DOI: 10.57992/nmrxiv.p90.s747
title: 10043_M18

description: This dataset contains NMR spectra obtained for the sample -10043_M18 date: 2018-04-24T09:47:13.000Z isFt: true name: 10043_M18/10 phc0: -138.92 phc1: 0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 21 nucleus: 1H reverse: false solvent: DMSO dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: 1d groupDelay: 76 temperature: 297.9991 spectrumSize: 65536 baseFrequency: 600.17 fieldStrength: 14.095949804745555 numberOfScans: 16 pulseSequence: zg30 spectralWidth: 16.0209895665619 numberOfPoints: 1 relaxationTime: 5 acquisitionTime: 0 frequencyOffset: 4201.1900000034075 originFrequency: 600.17420119 pulseStrength90: 31250 experimentNumber: 10 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2018-04-24T11:17:06.000Z isFt: true name: 10043_M18/11 phc0: -113.64 phc1: 0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 21 nucleus: 1H reverse: false solvent: MeOD dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: 1d groupDelay: 76 temperature: 297.9988 spectrumSize: 65536 baseFrequency: 600.17 fieldStrength: 14.095949804745555 numberOfScans: 16 pulseSequence: zg30 spectralWidth: 16.0209895665619 numberOfPoints: 1 relaxationTime: 5 acquisitionTime: 0 frequencyOffset: 4201.1900000034075 originFrequency: 600.17420119 pulseStrength90: 31250 experimentNumber: 11 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2018-04-24T15:05:34.000Z isFt: true name: 10043_M18/12 phc0: -114.06 phc1: 0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 21 nucleus: 1H reverse: false solvent: MeOD dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: 1d groupDelay: 76 temperature: 297.9994 spectrumSize: 65536 baseFrequency: 600.17 fieldStrength: 14.095949804745555 numberOfScans: 16 pulseSequence: zg30 spectralWidth: 16.0209895665619 numberOfPoints: 1 relaxationTime: 5 acquisitionTime: 0 frequencyOffset: 4201.1900000034075 originFrequency: 600.17420119 pulseStrength90: 31250 experimentNumber: 12 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2018-04-24T15:13:52.000Z isFt: true name: 10043_M18/13 phc0: 0,0 phc1: 0,0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 20 nucleus: 1H,1H reverse: false,false solvent: MeOD dimension: 2 increment: null isComplex: false probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: cosy groupDelay: 68 temperature: 297.998 spectrumSize: 1024,1024 baseFrequency: 600.17,600.17 fieldStrength: 14.095949804745555 numberOfScans: 2 pulseSequence: cosygpppqf spectralWidth: 16.0209894419014,16.0209894419014 numberOfPoints: 1 relaxationTime: 2 acquisitionTime: 0 frequencyOffset: 4205.860000070061,4205.860000070061 originFrequency: 600.17420586,600.17420586 pulseStrength90: 31250 experimentNumber: 13 acquisitionScheme: notPhaseSensitive linearPredictionBin: 0,1024 lpNumberOfCoefficients: 0,32 windowMultiplicationMode: 4,4 date: 2018-04-24T16:05:33.000Z isFt: true name: 10043_M18/14 phc0: 246.5069 phc1: 428.6 type: NMR Spectrum DECIM: 584 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 20 nucleus: 13C reverse: false solvent: MeOD dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: dept groupDelay: 68 temperature: 298.0005 spectrumSize: 32768 baseFrequency: 150.912866534 fieldStrength: 14.092947112083596 numberOfScans: 1024 pulseSequence: deptqgpsp spectralWidth: 226.905635125986 numberOfPoints: 1 relaxationTime: 2 acquisitionTime: 0 frequencyOffset: 15845.851000023004 originFrequency: 150.928712385 pulseStrength90: 20833.333333333332 experimentNumber: 14 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2018-04-24T16:14:33.000Z isFt: true name: 10043_M18/15 phc0: -203.0496,0 phc1: -1.737869,0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 20 nucleus: 1H,13C reverse: false,false solvent: MeOD dimension: 2 increment: null isComplex: false probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: hsqc groupDelay: 68 temperature: 297.9998 spectrumSize: 1024,1024 baseFrequency: 600.17,150.912866534 fieldStrength: 14.095949804745555 numberOfScans: 2 pulseSequence: hsqcedetgpsisp2.3 spectralWidth: 16.0209894419014,180.049189498831 numberOfPoints: 1 relaxationTime: 2 acquisitionTime: 0 frequencyOffset: 4205.860000070061,12073.029000021052 originFrequency: 600.17420586,150.924939563 pulseStrength90: 31250 experimentNumber: 15 acquisitionScheme: Echo-antiecho linearPredictionBin: 0,1024 lpNumberOfCoefficients: 0,60 windowMultiplicationMode: 4,4 date: 2018-04-24T16:38:19.000Z isFt: true name: 10043_M18/16 phc0: 0,0 phc1: 0,0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 20 nucleus: 1H,13C reverse: false,false solvent: MeOD dimension: 2 increment: null isComplex: false probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: hmbc groupDelay: 68 temperature: 298.0014 spectrumSize: 2048,1024 baseFrequency: 600.17,150.912866534 fieldStrength: 14.095949804745555 numberOfScans: 8 pulseSequence: hmbcgplpndqf spectralWidth: 16.0209894419014,230.057102280514 numberOfPoints: 1 relaxationTime: 1.5 acquisitionTime: 0 frequencyOffset: 4205.860000070061,15845.851000023004 originFrequency: 600.17420586,150.928712385 pulseStrength90: 31250 experimentNumber: 16 acquisitionScheme: notPhaseSensitive linearPredictionBin: 0,1024 lpNumberOfCoefficients: 0,32 windowMultiplicationMode: 3,3 date: 2018-04-24T19:26:21.000Z isFt: true name: 10043_M18/17 phc0: 39.05418,90 phc1: 71.03886,-180 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.3.b.13 DSPFVS: 20 nucleus: 1H,1H reverse: false,false solvent: MeOD dimension: 2 increment: null isComplex: false probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: roesy groupDelay: 68 temperature: 298.0011 spectrumSize: 2048,1024 baseFrequency: 600.17,600.17 fieldStrength: 14.095949804745555 numberOfScans: 8 pulseSequence: roesyphpr.2 spectralWidth: 16.0209894419014,16.0209894419014 numberOfPoints: 1 relaxationTime: 2 acquisitionTime: 0 frequencyOffset: 4205.860000070061,4205.860000070061 originFrequency: 600.17420586,600.17420586 pulseStrength90: 31250 experimentNumber: 17 acquisitionScheme: States-TPPI linearPredictionBin: 0,1024 lpNumberOfCoefficients: 0,32 windowMultiplicationMode: 4,4 date: 2019-10-18T19:31:13.000Z isFt: true name: 10043_M18/20 phc0: -121.98 phc1: 0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.5 DSPFVS: 21 nucleus: 1H reverse: false solvent: DMSO dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: 1d groupDelay: 76 temperature: 298.0016 spectrumSize: 65536 baseFrequency: 600.17 fieldStrength: 14.095949804745555 numberOfScans: 16 pulseSequence: zg30 spectralWidth: 16.0209895665619 numberOfPoints: 1 relaxationTime: 5 acquisitionTime: 0 frequencyOffset: 4201.1900000034075 originFrequency: 600.17420119 pulseStrength90: 31250 experimentNumber: 20 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-10-18T20:02:25.000Z isFt: true name: 10043_M18/21 phc0: -222.0082,0 phc1: 19.74452,0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0,0 title: Parameter file, TopSpin 4.0.5 DSPFVS: 20 nucleus: 1H,13C reverse: false,false solvent: DMSO dimension: 2 increment: null isComplex: false probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: hsqc groupDelay: 68 temperature: 298.0019 spectrumSize: 1024,1024 baseFrequency: 600.17,150.912866534 fieldStrength: 14.095949804745555 numberOfScans: 4 pulseSequence: hsqcedetgpsisp2.3 spectralWidth: 16.0209895665619,180.049189498831 numberOfPoints: 1 relaxationTime: 2 acquisitionTime: 0 frequencyOffset: 4201.1900000034075,12073.029000021052 originFrequency: 600.17420119,150.924939563 pulseStrength90: 31250 experimentNumber: 21 acquisitionScheme: Echo-antiecho linearPredictionBin: 0,0 lpNumberOfCoefficients: 0,0 windowMultiplicationMode: 4,4 date: 2019-10-04T15:29:47.000Z isFt: true name: 10043_M18/0 phc0: -80.5 phc1: 0 type: NMR Spectrum DECIM: 2080 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.5 DSPFVS: 21 nucleus: 1H reverse: false solvent: DMSO dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: 1d groupDelay: 76 temperature: 298.0026 spectrumSize: 65536 baseFrequency: 600.17 fieldStrength: 14.095949804745555 numberOfScans: 16 pulseSequence: zg30 spectralWidth: 16.0209895665619 numberOfPoints: 1 relaxationTime: 5 acquisitionTime: 0 frequencyOffset: 4201.1900000034075 originFrequency: 600.17420119 pulseStrength90: 31250 experimentNumber: 0 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1 date: 2019-10-25T16:12:35.000Z isFt: true name: 10043_M18/0 phc0: -259.94 phc1: 0 type: NMR Spectrum DECIM: 1680 aqMod: 3 isFid: false tdOff: 0 title: Parameter file, TopSpin 4.0.5 DSPFVS: 21 nucleus: 1H reverse: false solvent: DMSO dimension: 1 increment: null isComplex: true probeName: Z151284_0001 (CP QCI 600S3 H/P/C-N-D-05 Z) experiment: noesy groupDelay: 76 temperature: 298.0008 spectrumSize: 65536 baseFrequency: 600.17 fieldStrength: 14.095949804745555 numberOfScans: 16 pulseSequence: noesyigld1d spectralWidth: 19.8355208096248 numberOfPoints: 1 relaxationTime: 10 acquisitionTime: 0 frequencyOffset: 3901.105000068128 originFrequency: 600.173901105 pulseStrength90: 26150.62761506276 experimentNumber: 0 linearPredictionBin: 0 lpNumberOfCoefficients: 0 windowMultiplicationMode: 1