cometadata/datacite-titles-descriptions-related-identifiers huggingface dataset:
DOI: 10.17188/1275215
title: Materials Data on Rb by Materials Project

description: Rb is Magnesium tetraboride-derived structured and crystallizes in the orthorhombic C222_1 space group. The structure is three-dimensional. there are seven inequivalent Rb sites. In the first Rb site, Rb is bonded in a 9-coordinate geometry to nine Rb atoms. There are a spread of Rb–Rb bond distances ranging from 4.84–5.08 Å. In the second Rb site, Rb is bonded in a 7-coordinate geometry to seven Rb atoms. There are a spread of Rb–Rb bond distances ranging from 4.69–5.05 Å. In the third Rb site, Rb is bonded in a 4-coordinate geometry to ten Rb atoms. There are a spread of Rb–Rb bond distances ranging from 4.86–5.21 Å. In the fourth Rb site, Rb is bonded in a 8-coordinate geometry to eight Rb atoms. There are a spread of Rb–Rb bond distances ranging from 4.80–5.07 Å. In the fifth Rb site, Rb is bonded in a 8-coordinate geometry to eight Rb atoms. There are a spread of Rb–Rb bond distances ranging from 4.43–5.00 Å. In the sixth Rb site, Rb is bonded in a 5-coordinate geometry to nine Rb atoms. The Rb–Rb bond length is 4.83 Å. In the seventh Rb site, Rb is bonded to eight Rb atoms to form distorted corner-sharing RbRb8 hexagonal bipyramids. The Rb–Rb bond length is 4.30 Å.
DOI: 10.6084/m9.figshare.13490232
title: PollenDiameter-FINAL.csv

description: Pollen grain diameters from <i>Citrullus lanatus, Cucurbits maxima, Cucurbita moschata, Cucurbita pepo, Delosperma cooperi, Typha</i> spp., and <i>Trifolium incarnatum</i> were measured using a Zeiss Axio Imager.A1 microscope (Zeiss, Jena, Germany) outfitted with a Jenoptik ProgRes<sup>®</sup> C3 camera with ProgRes<sup>®</sup> CapturePro software (both Jenoptik AG, Jena, Germany). For each species of pollen, approximately 1.5 mg of previously frozen pollen was placed on a concave slide, mixed with 50% glycerol, and covered with a cover slip. Ten pollen grains were chosen haphazardly and the diameter of each grain was measured using the ProgRes<sup>®</sup> CapturePro software “Measure” module in two directions, one perpendicular to the other. Both diameter measurements were used in a cluster analysis to group species by pollen diameter.<br><b>TYPE:</b> abbreviation of plant species<b>M1final:</b> Diameter length 1 in microns (μm)<b>M2final:</b> Diameter length 2 in microns (μm)<b>SIZE1:</b> Designation of pollen grain as "Small" or "Large" based on k-means cluster analysis<b>SIZE2:</b> Designation of pollen grain as "Small" or "Large" based on <i>k</i>-means cluster analysis with "<i>Typha</i>" pollen labeled separately due to the difference in performance of <i>P. mexicanus</i> on this pollen diet.<br>
DOI: 10.6084/m9.figshare.13490232.v1
title: PollenDiameter-FINAL.csv

description: Pollen grain diameters from <i>Citrullus lanatus, Cucurbits maxima, Cucurbita moschata, Cucurbita pepo, Delosperma cooperi, Typha</i> spp., and <i>Trifolium incarnatum</i> were measured using a Zeiss Axio Imager.A1 microscope (Zeiss, Jena, Germany) outfitted with a Jenoptik ProgRes<sup>®</sup> C3 camera with ProgRes<sup>®</sup> CapturePro software (both Jenoptik AG, Jena, Germany). For each species of pollen, approximately 1.5 mg of previously frozen pollen was placed on a concave slide, mixed with 50% glycerol, and covered with a cover slip. Ten pollen grains were chosen haphazardly and the diameter of each grain was measured using the ProgRes<sup>®</sup> CapturePro software “Measure” module in two directions, one perpendicular to the other. Both diameter measurements were used in a cluster analysis to group species by pollen diameter.<br><b>TYPE:</b> abbreviation of plant species<b>M1final:</b> Diameter length 1 in microns (μm)<b>M2final:</b> Diameter length 2 in microns (μm)<b>SIZE1:</b> Designation of pollen grain as "Small" or "Large" based on k-means cluster analysis<b>SIZE2:</b> Designation of pollen grain as "Small" or "Large" based on <i>k</i>-means cluster analysis with "<i>Typha</i>" pollen labeled separately due to the difference in performance of <i>P. mexicanus</i> on this pollen diet.<br>
DOI: 10.17188/1275216
title: Materials Data on Eu2PI by Materials Project

description: Eu2PI is Caswellsilverite structured and crystallizes in the trigonal R-3m space group. The structure is three-dimensional. Eu2+ is bonded to three equivalent P3- and three equivalent I1- atoms to form a mixture of edge and corner-sharing EuP3I3 octahedra. The corner-sharing octahedral tilt angles are 0°. All Eu–P bond lengths are 2.96 Å. All Eu–I bond lengths are 3.45 Å. P3- is bonded to six equivalent Eu2+ atoms to form PEu6 octahedra that share corners with six equivalent IEu6 octahedra, edges with six equivalent PEu6 octahedra, and edges with six equivalent IEu6 octahedra. The corner-sharing octahedral tilt angles are 12°. I1- is bonded to six equivalent Eu2+ atoms to form distorted IEu6 octahedra that share corners with six equivalent PEu6 octahedra, edges with six equivalent PEu6 octahedra, and edges with six equivalent IEu6 octahedra. The corner-sharing octahedral tilt angles are 12°.
DOI: 10.17188/1275217
title: Materials Data on YbCu9Sn4 by Materials Project

description: YbCu9Sn4 is Bergman Structure: Mg32(Al,Zn)49 Bergman-like structured and crystallizes in the tetragonal I4/mcm space group. The structure is three-dimensional. Yb is bonded in a 8-coordinate geometry to sixteen Cu and eight equivalent Sn atoms. There are eight shorter (3.58 Å) and eight longer (3.63 Å) Yb–Cu bond lengths. All Yb–Sn bond lengths are 3.50 Å. There are three inequivalent Cu sites. In the first Cu site, Cu is bonded to two equivalent Yb, six Cu, and four equivalent Sn atoms to form a mixture of distorted corner, edge, and face-sharing CuYb2Cu6Sn4 cuboctahedra. There are a spread of Cu–Cu bond distances ranging from 2.53–2.76 Å. There are a spread of Cu–Sn bond distances ranging from 2.58–2.69 Å. In the second Cu site, Cu is bonded in a 12-coordinate geometry to two equivalent Yb, six Cu, and four equivalent Sn atoms. There are a spread of Cu–Cu bond distances ranging from 2.54–2.99 Å. There are two shorter (2.74 Å) and two longer (2.79 Å) Cu–Sn bond lengths. In the third Cu site, Cu is bonded to eight Cu and four equivalent Sn atoms to form a mixture of corner and face-sharing CuCu8Sn4 cuboctahedra. All Cu–Sn bond lengths are 2.76 Å. Sn is bonded in a 11-coordinate geometry to two equivalent Yb and nine Cu atoms.
DOI: 10.17188/1275218
title: Materials Data on La(AlGa)2 by Materials Project

description: LaAl2Ga2 crystallizes in the tetragonal I4/mmm space group. The structure is three-dimensional. La is bonded in a 8-coordinate geometry to eight equivalent Ga and eight equivalent Al atoms. All La–Ga bond lengths are 3.29 Å. All La–Al bond lengths are 3.52 Å. Ga is bonded in a 9-coordinate geometry to four equivalent La, one Ga, and four equivalent Al atoms. The Ga–Ga bond length is 2.56 Å. All Ga–Al bond lengths are 2.63 Å. Al is bonded to four equivalent La and four equivalent Ga atoms to form a mixture of distorted corner, edge, and face-sharing AlLa4Ga4 tetrahedra.
DOI: 10.17188/1275219
title: Materials Data on Ce(NiP)2 by Materials Project

description: CeNi2P2 crystallizes in the tetragonal I4/mmm space group. The structure is three-dimensional. Ce3+ is bonded in a distorted body-centered cubic geometry to eight equivalent P3- atoms. All Ce–P bond lengths are 3.03 Å. Ni+1.50+ is bonded to four equivalent P3- atoms to form a mixture of edge and corner-sharing NiP4 tetrahedra. All Ni–P bond lengths are 2.30 Å. P3- is bonded in a 9-coordinate geometry to four equivalent Ce3+, four equivalent Ni+1.50+, and one P3- atom. The P–P bond length is 2.38 Å.
DOI: 10.17188/1275220
title: Materials Data on UAl2Pd5 by Materials Project

description: UPd5Al2 crystallizes in the tetragonal I4/mmm space group. The structure is three-dimensional. U is bonded to twelve Pd atoms to form a mixture of corner and face-sharing UPd12 cuboctahedra. There are four shorter (2.97 Å) and eight longer (3.00 Å) U–Pd bond lengths. There are two inequivalent Pd sites. In the first Pd site, Pd is bonded in a distorted square co-planar geometry to four equivalent U atoms. In the second Pd site, Pd is bonded in a 6-coordinate geometry to two equivalent U and four equivalent Al atoms. There are two shorter (2.59 Å) and two longer (2.67 Å) Pd–Al bond lengths. Al is bonded in a body-centered cubic geometry to eight equivalent Pd atoms.
DOI: 10.17188/1275221
title: Materials Data on ErTe3 by Materials Project

description: ErTe3 crystallizes in the orthorhombic Cmcm space group. The structure is two-dimensional and consists of four ErTe3 sheets oriented in the (0, 1, 0) direction. Er3+ is bonded to five Te1- atoms to form a mixture of distorted edge and corner-sharing ErTe5 square pyramids. There are four shorter (3.01 Å) and one longer (3.17 Å) Er–Te bond lengths. There are three inequivalent Te1- sites. In the first Te1- site, Te1- is bonded in a 4-coordinate geometry to four equivalent Te1- atoms. All Te–Te bond lengths are 3.08 Å. In the second Te1- site, Te1- is bonded in a distorted square co-planar geometry to four equivalent Er3+ atoms. In the third Te1- site, Te1- is bonded in a distorted single-bond geometry to one Er3+ and four equivalent Te1- atoms.
DOI: 10.17188/1275224
title: Materials Data on Tl2Ni(CN)4 by Materials Project

description: Ni(Tl(CN)2)2 crystallizes in the monoclinic P2_1/c space group. The structure is three-dimensional and consists of two nickel molecules and one Tl(CN)2 framework. In the Tl(CN)2 framework, Tl1+ is bonded in a 5-coordinate geometry to five N3- atoms. There are a spread of Tl–N bond distances ranging from 2.83–3.11 Å. There are two inequivalent C2+ sites. In the first C2+ site, C2+ is bonded in a single-bond geometry to one N3- atom. The C–N bond length is 1.18 Å. In the second C2+ site, C2+ is bonded in a single-bond geometry to one N3- atom. The C–N bond length is 1.18 Å. There are two inequivalent N3- sites. In the first N3- site, N3- is bonded in a distorted single-bond geometry to two equivalent Tl1+ and one C2+ atom. In the second N3- site, N3- is bonded in a distorted single-bond geometry to three equivalent Tl1+ and one C2+ atom.
DOI: 10.17188/1275225
title: Materials Data on BiSeBr by Materials Project

description: BiSeBr crystallizes in the orthorhombic Pnma space group. The structure is one-dimensional and consists of two BiSeBr ribbons oriented in the (1, 0, 0) direction. Bi3+ is bonded to three equivalent Se2- and two equivalent Br1- atoms to form edge-sharing BiSe3Br2 square pyramids. There are one shorter (2.75 Å) and two longer (2.88 Å) Bi–Se bond lengths. Both Bi–Br bond lengths are 3.06 Å. Se2- is bonded in a 3-coordinate geometry to three equivalent Bi3+ atoms. Br1- is bonded in a distorted L-shaped geometry to two equivalent Bi3+ atoms.
DOI: 10.17188/1275227
title: Materials Data on RbNb3CuCl9 by Materials Project

description: RbNb3CuCl9 crystallizes in the triclinic P-1 space group. The structure is one-dimensional and consists of one RbNb3CuCl9 ribbon oriented in the (1, 2, 1) direction. Rb1+ is bonded in a 2-coordinate geometry to two Cl1- atoms. There are one shorter (2.30 Å) and one longer (2.70 Å) Rb–Cl bond lengths. There are three inequivalent Nb+2.33+ sites. In the first Nb+2.33+ site, Nb+2.33+ is bonded in a 2-coordinate geometry to one Nb+2.33+ and three Cl1- atoms. The Nb–Nb bond length is 1.90 Å. There are a spread of Nb–Cl bond distances ranging from 2.16–2.44 Å. In the second Nb+2.33+ site, Nb+2.33+ is bonded in a 3-coordinate geometry to four Cl1- atoms. There are a spread of Nb–Cl bond distances ranging from 2.05–2.65 Å. In the third Nb+2.33+ site, Nb+2.33+ is bonded in a 1-coordinate geometry to one Nb+2.33+ and three Cl1- atoms. There are a spread of Nb–Cl bond distances ranging from 1.93–2.48 Å. Cu1+ is bonded in a distorted single-bond geometry to three Cl1- atoms. There are a spread of Cu–Cl bond distances ranging from 2.08–3.04 Å. There are nine inequivalent Cl1- sites. In the first Cl1- site, Cl1- is bonded in a 2-coordinate geometry to one Rb1+ and one Cu1+ atom. In the second Cl1- site, Cl1- is bonded in a 2-coordinate geometry to one Nb+2.33+, one Cu1+, and two Cl1- atoms. There are one shorter (2.10 Å) and one longer (2.72 Å) Cl–Cl bond lengths. In the third Cl1- site, Cl1- is bonded in a bent 120 degrees geometry to one Rb1+ and one Nb+2.33+ atom. In the fourth Cl1- site, Cl1- is bonded in a 1-coordinate geometry to one Nb+2.33+ and one Cl1- atom. The Cl–Cl bond length is 2.12 Å. In the fifth Cl1- site, Cl1- is bonded in a 1-coordinate geometry to two Nb+2.33+, one Cu1+, and two Cl1- atoms. In the sixth Cl1- site, Cl1- is bonded in a single-bond geometry to one Nb+2.33+ atom. In the seventh Cl1- site, Cl1- is bonded in a single-bond geometry to one Nb+2.33+ and one Cl1- atom. In the eighth Cl1- site, Cl1- is bonded in a 1-coordinate geometry to one Nb+2.33+ atom. In the ninth Cl1- site, Cl1- is bonded in a water-like geometry to two Nb+2.33+ atoms.
DOI: 10.17188/1275228
title: Materials Data on K5Nb(CN)8 by Materials Project

description: NbK5(CN)8 crystallizes in the tetragonal I-4 space group. The structure is three-dimensional and consists of two columbium molecules and one K5(CN)8 framework. In the K5(CN)8 framework, there are two inequivalent K1+ sites. In the first K1+ site, K1+ is bonded in a 6-coordinate geometry to six N3- atoms. There are a spread of K–N bond distances ranging from 2.88–3.25 Å. In the second K1+ site, K1+ is bonded in a distorted square co-planar geometry to four equivalent N3- atoms. All K–N bond lengths are 2.86 Å. There are two inequivalent C+1.75+ sites. In the first C+1.75+ site, C+1.75+ is bonded in a single-bond geometry to one N3- atom. The C–N bond length is 1.18 Å. In the second C+1.75+ site, C+1.75+ is bonded in a single-bond geometry to one N3- atom. The C–N bond length is 1.19 Å. There are two inequivalent N3- sites. In the first N3- site, N3- is bonded in a distorted single-bond geometry to four equivalent K1+ and one C+1.75+ atom. In the second N3- site, N3- is bonded in a distorted single-bond geometry to three K1+ and one C+1.75+ atom.
DOI: 10.17188/1275229
title: Materials Data on La(AlZn)2 by Materials Project

description: Al2LaZn2 crystallizes in the tetragonal I4/mmm space group. The structure is three-dimensional. La is bonded in a 8-coordinate geometry to eight equivalent Zn and eight equivalent Al atoms. All La–Zn bond lengths are 3.26 Å. All La–Al bond lengths are 3.49 Å. Zn is bonded in a 9-coordinate geometry to four equivalent La, one Zn, and four equivalent Al atoms. The Zn–Zn bond length is 2.50 Å. All Zn–Al bond lengths are 2.61 Å. Al is bonded to four equivalent La and four equivalent Zn atoms to form a mixture of distorted corner, edge, and face-sharing AlLa4Zn4 tetrahedra.
DOI: 10.17188/1275230
title: Materials Data on CuBi(PSe3)2 by Materials Project

description: CuBi(PSe3)2 crystallizes in the trigonal P-31c space group. The structure is two-dimensional and consists of two CuBi(PSe3)2 sheets oriented in the (0, 0, 1) direction. Cu1+ is bonded to six equivalent Se2- atoms to form CuSe6 octahedra that share edges with three equivalent BiSe6 octahedra. All Cu–Se bond lengths are 2.69 Å. Bi1+ is bonded to six equivalent Se2- atoms to form BiSe6 octahedra that share edges with three equivalent CuSe6 octahedra. All Bi–Se bond lengths are 2.99 Å. P5+ is bonded in a trigonal non-coplanar geometry to three equivalent Se2- atoms. All P–Se bond lengths are 2.22 Å. Se2- is bonded in a 3-coordinate geometry to one Cu1+, one Bi1+, and one P5+ atom.
DOI: 10.17188/1275231
title: Materials Data on CdI2 by Materials Project

description: CdI2 is trigonal omega-like structured and crystallizes in the trigonal P3m1 space group. The structure is two-dimensional and consists of seventeen CdI2 sheets oriented in the (0, 0, 1) direction. Cd2+ is bonded to six equivalent I1- atoms to form edge-sharing CdI6 octahedra. All Cd–I bond lengths are 3.04 Å. I1- is bonded in a distorted T-shaped geometry to three equivalent Cd2+ atoms.
DOI: 10.17188/1275232
title: Materials Data on ErAgSn by Materials Project

description: ErAgSn crystallizes in the hexagonal P6_3mc space group. The structure is three-dimensional. Er is bonded in a 12-coordinate geometry to six equivalent Ag and six equivalent Sn atoms. There are three shorter (3.06 Å) and three longer (3.56 Å) Er–Ag bond lengths. There are three shorter (3.17 Å) and three longer (3.43 Å) Er–Sn bond lengths. Ag is bonded in a 10-coordinate geometry to six equivalent Er and four equivalent Sn atoms. There are three shorter (2.81 Å) and one longer (2.99 Å) Ag–Sn bond lengths. Sn is bonded in a 10-coordinate geometry to six equivalent Er and four equivalent Ag atoms.
DOI: 10.17188/1275233
title: Materials Data on HoAlB14 by Materials Project

description: HoAlB14 is Magnesium tetraboride-derived structured and crystallizes in the orthorhombic Imma space group. The structure is three-dimensional. Ho3+ is bonded in a 12-coordinate geometry to sixteen B+0.43- atoms. There are a spread of Ho–B bond distances ranging from 2.54–2.84 Å. Al3+ is bonded to twelve B+0.43- atoms to form distorted face-sharing AlB12 cuboctahedra. There are a spread of Al–B bond distances ranging from 2.12–2.44 Å. There are five inequivalent B+0.43- sites. In the first B+0.43- site, B+0.43- is bonded in a 7-coordinate geometry to one Ho3+, two equivalent Al3+, and four B+0.43- atoms. There are a spread of B–B bond distances ranging from 1.75–2.25 Å. In the second B+0.43- site, B+0.43- is bonded in a 8-coordinate geometry to one Ho3+, one Al3+, and six B+0.43- atoms. There are a spread of B–B bond distances ranging from 1.76–1.86 Å. In the third B+0.43- site, B+0.43- is bonded in a 1-coordinate geometry to one Ho3+ and six B+0.43- atoms. There are a spread of B–B bond distances ranging from 1.74–1.84 Å. In the fourth B+0.43- site, B+0.43- is bonded in a 8-coordinate geometry to two equivalent Ho3+ and six B+0.43- atoms. There are a spread of B–B bond distances ranging from 1.78–1.92 Å. In the fifth B+0.43- site, B+0.43- is bonded in a 8-coordinate geometry to two equivalent Al3+ and six B+0.43- atoms.
DOI: 10.17188/1275234
title: Materials Data on Tb(SiPt)2 by Materials Project

description: Tb(PtSi)2 crystallizes in the tetragonal I4/mmm space group. The structure is three-dimensional. Tb4+ is bonded in a 8-coordinate geometry to eight equivalent Pt2- atoms. All Tb–Pt bond lengths are 3.24 Å. Pt2- is bonded in a 4-coordinate geometry to four equivalent Tb4+ and four equivalent Si atoms. All Pt–Si bond lengths are 2.47 Å. Si is bonded in a 5-coordinate geometry to four equivalent Pt2- and one Si atom. The Si–Si bond length is 2.33 Å.
DOI: 10.17188/1275235
title: Materials Data on ErAl9(Fe2Si3)2 by Materials Project

description: ErAl9(Fe2Si3)2 crystallizes in the tetragonal P4_2/nmc space group. The structure is three-dimensional. Er is bonded in a 6-coordinate geometry to six Fe, eight Al, and six Si atoms. There are two shorter (3.14 Å) and four longer (3.32 Å) Er–Fe bond lengths. There are a spread of Er–Al bond distances ranging from 2.99–3.09 Å. There are a spread of Er–Si bond distances ranging from 3.00–3.17 Å. There are two inequivalent Fe sites. In the first Fe site, Fe is bonded in a 9-coordinate geometry to one Er, seven Al, and two equivalent Si atoms. There are a spread of Fe–Al bond distances ranging from 2.43–2.54 Å. Both Fe–Si bond lengths are 2.31 Å. In the second Fe site, Fe is bonded in a 12-coordinate geometry to two equivalent Er, six Al, and four Si atoms. There are four shorter (2.59 Å) and two longer (2.83 Å) Fe–Al bond lengths. There are two shorter (2.40 Å) and two longer (2.41 Å) Fe–Si bond lengths. There are four inequivalent Al sites. In the first Al site, Al is bonded in a 11-coordinate geometry to one Er, three Fe, two equivalent Al, and five Si atoms. Both Al–Al bond lengths are 2.64 Å. There are a spread of Al–Si bond distances ranging from 2.61–2.82 Å. In the second Al site, Al is bonded in a 12-coordinate geometry to one Er, three Fe, two Al, and three Si atoms. The Al–Al bond length is 2.72 Å. There are a spread of Al–Si bond distances ranging from 2.56–2.85 Å. In the third Al site, Al is bonded in a 11-coordinate geometry to one Er, three Fe, four Al, and three equivalent Si atoms. There are one shorter (2.70 Å) and one longer (2.91 Å) Al–Al bond lengths. There are one shorter (2.64 Å) and two longer (2.71 Å) Al–Si bond lengths. In the fourth Al site, Al is bonded in a 2-coordinate geometry to two equivalent Fe, two equivalent Al, and two equivalent Si atoms. Both Al–Si bond lengths are 2.93 Å. There are three inequivalent Si sites. In the first Si site, Si is bonded in a 9-coordinate geometry to one Er, two equivalent Fe, five Al, and one Si atom. The Si–Si bond length is 2.56 Å. In the second Si site, Si is bonded in a 10-coordinate geometry to one Er, two equivalent Fe, four Al, and three equivalent Si atoms. There are two shorter (2.58 Å) and one longer (2.71 Å) Si–Si bond lengths. In the third Si site, Si is bonded in a 11-coordinate geometry to one Er, two equivalent Fe, six Al, and two Si atoms. The Si–Si bond length is 2.39 Å.
DOI: 10.17188/1275236
title: Materials Data on Yb2(Ni5B3)3 by Materials Project

description: YbYb(Ni5B3)3 crystallizes in the orthorhombic Cmce space group. The structure is three-dimensional and consists of eight ytterbium molecules and one Yb(Ni5B3)3 framework. In the Yb(Ni5B3)3 framework, Yb2+ is bonded in a 2-coordinate geometry to four B3- atoms. There are two shorter (2.74 Å) and two longer (2.90 Å) Yb–B bond lengths. There are ten inequivalent Ni+1.53+ sites. In the first Ni+1.53+ site, Ni+1.53+ is bonded in a square co-planar geometry to four B3- atoms. There are two shorter (2.00 Å) and two longer (2.12 Å) Ni–B bond lengths. In the second Ni+1.53+ site, Ni+1.53+ is bonded in a distorted T-shaped geometry to four B3- atoms. There are a spread of Ni–B bond distances ranging from 2.06–2.56 Å. In the third Ni+1.53+ site, Ni+1.53+ is bonded in an octahedral geometry to six B3- atoms. There are two shorter (2.32 Å) and four longer (2.49 Å) Ni–B bond lengths. In the fourth Ni+1.53+ site, Ni+1.53+ is bonded in a 4-coordinate geometry to four B3- atoms. There are a spread of Ni–B bond distances ranging from 2.15–2.21 Å. In the fifth Ni+1.53+ site, Ni+1.53+ is bonded in a 4-coordinate geometry to five B3- atoms. There are a spread of Ni–B bond distances ranging from 2.01–2.54 Å. In the sixth Ni+1.53+ site, Ni+1.53+ is bonded in a 4-coordinate geometry to four B3- atoms. There are two shorter (2.02 Å) and two longer (2.06 Å) Ni–B bond lengths. In the seventh Ni+1.53+ site, Ni+1.53+ is bonded in a 4-coordinate geometry to four B3- atoms. There are a spread of Ni–B bond distances ranging from 1.97–2.12 Å. In the eighth Ni+1.53+ site, Ni+1.53+ is bonded in a 4-coordinate geometry to four B3- atoms. There are a spread of Ni–B bond distances ranging from 1.96–2.15 Å. In the ninth Ni+1.53+ site, Ni+1.53+ is bonded in a distorted see-saw-like geometry to four B3- atoms. There are a spread of Ni–B bond distances ranging from 2.02–2.14 Å. In the tenth Ni+1.53+ site, Ni+1.53+ is bonded in a 5-coordinate geometry to five B3- atoms. There are a spread of Ni–B bond distances ranging from 2.07–2.15 Å. There are six inequivalent B3- sites. In the first B3- site, B3- is bonded in a 9-coordinate geometry to one Yb2+, seven Ni+1.53+, and one B3- atom. The B–B bond length is 1.68 Å. In the second B3- site, B3- is bonded to seven Ni+1.53+ atoms to form distorted corner-sharing BNi7 pentagonal bipyramids. In the third B3- site, B3- is bonded in a 9-coordinate geometry to one Yb2+, seven Ni+1.53+, and one B3- atom. The B–B bond length is 1.98 Å. In the fourth B3- site, B3- is bonded in a 9-coordinate geometry to seven Ni+1.53+ and one B3- atom. In the fifth B3- site, B3- is bonded in a 9-coordinate geometry to eight Ni+1.53+ and one B3- atom. The B–B bond length is 1.86 Å. In the sixth B3- site, B3- is bonded in a 9-coordinate geometry to eight Ni+1.53+ and one B3- atom.