cometadata/datacite-titles-descriptions-related-identifiers huggingface dataset:
DOI: 10.6084/m9.figshare.6318710.v1
title: Ultrasound assisted miniemulsion polymerization to prepare poly(urea-urethane) nanoparticles

description: Abstract Recently, the physical and chemical effects of ultrasound in polymeric materials synthesis have attracted great attention. This work presents the synthesis of novel polymeric materials by polymerization of isophorone diisocyanate with different polyols. Polymers were synthesized by step miniemulsion polymerizations, using ultrasound bath and thermostatic bath. The effects of ultrasound, temperature and polyol type were evaluated by Fourier transform infrared spectroscopy, gel permeation chromatography, dynamic light scattering and titrimetry. Polymerization under ultrasound bath showed that different reaction temperatures in the range between 50 °C and 80 °C directly influence the molecular weight of the polymers, urea/urethane formation and increase of diisocyanate consumption rate. In addition, different polyols used in polymerizations in miniemulsion had a significant effect on the characteristics of the resulting poly(urea-urethane) nanoparticles. Finally, ultrasound assisted polymerizations showed a faster diisocyanate consumption rate, but did not lead to enhanced molecular weights.
DOI: 10.6084/m9.figshare.6318707
title: Effect of heat cycling on melting and crystallization of PHB/TiO2 compounds

description: Abstract Compounds of poly(3-hydroxybutyrate) (PHB) and titanium dioxide (TiO2) with filler content between 1% and 10% were prepared in a laboratory internal mixer. The effect of heating and cooling rates on the crystallization and melting of PHB/TiO2 compounds was investigated by differential scanning calorimetry (DSC). Melt and cold crystallization rates rise with increasing cooling/heating rates. A higher cooling rate translates to a lower melt crystallization temperature, while a higher heating rate results in a higher cold crystallization temperature. TiO2 promotes melt crystallization of PHB, behaving as a nucleant agent. The total crystallinity developed after melt and cold crystallization decreases for low levels of TiO2, i.e. 2% per weight, and is almost independent of the heating/cooling rate. The melting temperatures and rates are minimally affected by both the heating rate and filler content. The results suggest that the desired PHB microstructure can be controlled by filler content and adjusted heating/cooling rate.
DOI: 10.6084/m9.figshare.6318707.v1
title: Effect of heat cycling on melting and crystallization of PHB/TiO2 compounds

description: Abstract Compounds of poly(3-hydroxybutyrate) (PHB) and titanium dioxide (TiO2) with filler content between 1% and 10% were prepared in a laboratory internal mixer. The effect of heating and cooling rates on the crystallization and melting of PHB/TiO2 compounds was investigated by differential scanning calorimetry (DSC). Melt and cold crystallization rates rise with increasing cooling/heating rates. A higher cooling rate translates to a lower melt crystallization temperature, while a higher heating rate results in a higher cold crystallization temperature. TiO2 promotes melt crystallization of PHB, behaving as a nucleant agent. The total crystallinity developed after melt and cold crystallization decreases for low levels of TiO2, i.e. 2% per weight, and is almost independent of the heating/cooling rate. The melting temperatures and rates are minimally affected by both the heating rate and filler content. The results suggest that the desired PHB microstructure can be controlled by filler content and adjusted heating/cooling rate.
DOI: 10.6084/m9.figshare.6318704
title: Effectiveness and safety of carbohydrate counting in the management of adult patients with type 1 diabetes mellitus: a systematic review and meta-analysis

description: Abstract Objective: This study aimed to evaluate the effectiveness and safety of carbohydrate counting (CHOC) in the treatment of adult patients with type 1 diabetes mellitus (DM1). Materials and methods: We performed a systematic review of randomized studies that compared CHOC with general dietary advice in adult patients with DM1. The primary outcomes were changes in glycated hemoglobin (HbA1c), quality of life, and episodes of severe hypoglycemia. We searched the following electronic databases: Embase, PubMed, Lilacs, and the Cochrane Central Register of Controlled Trials. The quality of evidence was analyzed using the Grading of Recommendations Assessment, Development and Evaluation (GRADE). Results: A total of 3,190 articles were identified, and two reviewers independently screened the titles and abstracts. From the 15 potentially eligible studies, five were included, and 10 were excluded because of the lack of randomization or different control/intervention groups. Meta-analysis showed that the final HbA1c was significantly lower in the CHOC group than in the control group (mean difference, random, 95% CI: −0.49 (-0.85, −0.13), p = 0.006). The meta-analysis of severe hypoglycemia and quality of life did not show any significant differences between the groups. According to the GRADE, the quality of evidence for severe hypoglycemia, quality of life, and change in HbA1c was low, very low, and moderate, respectively. Conclusion: The meta-analysis showed evidence favoring the use of CHOC in the management of DM1. However, this benefit was limited to final HbA1c, which was significantly lower in the CHOC than in the control group.
DOI: 10.6084/m9.figshare.6318704.v1
title: Effectiveness and safety of carbohydrate counting in the management of adult patients with type 1 diabetes mellitus: a systematic review and meta-analysis

description: Abstract Objective: This study aimed to evaluate the effectiveness and safety of carbohydrate counting (CHOC) in the treatment of adult patients with type 1 diabetes mellitus (DM1). Materials and methods: We performed a systematic review of randomized studies that compared CHOC with general dietary advice in adult patients with DM1. The primary outcomes were changes in glycated hemoglobin (HbA1c), quality of life, and episodes of severe hypoglycemia. We searched the following electronic databases: Embase, PubMed, Lilacs, and the Cochrane Central Register of Controlled Trials. The quality of evidence was analyzed using the Grading of Recommendations Assessment, Development and Evaluation (GRADE). Results: A total of 3,190 articles were identified, and two reviewers independently screened the titles and abstracts. From the 15 potentially eligible studies, five were included, and 10 were excluded because of the lack of randomization or different control/intervention groups. Meta-analysis showed that the final HbA1c was significantly lower in the CHOC group than in the control group (mean difference, random, 95% CI: −0.49 (-0.85, −0.13), p = 0.006). The meta-analysis of severe hypoglycemia and quality of life did not show any significant differences between the groups. According to the GRADE, the quality of evidence for severe hypoglycemia, quality of life, and change in HbA1c was low, very low, and moderate, respectively. Conclusion: The meta-analysis showed evidence favoring the use of CHOC in the management of DM1. However, this benefit was limited to final HbA1c, which was significantly lower in the CHOC than in the control group.
DOI: 10.6084/m9.figshare.6318701
title: Growth and quality of potted ornamental peppers treated with paclobutrazol

description: Abstract: The objective of this work was to evaluate the action of paclobutrazol (PBZ) on the growth and ornamental value of two pepper accessions and two commercial cultivars of ornamental pepper - Biquinho Vermelha and Bode Amarela. A PBZ aqueous solution (250 mL) was used to soak the substrate at 0, 20, 40, and 60 mg L-1 a.i. concentrations when the plants had 12 cm height. At the end of plant growth, the follwoing parameters were evaluated: plant height, chlorophyll content in leaves, number of fruit and leaves, and canopy compactness at the time the plants reached maturity to be marketed, with 30% of ripe fruit. Irrespective of the applied PBZ concentration, plant height diminished, and chlorophyll content increased. PBZ did not improve the ornamental characteristics of the genotypes 'Biquinho Vermelha' and 2334PB, which resulted in unsuitable plants for market requirements. For the genotypes 2345PB and 'Bode Amarela', the application of 20 mg L-1 of PBZ is the most indicated, and it results in plants with adequate ornamental characteristics required by the national market of flowers and ornamental plants.
DOI: 10.6084/m9.figshare.6318701.v1
title: Growth and quality of potted ornamental peppers treated with paclobutrazol

description: Abstract: The objective of this work was to evaluate the action of paclobutrazol (PBZ) on the growth and ornamental value of two pepper accessions and two commercial cultivars of ornamental pepper - Biquinho Vermelha and Bode Amarela. A PBZ aqueous solution (250 mL) was used to soak the substrate at 0, 20, 40, and 60 mg L-1 a.i. concentrations when the plants had 12 cm height. At the end of plant growth, the follwoing parameters were evaluated: plant height, chlorophyll content in leaves, number of fruit and leaves, and canopy compactness at the time the plants reached maturity to be marketed, with 30% of ripe fruit. Irrespective of the applied PBZ concentration, plant height diminished, and chlorophyll content increased. PBZ did not improve the ornamental characteristics of the genotypes 'Biquinho Vermelha' and 2334PB, which resulted in unsuitable plants for market requirements. For the genotypes 2345PB and 'Bode Amarela', the application of 20 mg L-1 of PBZ is the most indicated, and it results in plants with adequate ornamental characteristics required by the national market of flowers and ornamental plants.
DOI: 10.6084/m9.figshare.6318698
title: Applicability of Longitudinal Strain of Left Ventricle in Unstable Angina

description: Abstract Background: Unstable angina (UA) is a common cause of hospital admission; risk stratification helps determine strategies for treatment. Objective: To determine the applicability of two-dimensional longitudinal strain (SL2D) for the identification of myocardial ischemia in patients with UA. Methods: Cross-sectional, descriptive, observational study lasting 60 days. The sample consisted of 78 patients, of which fifteen (19.2%) were eligible for longitudinal strain analysis. The value of p &lt; 0.05 was considered significant. Results: The group of ineligible patients presented: a lower proportion of women, a higher prevalence of diabetes mellitus (DM), use of ASA, statins and beta-blockers and larger cavity diameters. The main causes of non-applicability were: presence of previous infarction (56.4%), previous CTA (22.1%), previous MRI (11.5%) or both (16.7%) and the presence of specific electrocardiographic abnormalities (12.8%). SL2D assessment revealed a lower global strain value in those with stenosis greater than 70% in some epicardial coronary arteries (17.1 [3.1] versus 20.2 [6.7], with p = 0.014). Segmental strain assessment showed an association between severe CX and RD lesions with longitudinal strain reduction of lateral and inferior walls basal segments; (14 [5] versus 21 [10], with p = 0.04) and (12.5 [6] versus 19 [8], respectively). Conclusion: There was very low SL2D applicability to assess ischemia in the studied population. However, the global strain showed a correlation with the presence of significant coronary lesion, which could be included in the UA diagnostic arsenal in the future.
DOI: 10.6084/m9.figshare.6318698.v1
title: Applicability of Longitudinal Strain of Left Ventricle in Unstable Angina

description: Abstract Background: Unstable angina (UA) is a common cause of hospital admission; risk stratification helps determine strategies for treatment. Objective: To determine the applicability of two-dimensional longitudinal strain (SL2D) for the identification of myocardial ischemia in patients with UA. Methods: Cross-sectional, descriptive, observational study lasting 60 days. The sample consisted of 78 patients, of which fifteen (19.2%) were eligible for longitudinal strain analysis. The value of p &lt; 0.05 was considered significant. Results: The group of ineligible patients presented: a lower proportion of women, a higher prevalence of diabetes mellitus (DM), use of ASA, statins and beta-blockers and larger cavity diameters. The main causes of non-applicability were: presence of previous infarction (56.4%), previous CTA (22.1%), previous MRI (11.5%) or both (16.7%) and the presence of specific electrocardiographic abnormalities (12.8%). SL2D assessment revealed a lower global strain value in those with stenosis greater than 70% in some epicardial coronary arteries (17.1 [3.1] versus 20.2 [6.7], with p = 0.014). Segmental strain assessment showed an association between severe CX and RD lesions with longitudinal strain reduction of lateral and inferior walls basal segments; (14 [5] versus 21 [10], with p = 0.04) and (12.5 [6] versus 19 [8], respectively). Conclusion: There was very low SL2D applicability to assess ischemia in the studied population. However, the global strain showed a correlation with the presence of significant coronary lesion, which could be included in the UA diagnostic arsenal in the future.
DOI: 10.6084/m9.figshare.6318695
title: The Iron Sulfides Crystal Growth from the Halide Melts

description: A new approach to a single crystals growth of the iron sulfide phases of definite structure and nonstoichiometry is developed and applied. This approach is based on the method of crystal growing from solution melts. This approach is based on the crystallization or recrystallization of iron sulfides from iron sulfide solutions in iron dihalide melts under fixed sulfur vapor pressure in the closed system in non-isothermal (two-temperature) conditions. It allows to regulate the composition and structure of the resulting iron sulphide. In particular, at a relatively low pressure (&lt;0.4 atm), pyrrhotite with a trigonal 3T structure is synthesized. At higher pressure pyrite β-FeS2 is grown. Reaction scheme for the formation of iron sulphides based on the reversible oxidation of sulfur by iron dihalide is proposed and substantiated. On the base of the {pyrite + marcasite} - mixture annealing under the melts of the deepest eutectic compositions of KCl - FeCl2 and NaCl - KCl - FeCl2 systems, the instability of the marcasite phase regarding the pyrite one (at least, for T ≥ 340°C) was shown.
DOI: 10.6084/m9.figshare.6318695.v1
title: The Iron Sulfides Crystal Growth from the Halide Melts

description: A new approach to a single crystals growth of the iron sulfide phases of definite structure and nonstoichiometry is developed and applied. This approach is based on the method of crystal growing from solution melts. This approach is based on the crystallization or recrystallization of iron sulfides from iron sulfide solutions in iron dihalide melts under fixed sulfur vapor pressure in the closed system in non-isothermal (two-temperature) conditions. It allows to regulate the composition and structure of the resulting iron sulphide. In particular, at a relatively low pressure (&lt;0.4 atm), pyrrhotite with a trigonal 3T structure is synthesized. At higher pressure pyrite β-FeS2 is grown. Reaction scheme for the formation of iron sulphides based on the reversible oxidation of sulfur by iron dihalide is proposed and substantiated. On the base of the {pyrite + marcasite} - mixture annealing under the melts of the deepest eutectic compositions of KCl - FeCl2 and NaCl - KCl - FeCl2 systems, the instability of the marcasite phase regarding the pyrite one (at least, for T ≥ 340°C) was shown.
DOI: 10.6084/m9.figshare.6318692
title: Preparation and characterization of composites from plastic waste and sugar cane fiber

description: Abstract This study presents the preparation and characterization of composite materials using Plastic Waste from Hydrapulper (PWH) from paper industries extruded with sugar cane fiber residues from ethanol industries. The factorial design showed that composite material with 40% of sugar cane fiber, pressed with 5 ton was the optimized condition. The main findings attested that the composite is resistant up to 250 °C and its hardness is increased compared to the raw PWH. The material presented woodsy aspect although water absorption has increased. So, this study offers a good alternative for the use of plastic waste generated as a by-product of recycled paper industry as well as a destination to the sugar cane bagasse.
DOI: 10.6084/m9.figshare.6318692.v1
title: Preparation and characterization of composites from plastic waste and sugar cane fiber

description: Abstract This study presents the preparation and characterization of composite materials using Plastic Waste from Hydrapulper (PWH) from paper industries extruded with sugar cane fiber residues from ethanol industries. The factorial design showed that composite material with 40% of sugar cane fiber, pressed with 5 ton was the optimized condition. The main findings attested that the composite is resistant up to 250 °C and its hardness is increased compared to the raw PWH. The material presented woodsy aspect although water absorption has increased. So, this study offers a good alternative for the use of plastic waste generated as a by-product of recycled paper industry as well as a destination to the sugar cane bagasse.
DOI: 10.6084/m9.figshare.6318689
title: Low-protein diet does not alter reproductive, biochemical, and hematological parameters in pregnant Wistar rats

description: The aim of this study was to investigate the reproductive, biochemical, and hematological outcomes of pregnant rats exposed to protein restriction. Wistar rat dams were fed a control normal-protein (NP, 17% protein, n=8) or a low-protein (LP, 8% protein, n=14) diet from the 1st to the 20th day of pregnancy. On the 20th day, the clinical signs of toxicity were evaluated. The pregnant rats were then anesthetized and blood samples were collected for biochemical-hematological analyses, and laparotomy was performed to evaluate reproductive parameters. No sign of toxicity, or differences (P&gt;0.05) in body weight gain and biochemical parameters (urea, creatinine, albumin, globulin, and total protein) between NP and LP pregnant dams were observed. Similarly, hematological data, including red blood cell count, white blood cell count, hemoglobin, hematocrit, red blood cell distribution width (coefficient of variation), mean corpuscular volume, mean corpuscular hemoglobin, mean corpuscular hemoglobin concentration, % lymphocytes, absolute lymphocyte count, platelet count, and mean platelet volume were similar (P&gt;0.05) at the end of pregnancy. Reproductive parameters (the dam-offspring relationship, ovary mass, placenta mass, number of corpora lutea, implantation index, resorption index, and the pre- and post-implantation loss rates) were also not different (P&gt;0.05) between NP and LP pregnant dams. The present data showed that a protein-restricted diet during pregnancy did not alter reproductive, biochemical, and hematological parameters and seems not to have any toxic effect on pregnant Wistar rats.
DOI: 10.6084/m9.figshare.6318689.v1
title: Low-protein diet does not alter reproductive, biochemical, and hematological parameters in pregnant Wistar rats

description: The aim of this study was to investigate the reproductive, biochemical, and hematological outcomes of pregnant rats exposed to protein restriction. Wistar rat dams were fed a control normal-protein (NP, 17% protein, n=8) or a low-protein (LP, 8% protein, n=14) diet from the 1st to the 20th day of pregnancy. On the 20th day, the clinical signs of toxicity were evaluated. The pregnant rats were then anesthetized and blood samples were collected for biochemical-hematological analyses, and laparotomy was performed to evaluate reproductive parameters. No sign of toxicity, or differences (P&gt;0.05) in body weight gain and biochemical parameters (urea, creatinine, albumin, globulin, and total protein) between NP and LP pregnant dams were observed. Similarly, hematological data, including red blood cell count, white blood cell count, hemoglobin, hematocrit, red blood cell distribution width (coefficient of variation), mean corpuscular volume, mean corpuscular hemoglobin, mean corpuscular hemoglobin concentration, % lymphocytes, absolute lymphocyte count, platelet count, and mean platelet volume were similar (P&gt;0.05) at the end of pregnancy. Reproductive parameters (the dam-offspring relationship, ovary mass, placenta mass, number of corpora lutea, implantation index, resorption index, and the pre- and post-implantation loss rates) were also not different (P&gt;0.05) between NP and LP pregnant dams. The present data showed that a protein-restricted diet during pregnancy did not alter reproductive, biochemical, and hematological parameters and seems not to have any toxic effect on pregnant Wistar rats.
DOI: 10.6084/m9.figshare.6318680
title: Eficiência Produtiva das Fazendas de Carcinicultura no Estado do Ceará

description: Abstract: The productive efficiency of shrimp farming has been pointed out in the literature as an important factor for the consolidation of this activity in Northeast Brazil. In order to assist decision making on the farm and the formulation of policies for the sector, this research investigated the degree and determinants of technical efficiency in shrimp production in Ceará State. Based on data from the Carcinculture Census, collected by the Brazilian Association of Shrimp Breeders (ABCC, 2011), 100 farms were characterized by a set of explanatory variables that describe the inputs used in the production and the way of managing the farms. To analyze data, we estimated frontier models of stochastic production efficiency. The results showed that almost all farms (99%) can be considered technically inefficient. The factor that determined the inefficiency of the sample farms was the average storage density, since other variables tested as inefficiency (which were: power of aerators per area, receipt of technical assistance and use of feed trays) were not significant at a significance level of 5%. As a result, these variables do not generate inefficiency in the model.
DOI: 10.6084/m9.figshare.6318680.v1
title: Eficiência Produtiva das Fazendas de Carcinicultura no Estado do Ceará

description: Abstract: The productive efficiency of shrimp farming has been pointed out in the literature as an important factor for the consolidation of this activity in Northeast Brazil. In order to assist decision making on the farm and the formulation of policies for the sector, this research investigated the degree and determinants of technical efficiency in shrimp production in Ceará State. Based on data from the Carcinculture Census, collected by the Brazilian Association of Shrimp Breeders (ABCC, 2011), 100 farms were characterized by a set of explanatory variables that describe the inputs used in the production and the way of managing the farms. To analyze data, we estimated frontier models of stochastic production efficiency. The results showed that almost all farms (99%) can be considered technically inefficient. The factor that determined the inefficiency of the sample farms was the average storage density, since other variables tested as inefficiency (which were: power of aerators per area, receipt of technical assistance and use of feed trays) were not significant at a significance level of 5%. As a result, these variables do not generate inefficiency in the model.