DOI: 10.57992/nmrxiv.p159.s1619
title: 1-hydroxy-8-epi-6,11-dideoxytetrodotoxin

description: This dataset contains NMR spectra obtained for the sample -1-hydroxy-8-epi-6,11-dideoxytetrodotoxin Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: 1d Temperature: 293.1472 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 100 NMR Pulse Sequence: zg30 Spectral Width: 19.8351967631727 Number of Data Points: 65536 Relaxation Delay: 1 Observed Frequency: 600.183706111 Nucleus: 1H,1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: cosy Temperature: 293.1519 Observed Frequency: 600.18,600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 92 NMR Pulse Sequence: cosygpppqf Spectral Width: 5.95057892166942,5.95057892166941 Number of Data Points: 2048,128 Relaxation Delay: 2 Observed Frequency: 600.181699703702,600.181699703702 Nucleus: 1H,13C NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: hmbc Temperature: 293.1523 Observed Frequency: 600.18,150.915381036 Magnetic Field Strength: 14.096184638414169 Number of Scans: 360 NMR Pulse Sequence: hmbcetgpl3nd Spectral Width: 5.95057893728648,220 Number of Data Points: 4096,128 Relaxation Delay: 2 Observed Frequency: 600.181698128548,150.930472574 Nucleus: 1H,13C NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: hsqc Temperature: 293.2053 Observed Frequency: 600.18,150.915381036 Magnetic Field Strength: 14.096184638414169 Number of Scans: 200 NMR Pulse Sequence: hsqcedetgpsisp2.3 Spectral Width: 5.9505789351868,165 Number of Data Points: 2048,128 Relaxation Delay: 1.5 Observed Frequency: 600.181698340324,150.92669969 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1495 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1505 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1508 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1483 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.148 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1523 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1462 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: null Temperature: 293.1521 Observed Frequency: 600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 2400 NMR Pulse Sequence: selnogpzs.2 Spectral Width: 15.146877528241 Number of Data Points: 65536 Relaxation Delay: 2 Observed Frequency: 600.183706111 Nucleus: 1H,1H NMR Solvent: D2O NMR Probe: Z816801_0204 (PA TXI 600S3 H-C/N-D-05 Z) NMR Pulse Sequence: tocsy Temperature: 293.1482 Observed Frequency: 600.18,600.18 Magnetic Field Strength: 14.096184638414169 Number of Scans: 64 NMR Pulse Sequence: mlevphpp Spectral Width: 5.95057892166942,5.95057892166941 Number of Data Points: 2048,128 Relaxation Delay: 2 Observed Frequency: 600.181699703702,600.181699703702