DOI: 10.57992/nmrxiv.p122.s1249
title: 6-Br kynuramine

description: This dataset contains NMR spectra obtained for the sample -6-Br kynuramine date: 2024-06-11T03:47:12.000Z isFt: true name: 6-Br kynuramine/10 phc0: 57.35987 phc1: 11.09468 type: NMR Spectrum DECIM: 2448 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.6 DSPFVS: 20 nucleus: 1H reverse: false solvent: MeOD dimension: 1 increment: 0.5521715599250757 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z108618/0212 experiment: 1d groupDelay: 67.9861145019531 temperature: 300 spectrumSize: 16384 baseFrequency: 399.89 fieldStrength: 9.392054530249265 numberOfScans: 16 pulseSequence: zg30 spectralWidth: 20.4303477172278 numberOfPoints: 38 relaxationTime: 0.1 acquisitionTime: 0.0022644000000000015 frequencyOffset: 2099.420002025454 originFrequency: 399.892099420002 pulseStrength90: 18939.39393939394 experimentNumber: 10 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2024-06-11T14:46:29.000Z isFt: true name: 6-Br kynuramine/11 phc0: -259.8941 phc1: 39.85792 type: NMR Spectrum DECIM: 832 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.6 DSPFVS: 20 nucleus: 13C reverse: false solvent: MeOD dimension: 1 increment: 8.537060021509678 isComplex: true probeName: 5 mm PABBO BB-1H/D Z-GRD Z108618/0212 experiment: 1d groupDelay: 67.9839324951172 temperature: 300 spectrumSize: 32768 baseFrequency: 100.55242 fieldStrength: 9.390053807855773 numberOfScans: 1700 pulseSequence: zgpg30 spectralWidth: 239.037680602271 numberOfPoints: 29 relaxationTime: 0.6316769 acquisitionTime: 0.000582399999999999 frequencyOffset: 11062.200359006623 originFrequency: 100.563482200359 pulseStrength90: 16983.695652173912 experimentNumber: 11 acquisitionScheme: undefined linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2024-06-12T12:42:55.000Z isFt: true name: 6-Br kynuramine/20 phc0: -96.96461,0 phc1: -1,0 type: NMR Spectrum DECIM: 3584 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.6 DSPFVS: 20 nucleus: 1H,1H reverse: false,false solvent: MeOD dimension: 2 increment: 1.9935243434790144 isComplex: false probeName: 5 mm PABBO BB-1H/D Z-GRD Z108618/0212 experiment: cosy groupDelay: 67.9842834472656 temperature: 300 spectrumSize: 1024,256 baseFrequency: 399.89,399.89 fieldStrength: 9.392054530249265 numberOfScans: 2 pulseSequence: cosygpppqf spectralWidth: 13.9546704043531,13.9462766123889 numberOfPoints: 8 relaxationTime: 1.4 acquisitionTime: 0.0006272000000000016 frequencyOffset: 1719.4859980236288,1719.4859980236288 originFrequency: 399.891719485998,399.891719485998 pulseStrength90: 18939.39393939394 experimentNumber: 20 acquisitionScheme: notPhaseSensitive linearPredictionBin: 0,0 lpNumberOfCoefficients: 0,0 windowMultiplicationMode: 3,3 date: 2024-06-12T12:58:57.000Z isFt: true name: 6-Br kynuramine/21 phc0: -208.9391,0 phc1: -12.757,0 type: NMR Spectrum DECIM: 3584 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.6 DSPFVS: 20 nucleus: 1H,13C reverse: false,false solvent: MeOD dimension: 2 increment: 0.9967621717395072 isComplex: false probeName: 5 mm PABBO BB-1H/D Z-GRD Z108618/0212 experiment: hsqc groupDelay: 67.9842834472656 temperature: 300.1 spectrumSize: 1024,256 baseFrequency: 399.89,100.55242 fieldStrength: 9.392054530249265 numberOfScans: 4 pulseSequence: hsqcedetgpsisp.2 spectralWidth: 13.9546704043531,180 numberOfPoints: 15 relaxationTime: 1 acquisitionTime: 0.0012544000000000032 frequencyOffset: 1719.4859980236288,9051.15192900041 originFrequency: 399.891719485998,100.561471151929 pulseStrength90: 18939.39393939394 experimentNumber: 21 acquisitionScheme: Echo-antiecho linearPredictionBin: 0,0 lpNumberOfCoefficients: 0,0 windowMultiplicationMode: 4,4 date: 2024-06-12T13:10:58.000Z isFt: true name: 6-Br kynuramine/22 phc0: 0,0 phc1: 0,0 type: NMR Spectrum DECIM: 3584 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.6 DSPFVS: 20 nucleus: 1H,13C reverse: false,false solvent: MeOD dimension: 2 increment: 1.9935243434790144 isComplex: false probeName: 5 mm PABBO BB-1H/D Z-GRD Z108618/0212 experiment: hmbc groupDelay: 67.9842834472656 temperature: 299.9 spectrumSize: 1024,256 baseFrequency: 399.89,100.55242 fieldStrength: 9.392054530249265 numberOfScans: 8 pulseSequence: hmbcgplpndqf spectralWidth: 13.9546704043531,240 numberOfPoints: 8 relaxationTime: 1 acquisitionTime: 0.0006272000000000016 frequencyOffset: 1719.4859980236288,11062.200359006623 originFrequency: 399.891719485998,100.563482200359 pulseStrength90: 18939.39393939394 experimentNumber: 22 acquisitionScheme: notPhaseSensitive linearPredictionBin: 0,0 lpNumberOfCoefficients: 0,0 windowMultiplicationMode: 3,3