bluuebunny/crossref_metadata_2025_split huggingface dataset:
In Quest of Intercivilizational Human Rights: "Universal" vs. "Relative" Human Rights Viewed from an Asian Perspective
Authors:   Yasuaki
Published: November 2003

AbstractProfessor Onuma Yasuaki is one of Japan's leading experts on human rights. He is a Professor of International Law at the University of Tokyo's Graduate School of Law and Politics and has been visiting professor and scholar at several universities including Yale Law School, Harvard Law School, Princeton University, the University of Edinburgh, and the Max Planck Institute für auslandisches und internationales Strafrecht. Professor Yasuaki has been widely published in English and Japanese dealing with international law. His article was initially prepared as an Occasional Paper of The Asia Foundation and is published with the Foundation's permission.
Japan's Wartime Compensation: Forced Labour
Authors:   Schmidt
Published: November 2003

AbstractHalf-a-century after the end of the war, today the victims of Japanese aggression in the Asia-Pacific region seek compensation for the wrong they had suffered.One of the largest groups of victimised people is that of Korean forced labourers. The still unsolved issues caused by the wrong those individuals suffered, include, among others, the non-payment of wages and savings, compensation for inhumane treatment during deportation and forced labour, compensation for hibakusha, and for those labourers who after the end of the war had been left behind on the Soviet island of Sakhalin.Both the Japanese Government as well as private companies employing forced labourers reject any and all demands, pointing both at the expiry of claims under municipal Japanese law and at the waiver of claims by the Korean Government in a 1965 bilateral agreement with Japan.This article studies possible regimes in municipal Japanese and in international law under which the affected individuals could seek payment and compensation from the Japanese Government.
Day-case myringoplasty: five years’ experience
Authors: Karkanevatos A. , De S. , Srinivasan V. R. , Roland N. J. , Lesser T. H. J. 
Published: November 2003

A retrospective study of patients who underwent myringoplasty as a day-case procedure in two freestanding day-surgery units during a five-year period was carried out.Their case notes were identified and details including age, site and size of perforation, grade of surgeon, surgical approach, graft material, post-operative dressings, overnight stay, complications, and outcome were noted and analysed.The total number of patients including both children and adults who had myringoplasty as a day case was 144. Of these, 125 patients with 143 procedures were included in this study. Their ages ranged from four to 74 years (mean = 31 years). The perforation size was small in 40 cases, medium in 61 cases, and large/subtotal in 42 cases. The overnight stay rate was 2.7 per cent and this was for immediate post-operative problems such as nausea and bleeding from the wound. The readmission rate for post-operative complications was 2.1 per cent. The follow-up ranged from six months to five years (mean = 19 months). The success rate was 83.3 per cent and thresholds on pure tone audiometry improved in 69.2 per cent of cases. The age of the patient, grade of the surgeon, and graft material did not influence the surgical outcome. There was no case of dead ear as a result of surgery.Myringoplasty can be safely performed in both adults and children as a day-case procedure with low overnight stay and readmission rates. Success rates are comparable to when the procedure is performed on an in-patient basis.
Conversion from a non-indwelling to a Provox®2 indwelling voice prosthesis for speech rehabilitation: comparison of voice quality and patient preference
Authors: Vlantis A. C. , Gregor R. T. , Elliot H. , Oudes M. 
Published: November 2003

This prospective study assessed the advantages and problems associated with converting a patient using an older generation non-indwelling voice prosthesis to a newer generation indwelling voice prosthesis, in this case the Provox®2. The voice characteristics of each patient were measured using the old and then the new voice prosthesis. Technical aspects of the insertion of the indwelling prosthesis were noted. Each patient completed a questionnaire after a period of use with the indwelling prosthesis.Changing the prosthesis was simple and uncomplicated in 15 of 17 patients. Acoustic analysis showed improved parameters with the indwelling prosthesis, but no perceptual difference between the two prostheses. The questionnaire revealed that most patients preferred the indwelling prosthesis.Replacing a non-indwelling with an indwelling prosthesis is technically simple, leading to improvement in voice quality and patient satisfaction. It may be reasonable to offer this choice to patients currently using an older generation non-indwelling voice prosthesis.
Alkyl and Alkylene Bromides
Authors: Kamm Oliver , Marvel C. S. , Goshorn R. H. , Boyd Thomas , Degering E. F. 
Published: November 2003

AbstractAlkyl and alkylene bromidesreactant: 48 per cent) hydrobromic acidproduct: allyl bromideproduct:iso‐amyl bromideproduct: butyl bromidereactant: 40 g. (0.22 mole) of lauryl alcoholproduct: bromideproduct: ethyl bromidereactant:n‐octyl alcoholproduct: bromidereactant: 456 g. (433 cc., 6 moles) of trimethylene glycolproduct: trimethylene bromideproduct: ethyl bromideproduct:iso‐propyl bromideproduct:n‐propyl bromideproduct: butyl bromideproduct: secondary butyl bromideproduct: bromide
1,4‐Aminonaphthol Hydrochloride
Authors: Conant J. B. , Lutz R. E. , Corson B. B. 
Published: November 2003

Abstract

1,4‐Aminonaphthol hydrochloride

reactant: 200 g. (1.39 moles) of α‐naphthol

intermediate: benzeneazo‐α‐naphthol

product: aminonaphthol hydrochloride
3‐Cyclohexyl‐2‐Bromopropene
Authors: Lespieau R. , Bourguel M. 
Published: November 2003

Abstract

3‐Cyclohexyl‐2‐bromopropene

reactant: 200 g. (1 mole) of 2,3‐dibromopropene

product: cyclohexylbromopropene

: 4‐phenyl‐2‐bromobutene

: 2‐bromodecene
Phenyl Isothiocyanate
Authors: Dains F. B. , Brewster R. Q. , Olander C. P. 
Published: November 2003

Abstract

Phenyl isothiocyanate

product: phenyl isothiocyanate

product:
p
‐iodophenyl

product:
p
‐isopropylphenyl

product:
m
‐(trifluoromethyl) phenyl

product:
m
‐bromophenyl

product: β‐naphthyl

product:
p
‐dimethylaminophenyl

product: 2‐methyl‐4‐isopropylphenyl
β‐Bromoethylphthalimide
Authors: Salzberg P. L. , Supniewski J. V. 
Published: November 2003

Abstract

β‐Bromoethylphthalimide

intermediate: potassium phthalimide

reactant: 450 g. (2.4 moles) of ethylene dibromide

product: bromoethylphthalimide
Ethyl Benzoylformate
Authors: Corson B. B. , Dodge Ruth A. , Harris S. A. , Hazen R. K. 
Published: November 2003

Abstract

Ethyl benzoylformate

product: ethyl benzoylformate

byproduct: ethyl benzoate

byproduct: 60 g. of impure methyl benzoate

product: 20 per cent of methyl benzoylformate
Sodium
p
‐Arsono‐
N
‐phenylglycinamide
Authors: Jacobs W. A. , Heidelberger M. 
Published: November 2003

Abstract

Sodium
p
‐arsono‐
N
‐phenylglycinamide

reactant: 130 g. (0.6 mole) of arsanilic acid

product: sodium
p
‐arsono‐
N
‐phenylglycinamide
α‐Bromoisovaleric Acid
Authors: Marvel C. S. , du Vigneaud V. 
Published: November 2003

Abstractα‐bromoisovaleric acidreactant: 202 g. (1 mole) of isopropylmalonic esterproduct: α‐bromo‐n‐caproic acidproduct: α‐bromoisocaproic acidproduct: α‐bromo‐β‐methylvaleric acidproduct: α‐Bromoisovaleric acid
Triethyl Carbinol
Authors: Moyer W. W. , Marvel C. S. 
Published: November 2003

Abstract

Triethyl carbinol

reactant: 5 cc. (7 g., 0.06 mole) of ethyl bromide

product: triethyl carbinol

product: tri‐
n
‐propyl carbinol

product: tri‐
n
‐butyl carbinol

product: tri‐
n
‐amyl carbinol

product: tri‐
n
‐heptyl carbinol
2,4‐Dinitrobenzaldehyde
Authors: Bennett G. M. , Bell E. V. 
Published: November 2003

Abstract

2,4‐Dinitrobenzaldehyde

intermediate:
p
‐nitrosodimethylaniline hydrochloride

reactant: 300 g. (1.6 moles) of 2,4‐dinitrotoluene

solvent: 8 l. of naphtha

intermediate:
p
‐nitrosodiethylaniline

product: 2,4‐Dinitrobenzaldehyde
dl
‐Methionine
Authors: Barger G. , Weichselbaum T. E. 
Published: November 2003

Abstract

dl
‐Methionine

intermediate: Ethyl 1‐Methylthiol‐3‐phthalimidopropane‐3,3‐dicarboxylate

reactant: 85 g. (0.26 mole) of ethyl sodium phthalimidomalonate

intermediate: 1‐
Methylthiol
‐3‐
phthalamidopropane
‐3,3‐
dicarboxylic Acid

byproduct: phthalic acid

product: Methionine
2,6‐Dibromoquinone‐4‐chloroimide
Authors: Hartman W. W. , Dickey J. B. , Stampfli J. G. 
Published: November 2003

Abstract2,6‐Dibromoquinone‐4‐chloroimideintermediate: 2,6‐Dibromo‐4‐aminophenol Chlorostannateproduct: 2,6‐dibromoquinone‐4‐chloroimide
Homoveratric Acid
Authors: Snyder H. R. , Buck J. S. , Ide W. S. 
Published: November 2003

AbstractHomoveratric acidreactant: 200 g. (0.65 mole) of the azlactone of α‐benzoylamino‐β‐(3,4‐dimethoxyphenyl) acrylic acidbyproduct: methyl benzoateintermediate: methyl homoveratrateproduct: hydrate of homoveratric acidsolvent: 150 cc. of hot ligroinproduct: homoveratric acidintermediate: 3,4‐Dimethoxyphenylpyruvic acid
Coupling of
o
‐Tolidine and Chicago Acid
Authors: Hartwell J. L. , Fieser Louis F. 
Published: November 2003

Abstract

Coupling of
o
‐tolidine and chicago acid

product: 1,3‐Naphthalenedisulfonic acid, 6,6′‐[(3,3′‐dimethyl[1,1′‐biphenyl]‐4,4′diyl)bis(azo)]bis[4‐amino‐5‐hydroxy‐, tetrasodium salt

product: dye (“Tolidine‐1824”)
2,5‐Dimethylpyrrole
Authors: Young D. M. , Allen C. F. H. 
Published: November 2003

Abstract2,5‐Dimethylpyrrolereactant: 100 g. (0.88 mole) of acetonylacetonereactant: 125 g. (1.2 moles) of 2,5‐dimethylfuranproduct: 2,5‐dimethylpyrrole
2,4‐Dimethyl‐5‐carbethoxypyrrole
Authors: Fischer Hans 
Published: November 2003

Abstract2,4‐Dimethyl‐5‐Carbethoxypyrrolereactant: 58 g. (51 cc., 0.53 mole) of freshly distilled ethyl chloroformateproduct: 2,4‐dimethyl‐5‐carbethoxypyrrole
α‐Phenylethylamine
Authors: Ingersoll A. W. 
Published: November 2003

Abstractα‐Phenylethylaminereactant: 150 g. (1.25 moles) of acetophenoneproduct: α‐p‐tolylethylamineproduct: α‐p‐chlorophenylethylamineproduct: α‐p‐bromophenylethylamineproduct: α‐p‐xenylethylamineproduct: α‐(β‐naphthyl)‐ethylamineproduct: α‐Phenylethylamine
3,4‐Dihydro‐1,2‐naphthalic Anhydride
Authors: Hershberg E. B. , Fieser Louis F. 
Published: November 2003

Abstract

3,4‐Dihydro‐1,2‐Naphthalic Anhydride

product: 3,4‐Dihydro‐1,2‐naphthalic anhydride

reactant: 50 g. (0.26 mole) of ethyl γ‐phenylbutyrate

solvent: 75 cc. of ligroin
Diphenylselenium Dichloride and Triphenylselenonium Chloride
Authors: Leicester Henry M. 
Published: November 2003

Abstract

Diphenylselenium Dichloride and Triphenylselenonium Chloride

product: 40 g. (0.13 mole) of diphenylselenium dichloride in portions of approximately 1 g.

product: triphenylselenonium chloride
2‐Amino‐4‐methylthiazole
Authors: Byers J. R. , Dickey J. B. 
Published: November 2003

Abstract2‐amino‐4‐methylthiazolereactant: 92.5 g. (80 cc., 1 mole) of chloroacetoneproduct: 2‐amino‐4‐methylthiazole
Cyclohexylbenzene
Authors: Corson B. B. , Ipatieff V. N. 
Published: November 2003

AbstractCyclohexylbenzenereactant: 164 g. (203 cc., 2 moles) of cyclohexeneproduct: cyclohexylbenzenereactant: cyclopentenebyproduct: 1,4‐dicyclohexylbenzene
5,5‐Dimethylhydantoin
Authors: Wagner E. C. , Baizer Manuel 
Published: November 2003

Abstract

5,5‐Dimethylhydantoin

product: 5,5‐dimethylhydantoin

reactant: 85 g. (1 mole) of acetone cyanohydrin

product: 5‐methyl‐5‐ethylhydantoin
Terephthalaldehyde
Authors: Snell J. M. , Weissberger A. 
Published: November 2003

Abstract

Terephthalaldehyde

intermediate: α,α,α′,α′‐
Tetrabromo‐p‐xylene

reactant: 100 g. (0.94 mole) of dry
p
‐xylene

product: Terephthalaldehyde
dl‐Threonine
Authors: Carter Herbert E. , West Harold D. 
Published: November 2003

Abstractdl‐Threonineintermediate: α‐Bromo‐β‐methoxy‐n‐butyric acid.intermediate: formyl‐dl‐O‐methylthreonineproduct:dl‐threonineintermediate: Formyl‐dl‐O‐methylallothreonine
2,6‐Dihydroxyacetophenone
Authors: Russell Alfred , Frye John R. 
Published: November 2003

Abstract

2,6‐Dihydroxyacetophenone

intermediate: 4‐methyl‐7‐hydroxycoumarin

intermediate: 4‐methyl‐7‐acetoxycoumarin

intermediate: 4‐
Methyl
‐7‐
hydroxy
‐8‐
acetylcoumarin

product: 2,6‐dihydroxyacetophenone
4,4′‐Diaminodiphenylsulfone
Authors: Ferry C. W. , Buck J. S. , Baltzly R. 
Published: November 2003

Abstract

4,4′‐Diaminodiphenylsulfone

reactant: 48.5 g. (0.22 mole) of the sodium sulfinate

reactant: 31.5 g. (0.2 mole) of 4‐chloronitrobenzene

intermediate:
p
‐nitro‐
p
′‐acetylaminodiphenylsulfone

product: 4,4′‐Diaminodiphenylsulfone
2,3‐Dimethyl‐1,3‐Butadiene
Authors: Allen C. F. H. , Bell Alan , Newton L. W. , Coburn E. R. 
Published: November 2003

Abstract

2,3‐Dimethyl‐1,3‐butadiene

product: 2,3‐Dimethylbutadiene

intermediate: Pinacolone

reactant: pinacol hydrate

reactant: pinacol
2,5‐Dinitrobenzoic Acid
Authors: Langley Wilson D. 
Published: November 2003

Abstract

2,5‐Dinitrobenzoic acid

intermediate: 2‐nitroso‐5‐nitrotoluene

product: 2,5‐dinitrobenzoic acid

product: 3,4‐dinitrobenzoic acid

intermediate: nitrosonitrotoluene
β‐
d
‐Glucose‐1,2,3,4‐Tetraacetate
Authors: Reynolds Delbert D. , Evans William Lloyd 
Published: November 2003

Abstract

β‐
d
‐Glucose‐1,2,3,4‐tetraacetate

intermediate: 6‐trityl‐β‐
d
‐glucose‐1,2,3,4‐tetraacetate

product: β‐
d‐Glucose‐1,2,3,4‐tetraacetate
Imidazole
Authors: Snyder H. R. , Handrick R. G. , Brooks L. A. 
Published: November 2003

Abstract

Imidazole

reactant: 200 g. (1.33 moles) of powdered
d
‐tartaric acid

intermediate: imidazole‐4,5‐dicarboxylic acid

product: imidazole
l
‐Menthoxyacetic Acid
Authors: Leffler M. T. , Calkins A. E. 
Published: November 2003

Abstract

l
‐Menthoxyacetic acid

reactant: 400 g. (2.56 moles) of
l
‐menthol

reactant: 95 g. (1.01 moles) of monochloroacetic acid

product:
l
‐menthoxyacetic acid
Mesitaldehyde
Authors: Fuson R. C. , Horning E. C. , Rowland S. P. , Ward M. L. , Barnes R. P. 
Published: November 2003

Abstract

Mesitaldehyde

product: mesitaldehyde

product: 2,4,6‐Triethylbenzaldehyde

product: 2,4,6‐triisopropylbenzaldehyde
β‐Naphthaldehyde
Authors: Williams Jonathan W. , Hershberg E. B. , Cason James 
Published: November 2003

Abstractβ‐Naphthaldehydecatalyst: 76 g. (0.4 mole) of anhydrous stannous chloridereactant: 30.6 g. (0.2 mole) of β‐naphthonitrilereactant: 57 g. (0.30 mole) of β‐naphthoyl chlorideproduct: β‐naphthaldehyde: 1‐Acetoxy‐3‐naphthaldehyde: Methyl β‐formylpropionate
1‐(α‐Pyridyl)‐2‐Propanol
Authors: Walter L. A. 
Published: November 2003

Abstract

1‐(α‐Pyridyl)‐2‐propanol

reactant: Forty‐six grams (0.5 mole) of α‐picoline

product: 1‐(α‐pyridyl)‐2‐propanol

byproduct: α‐picoline‐water azeotrope
γ‐Di‐
n
‐Butylaminopropylamine
Authors: Amundsen Lawrence H. , Sanderson James J. 
Published: November 2003

Abstract

γ‐di‐
n
‐butylaminopropylamine

reactant: 107 g. (0.40 mole) of γ‐bromopropylphthalimide

product: γ‐di‐
n
‐butylaminopropylamine

product: γ‐diethylaminopropylamine

product: γ‐di‐
n
‐propylaminopropylamine
Sorbic Acid
Authors: Allen C. F. H. , VanAllan J. 
Published: November 2003

AbstractSorbic acidreactant: 80 g. (93.2 ml., 1.14 moles) of crotonaldehydereactant: 120 g. (1.15 moles) of malonic acidsolvent: 120 g. (122 ml., 1.52 moles) of pyridineproduct: sorbic acid
Mesitylacetic Acid
Authors: Fuson Reynold C. , Rabjohn Norman 
Published: November 2003

Abstract

Mesitylacetic acid

intermediate: α
2
‐chloroisodurene

intermediate: mesitylacetonitrile

product: mesitylacetic acid

byproduct: α
2
,α
4
‐dichloropentamethylbenzene

product: 2,4,6‐triethylphenylacetonitrile

product: durylacetonitrile

product: isodurylacetonitrile
β‐Phenylethyldimethylamine
Authors: Icke Roland N. , Wisegarver Burnett B. , Alles Gordon A. 
Published: November 2003

Abstract

β‐Phenylethyldimethylamine

product: β‐phenylethyldimethylamine

product: benzyldodecylmethylamine

product: α‐amylhexyldimethylamine
Sebaconitrile and ω‐Cyanopelargonic Acid
Authors: Biggs B. S. , Bishop W. S. 
Published: November 2003

AbstractSebaconitrile and ω‐cyanopelargonic acidreactant: 505 g. (2.5 moles) of commercial sebacic acidreactant: 180 g. (3 moles) of ureaproduct: sebaconitrileproduct: ω‐cyanopelargonic acid
6,7‐Dimethoxy‐3,4‐Dihydro‐2‐Naphthoic Acid
Authors: Holmes H. L. , Trevoy L. W. 
Published: November 2003

Abstract

6,7‐dimethoxy‐3,4‐dihydro‐2‐naphthoic acid

reactant: 47.85 g. (0.19 mole) of ethyl γ‐veratrylbutyrate

intermediate: 3,4‐dihydro‐2‐naphthoic acid

byproduct: 7‐methoxy‐3,4‐dihydro‐2‐naphthoic acid

product: 6,7‐Dimethoxy‐3,4‐dihydro‐2‐naphthoic acid

product: 6,7‐dimethoxy‐2‐naphthoic acid
Salicyl‐
o
‐toluide
Authors: Allen C. F. H. , VanAllan J. 
Published: November 2003

Abstract

Salicyl‐
o
‐toluide

reactant: 42.8 g. (0.2 mole) of phenyl salicylate

solvent: 60 g. of 1,2,4‐trichlorobenzene

solvent: 75 ml. of ligroin

product: salicyl‐
o
‐toluide

product: Salicylanilide
4‐Ethylpyridine
Authors: Frank Robert L. , Smith Paul V. 
Published: November 2003

Abstract

4‐Ethylpyridine

product: 4‐ethylpyridine

product: 4‐propylpyridine

product: 4‐
n
‐butylpyridine

product: 4‐isobutylpyridine

product: 4‐isoamylpyridine

product: 4‐
n
‐octylpyridine
6‐Methoxy‐8‐nitroquinoline
Authors: Mosher Harry S. , Yanko William H. , Whitmore Frank C. 
Published: November 2003

Abstract

6‐Methoxy‐8‐nitroquinoline

reactant: 588 g. (3.5 moles) of 3‐nitro‐4‐aminoanisole

product: 6‐methoxy‐8‐nitroquinoline

product: 6‐ethoxy‐8‐nitroquinoline

product: 8‐methoxy‐6‐nitroquinoline

product: 6‐chloro‐8‐nitroquinoline

product: 6‐methoxy‐5‐bromo‐8‐nitroquinoline
Methyl 4‐Keto‐7‐Methyloctanoate
Authors: Cason James , Prout Franklin S. 
Published: November 2003

Abstract

Methyl 4‐keto‐7‐methyloctanoate

reactant: 151 g. (1.0 mole) of pure isoamyl bromide

product: methyl 4‐keto‐7‐methyloctanoate

reactant: methyl hydrogen succinate

: Ethyl 10‐keto‐13‐methyltetradecanoate

: Ethyl 10‐keto‐16‐methyloctadecanoate

: Ethyl 6‐ketoheptanoate

: Ethyl 10‐ketohendecanoate

: Ethyl 10‐keto‐14‐methyltetracosanoate
4‐Nitro‐1‐Naphthylamine
Authors: Price Charles C. , Voong Sing‐Tuh 
Published: November 2003

Abstract4‐Nitro‐1‐naphthylaminereactant: Twenty grams (0.115 mole) of α‐nitronaphthaleneproduct: 4‐nitro‐1‐naphthylamine
5‐Amino‐2,3‐dihydro‐1,4‐phthalazinedione
Authors: Redemann Carl T. , Redemann C. Ernst 
Published: November 2003

Abstract

5‐Amino‐2,3‐dihydro‐1,4‐phthalazinedione

product: 5‐amino‐2,3‐dihydro‐1,4‐phthalazinedione
2,6‐Dichlorophenol
Authors: Tarbell D. S. , Wilson J. W. , Fanta Paul E. 
Published: November 2003

Abstract

2,6‐Dichlorophenol

reactant: 250 g. (1.5 moles) of ethyl 4‐hydroxybenzoate

intermediate: ethyl 3,5‐dichloro‐4‐hydroxybenzoate hydrate

intermediate: 3,5‐
Dichloro
‐4‐
hydroxybenzoic acid

product: 2,6‐
Dichlorophenol

byproduct: 5% potassium chloride
Benzoylcholine Iodide and Chloride
Authors: Ford‐Moore A. H. 
Published: November 2003

Abstract

Benzoylcholine Iodide and Chloride

reactant: 80.5 g. (66ml., 1 mole) of redistilled ethylene chlorohydrin

intermediate: 2‐chloroethyl benzoate

intermediate: 194 g. (0.70 mole) of 2‐iodoethyl benzoate

reactant: 270 ml. of a 19.5% solution of trimethylamine

product: 210 g. (0.63 mole) of benzoylcholine iodide

product: Benzoylcholine chloride
Diethyl
cis
‐Δ
4
‐Tetrahydrophthalate and Diethyl
cis
‐Hexahydrophthalate
Authors: Cope Arthur C. , Herrick Elbert C. 
Published: November 2003

Abstract

Diethyl
cis
‐Δ
4
‐tetrahydrophthalate and diethyl
cis
‐hexahydrophthalate

product: Two hundred and twenty‐six grams (1 mole) of diethyl
cis
‐Δ
4
‐tetrahydrophthalate

product: diethyl
cis
‐hexahydrophthalate

product: Dimethyl
cis
‐Δ
4
‐tetrahydrophthalate

product: Dimethyl
cis
‐hexahydrophthalate
1‐Methyl‐3‐Ethyloxindole
Authors: Rutenberg M. W. , Horning E. C. 
Published: November 2003

Abstract

1‐Methyl‐3‐ethyloxindole

reactant: 237 g. (2.21 moles) of methylaniline

intermediate: 197 g. (1.06 moles) of α‐bromo‐
n
‐butyryl chloride

intermediate: N‐methyl‐α‐bromo‐
n
‐butyranilide

product: 1‐methyl‐3‐ethloxindole
α‐Acetyl‐δ‐chloro‐γ‐valerolactone
Authors: Zuidema G. D. , van Tamelen E. , Van Zyl G. 
Published: November 2003

Abstract

α‐Acetyl‐δ‐chloro‐γ‐valerolactone

reactant: Eastman Kodak Company white label quality ethyl acetoacetate

Butadiene monoxide

Propylene oxide

Styrene oxide

Ethyl glycidyl ether

Phenyl glycidyl ether

product: α‐Acetyl‐δ‐chloro‐γ‐valerolactone
Cyclohexylidenecyanoacetic Acid and 1‐Cyclohexenylacetonitrile
Authors: Cope Arthur C. , D'Addieco Alfred A. , Whyte Donald Edward , Glickman Samuel A. 
Published: November 2003

Abstract

Cyclohexylidenecyanoacetic acid and 1‐cyclohexenylacetonitrile

product: cyclohexylidenecyanoacetic acid

product: 1‐cyclohexenylacetonitrile
Diisopropyl Methylphosphonate
Authors: Ford‐Moore A. H. , Perry B. J. 
Published: November 2003

Abstract

Diisopropyl methylphosphonate

byproduct: isopropyl iodide

product: Diisopropyl ethylphosphonate

product: Diethyl ethylphosphonate

product: Diethyl methylphosphonate

product: Diisopropyl methylphosphonate
Hexamethylene Diisocyanate
Authors: Farlow Mark W. 
Published: November 2003

Abstract

Hexamethylene diisocyanate

intermediate: hexamethylenediammonium chloride

solvent: 500 ml. of anhydrous redistilled amylbenzene

solvent: tetralin

product: hexamethylene diisocyanate

product: polyhexamethylene urea
dl
‐4,4′,6,6′‐Tetrachlorodiphenic Acid
Authors: Atkinson Edward R. , Murphy Donald M. , Lufkin James E. 
Published: November 2003

Abstract

dl
‐4,4′,6,6′‐Tetrachlorodiphenic acid

intermediate: 3,5‐dichloro‐2‐aminobenzoic acid

product: dl‐4,4′,6,6′‐Tetrachlorodiphenic acid.
1,1′‐Azo‐
bis
‐1‐Cyclohexanenitrile
Authors: Overberger C. G. , Huang Pao‐tung , Berenbaum M. B. 
Published: November 2003

Abstract

1,1′‐Azo‐
bis
‐1‐cyclohexanenitrile

product: 2,2′‐Azo‐
bis
‐isobutyronitrile

product: 1,1′‐Azo‐
bis
‐1‐cyclohexanenitrile
Methyl
p
‐Acetylbenzoate
Authors: Emerson William S. , Deebel George F. 
Published: November 2003

Abstract

Methyl
p
‐acetylbenzoate

reactant: 29–32 g. of unreacted methyl
p
‐ethylbenzoate

product: methyl
p
‐acetylbenzoate

intermediate:
p
‐ethylbenzoic acid
Neophyl Chloride
Authors: Smith W. T. , Sellas J. T. 
Published: November 2003

Abstract

Neophyl chloride

reactant: 201 g. (219 ml., 2.22 moles) of methallyl chloride

product: neophyl chloride

byproduct:
p
‐di(chloro‐
tert
‐butyl)benzene
Diethyl 1,1‐Cyclobutanedicarboxylate
Authors: Mariella Raymond P. , Raube Richard 
Published: November 2003

Abstract

Diethyl 1,1‐cyclobutanedicarboxylate

reactant: 480 g. (3.0 moles) of diethyl malonate

reactant: 472 g. (3.0 moles) of trimethylene chlorobromide

product: cyclobutanecarboxylic acid

product: diethyl 1,1‐cyclobutanedicarboxylate
3‐Methylcoumarone
Authors: Boehme Werner R. 
Published: November 2003

Abstract

3‐Methylcoumarone

intermediate: ethyl α‐phenoxyacetoacetate

solvent: petroleum ether

intermediate: Ethyl 3‐methylcoumarilate (70 g.)

intermediate: 3‐methylcoumarilic acid

product:
3‐Methylcoumarone

reactant: ethyl α‐chloroacetoacetate
m
‐Nitrobenzazide
Authors: Munch‐Petersen Jon 
Published: November 2003

Abstract

m
‐Nitrobenzazide

intermediate: 185.5 g. (1 mole) of
m
‐nitrobenzoyl chloride in 300 ml. of acetone

product:
m
‐nitrobenzazide

solvent: ligroin

product:
p
‐nitrobenzazide
m‐Nitrostyrene
Authors: Wiley Richard H. , Smith Newton R. 
Published: November 2003

Abstractm‐Nitrostyrenereactant: 151 g. (1 mole) ofm‐nitrobenzaldehydeintermediate:m‐nitrocinnamic acidproduct:m‐nitrostyreneproduct:o‐nitrocinnamic acidproduct:p‐nitrocinnamic acidproduct:m‐cyanocinnamic acidproduct:o‐chlorocinnamic acidproduct:m‐chlorocinnamic acidproduct:p‐chlorocinnamic acidproduct: 2,4‐dichlorocinnamic acidproduct: 3,4‐dichlorocinnamic acidproduct:m‐bromocinnamic acidproduct:p‐methoxycinnamic acidproduct: 3,4‐dimethoxycinnamic acidproduct:o‐nitrostyreneproduct:p‐nitrostyreneproduct: 3‐nitro‐4‐hydroxystyreneproduct:o‐chlorostyreneproduct:m‐chlorostyreneproduct:p‐chlorostyreneproduct:m‐bromostyreneproduct:o‐methoxystyreneproduct:p‐methoxystyreneproduct:m‐cyanostyreneproduct:p‐formylstyrene