DOI: 10.18150/os7f0o
title: Photochemical stability of chitosan films doped with cannabis oil

description: 1. General Information- **Data Set Title**: Photochemical stability of chitosan films doped with cannabis oil- **Authors**: - Principal investigator and contact person: Dorota Chełminiak-Dudkiewicz, Nicolaus Copernicus University in Torun, e-mail: dorotachd@umk.pl.-Investigator: Aleksander Smolarkiewicz-Wyczachowski, Nicolaus Copernicus University in Torun, e-mail: asmolarkiewicz@doktorant.umk.pl- **Date of data collection**: year 2024.- **Place of data collection**: Torun- **Keywords***: Chitosan films; cannabis oil; Crosslinking; UV-irradiation; FTIR spectroscopyData language**: Polish- **Sources of funding**: National Science Center (NCN) competition: SONATA 18- UMO-2022/47/D/NZ7/01821.2. Overview of data and files- **File List**:Fig.1.tiff: Chemical structure of cannabidiol (a); linolenic acid (b) – dominant constituents of hemp oil.Fig.2. tiff: Difference ATR-FTIR spectra of cannabis oil exposed 48 h under HPK (a), UV-C (b), and LED (c). Offset applied; values on the ordinate axis refer to the c spectrum (str. and def. Mean stretching and deformation vibration, respectively).Fig.3.tiff: Enlargement of hydroxyl (left side) and carbonyl (right side) range of difference ATR-FTIR spectra of cannabis oil exposed 48 h under HPK (a), UV-C (b), and LED (c).Fig.4.tiff: Comparison of the FTIR spectra of chitosan (a), chitosan with 10% cannabis oil (b), and cannabis oil alone (c) with the main absorption bands marked.Fig.5a.tiff: FTIR changes induced in chitosan-based film enriched with cannabis oil by exposure to HPK lamp: full spectral range. The green arrows indicate the trend of changes during exposure time up to 48 h. Fig.5b.tiff: FTIR changes induced in chitosan-based film enriched with cannabis oil by exposure to HPK lamp: enlarged carbonyl range. The green arrows indicate the trend of changes during exposure time up to 48 h.Fig.6.tiff: The difference in FTIR spectra of chitosan-based film enriched with cannabis oil after 48 h UV-irradiation under: HPK (a), UV-C (b), and LED (c) lamp.Fig.7a.tab: Changes in the content of methyl/methylene groups in film based on chitosan and enriched with cannabis oil sample after UV-irradiation from three different sources (calculated as relative percent changes in absorbance at 2930 cm−1). Legend: LED- LED lamp HPK - high-pressure lamp UV-C - UV lamp delta A- absorption differenceFig.7b.tab: Changes in the content of carbonyl groups in film based on chitosan and enriched with cannabis oil sample after UV-irradiation from three different sources (calculated as relative percent changes in absorbance at 1744 cm−1. Legend: LED- LED lamp HPK - high-pressure lamp UV-C - UV lamp delta A- absorption differenceFig.8.tiff: FTIR spectra of cross-linked (a) and uncross-linked (b) chitosan (the green arrow shows a new band resulting from cross-linking).Fig.9.tiff: FTIR spectra of cross-linked (a) and uncross-linked (b) chitosan with 10% cannabis oil (the green arrow shows a new band resulting from crosslinking).Fig.10.tiff: Examples of changes in FTIR spectra in cross-linked film based on chitosan enriched with cannabis oil irradiated with UV-C up to 48 h.Fig.11.tiff: FTIR changes in the 400–1000 cm−1 range in crosslinked films based on chitosan and enriched with cannabis oil UV-irradiated under a) HPK, b) UV-C, c) LED.Fig.12.tiff: The difference FTIR spectra of cross-linked CS + CBD oil after 48 h UV-irradiation under HPK (a), UV-C (b), and LED (c) lamp.Fig.13a.tiff: Changes in the content of methyl/methylene groups in cross-linked the film based on chitosan and enriched with cannabis oil sample after UV-irradiation from three different sources (calculated as relative percent changes in absorbance at 2930 cm−1). Legend: LED- LED lamp HPK - high-pressure lamp UV-C - UV lamp delta A- absorption differenceFig.13b.tiff: Changes in the content of carbonyl groups in cross-linked the film based on chitosan and enriched with cannabis oil sample after UV-irradiation from three different sources (calculated as relative percent changes in absorbance at 1744 cm−1). Legend: LED- LED lamp HPK - high-pressure lamp UV-C - UV lamp delta A- absorption differenceFig.14.tiff: AFM images of uncross-linked chitosan containing cannabis oil before irradiation and after 48 h exposure under different lamps. Legend: Rq- root mean square roughness Ra-The average roughnessFig.15.tiff: AFM images of cross-linked chitosan containing cannabis oil before irradiation and after 48 h exposure under different lamps. Legend: Rq- root mean square roughness Ra-The average roughness- **File formats**: tiff, tab3. sharing and access information- **Licenses/Restrictions**: CC BY - Creative Commons Attribution 4.0. - **Related Publications**: https://www.sciencedirect.com/science/article/pii/S1011134424000101#ks0005