horses 1

description: [Text Description:] Blue glass scarab with horses 1 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Glass ❧ [Physical Object Description:] Blue glass scarab seal, 2.8 cm x 2.15 cm
DOI: 10.13130/rd_unimi/qa4bro/ot7w7b
title: 250408_OPT1_TensileTest_1112.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1112.tif
DOI: 10.21950/ejycrm
title: Firm-Level Panel on Climate, Economic, and Financial Data in Spain

description: &lt;p&gt;This dataset merges firm-level financial data from the SABI database with climatic and macro-financial variables to assess the effects of climate change on business performance across five climate-sensitive sectors in Spain: Construction, Water, Agriculture, Energy, and Transport.&lt;/p&gt;

&lt;p&gt;It covers annual data from 2001 to 2020 and includes variables such as firm revenues, employment, capital, and material expenditures. It also incorporates biophysical indicators (e.g. seasonal temperatures, precipitation, droughts, and heatwaves) and macro-financial variables at the national level (e.g. interest rates, credit-to-GDP ratios, real effective exchange rate, and commodity indices).&lt;/p&gt;
description: &lt;p&gt;Description of the project&lt;/p&gt;
&lt;p&gt;This project proposes a methodology based on sustainable finance to assess the climate vulnerability of key economic sectors in Spain. It builds a panel dataset combining biophysical, economic, and financial information to analyse how firm revenues respond to climate conditions.&lt;/p&gt;

&lt;p&gt;The study produces 10-year projections of financial and economic variables under the RCP4.5 scenario, aligned with the EU’s 2030 climate policy. The approach incorporates uncertainty through confidence intervals, providing insight into the interaction between climate risks and financial performance.&lt;/p&gt;
DOI: 10.13130/rd_unimi/qa4bro/mpgrbt
title: 250408_OPT1_TensileTest_1113.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1113.tif
DOI: 10.13130/rd_unimi/qa4bro/zdmwjz
title: 250408_OPT1_TensileTest_1114.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1114.tif
DOI: 10.21950/ihgbea
title: Decision support system in multimorbidity and polypharmacy: usability and cognitive load of primary care physicians

description: Objetivo: Evaluar la eficiencia de la usabilidad de un sistema de apoyo a la toma de decisiones (SAD) para médicos de atención primaria (MAP) que gestionan pacientes con multimorbilidad y polifarmacia.
Materiales y métodos: Estudio descriptivo transversal de usabilidad. La población de estudio fueron PCP con práctica asistencial activa en multimorbilidad y sin experiencia previa en el uso de la herramienta DSS. La variable principal fue la eficiencia de la usabilidad, medida por el tiempo de finalización de la tarea y las métricas de carga cognitiva (cuestionario NASA-TLX, métricas de seguimiento ocular y número de clics realizados). Se evaluaron nueve tareas basadas en un caso clínico simulado.
description: STATA
DOI: 10.25549/inscriptifact-ouc15264565
title: Ostracon 1

description: [Text Description:] Ostracon 1 ❧ [Text or Publication Number Note:] Lemaire Aramaic 6 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Clay ❧ [Script Note:] Aramaic ❧ [Physical Object Description:] Ostracon, 5.2 cm x 6.5 cm (average length and width)
DOI: 10.25549/inscriptifact-ouc15264587
title: Ostracon 10

description: [Text Description:] Ostracon 10 ❧ [Excavation Description:] unprovenanced ❧ [Medium:] Clay ❧ [Script Note:] Hebrew or Aramaic ❧ [Physical Object Description:] Ostracon, 5 sided shape, 7.28 cm x 7.15 cm
DOI: 10.13130/rd_unimi/qa4bro/2c3ub1
title: 250408_OPT1_TensileTest_1115.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1115.tif
DOI: 10.21950/ajsmci
title: Thermus thermophilus TnSeq

description: &lt;p&gt;In this study we develop a procedure for thermostable selection of random insertion mutants based on a gene cassette encoding a thermostable resistance to kanamycin flanked by the recognition sites (ME sites) for Tn5 transposase. The transposition library generated in vitro was initialy transformed in a PrimPol mutant HB27 derivative (ppol), which shows ~2 log fold transformation efficiency. This allowed the generation of the generation of a large library of insertion mutants (“Mother”), which was later transferred to a wild type HB27 strain (“Daughter”). Both libraries were sequenced straightforward and after several culture passages. See the manuscript for more details.&lt;/p&gt;
&lt;p&gt;This dataset contains the raw data of the sequencing libraries as well as the GitHub repository containing the scrips and reports from the analysis.&lt;/p&gt;
description: Methodology:
Genomic DNA extracted from pooled libraries was processed for Tn-seq (see manuscript) and the sequencing was performed using an Illumina MiSeq system with 150 cycles.
Briefly, filtered and trimmed reads were mapped against HB27 assembly GCA_000008125 using Bowtie2 2.5.1 (with --very-sensitive option). 
We considered only Tn-seq insertions derived from reads mapping within the 10-90% interval of each gene to avoid issues with truncated or chimeric proteins. Tn insertion counts are derived from read mapping coordinates, normalized by the total mapped reads in coding regions. We use a log2 transformation to manage pseudocounts and scale the data with the R function scale() to obtain a Z-score, facilitating sample comparison. 
To analyze the gene scores, we compared PAM, Kmeans and DBSCAN clustering methods using the R packages cluster, factoextra and dbscan, respectively. The best results by highest average silhouette width were obtained for a Kmeans clustering in two main groups. Then, the large group with less insertion rate was split into two groups by shortlisting the 20% of genes with lower Z-score, obtaining the three groups of Less Permissive, Intermediate and Highly Permissive genes. 
Finally, gene insertion rates were analyzed in the context of gene conservation and available data of both essential genes in other prokaryotic organisms and Thermus thermophilus transcription data.
description: R, v.4.4.1
description: R Studio, v.2024.12.0
description: Quarto
DOI: 10.21950/czijwk
title: Microstructure and corrosion behavior of 316L stainless steel lattice and bulk parts manufactured by LPBF using fiber and CO2 lasers

description: The metadata supporting this article includes material characterization such as microstructure, hardness, polarization resistance data, tafel and cyclic curves and EIS tests.
description: Excel
description: Origin software
description: NOVA
description: AISI 316L stainless steel lattices were manufactured using two distinct Laser Powder Bed Fusion (LPBF) techniques: a commercial printer equipped with a fiber laser and a novel system equipped with a CO2 laser. Fiber laser systems produce parts exhibiting superior detail, finer cell size, and lower porosity compared to CO2 laser ones because of the stability of the laser beam and the higher absorptivity of the laser light by the material powder. Electrochemical tests indicated that lattices exhibited inferior corrosion resistance compared to solid counterparts for both manufacturing techniques. This disparity is caused by the distinct corrosion mechanisms exhibited by lattices and solid parts, as observed through Electrochemical Impedance Spectroscopy (EIS). The observed differences are attributed not only to the increased different specific surface areas but also to the distinctive morphologies formed in the material beneath the surface. CO2 LPBF lattices demonstrated higher corrosion sensitivity than the fiber LPBF lattices due to their distinct microstructure and the more prevalent presence of defects.
DOI: 10.13130/rd_unimi/qa4bro/q9j2qi
title: 250408_OPT1_TensileTest_1116.tif

description: 250729_EXPERIMENTAL_DATA/250408_OPT1_Video 250408_OPT1_TensileTest_1116.tif