DOI: 10.57992/nmrxiv.p159.s1620
title: 8-epi-6-deoxytetrodotoxin

description: This dataset contains NMR spectra obtained for the sample -8-epi-6-deoxytetrodotoxin Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: 1d Temperature: 293.147 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 100 NMR Pulse Sequence: zg30 Spectral Width: 19.8351967631727 Number of Data Points: 65536 Relaxation Delay: 1 Observed Frequency: 600.183706111 Nucleus: 1H,1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: cosy Temperature: 293.1434 Observed Frequency: 600.18,600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 60 NMR Pulse Sequence: cosygpppqf Spectral Width: 5.95057893434693,5.95057893434693 Number of Data Points: 2048,128 Relaxation Delay: 2 Observed Frequency: 600.181698425034,600.181698425034 Nucleus: 1H,13C NMR Solvent: D2O NMR Probe: Z128744_0002 (CP TCI 600S3  H&F-C/N-D-05 Z LT) NMR Pulse Sequence: hmbc Temperature: 293.1536 Observed Frequency: 600.03,150.877663506 Magnetic Field Strength: 14.092661649151344 Number of Scans: 280 NMR Pulse Sequence: hmbcetgpl3nd Spectral Width: 5.9948871209802,209.721216838969 Number of Data Points: 4096,128 Relaxation Delay: 2 Observed Frequency: 600.031698606883,150.893505660668 Nucleus: 1H,13C NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: hsqc Temperature: 293.1446 Observed Frequency: 600.18,150.915381036 Magnetic Field Strength: 14.096184638414169 Number of Scans: 280 NMR Pulse Sequence: hsqcedetgpsisp2.3 Spectral Width: 5.95057893249694,165 Number of Data Points: 2048,128 Relaxation Delay: 1.5 Observed Frequency: 600.181698611626,150.92669969 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1481 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.3929 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1499 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.2077 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1499 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1475 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1553 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.15 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1494 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 13.6570207221845 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H,1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: tocsy Temperature: 293.1461 Observed Frequency: 600.18,600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 60 NMR Pulse Sequence: mlevphpp Spectral Width: 5.95057893434693,5.95057893434693 Number of Data Points: 2048,128 Relaxation Delay: 2 Observed Frequency: 600.181698425034,600.181698425034