bluuebunny/crossref_metadata_2025_split huggingface dataset:
Clustering of variables to analyze spectral data
Authors: Vigneau E. , Sahmer K. , Qannari E. M. , Bertrand D. 
Published: November 2005

AbstractA cluster analysis of variables around latent variables is presented and applied in order to identify groups among near‐infrared (NIR) spectral variables. By organizing multivariate data into a small number of clusters, each of them being represented by a component, this approach makes it possible to reduce the dimensionality of the problem. For the NIR data considered herein, it turned out that the groups of spectral variables are associated with various spectral regions. This feature can be helpful for the interpretation of the outcomes. For a predictive perspective the groups of variables can be used as blocks in multiblock partial least squares models. Alternatively the latent variables associated with the various clusters can be used as predictors. The cluster analysis procedure together with how its outcomes can be used for prediction purposes are illustrated on the basis of sensory and NIR data on green peas. Copyright © 2005 John Wiley & Sons, Ltd.
Paired comparisons for the evaluation of crispness of cereal flakes by untrained assessors: correlation with descriptive analysis and acoustic measurements
Authors: Courcoux Philippe , Chaunier Laurent , Valle Guy Della , Lourdin Denis , Séménou Michel 
Published: November 2005

AbstractThis study investigates the effectiveness of the paired comparison method in the evaluation of a complex sensory attribute by untrained assessors. The crispness perception of cereal flakes by a panel of 100 consumers is measured using a complete block design, and the fitting of the Bradley–Terry–Luce model leads to a ranking of the samples on a crispness intensity scale. A log–linear formulation of the Bradley model provides insight into goodness‐of‐fit tests and allows the effects of covariates to be incorporated in the prediction of the sensory scores. Results show a high correlation between crispness assessment by consumers and rating of texture attributes by trained assessors. Acoustic emission is shown to have a significant effect on crispness perception, and the power spectra of signals recorded during compression provide a prediction of the crispness of cereal flakes. Copyright © 2005 John Wiley & Sons, Ltd.
Assessing the performance of a sensory panel–panellist monitoring and tracking
Authors: Kermit Martin , Lengard Valérie 
Published: November 2005

AbstractSensory science uses the human senses as instruments of measurement. This study presents univariate and multivariate data analysis methods to assess individual and group performances in a sensory panel. Green peas were evaluated by a trained panel of 10 assessors for six attributes over two replicates. A consonance analysis with principal component analysis (PCA) is run to get an overview of the panel agreement and detect major individual errors. The origin of the panellist errors is identified by a series of tests based on analysis of variance, i.e. sensitivity, reproducibility, crossover and panel agreement, complemented with an eggshell correlation test. One assessor is identified with further need for training in attributes pea flavour, sweetness, fruity and off‐flavour, showing errors in sensitivity, reproducibility and crossover. Another assessor shows poor performance for attribute mealiness and to some extent also fruity flavour. Only one panellist performs well to very well in all attributes. The specificity and complementarity of the series of univariate tests are explored and verified with the use of a PCA model. Copyright © 2005 John Wiley & Sons, Ltd.
Probabilistic scaling analyses of sensory profile, instrumental and hedonic data
Authors: MacKay David B. 
Published: November 2005

AbstractSensory and hedonic variability are fundamental psychological characteristics that must be explicitly modeled if one is to develop meaningful statistical models of sensory phenomena. Sensory objects are perceived with differential uncertainty. Subjects also differ; some are very certain about what they desire and others are not. When variability is not modeled, the variability becomes confounded with dissimilarity or disutility and the estimates lose their meaning. Probabilistic scaling models are proposed that explicitly measure sensory and hedonic variability. The resulting estimates are shown to be free of the systematic bias that characterizes traditional deterministic models. Applications of the proposed models are presented and extensions of the models that can help bridge the gap between sensory science, marketing and product development are illustrated. Copyright © 2005 John Wiley & Sons, Ltd.
Relating the sensory sensation ‘creamy mouthfeel’ in custards to rheological measurements
Authors: Jellema Renger H. , Janssen Anke M. , Terpstra Marjolein E. J. , de Wijk Rene A. , Smilde Age K. 
Published: November 2005

AbstractCharacteristics of food products are commonly assessed in series of sensory studies to gain insight which can be used, for instance, for product development. Sensory studies are very time‐consuming and susceptible to large sources of variation. Assessing information about (new) products by means of instrumental measurements would be very beneficial for numerous reasons, including repeatability, reproducibility and, most of all, the fact that instruments do not suffer from fatigue or adaptation. Measurements simulating sensory assessment of product properties can be performed at different stages of consumption and on different types of sensory attributes. In this study the relation between rheological parameters and creamy mouthfeel was investigated. The goal was to discover whether a model using a limited mechanical characterization, namely parameters describing bulk rheological behaviour, would suffice to describe the sensory attribute ‘creamy mouthfeel’, also called creaminess. The two main reasons for performing this study were (i) to investigate the possibility of using rheological measurements for high‐throughput screening of newly developed custard products without the need for involving sensory panels already at an early stage of product development and (ii) to gain knowledge about the correlation between rheological measurements and the multidimensional attribute creamy mouthfeel. The resulting model shows that prediction of creamy mouthfeel by means of rheological measurements is possible only to a certain extent ($Q_{\rm CV}^2=0.48$). Reasons that can be mentioned for deviations between measured creaminess and modelled creaminess are (i) variation in measured creamy mouthfeel scores (variation in y‐variable) and (ii) lack of description of surface properties of the food product by the rheological measurements used here. The results show that instrumental measurements are complementary to sensory analysis and can greatly facilitate the task for the practitioner at an early stage of product development, making high‐throughput screening of novel products feasible. Copyright © 2005 John Wiley & Sons, Ltd.
Mathematical improvements to maximum likelihood parallel factor analysis: theory and simulations
Authors: Vega‐Montoto Lorenzo , Gu Hong , Wentzell Peter D. 
Published: November 2005

AbstractA number of simplified algorithms for carrying out maximum likelihood parallel factor analysis (MLPARAFAC) for three‐way data affected by different error structures are described. The MLPARAFAC method was introduced to establish the theoretical basis to treat heteroscedastic and/or correlated noise affecting trilinear data. Unfortunately, the large size of the error covariance matrix employed in the general formulation of this algorithm prevents its application to solve standard three‐way problems. The algorithms developed here are based on the principle of alternating least squares, but differ from the generalized MLPARAFAC algorithm in that they do not use equivalent alternatives of the objective function to estimate the loadings for the different modes. Instead, these simplified algorithms tackle the loss of symmetry of the PARAFAC model by using only one representation of the objective function to estimate the loadings of all of the modes. In addition, a compression step is introduced to allow the use of the generalized algorithm. Simulation studies carried out under a variety of measurement error conditions were used for statistical validation of the maximum likelihood properties of the algorithms and to assess the quality of the results and computation time. The simplified MLPARAFAC methods are also shown to produce more accurate results than PARAFAC under a variety of conditions. Copyright © 2005 John Wiley & Sons, Ltd.
Coinage Metal Lanthanide Chalcogenides. Part 1. Copper(I) Lanthanide(III) Sulfides of the Composition CuLnS2 (Ln: La—Nd, Sm, Gd, Tb) with the Monoclinic A‐Type Structure.
Authors: Strobel Sabine , Lauxmann Petra , Schleid Thomas 
Published: November 2005

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CsGa(H1.5AsO4)2 (H2AsO4) and Isotypic CsCr(H1.5AsO4)2 (H2AsO4): Decorated Kroehnkite‐Like Chains in Two Unusual Hydrogen Arsenates.
Authors: Schwendtner Karolina , Kolitsch Uwe 
Published: November 2005

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Peculiar Magnetic Behavior of the TbCu3Mn4O12 Complex Perovskite.
Authors: Sanchez‐Benitez J. , Alonso J. A. , de Andres A. , Martinez‐Lope M. J. , Martinez J. L. , Munoz A. 
Published: November 2005

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Photocatalytic Water Splitting on Ni‐Intercalated Ruddlesden—Popper Tantalate H2La2/3Ta2O7.
Authors: Shimizu Ken‐ichi , Itoh Seiichiroh , Hatamachi Tsuyoshi , Kodama Tatsuya , Sato Mineo , Toda Kenji 
Published: November 2005

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Synthesis, Crystal Structures and Properties of the Trimetaphosphimates NaBa(PO2NH)3, KSr(PO2NH)3×4H2O, and NH4Sr(PO2NH)3×4H2O.
Authors: Correll Sascha , Sedlmaier Stefan , Schnick Wolfgang 
Published: November 2005

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Hydrothermal Synthesis and Structural Characterization of Organically Templated Zincophosphites: [C6H22N4]0.5× [Zn2(HPO3)3] and [C3N2H5]× [Zn1.5(HPO3)2].
Authors: Zhang Dong , Yue Huijuan , Shi Zhan , Feng Shouhua 
Published: November 2005

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Highly Enantioselective Organocatalysis of the Hajos—Parrish—Eder—Sauer—Wiechert Reaction by the β‐Amino Acid Cispentacin.
Authors: Davies Stephen G. , Sheppard Ruth L. , Smith Andrew D. , Thomson James E. 
Published: November 2005

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Asymmetric Ring Opening of meso‐Epoxides Catalyzed by the Chiral Phosphine Oxide BINAPO.
Authors: Tokuoka Eisuke , Kotani Shunsuke , Matsunaga Hirofumi , Ishizuka Tadao , Hashimoto Shunichi , Nakajima Makoto 
Published: November 2005

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Z‐Selective or Stereospecific Alkenylation Reaction: A Novel Synthetic Method for α‐Fluoro‐α,β‐unsaturated Esters.
Authors: Yoshimatsu Mitsuhiro , Murase Yoshinori , Itoh Akinori , Tanabe Genzoh , Muraoka Osamu 
Published: November 2005

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New Heterocycles Having Double Characters as Antimicrobial and Surface Active Agents. Part 1. Nonionic Compounds from Fatty Acid Isothiocyanate.
Authors: Amine M. S. , Eissa A. M. F. , El‐Sawy A. A. , Shaaban A. F. , El‐Sayed R. 
Published: November 2005

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Two Variations of Solvent‐Reduced Wittig Olefination Reactions — Comparison of Solventless Wittig Reactions to Wittig Reactions under Ultrasonication with Minimal Work‐Up.
Authors: Watanabe Masataka , Morais Goreti Ribeiro , Mataka Shuntaro , Ideta Keiko , Thiemann Thies 
Published: November 2005

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Hydrogen‐Mediated Reductive Coupling of Conjugated Alkynes with Ethyl (N‐Sulfinyl)iminoacetates: Synthesis of Unnatural α‐Amino Acids via Rhodium‐Catalyzed C—C Bond Forming Hydrogenation.
Authors: Kong Jong‐Rock , Cho Chang‐Woo , Krische Michael J. 
Published: November 2005

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Stereoselective Hydrothiolation of Alkynes Catalyzed by Cesium Base: Facile Access to (Z)‐1‐Alkenyl Sulfides.
Authors: Kondoh Azusa , Takami Kazuaki , Yorimitsu Hideki , Oshima Koichiro 
Published: November 2005

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Ruthenium‐Catalyzed Cycloisomerization of cis‐3‐En‐1‐ynes to Cyclopentadiene and Related Derivatives Through a 1,5‐Sigmatropic Hydrogen Shift of Ruthenium—Vinylidene Intermediates.
Authors: Datta Swarup , Odedra Arjan , Liu Rai‐Shung 
Published: November 2005

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Lithium Benzocyclobuteneoxide as a Precursor of a Vinylogous Enolate: Solvent‐Controlled Synthesis of Highly Functionalized Seven‐Membered Benzocarbocycles.
Authors: Barluenga Jose , Garcia‐Garcia Patricia , Fernandez‐Rodriguez Manuel A. , Aguilar Enrique , Merino Isabel 
Published: November 2005

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Esters of 2‐Iodoxybenzoic Acid: Hypervalent Iodine Oxidizing Reagents with a Pseudobenziodoxole Structure.
Authors: Zhdankin Viktor V. , Koposov Alexey Y. , Litvinov Dmitry N. , Ferguson Michael J. , McDonald Robert , Luu Thanh , Tykwinski Rik R. 
Published: November 2005

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One‐Pot Synthesis of aza‐Moirta—Baylis—Hillman Adducts from α‐Oxo Ketene‐S,S‐acetals, Arylaldehydes and Nitriles.
Authors: Sun Shaoguang , Zhang Qian , Liu Qun , Kang Jing , Yin Yanbing , Li Dongwei , Dong Dewen 
Published: November 2005

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New Synthesis of (Z,E)‐2,7‐Bis(4‐cyanobenzylidene)cycloheptan‐1‐one under Stereospecific Constraints Induced by Host—Guest Interactions.
Authors: Grandeury Arnaud , Petit Samuel , Coste Servane , Coquerel Gerard , Perrio Cecile , Gouhier Geraldine 
Published: November 2005

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Asymmetric Epoxidation of α,β‐Unsaturated Ketones Catalyzed by Silica‐Grafted Poly‐(L)‐leucine Catalysts.
Authors: Yi Hua , Zou Gang , Li Qiang , Chen Qun , Tang Jie , He Ming‐yuan 
Published: November 2005

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An Ir(I)‐Catalyzed exo‐Selective Tandem Cycloisomerization/Hydroalkoxylation of Bis‐Homopropargylic Alcohols at Room Temperature.
Authors: Genin Emilie , Antoniotti Sylvain , Michelet Veronique , Genet Jean‐Pierre 
Published: November 2005

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Syntheses of Tetrahydrofurobenzofurans and Dihydromethanobenzodioxepines from 5‐Hydroxy‐3‐methyl‐3H‐benzofuran‐2‐one. Rearrangement and Ring Expansion under Reductive Conditions on Treatment with Hydrides.
Authors: Luo Weiming , Yu Qian‐sheng , Holloway Harold W. , Parrish Damon , Greig Nigel H. , Brossi Arnold 
Published: November 2005

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Three New Synthetic Methods for the 1,2,3,3a,8,8a‐Hexahydropyrrolo[2,3‐b]indoles Having an Alkoxy Group at the 3a‐Position.
Authors: Iwaki Takako , Yamada Fumio , Funaki Shiho , Somei Masanori 
Published: November 2005

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Chemoselective Reaction of Indole 1,3‐Dicarboxylates Towards Hydrazine Hydrate: Bisheterocycles: Synthesis and Antimicrobial Activity of Some New 2‐Methyl‐3‐ethoxycarbonyl‐1‐oxadiazolyl/thiazolidinonyl/pyrrolylaminocar bonylmethylindoles.
Authors: Bhovi Manjunath G. , Gadaginamath Guru S. 
Published: November 2005

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Novel, Selective Indole‐Based ECE Inhibitors: Lead Optimization via Solid‐Phase and Classical Synthesis.
Authors: Brands Michael , Ergueden Jens‐Kerim , Hashimoto Kentaro , Heimbach Dirk , Schroeder Christian , Siegel Stephan , Stasch Johannes‐Peter , Weigand Stefan 
Published: November 2005

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Microwave‐Assisted Cyclocondensation of Hydrazine Derivatives with Alkyl Dihalides or Ditosylates in Aqueous Media: Syntheses of Pyrazole, Pyrazolidine and Phthalazine Derivatives.
Authors: Ju Yuhong , Varma Rajender S. 
Published: November 2005

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Synthesis and Antibacterial Activity of a Novel Series of DNA Gyrase Inhibitors: 5‐[(E)‐2‐Arylvinyl]pyrazoles.
Authors: Tanitame Akihiko , Oyamada Yoshihiro , Ofuji Keiko , Terauchi Hideo , Kawasaki Motoji , Wachi Masaaki , Yamagishi Jun‐ichi 
Published: November 2005

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Synthesis, Structure—Activity Relationships, and Anxiolytic Activity of 7‐Aryl‐6,7‐dihydroimidazoimidazole Corticotropin‐Releasing Factor 1 Receptor Antagonists.
Authors: Han Xiaojun , Dubowchik Gene M. , et al. et al. 
Published: November 2005

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Design, Synthesis, and Evaluation of Novelly Substituted Benzimidazole Compounds as Angiotensin II Receptor Antagonists.
Authors: Bali Alka , Bansal Yogita , Sugumaran M. , Saggu Jatinder Singh , Balakumar P. , Kaur Gurpreet , Bansal Gulshan , Sharma Ajay , Singh Manjeet 
Published: November 2005

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Synthesis of Some New N‐[5‐Methyl‐1‐(4‐chlorophenyl)‐1,2,3‐triazol‐4‐yl]carbamic Acid Ester Derivatives (V)
Authors: Quan Bin , Zhuang Shan‐Xue , Li Chun‐Cheng , Dong Heng‐Shan 
Published: November 2005

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Synthesis of Some New 2‐(6‐Methoxy‐2‐naphthyl)‐5‐aryl‐1,3,4‐oxadiazoles as Possible Non‐steroidal Antiinflammatory and Analgesic Agents.
Authors: Narayana Badiadka , Raj Kuniyil Kulangara Vijaya , Ashalatha Badiadka Valamale , Kumari Nalilu Suchetha 
Published: November 2005

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Synthesis of 3‐Substituted Bicyclic Imidazo[1,2‐d][1,2,4]thiadiazoles and Tricyclic Benzo[4,5]imidazo[1,2‐d][1,2,4]thiadiazoles.
Authors: Leung‐Toung Regis , Tam Tim F. , Zhao Yanqing , Simpson Craig D. , Li Wanren , Desilets Denis , Karimian Khashayar 
Published: November 2005

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Synthesis and Antiinflammatory Activity of 4‐(5′‐Acetyl‐6′‐hydroxy‐3′‐methylbenzofuran‐2′‐yl)coumarin and 6‐Acetyl‐3,7‐dimethyl‐2‐(coumarin‐4′‐yl)furo[3,2‐g]chromen‐5‐one.
Authors: Ghate Manjunath , Kulkarni Manohar V. 
Published: November 2005

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Synthesis and Characterization of Alkyl and Aryl‐(4‐methyl‐6‐nitro‐quinolin‐2‐yl)amines: X‐Ray Structures of Ethyl and Cyclohexyl‐(4‐methyl‐6‐nitro‐quinolin‐2‐yl)amine.
Authors: Heiskell Melody R. , Rudd Martin D. , Penn Benjamin B. , Kautz Jason A. 
Published: November 2005

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New Synthesis of 1‐Benzoyltetrahydroisoquinoline Derivatives Using Polymer‐Supported Bis(trifluoroacetoxyiodo)benzene.
Authors: Huang Hsin‐Yu , Hou Rei‐Sheu , Wang Huey‐Min , Chen Ling‐Ching 
Published: November 2005

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Direct Mannich and Nitro‐Mannich Reactions with Non‐Activated Imines: AgOTf‐Catalyzed Addition of Pronucleophiles to ortho‐Alkynylaryl Aldimines Leading to 1,2‐Dihydroisoquinolines.
Authors: Asao Naoki , Yudha S. Salprima , Nogami Tsutomu , Yamamoto Yoshinori 
Published: November 2005

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A Facile Synthesis of Isoindolo[2,1‐a]quinolin‐11‐one via [4 + 2] Reactions of N‐Acyliminium Intermediates with Olefins.
Authors: Zhang Wei , Zheng Airong , Liu Zhengang , Yang Li , Liu Zhongli 
Published: November 2005

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Thermal Intramolecular [2 + 2] Cycloaddition of Allenenes and Allenynes: Diastereoselective Access to Bicyclic Nitrogen Heterocycles.
Authors: Ohno Hiroaki , Mizutani Tsuyoshi , Kadoh Yoichi , Miyamura Kumiko , Tanaka Tetsuaki 
Published: November 2005

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Syntheses of 1,3‐Disubstituted‐5a‐hydropyrrolo[2,3‐d]quinazolino [3,2‐e]pyrimidin‐6(5H)‐ones: A Comparison of Conventional and Microwave Technique.
Authors: Augustine Cicily , Agrawal Y. K. 
Published: November 2005

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Synthesis of Fused Tetrahydro‐β‐carbolinequinoxalinones in 1‐n‐Butyl‐2,3‐dimethylimidazolium Bis(trifluoromethylsulfonyl)imide ([bdmim][Tf2N]) and 1‐n‐Butyl‐2,3‐dimethylimidazolium Perfluorobutylsulfonate ([bdmim][PFBuSO3]) Ionic Liquids.
Authors: Tseng Ming‐Chung , Liang Yang‐Min , Chu Yen‐Ho 
Published: November 2005

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Regio‐ and Stereoselective Cycloaddition and Further Transformations of Azomethine Imine Derivatives of Fused [1,2,4]Triazines.
Authors: Grof Csilla , Riedl Zsuzsanna , Hajos Gyoergy , Egyed Orsolya , Csampai Antal , Stanovnik Branko 
Published: November 2005

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Convenient Synthesis of Fused Heterocyclic 1,3,5‐Triazines from Some N‐Acyl Imidates and Heterocyclic Amines as Anticancer and Antioxidant Agents.
Authors: Bekircan Olcay , Kuexuek Murat , Kahveci Bahittin , Kolayli Sevgi 
Published: November 2005

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A Simple Synthesis of B‐2‐(1‐Trimethylgermyl‐1‐alkyl)‐1,3,2‐dioxaborinanes. Isolation and Selective Oxidation to 1‐Trimethylgermyl‐1‐alkanols.
Authors: Bhat Narayan G. , Carroll Matthew B. , Lai Wendy C. 
Published: November 2005

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Structural and Stereochemical Revision of Isocyanide and Isothiocyanate Amphilectenes from the Caribbean Marine Sponge Cribochalina sp.
Authors: Ciavatta Maria Letizia , Gavagnin Margherita , Manzo Emiliano , Puliti Raffaella , Mattia Carlo Andrea , Mazzarella Lelio , Cimino Guido , Simpson Jamie S. , Garson Mary J. 
Published: November 2005

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2,2‐Dimethyl Cyclopentanones by Acid Catalyzed Ring Expansion of Isopropenylcyclobutanols. A Short Synthesis of (.+‐.)‐α‐Cuparenone and (.+‐.)‐Herbertene.
Authors: Bernard Angela M. , Frongia Angelo , Secci Francesco , Piras Pier P. 
Published: November 2005

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Synthesis and Pharmacological Activity of N‐[β‐(para‐Substituted Benzoyl)ethyl]isoleucine and ‐methionine.
Authors: Agababyan A. G. , Isakhanyan A. U. , Papoyan O. A. , Tumadzhyan A. E. , Balasanyan A. S. , Gevorgyan G. A. 
Published: November 2005

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Microwave‐Assisted Rapid Deacetalation of Carbohydrates.
Authors: Couri Mara Rubia C. , Evangelista Eruzia A. , Alves Rosemeire B. , Prado Maria Auxiliadora F. , Gil Rossimiriam P. F. , De Almeida Mauro V. , Raslan Delio S. 
Published: November 2005

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Synthetic Studies of Norzoanthamine. Preparation of the Diene‐yne‐diene Precursor of an ABC‐Ring Fragment.
Authors: Irifune Taiji , Ohashi Tomohiro , Ichino Takao , Sakai Emi , Suenaga Kiyotake , Uemura Daisuke 
Published: November 2005

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Copper‐Catalyzed Arylation with Boronic Acids for the Synthesis of N1‐Aryl Purine Nucleosides.
Authors: Strouse J. Jacob , Jeselnik Marjan , Tapaha Frederick , Jonsson Colleen B. , Parker William B. , Arterburn Jeffrey B. 
Published: November 2005

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Constituents of Holothuroidea. Part 15. Isolation of Ante‐iso Type Regioisomer on Long Chain Base Moiety of Glucocerebroside from the Sea Cucumber Holothuria leucospilota.
Authors: Yamada Koji , Wada Noriko , Onaka Hiroyuki , Matsubara Rei , Isobe Ryuichi , Inagaki Masanori , Higuchi Ryuichi 
Published: November 2005

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