DOI: 10.57992/nmrxiv.p143.s1399
title: Alpha-amanitin

description: This dataset contains NMR spectra obtained for the sample -Alpha-amanitin Nucleus: 1H NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: 1d Temperature: 342.9922 Observed Frequency: 500.19 Magnetic Field Strength: 11.74775999581523 Number of Scans: 32 NMR Pulse Sequence: zg30 Spectral Width: 19.9922629410624 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 500.19350133 Nucleus: 1H,1H NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: cosy Temperature: 342.9922 Observed Frequency: 500.19,500.19 Magnetic Field Strength: 11.74775999581523 Number of Scans: 16 NMR Pulse Sequence: cosygpppqf Spectral Width: 12.0145931088975,12.0001698278544 Number of Data Points: 4096,128 Relaxation Delay: 1 Observed Frequency: 500.19300114,500.19300114 Nucleus: 1H,13C NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: hsqc Temperature: 343.0969 Observed Frequency: 500.19,125.772876 Magnetic Field Strength: 11.74775999581523 Number of Scans: 48 NMR Pulse Sequence: hsqcedetgpsisp2.4 Spectral Width: 12.0145931088975,190.194363209053 Number of Data Points: 2048,64 Relaxation Delay: 1 Observed Frequency: 500.19300114,125.78419555884 Nucleus: 1H,13C NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: hsqc Temperature: 342.9922 Observed Frequency: 500.19,125.772876 Magnetic Field Strength: 11.74775999581523 Number of Scans: 64 NMR Pulse Sequence: hsqcdiedetgpsisp.2 Spectral Width: 12.0145931088975,190.194363209053 Number of Data Points: 2048,64 Relaxation Delay: 1 Observed Frequency: 500.19300114,125.78419555884 Nucleus: 1H,1H NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: tocsy Temperature: 342.8876 Observed Frequency: 500.19,500.19 Magnetic Field Strength: 11.74775999581523 Number of Scans: 16 NMR Pulse Sequence: mlevph Spectral Width: 12.0145931088975,12.0001698278544 Number of Data Points: 2048,64 Relaxation Delay: 1.3 Observed Frequency: 500.19300114,500.19300114 Nucleus: 1H,1H NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: roesy Temperature: 342.9922 Observed Frequency: 500.19,500.19 Magnetic Field Strength: 11.74775999581523 Number of Scans: 32 NMR Pulse Sequence: roesyphpp.2 Spectral Width: 12.0145931088975,12.0001698278544 Number of Data Points: 4096,256 Relaxation Delay: 1.3 Observed Frequency: 500.19300114,500.19300114 Nucleus: 1H,13C NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: hmbc Temperature: 342.9922 Observed Frequency: 500.19,125.772876 Magnetic Field Strength: 11.74775999581523 Number of Scans: 200 NMR Pulse Sequence: hmbcctetgpl2nd Spectral Width: 12.0145931088975,219.615597660012 Number of Data Points: 2048,128 Relaxation Delay: 1 Observed Frequency: 500.19300114,125.78482442322 Nucleus: 13C NMR Solvent: DMSO NMR Probe: Z810701_0059 (PA BBI 500S2 H-BB-D-05 Z) NMR Pulse Sequence: 1d Temperature: 342.9922 Observed Frequency: 125.772876 Magnetic Field Strength: 11.745970784482695 Number of Scans: 8192 NMR Pulse Sequence: udeft-jfg Spectral Width: 236.606113010093 Number of Data Points: 21424 Relaxation Delay: 2 Observed Frequency: 125.78671101636