DOI: 10.18419/darus-4004
title: Data for: Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty

description: &lt;p&gt;This dataset includes the measurement data described in the paper &quot;Rheological Analysis and Evaluation of Measurement Techniques for the Curing Polymethylmethacrylate Bone Cement in Vertebroplasty&quot; and additional supplementary data. All data in .csv files except 'Inj1 -- 5' are generated directly by the rheometer software from the rheometer measurements. &lt;/p&gt;

&lt;p&gt;Microsoft Excel files:&lt;/p&gt;

&lt;ul&gt;
 &lt;li&gt;settings.xlsx: Contains settings for all the measurements&lt;/li&gt;
&lt;/ul&gt;

&lt;p&gt;Comma separated value files:&lt;/p&gt;

&lt;ul&gt;
 &lt;li&gt;Benchmark-1 -- 4.csv: Oscillatory test at 3 mNm torque amplitude and 1 Hz frequency (Fig.S1)&lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Inj1 -- 5.csv: Injection test at 0.025 mL/s (Fig. 7a, 7b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh1a.csv: Oscillatory deformation of 0.2\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2a)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh1b.csv: Oscillatory deformation of 20\% strain amplitude and 1 Hz frequency for 30 minutes (Fig. 2b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh2a.csv: Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz (5 mins) (ii) 20\% strain amplitude, 1 Hz (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz (22 mins) (Fig. 2c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh2b.csv: Oscillatory deformation in three stages: (i) 0.1\% strain amplitude, 0.1 Hz, 23 &deg;C (5 mins) (ii) 20\% strain amplitude, 1 Hz, 23 &deg;C (3 mins) (iii) 0.1\% strain amplitude, 0.1 Hz, 37 &deg;C (22 mins) (Fig. 2d)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh3.csv: Rotational shear stress was applied in steps of (i) 0 Pa (ii) 100 Pa (iii) 0 Pa (iv) 500 Pa (v) 0 Pa (vi) 2000 Pa (vii) 0 Pa, of one minute each, to evaluate creep behaviour. (Fig. 3a)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh4-1.csv: Rotational shear strain was applied in steps of (i) 0\% (ii) 1\% (iii) 0\%, of two minutes each. (Fig. 3b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh4-2.csv: Rotational shear strain was applied in steps of (i) 0\% (ii) 100\% (iii) 0\%, of two minutes each. (Fig. 3b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh5-1 -- 3.csv: Amplitude sweep test, where the strain amplitude was gradually increased from 0.01\% to 1000\%. The test was done at 1 Hz frequency (Fig. 3c, 3d)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh6-1 -- 3.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.01% strain amplitude (Fig. 3e, 3f)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh6-4 -- 6.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.03% strain amplitude (Fig. 5)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh6-7 -- 9.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 0.2% strain amplitude (Fig. 5)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh6-10.csv: Frequency sweep test, where the frequency was gradually increased from 0.1 Hz to 100 Hz at 200% strain amplitude (Fig. 5)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7a-1.csv: Rotational shear rate sweep from 0.001 to 1000 1/s (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7a-2.csv: Rotational shear rate sweep from 0.01 to 1 1/s (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7a-3.csv: Rotational shear rate sweep from 0.001 to 0.01 1/s (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7a-4.csv: Rotational shear rate sweep from 1 to 100 1/s (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7a-5.csv: Rotational shear rate sweep from 10 to 1000 1/s (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7b-1.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7b-2.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh7b-3.csv: Rotational shear rate sweep from 0.1 to 100 1/s with sandpaper (Fig. 4a, 4b)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh8-1.csv: Constant rotational shear rate 0.0001 1/s for 20 minutes (Fig. 4c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh8-2.csv: Constant rotational shear rate 0.001 1/s for 20 minutes (Fig. 4c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh8-3.csv: Constant rotational shear rate 0.01 1/s for 20 minutes (Fig. 4c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh8-4.csv: Constant rotational shear rate 0.1 1/s for 20 minutes (Fig. 4c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh8-5.csv: Constant rotational shear rate 1 1/s for 20 minutes (Fig. 4c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh8-6.csv: Constant rotational shear rate 100 1/s for 20 minutes (Fig. 4c)&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh9.csv: Bone cement was prepared and simply left on the rheometer between the plates while maintaining 1.5 mm gap for 45 minutes without any action.&lt;/p&gt;
 &lt;/li&gt;
 &lt;li&gt;
 &lt;p&gt;Rh10.csv: Bone cement was prepared and subjected to 15 minutes of rotational 100 1/s shear rate and then 30 minutes of no action on the rheometer.&lt;/p&gt;
 &lt;/li&gt;
&lt;/ul&gt;