DOI: 10.5281/zenodo.12592764
title: Natrolite - Sample 2 NanED Round Robin, Data: ESR10

description: Natrolite


The following submission contains the data collection and processing of the dataset for the sample natrolite under the NanEd round-robin project. A single crystal was identified, and the rotation data acquisition technique was used to collect the dataset on the same crystal. The dataset was processed with XDS software. The table below summarizes the data collection parameters for the dataset. The following data is also in the data folder as a Word file.


 


Continuous Rotation:



	
		
			
			
General information:
			
			
			
 
			
		
		
			
			
Project
			
			
			
NanED (www.naned.eu)
			
		
		
			
			
ESR Project
			
			
			
ESR10 - Round Robin
			
		
		
			
			
Project Label
			
			
			
RR-2
			
		
		
			
			
Sample Label
			
			
			
RR-2_SU
			
		
		
			
			
Data set Label
			
			
			
RR-2
			
		
		
			
			
 
			
			
			
 
			
		
		
			
			
Instrumental:
			
			
			
 
			
		
		
			
			
Instrument
			
			
			
Transmission electron microscope JEOL 2100 LaB6
			
		
		
			
			
Radiation source
			
			
			
LaB6
			
		
		
			
			
Accelerating voltage
			
			
			
200 kV
			
		
		
			
			
Wavelength
			
			
			
0.0251 Å
			
		
		
			
			
Probe Type
			
			
			
Parallel beam
			
		
		
			
			
Beam Diameter
			
			
			
6 μm
			
		
		
			
			
Beam Convergence
			
			
			
Parallel beam, convergence <0.1mrad
			
		
		
			
			
Detector
			
			
			
Hybrid pixel detector ASI Timepix (bottom mounted)
			
		
		
			
			
Number of pixels in the image
			
			
			
512 x 512
			
		
		
			
			
Pixel size
			
			
			
55 µm x 55 µm
			
		
		
			
			
Effective camera length
			
			
			
250 mm
			
		
		
			
			
Calibration constant
			
			
			
0.004990 Å-1/pixel
			
		
		
			
			
 
			
			
			
 
			
		
		
			
			
Sample description:
			
			
			
 
			
		
		
			
			
Name
			
			
			
Natrolite
			
		
		
			
			
Chemical composition
			
			
			
Na2Si3Al2O10.(H2O)2
			
		
		
			
			
Sample source
			
			 
		
		
			
			
Sample preparation
			
			
			
Powder crushed in an agate mortar and deposited on a Cu grid with lacey C film
			
		
		
			
			
Experimental:
			
			
			
 
			
		
		
			
			
Data Type
			
			
			
Electron diffraction data - 3D ED
			
		
		
			
			
Data collection method
			
			
			
Continuous Rotation
			
		
		
			
			
Temperature (K) used during data collection
			
			
			
293 K
			
		
		
			
			
Number of crystals contributing to the data set
			
			
			
1
			
		
		
			
			
Number of experimental frames
			
			
			
513
			
		
		
			
			
tilt range, tilt step, tilt per frame
			
			
			
 -48.35°-70.58°, 0.453°/s, 0.2318°/frame
			
		
		
			
			
Exposure time per frame
			
			
			
0.5
			
		
		
			
			
 
			
			
			
 
			
		
		
			
			
Software:
			
			
			
 
			
		
		
			
			
Software used for the data collection
			
			
			
Instamatic
			
		
		
			
			
Software used for processing
			
			
			
XDS
			
		
		
			
			
 
			
			
			
 
			
		
		
			
			
Authorship and bibliography
			
			
			
 
			
		
		
			
			
Author(s) of the data
			
			
			
Lei Wang (ESR 10)
			
		
		
			
			
Related data
			
			
			
 
			
		
		
			
			
Publication(s)
			
			
			
 
			
		
		
			
			
 
			
			
			
 
			
		
		
			
			
Files and data formats
			
			
			
 
			
		
		
			
			
Image folder
			
			
			
REDp: Folder containing images of the diffraction pattern from each frame

			
XDS: Folder containing images of the diffraction pattern from each frame
			
		
		
			
			
Image format
			
			
			
mrc and img
			
		
		
			
			
Additional folders/files
			
			
			
Crystal image : image of the crystal
			
		
		
			
			
 
			
			
			
cRED_log: log file of data collection
			
		
		
			
			
 
			
			
			
1.ed3d: input file for REDp
			
		
		
			
			
 
			
			
			
XDS.INP: input file for the program XDS
			
		
	



 



	
		
			
			
Notes:

			
*Project Label "RR-2" stands for Round Robin 2

			
*RR-2 contains 1 dataset.