DOI: 10.57992/nmrxiv.p156.s1590
title: Compound 45

description: This dataset contains NMR spectra obtained for the sample -Compound 45 Nucleus: 13C NMR Solvent: CDCl3 NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: 1d Temperature: 298.1572 Observed Frequency: 100.612769 Magnetic Field Strength: 9.39626001094152 Number of Scans: 2048 NMR Pulse Sequence: zgpg30 Spectral Width: 250.960929380182 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 100.623333340745 Nucleus: 13C NMR Solvent: Acetone NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: 1d Temperature: 323.1185 Observed Frequency: 100.612769 Magnetic Field Strength: 9.39626001094152 Number of Scans: 256 NMR Pulse Sequence: zgpg30 Spectral Width: 250.960929380182 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 100.623333340745 Nucleus: 1H NMR Solvent: CDCl3 NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: 1d Temperature: 298.1607 Observed Frequency: 400.13 Magnetic Field Strength: 9.397691291560301 Number of Scans: 16 NMR Pulse Sequence: zg30 Spectral Width: 24.9916902020906 Number of Data Points: 65536 Relaxation Delay: 1 Observed Frequency: 400.133000975 Nucleus: 1H NMR Solvent: Acetone NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: 1d Temperature: 323.0763 Observed Frequency: 400.13 Magnetic Field Strength: 9.397691291560301 Number of Scans: 16 NMR Pulse Sequence: zg30 Spectral Width: 24.9916902020906 Number of Data Points: 65536 Relaxation Delay: 1 Observed Frequency: 400.133000975 Nucleus: 1H,1H NMR Solvent: CDCl3 NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: cosy Temperature: 298.1187 Observed Frequency: 400.13,400.13 Magnetic Field Strength: 9.397691291560301 Number of Scans: 1 NMR Pulse Sequence: cosygpppqf Spectral Width: 8.98984358878553,8.98984358878553 Number of Data Points: 2048,256 Relaxation Delay: 2 Observed Frequency: 400.131800585,400.131800585 Nucleus: 1H,1H NMR Solvent: Acetone NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: cosy Temperature: 323.1263 Observed Frequency: 400.13,400.13 Magnetic Field Strength: 9.397691291560301 Number of Scans: 1 NMR Pulse Sequence: cosygpppqf Spectral Width: 7.99992883247644,7.99992883247643 Number of Data Points: 2048,256 Relaxation Delay: 2 Observed Frequency: 400.13160052,400.13160052 Nucleus: 1H,13C NMR Solvent: CDCl3 NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: hmbc Temperature: 298.1587 Observed Frequency: 400.13,100.612768526 Magnetic Field Strength: 9.397691291560301 Number of Scans: 4 NMR Pulse Sequence: hmbcgpl2ndqf Spectral Width: 8.98984358878553,240.048385639511 Number of Data Points: 2048,256 Relaxation Delay: 1.5 Observed Frequency: 400.131800585,100.623835930538 Nucleus: 1H,13C NMR Solvent: Acetone NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: hmbc Temperature: 323.1114 Observed Frequency: 400.13,100.612768526 Magnetic Field Strength: 9.397691291560301 Number of Scans: 4 NMR Pulse Sequence: hmbcgpl2ndqf Spectral Width: 9.99670107240146,200.362967045882 Number of Data Points: 2048,256 Relaxation Delay: 1.5 Observed Frequency: 400.13200065,100.623835930538 Nucleus: 1H,13C NMR Solvent: CDCl3 NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: hsqc Temperature: 298.2058 Observed Frequency: 400.13,100.612768526 Magnetic Field Strength: 9.397691291560301 Number of Scans: 2 NMR Pulse Sequence: hsqcetgpsi2 Spectral Width: 8.98984358878553,178.10557964561 Number of Data Points: 1024,256 Relaxation Delay: 1.451667 Observed Frequency: 400.131800585,100.620918160251 Nucleus: 1H,13C NMR Solvent: Acetone NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: hsqc Temperature: 323.1703 Observed Frequency: 400.13,100.612768526 Magnetic Field Strength: 9.397691291560301 Number of Scans: 2 NMR Pulse Sequence: hsqcetgpsi2 Spectral Width: 9.99670107240146,130.083127850609 Number of Data Points: 1024,256 Relaxation Delay: 1.451667 Observed Frequency: 400.13200065,100.620314501 Nucleus: 1H,1H NMR Solvent: CDCl3 NMR Probe: Z116098_0484 (PA BBO 400S1 BBF-H-D-05 Z SP) NMR Pulse Sequence: noesy Temperature: 296.5615 Observed Frequency: 400.17,400.17 Magnetic Field Strength: 9.398630755363722 Number of Scans: 4 NMR Pulse Sequence: noesygpph Spectral Width: 7.89800141489631,7.89799685970687 Number of Data Points: 2048,256 Relaxation Delay: 2 Observed Frequency: 400.17165,400.1718808 Nucleus: 1H,1H NMR Solvent: Acetone NMR Probe: 5 mm PABBO BB/19F-1H/D Z-GRD Z116098/0035 NMR Pulse Sequence: noesy Temperature: 323.1237 Observed Frequency: 400.13,400.13 Magnetic Field Strength: 9.397691291560301 Number of Scans: 4 NMR Pulse Sequence: noesygpphpp Spectral Width: 7.99992883247644,7.99992883247643 Number of Data Points: 2048,128 Relaxation Delay: 1.928319 Observed Frequency: 400.13160052,400.13160052