Title: NMR spectroscopy explained : simplified theory, applications and examples for organic chemistry and structural biology /
Authors: Jacobsen, Neil E.
Publisher: Wiley-Interscience,
Year: 2007
Subjects: Nuclear magnetic resonance spectroscopy.; Chemistry, Organic.; Molecular biology.; Magnetic Resonance Spectroscopy; Chemistry, Organic; Molecular Biology
Abstract: "Used in concert with complementary analytical techniques such as light spectroscopy and mass spectrometry, Nuclear Magnetic Resonance (NMR) spectroscopy is the most powerful tool for the determination of organic structure. This book fosters a real-world understanding of NMR spectroscopy and how it works without burying the reader in technical details and physical and mathematical formalism." "It is an ideal reference for professionals in industry and academia who use NMR spectroscopy technology, NMR facility managers, and upper-level undergraduates and graduate students in organic chemistry, biochemistry, pharmacology, biophysics, and engineering."--Jacket.
Contents: Fundamentals of NMR spectroscopy in liquids -- Interpretation of proton (¹H) NMR spectra -- NMR hardware and software -- Carbon-13 (¹³C) NMR spectroscopy -- NMR relaxation - inversion-recovery and the nuclear Overhauser effect (NOE) -- The spin-echo and the attached proton test (APT) -- Coherence transfer: INEPT and DEPT -- Shaped pulses, pulsed field gradients and spin-locks: selective 1D NOE and 1D TOCSY -- Two-dimensional NMR spectroscopy: HETCOR, COSY and TOCSY -- Advanced NMR theory: NOESY and DQF-COSY -- Inverse heteronuclear 2D experiments: HSQC, HMQC and HMBC -- Biological NMR spectroscopy -- Appendix A: A pictorial guide to NMR spin states -- Appendix B: A survey of two-dimensional NMR experiments.