bluuebunny/crossref_metadata_2025_split huggingface dataset:
Fatigue Failure of a 1000 mm (40 in.) Diam Trailer Wheel at the Bolt Holes
Authors: Jones W.F. 
Published: May 2019

Abstract
The rear outside wheel of an over-the-road 18-wheel tractor-trailer failed at its bolt holes, permitting the tire and wheel to separate from the hub. Failure analysis was conducted using photographic examination of actual fracture surfaces and SEM examination of fracture replicas. The examinations indicated that fatigue cracks had originated at the rim backside and propagated to the rim midsection. Catastrophic failure occurred at a final overland. Fatigue fracture of the wheel rim was attributed to cyclic loading created by improper wheel mounting of a spare tire.
Embrittlement of a 76 mm (3 in.) Stainless Steel Pipe and Liner From a Hydrogen Plant Quench Pot Vessel
Authors: Bowman Ralph D. 
Published: May 2019

Abstract
A 76 mm (3 in.) type 304 stainless steel tube that was used as a heat shield and water nozzle support in a hydrogen gas plant quench pot failed in a brittle manner. Visual examination of a sample from the failed tube showed that one lip of the section was eroded from service failure, whereas the opposite side exhibited a planar-type fracture. Sections were removed from the eroded area and from the opposite lip for microscopic studies and chemical analysis. The eroded edges exhibited river bed ditching, indicative of thermal fatigue. Microstructural analysis showed massive carbide formations in a martensite matrix and outlining of prior-austenite grains by a network of fine, white lines. These features indicated that the material had been transformed by carburization by the impinging gas. The outer surface exhibited a heavy scale deposit and numerous cracks that originated at the surface of the tube. The cracks were covered with scale, indicating that thermal fatigue (heat cracking) had occurred. Chemical analysis confirmed that the original material was type 304 stainless steel that had been through-carburized by the formation of an endothermic gas mixture. It was recommended that plant startup and shutdown procedures be modified to reduce or eliminate the presence of the carburizing gas mixture.
Intergranular Corrosion in an E-Brite-Clad Ferralium Tube Sheet in Nitric Acid Service
Authors: Colwell Richard L. 
Published: May 2019

Abstract
An E-Brite /Ferralium explosively bonded tube sheet in a nitric acid condenser was removed from service because of corrosion. Visual and metallographic examination of tube sheet samples revealed severe cracking in the heat-affected zone between the outer tubes and the weld joining the tube sheet to the floating skirt. Cracks penetrated deep into the tube sheet, and occasionally into the tube walls. The microstructures of both alloys and of the weld appeared normal. Intergranular corrosion characteristic of end-grain attack was apparent. A low dead spot at the skirt / tube sheet joint allowed the Nox to condense and subsequently reboil. This, coupled with repeated repair welding in the area, reduced resistance to acid attack. Intergranular corrosion continued until failure. Recommendations included changing operating parameter inlet to prevent HNO3 condensation outside the inlet and replacement of the floating skirt with virgin material (i.e., material unaffected by weld repairs).
Corrosion Fatigue Cracking of a Steam Generator Vessel From a Pressurized Water Reactor
Authors: Czajkowski Carl J. 
Published: May 2019

Abstract
A pair of steam generators operating at a pressurized water reactor site were found to be leaking near a closure weld. The generators were the vertical U-tube type, constructed from ASTM A302 grade B steel. The shell material exhibited high hardness values prior to confirmatory heat treatment, indicating high residual stresses in the area of the weld. All cracks were transgranular and were associated with pits on the inside surfaces of the vessels. It was concluded that the cracking was caused by a low-cycle corrosion fatigue phenomenon, with cracks initiating at areas of localized corrosion and propagating by fatigue. The cause of the pitting/cracking was related to the unit's copper species in solution.
Failure of a High-Pressure Water-Line Plug in a Fire Sprinkler System
Authors: Leeser David O. 
Published: May 2019

Abstract
A white cast iron water-line plug in a fire sprinkler systems split during leak repair. Examination revealed no material flaws, fatigue, or excessive corrosion. The plug head exhibited signs of excessive loads used in attempts to force the plug farther into the pipe. The evidence obtained indicated that the failure resulted from human error.
Intergranular Stress-Corrosion Cracking of Carbon Steel Pipe Welds in a Kamyr Continuous Digester Equalizer Line
Authors: Chakrapani Durgam G. 
Published: May 2019

Abstract
Schedule 80 low-carbon steel pipes used to transfer kraft liquor in a Kamyr continuous pulp digester failed within 18 months after installation. Visual and metallographic examinations established that the cracking initiated on the internal surfaces of the equalizer pipes in the welds and heat-affected zones (HAZs). Fracture/crack morphology was brittle and primarily intergranular and deposits at crack tips were primarily iron oxides with significant amounts of sodium compounds. On these bases, the cracking was characterized as intergranular stress-corrosion cracking (IGSCC). Corrosion-related deterioration was not found, indicating that the material was generally suitable for the intended service. High residual tensile stresses in the welds and HAZS, resulting from field welding under highly constrained conditions using inadequate weld procedures, were the most probable cause of the failures. Minimizing residual stresses through use of welding procedures that include appropriate preweld and interpass temperatures and postweld stress relief heat treatment at 650 deg C (1200 deg F) was recommended to prevent further failures.
Pitting Corrosion of Stainless Steel by Potable Municipal Water in an Organic Chemical Plant
Authors: Perumal K.E. 
Published: May 2019

Abstract
Several tubes in a 35 m2 (115 ft2) type 316 stainless steel shell-and-tube condenser leaked unexpectedly in an organic chemical plant that produces vinyl acetate monomer. Leaks were discovered after 5 years of operation and relocation of the condenser to another unit in the same plant. Examination of tubes and tube sheets revealed pitting damage on the OD surface. Some of the pits had penetrated fully, resulting in holes. Inside diameter surfaces were free of corrosion. Macro- and microexaminations indicated that the tubes had been properly manufactured. Pitting was attributed to stagnant water on the shell side. It was recommended that the surfaces not be kept in contacts with closed stagnant water for appreciable lengths of time.
Stress-Corrosion Cracking of C-Mn Steel in a CO2 Absorber in a Chemical Plant
Authors: Chauhan Sushil K. 
Published: May 2019

Abstract
The source of cracking in the circumferential weld seam in a JIS-SM50B carbon-manganese steel pipe used in a CO2 absorber was investigated, the absorber had been in service for 18 years. The seam had been weld-repaired twice, and the repair welds had been locally stress relieved. Longitudinal seams in the same vessel, which had been stress relieved in a furnace, showed no tendency toward cracking. The solution passing through the vessel contained CO2-CO-H20, KHCO, and Cl− ions. Nondestructive testing revealed that the cracks originated in the heat-affected zone and propagated into the base metal and weld. Severe branching of the cracks characteristic of stress-corrosion cracking was observed. Microexamination revealed that crack propagation was transgranular further supporting the possibility of stress-corrosion cracking. Simulation tests carried out in the vessel confirmed this mode of cracking. It was recommended that weld seams be furnace heat treated at a temperature of 600 to 640 deg C (1110 to 1180 deg F) for a minimum of 1 h per inch of section thickness.
Unexpected Corrosion of Type 316L Stainless Steel Neutralization Tanks
Authors: Degnan Thomas F. 
Published: May 2019

Abstract
Although field corrosion tests had indicated that type 316L stainless steel would be a suitable material for neutralization tanks, the vessels suffered severe corrosion when placed in service. Welded coupons of type 316L had been tested along with similar Alloy 20Cb® (UNS NO8020) specimens in a lead-lined tank equipped with copper coils that had served in this function prior to construction of the new tanks. Both materials exhibited virtually no corrosion and no preferential weld attack. Type 316L was selected for the project. The subsequent corrosion was the result of the borderline passivity of type 316L in hot dilute sulfuric acid (about 0.1%). Inaccuracy of the testing was attributed to the presence of cupric ions in the lead-lined vessel fluids, which had been released by corrosion of the copper coils. Careful control of both temperature and pH was recommended to reduce the corrosion to an acceptable limit.
Environmental Cracking of a Low-Alloy Steel Welded Impeller Cover From a Centrifugal Unit
Authors: Ebert Harry E. 
Published: May 2019

Abstract
Radial cracking occurred adjacent to 11 vanes in a 19-vane impeller operating in a chemical plant environment. The impeller vanes were fillet welded to both the disk and the cover Cracks were next to the fillet welds and near the cover outer diameter They generally did not extend to the outer diameter. The entire impeller surface was tested by the dry magnetic particle method. Visual and microstructural examinations revealed intergranular cracking. Energy-dispersive spectroscopy of corrosion products contained in the cracks disclosed the presence of chlorine and sulfur The failure was attributed to stress-corrosion cracking caused by a corrosive atmosphere.
Excessive Wear of Plain Carbon Steel Sprockets in a Chemical Plant Producing Fibers
Authors: Mackay W.B.F. 
Published: May 2019

Abstract
Replacement sprockets installed on chain drive shafts for winding fibers exhibited excessive wear. Metallographic and chemical analyses conducted on the original and replacement sprockets showed that the material of the replacement sprocket was 1020 low-carbon steel, whereas the original (and specified) material was medium-carbon 1045 steel. The low-carbon steel also had lower hardness because of a lower pearlite fraction in the microstructure. It was recommended that replacement sprockets be made of normalized 1045 steel. It was further suggested that wear resistance could be improved by through hardening or induction surface hardening of the teeth.
Fatigue Fracture of Stainless Steel Wires in an Electrostatic Precipitator at a Paper Plant
Authors: Brooks Charlie R. 
Published: May 2019

Abstract
Several type 316L stainless steel wires in an electrostatic precipitator at a paper plant fractured in an unexpectedly short time. Failed wires were examined using optical and scanning electron microscope, and hardness tests were conducted. Fractography clearly established that fracture was caused by fatigue originating at corrosion pits on the surface of the wire. It was recommended that higher-molybdenum steel in the annealed condition be used to combat pitting corrosion.
Fatigue Fracture of Aircraft Engine Compressor Disks
Authors: Koul Ashok K. , Dainty Raymond V. 
Published: May 2019

Abstract
Several compressor disks in military fighter and trainer aircraft gas turbine engines cracked prematurely in the bolt hole regions. The disks were made of precipitation-hardened AM355 martensitic stainless steel. Experimental and analytical work was performed on specimens from the fifth-stage compressor disk (judged to be the most crack-prone disk in the compressor) to determine the cause of the failures. Failure was attributed to high-strain low-cycle fatigue during service. It was also determined that the cyclic engine usage assumed in the original life calculations had been under estimated, which led to low-cycle fatigue cracking earlier than expected. Fracture mechanics analysis of the disks was carried out to assess their damage tolerance and to predict safe inspection intervals.
Repeated Failure of Rubber Slurry Pump Impellers and Liners in a Flue Gas Desulfurization Plant
Authors: Ellis Peter F. 
Published: May 2019

Abstract
The repeated failure of rubber-covered rotors and volute liners in a flue gas desulfurization system after conversion from lime slurry reagent to limestone slurry reagent was investigated. The pump was a horizontal 50 x 65 mm (2 x 2.5 in.) Galiger pump with a split cast iron case and open rotor (impeller). Both the case and the ductile iron rotor core were covered by natural rubber. Analyses conducted included surface examination of wear patterns, chemical analysis of materials, measurement of mechanical properties, and in-place flow tests. It was determined that the proximate cause of failure was cavitation and vortexing between the rotor and the lining. The root cause of the failure was the conversion from lime to limestone slurry without appropriate modification of the pump. Conversion to the limestone slurry resulted in fluid dynamics outside the operational limits of the pump. The recommended remedial action was replacement with a pump appropriately sized for the desired pressures and flow rates for limestone slurry.
Cracking of an Alloy Steel Bolt
Authors: Levy Eli 
Published: May 2019

Abstract
A heat-treated, cadmium-plated AISI 8740 steel bolt broke through the head-to-shank fillet while being handled during assembly. Fractographic and metallographic examination of the bolt traced the cause of failure to quench cracking, which occurred when the part was water cooled following hot heading and prior to the production run. The process chart for hot heading was changed from water quenching to air cooling following the forming operation.
Environmentally-Induced Fracture of Type 410 Martensitic Stainless Steel Self-Drilling Tapping Screws
Authors: Chakrapani Durgam G. 
Published: May 2019

Abstract
Cadmium-coated type 410 martensitic stainless steel 14-14 self-drilling tapping screws fractured during retorquing tests within a few weeks after installation. The screws were used to assemble structural steel frames for granite panels that formed the outer skin of a high-rise building. Fractographic and metallographic examination showed that the fractures occurred in a brittle manner from intergranular crack propagation. Laboratory and simulated environmental tests showed that an aqueous environment was necessary for the brittle fracture/cracking phenomenon. The cracks were singular and intergranular with little branching. Secondary subsurface cracks suggested possible hydrogen embrittlement. The 410 screws had been introduced to replace conventional case-hardened carbon steel screws that conform to SAE specification J78. Carbon steel screws had a proven record of acceptable performance for the intended application. It was recommended that use of the 410 screws be discontinued in preference to the case-hardened carbon steel screws.
Fatigue Fracture of 316L Stainless Steel Screws Employed for Surgical Implanting
Authors: Snyder Harold J. , Snyder Casey B. 
Published: May 2019

Abstract
Two type 316L stainless steel orthopedic screws broke approximately 6 weeks after surgical implant. The screws had been used to fasten a seven-hole narrow dynamic compression plate to a patient's spine. The broken screws and screws of the same vintage and source were examined using macrofractography, SEM fractography, and hardness testing. Fractography established that fracture was by fatigue and that the fatigue cracking originated at corrosion pits. Hardness while below specification, still indicated that the screws were in the cold-worked condition and notch sensitive during fatigue loading. Use of a steel with a higher molybdenum content (317L) in the annealed condition was recommended.
Fatigue Failure of Six Cap Screws From a Hydraulic Coupling
Authors: Tanner G. Mark 
Published: May 2019

Abstract
Six ASTM A-574 steel cap screws from a hydraulic coupling failed after 3 months in service. The screws were replacements for smaller-diameter cap screws that had been installed during an outage. Six new cap screws were examined along with the failed screws. Eight fracture locations were identified—three at the head-to-shank fillet, four at the eighth thread root from the cap, and one at the sixth thread root from the cap. Fracture surfaces were examined using a stereomicroscope and SEM, and the fracture mode was shown to be transgranular. EDS on the fracture surfaces showed sulfur and chlorine in the surface deposits. The observations indicated that the screws had failed by fatigue. Insufficient preloading was considered to be the most likely cause of the fatigue cracking. It was recommended that the proper preload on the screws be verified and maintained.
Fracture of Alloy Steel Cap Screws in a Refrigeration Compressor
Authors: Witherell Charles E. 
Published: May 2019

Abstract
Uncoated high-strength alloy steel cap screws retaining a cast aluminum (356.0) diffuser assembly in a centrifugal refrigerant compressor failed in a brittle manner a short time after the system was placed in operation. Evidence obtained during the failure analysis indicated that the failures were the result of hydrogen embrittlement produced by galvanic corrosion and attendant evolution of hydrogen at the dissimilar junction, which was also the site of the highest tensile stress. Suggested measures for minimizing recurrences included use of lower-strength, galvanically-compatible fasteners and appropriately-applied and treated compatible coatings.
Furnace Element Tube Failures
Authors: Wellington K.G. 
Published: May 2019

Abstract
Three radiant heating element tubes from an aluminum holding furnace failed after a few months of service. One side of each of the tubes had disintegrated, leaving large holes and thinned cross sections. Microstructural analysis showed that the surface of the tube had been oxidized along the grain boundaries and had extensive precipitation inside the grains. Chemical analysis indicated that the steel used for the tubes was AISI type 316 stainless steel Specifications for the tubes had called for AISI type 310S to be used. It was recommended that other tubes made from the same batch of steel sheet be checked.
Hydrogen-Induced Cracking of Welded Truss Gusset Plates
Authors: Jones William F. 
Published: May 2019

Abstract
Six cracked A36 steel gusset plates that formed part of the roof trusses of a large manufacturing facility were discovered during a routine final inspection of a new building construction. Two different-size plates from different locations in the building were removed and tested. It was determined that the gusset plates failed in the heat-affected zone via an intergranular microcracking mode due to hydrogen-assisted underbead and toe-weld cracking. Proper nondestructive testing techniques for magnetic particle and radiographic inspection of the plate-weld gusset areas were recommended.
Failure of Two Plastic Toilet-Tank Floats
Authors: Leeser David O. 
Published: May 2019

Abstract
Two plastic tank floats in separate toilets in one dwelling failed within a relatively brief period of time. Examination of the floats and of a brass connecting rod revealed that the fracture occurred at the base of the threaded hole in the nipple and was brittle in nature. The fracture surfaces were coated with zinc oxide. It was concluded that the failure resulted from improper repairs and/or adjustments, including the use of a cosmetic zinc oxide cream as a lubricant. The cream initiated deterioration of the originally ductile plastic, causing it to become brittle and fragile.
Failure of Pendent Sprinkler Heads
Authors: Chaudhari Mohan D. 
Published: May 2019

Abstract
A sprinkler head unit that was installed in a smoking lounge of a multi story office building in 1975 failed, causing substantial water damage. There was no fire in the building. A set of four sprinkler heads -- three that had been installed in 1975 (the failed unit, an unfailed unit from the same room, and an unfailed unit from another room) and an unused 1991 unit -- were examined. casting revealed no material defects or mechanical damage. Because of several environmental factors, it was suspected that the failed unit was exposed to temperatures much above the normal office environment. On this basis, it was concluded that creep of the solder alloy was the most probable cause of failure.
Fatigue Failure of Steering Arms Due to Forging Defects
Authors: Baggerly Roy G. 
Published: May 2019

Abstract
Several heavy truck Cr-Mo steel steering arms in service less than three years fractured during stationary or low-speed turning maneuvers that required power-assisted steering. Metallographic examination of the cracked AISI 4135 arms, heat treated to a hardness of 285 to 341 HB, revealed that fatigue crack initiation occurred from the tip of oxide scale inclusions forged into the U-shaped arm at the inside radius. Corrective action involved redesigning the steering arm to increase the minimum forging radius and reduce the stress level at the inner-bend radius, and reducing the level of power assistance to the wheels to encourage the driver to put the vehicle in motion prior to turning.
Brittle Failure of a Titanium Nitride-Coated High Speed Steel Hob
Authors: Stone Alan 
Published: May 2019

Abstract
Recurring, premature failures occurred in TiN-coated M2 gear hobs used to produce carbon steel ring gears. Fractographic and metallographic examination, microhardness testing, and chemical analysis by means of EDS revealed that the primary cause of failure was a coarse cellular carbide network, which created a brittle path for fracture to occur longitudinally. As the cellular carbide network must be dispersed and refined during hot working of the original bar of material, the hobs were not salvageable. Minor factors contributing to the hob failures were premature wear resulting from lower matrix hardness and high sulfur content of the material, which contributed to lower ductility through increased nucleation sites. It was recommended that the hob manufacturer specify a minimum amount of required reduction for the original bar of tool steel material, to provide for sufficient homogenization of the carbides in the resultant hob, and lower sulfur content.
Cracking on the Parting Line of Closed-Die Forgings
Authors: Koprowski Anthony J. 
Published: May 2019

Abstract
An investigation was conducted to determine the factors responsible for the occasional formation of cracks on the parting lines of medium plain carbon and low-alloy medium-carbon steel forgings. The cracks were present on as-forged parts and grew during heat treatment. Examination revealed that areas near the parting line exhibited a large grain structure not present in the forged stock. High-temperature scale was also found in the cracks. It was concluded that the cracks were caused by material being folded over the parting line. The folding occurred because of a mismatch in the forgings and from material flow during trimming and/or material flow during forging.