bluuebunny/crossref_metadata_2025_split huggingface dataset:
Metal Waves or Laking on Zinc-Based Diecastings
Authors: Perger Gustav R. , Robinson Peter M. 
Published: May 2019

Abstract
Lakes in zinc die castings are areas encompassed by irregular lines or waves on flat or slightly contoured surfaces which are intended to look uniform. The laked areas have to be removed by polishing before the castings can be plated. This adds considerably to the overall cost of production. Castings examined were of an automobile name-plate holder with two flat sides of approximately 113 sq cm. All castings produced during a trial showed laking defects, the number and position varying from casting to casting. It was found that formation of metal waves and lakes depended primarily on the design of the gate and runner system and operating conditions. High flow efficiencies, with adequate feeding to all sections of the die, and short cavity fill times are desirable.
Leaky Socket Pipe from the Safety Return Circuit of a Heating Installation
Authors: Kauczor Egon 
Published: May 2019

Abstract
An elbow made from welded steel tube had become leaky along a well-defined line in the axial direction. The entire wall of the tube was corroded, and the longitudinally-welded seam stood out clearly as a result of particularly intensive corrosive attack. The appearance of the corroded surface indicates the action of water with a high oxygen content. The oxygen in the return water must have originated from the ventilation of the open expansion vessel. Because of the corrosion-favoring effect of a crevice, water with a high oxygen-content that was perhaps still warm or even hot found particularly favorable conditions for corrosion in the defective welded seam (crevice corrosion). The tube material itself is perfectly satisfactory and in no way responsible for the failure.
Decarburization
Authors: Naumann Friedrich Karl , Spies Ferdinand 
Published: May 2019

Abstract
Decarburization of steel may occur as skin decarburization by gases either wet or containing oxygen, and as a deep ongoing destruction of the material by hydrogen under high pressure. Guidelines are given for recognizing decarburization and determining at what point cracks occurred. How decarburization changes workpiece properties and the case of hydrogen decarburization are addressed through examples.
Cast Ingot Cracked During Forging
Authors: Naumann Friedrich Karl , Spies Ferdinand 
Published: May 2019

Abstract
An octagonal steel ingot weighing 13 tons made of manganese-molybdenum steel developed gaping cross-cracks on all eight sides in the forging press during initial pressure application. It was reported that the steel had been melted in a basic 12-ton arc furnace, oxygenated, furnished with 42 kg of 75% ferrosilicon and 12 kg aluminum additions, alloyed with 160 kg of 80% ferromanganese, and finally deoxidized in the ladle with 42 kg calcium silicon. For metallographic examination a plate approximately 100 mm thick was cut parallel to one of the eight planes. Platelet-like particles could be discerned on the conchoidal fracture planes with the SEM. The precipitates proved to be thin and partially transparent platelets of a hexagonal crystal lattice whose parameters resemble those of AIN. The precipitates were at least in part still undissolved in spite of the long holding period at high initial forging temperature. Another block melted under the same conditions and immediately after the defective one, was forged into a gear ring without any trouble. This ring was free of grain boundary precipitates, but it contained only 0.012 % AI and 0.0102 % N.
Primary Grain Boundary Cracks in Cast Ingots and Flaky Crankshafts
Authors: Naumann Friedrich Karl , Spies Ferdinand 
Published: May 2019

Abstract
Octagonal cast ingots weighing 6.5 tons and made of unalloyed heat treated steel CK 45 according to DIN 17200, and crankshafts forged from these ingots showed internal separations during ultrasonic testing. To determine the cause of defect, an ingot slice and a crank arm were examined metallographically. Investigation showed this was a case where flaky forgings were made from cast ingots with primary grain boundary cracks. This parallelity supports the often expressed opinion that both occurrences have the same origin, i.e. that hydrogen precipitation was the driving force in the formation of primary grain boundary cracks in cast ingots.
Poorly Drawable Steel Wire for Ball Bearings
Authors: Naumann Friedrich Karl , Spies Ferdinand 
Published: May 2019

Abstract
A drawing plant which processed steel wire of designation 105 Cr 2 for ball bearings had losses due to crack formation and wire breakage during drawing. To establish the reason for the breakage, seven fractures were submitted for investigation with contiguous wire segments on both sides of the fracture of 300 mm each. Missing in the lamellar surface structure, with the exception of the remnants of a coarse network, were the pre-eutectically precipitated carbides to be expected in this steel. Surrounding the ferritic region in the surface structure, a ring of lamellar pearlite is seen, which turns into the granular annealed structure towards the core. The described structural phenomena were noted in all of the seven fracture regions. Their intensity always decreased with increasing distance from the fracture. Surface decarburization caused the formation of lamellar pearlite during annealing. This investigation further revealed that the localized decarburization and pearlite formation was present already in the rolled wire in uneven distribution over the entire coil length.
Plating Adherence Problems in Electronic Components
Authors: Kumar Arun 
Published: May 2019

Abstract
Electroless nickel plating separation from copper alloy CDA175 retaining clips used on printed circuit boards was caused by a copper oxide layer that reduced adhesion of the nickel plating on the clips. Stresses that developed during module insertion caused flaking to occur at the oxidized copper surface. Electroless nickel plating separation from OFHC copper leads was caused by improper handling rather than a plating anomaly per se. Tin plating separation from copper underplating on a hybrid package lid occurred because of a four-week delay between the copper plating and tin plating steps. It was recommended that tin plating should follow the copper underplating within 24 h and a cleaning step of bright dipping after copper plating be performed.
Failure Analysis of an Aluminum Casting
Authors: Medeiros Steven C. 
Published: May 2019

Abstract
In the EMD-2 Joint Directed Attack Munition (JDAM), the A357 aluminum alloy housing had been redesigned and cast via permanent mold casting, but did not meet the design strength requirements of the previous design. Mechanical tests on thick and thin sections of the forward housing assembly revealed tensile properties well below the allowable design values. Radiology and CT evaluations revealed no casting defects. Optical microscopy revealed porosity uniformly distributed throughout the casting on the order of 0.1 mm pore diam. Scanning electron microscopy revealed elongated pores, which indicated turbulent filling of the mold. Spherical pores would have indicated the melt had been improperly degassed. Based on these findings, it was recommended that the manufacturer analyze and redesign the gating system to eliminate the turbulent flow problem during the permanent mold casting process.
Structural Instability of Cold Worked Alloy 304 in 650 °C Service
Authors: Krafft H. 
Published: May 2019

Abstract
A heavily worked 304 stainless steel wire basket recrystallized and distorted while in service at 650 deg C (1200 deg F). This case study demonstrates that heavily cold worked austenitic stainless steel components can experience large losses in creep strength, and potentially structural collapse, under elevated temperature service, even at temperatures more than 300 deg C (540 deg F) below the normal solution annealing temperature. The creep strength of the recrystallized 304/304L steel was more than 1000 times less than that achievable with solution annealed 304H. These observations are consistent with limitations (2000 Addendum to ASME Boiler and Pressure Vessel Code) on the use of cold worked austenitic stainless steels for elevated temperature service.
An Analysis of Fiber-Induced Surface Defects in Electroless Plated Components
Authors: Mehta S. , Vysotskaya A. , Mistry N. 
Published: May 2019

Abstract
The paper discusses the analysis of a coating defect on a high phosphorus electroless nickel (Ni-11 wt. % P) deposit plated on an aluminum alloy substrate. Preliminary investigations had indicated that the elongated defects were possibly caused by the entrapment of long fibers or particles during the plating. The possible sources of fibers were identified. The SEM/EDS analysis of fibers collected from the air duct filters correlated very well with the defect shape and the EDS profile collected from under the defect site. It appears that the fibers from air duct filters directly above the plating line were blown into the plating tank and getting co-deposited. The paper describes the step-by-step analysis of the defect that led to successful identification of the root cause of the defect.
An Investigation of the Development of Defects During Flow Forming of High Strength Thin Wall Steel Tubes
Authors: Rajan K.M. , Narasimhan K. 
Published: May 2019

Abstract
Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming of high strength SAE 4130 steel tubes. The major defects observed are fish scaling, premature burst, diametral growth, microcracks, and macrocracks. This paper analyzes the defects and arrives at the causative factors contributing to the various failure modes.
Discoloration of a Stainless Steel Tube after Pickling
Authors: Suess S.J. 
Published: May 2019

Abstract
A type 17-4PH stainless steel tube exhibited brown discoloration after a pickling operation. EDS analysis of the extracted substance revealed relatively high levels of iron and chromium, along with lower amounts of aluminum, silicon, sulfur, chlorine, calcium, manganese, and nickel. The iron, chromium, and nickel are likely in the form of dissolution products from the pickling solution. FTIR analysis revealed the presence of polypropylene and poly(ethylene:propylene). The EDS results showed that the discoloration of the tube was associated with oxidation products of the tube material, as well as adherent organic residue. Analysis by FTIR of the residue revealed detectable levels of two polymeric substances, which were later determined to be construction materials of the pickling tank. It was recommended that more frequent cleaning and/or replacement of the pickling solution be put into place and another type of tank material be considered.
Tinting of Electropolished Copper Parts
Authors: Suess S.J. 
Published: May 2019

Abstract
A large number of electropolished copper parts showed evidence of discoloration (tinting) after electropolishing. Because these parts are used in a high-vacuum application, even trace amounts of organic materials would be problematic. Scanning electron microscopy of nondiscolored and discolored areas both showed trace amounts of residue in the form of adherent deposits. EDS, FTIR spectroscopy, XPS, and secondary ion mass spectroscopy (SIMS) analyses indicated that the discoloration to the copper components was due to the development of CuO at localized regions. It was recommended that process changes be made to completely remove residual processing fluids from the part surfaces before electropolishing. The use of more aggressive detergents was suggested, and it was recommended also that a filtering and recirculating system be considered for use in the cleaning and electropolishing tanks.
Carbon Steel Heat Treating Problems
Authors: Aliya D. 
Published: May 2019

Abstract
A plant had manufactured and heat treated their product in house for years. As time went on, the special steel that they had been using became more expensive, and a switch was made to a more common and less highly alloyed material. However, no change in hardness specifications were made, because calculations of ideal critical diameter and analysis of available hardenability data indicated that the original hardness specification could be met. There was, however, less room for process variation. The parts ended up containing temper carbides, developed heavy decarburization, and experienced excessive distortion because they were left in the furnace for extended and varying periods with the temperature “turned down a couple hundred degrees.”
Investigation of Cracking and Erratic Behavior of the Uranium-Titanium Alloy
Authors: Bird E. L. 
Published: May 2019

Abstract
The U-0.8wt%Ti alloy is often used in weapon applications where high strength and fairly good ductility are necessary. Components are immersion quenched in water from the gamma phase to produce a martensitic structure that is amenable to aging. Undesirable conditions occur when a component occasionally cracks during the quenching process, and when tensile specimens fail prematurely during mechanical testing. These two failures prompted an investigative analysis and a series of studies to determine the causes of the cracking and erratic behavior observed in this alloy. Quench-related failures whereby components that cracked either during or immediately after the heat treatment/quenching operation were sectioned for metallographic examination of the microstructure to examine the degree of phase transformation. Examination of premature tensile specimen failures by scanning electron microscopy and X-ray imaging of fracture surfaces revealed pockets of inclusions at the crack origins. In addition, tests were conducted to evaluate the detrimental effects of internal hydrogen on ductility and crack initiation in this alloy.
Use of Electron Fractography to Diagnose Cracking in a Chromium-Plated AISI 4340 Pivot Bolt
Authors: Scott James A. 
Published: May 2019

Abstract
Overhaul mechanics discovered a crack in an AISI 4340 Cr-Mo-Ni alloy steel pivot bolt when grinding off the chromium plating. The bolt had served for an estimated 10,000 h and was replated when last overhauled. On checking the bolt, several fine cracks were found on the surface. A 6500x micrograph revealed the intergranular nature of a crack. By trying different grinding procedures, investigators were able to reproduce this type of failure in the laboratory. It was concluded that grinding cracks initiated the failure. It should be noted that governing specifications prohibit grinding on high-strength steel; chromium should be stripped by electrochemical methods.
Evaluating Component Failures: The Cure Can Be Worse Than the Illness
Authors: Suss Henry 
Published: May 2019

Abstract
The presence of secondary, branching intergranular stress-corrosion cracking in a type 440C stainless bearing caused the analyst to overlook the real culprit, which was a mechanically-initiated, primary transgranular crack that propagated through the steel's hard chromium carbide. Failure was actually caused by overload. Had the original conclusion been accepted, a relatively exotic alloy would have been specified. In another case, brass heat exchanger tube failure was automatically attributed to attack by an acidic cleaner, and a decision was made to stop using the solution. A more thorough analysis showed failure was caused by tube vibration. In a third case, a type 304 stainless steel bellows in a test loop was thought to have failed because of chloride stress corrosion. The report concluded with a recommendation that carbon steel be used as an alternative bellows material. Caustic, not chloride, stress corrosion was the culprit. Had material substitutions been made on the original premise of countering chloride stress corrosion, most of the loop's highly stressed components would have eventually failed.
Problematic Failure Analysis of a Cast Steel Crankshaft
Authors: Moore D.A. , Packer K.F. , Jones A.J. , Carlson D.M. 
Published: May 2019

Abstract
This case study involves two continuously cast steel crankshaft failures. Three parties performed their own failure analyses: (1) the engine manufacturer responsible for component design, specification, and application; (2) the steel supplier and forging supplier responsible for making the steel, forging the shape, and preliminary heat treatment; and (3) a supplier that provided induction hardening, finish machining, and inspection. An independent engineering firm was subsequently involved, but because each party had its own agenda, there was no agreement on the metallurgical source of the failure and thus no continued analysis to pin down and eliminate the root cause.
Failure of a Fairground Ride
Authors: Crosky A. 
Published: May 2019

Abstract
On 22 Feb 1997, one of the arms on an amusement park ride became detached from the central pylon, allowing the passenger carriage at the end of the arm to fall to the ground. Detachment of the arm was found to have occurred as a result of fracture of the cast steel bearing cap and the retaining bolt, which then allowed the axle to move out of its housing. The cap material was a cast 0.25% carbon steel. The retaining bolt failed in the threaded region, with no evidence of fatigue. One of the reinforcing straps welded to the outer surface of the cap had also fractured as the result of fatigue. Evidence of a weld repair could be seen at the location of the fracture. The bearing cap, cap 2L, failed by fatigue initiated from the corners of the two threaded holes. One of the two reinforcing straps then failed by overload, while the second one became detached by fracturing through the welds. The bolt then failed by overload. The cracking in cap 2L was not an isolated occurrence. Cracking was detected at the same location in almost all the other caps on the same device. The cracking had been in progress for considerable time. To prevent the reoccurrence of such a failure, recommendations are given for a more-rigorous inspection protocol.
Failure of Large Tantalum Heat Exchanger During Transportation to Site
Authors: Blum M. E. 
Published: May 2019

Abstract
A steam heated exchanger was designed for concentrating sulfuric acid. Tantalum was selected for the tubing and the tube sheet liner because of its outstanding corrosion resistance. However, although the exchanger passed a searching shop inspection, it leaked during site testing. Considerable argument ensued about whether the cracking observed was due to poor welding during fabrication, or through abuse during handling on site. An SEM examination of the fractures revealed high cycle, low amplitude fatigue, and the problem was traced to vibration during road transport. Further failures were avoided by improved design and packing. This paper illustrated the value of SEM fractography when a rapid investigation is needed under the pressures of a fast moving project.
Metallurgical Examinations of a Fragmented Blank Firing Adapter and Associated Components from an M-16 Rifle
Authors: Gray R. J. , Houck C. W. 
Published: May 2019

Abstract
Personnel responsible for laboratory protection at some plants are required to participate in exercises simulating a breach of security at the site. This document reports a metallurgical investigation of blank firing adapters (BFA), one of which exploded during such a training exercise. Determination of the cause of the explosion was the primary objective of the examination. Metallographic studies included the examination of BFAs fabricated from two different types of alloys that were tested for shock reaction. Optical microscopy supported by electron microscopy and analytical methods were used. Our investigation supports the supposition that a live round of ammunition was inadvertently fired.
Failure of Propeller Attachment Bolts
Authors: Craft C. Howard 
Published: May 2019

Abstract
The propeller from a small private airplane came off in flight. The head ends of all six attachment bolts remained in the propeller hub when it was found. Two threaded shanks with nuts remained with the engine, while the remaining four shank ends with their nuts were missing. Parts available for examination, in addition to the hub and attachment bolts, were the two propeller blades and the engine crankshaft. The purpose of this examination was to determine the nature and probable cause of failure in the six attachment bolts. Indications of fatigue failure and wear were the major findings in visual and low power microscopic examination. Fracture surfaces indicated failure was initiated in the threads in four bolts and in the shanks in two. The group of four bolts failed primarily due to tensile loads, while the other two bolts failed primarily due to bending loads. It was concluded that failure was due to improper installation torqueing of the bolts.
Exploring the Student-Centered Classroom Management and Self-Actualization Tendencies in Georgian Classrooms
Authors: TVALCHRELIDZE Nino , Alkesidze Nana 
Published: May 2019

The demands of the 21st century world have changed, these changes require the modernization of the tendencies almost in every field, including education. The demand of the globalized world caused the shifting of educational approaches from the conventional and traditional methods to more contemporary, person–oriented and challenging ones. Georgia is a developing country. The multi-ethnicity of the population makes its educational system to be more sophisticated and tailored to the population needs and contemporary challenges. Self-actualization is one of the best ways of students’ engagement and encouragement in the educational process and for their preparation as life-long self-directed learners. Adopting the student-centered approach in teaching enhances the process of students’ engagement in the classroom activities and their self-actualization. In order to find out the state of the student-centeredness and self-actualization in Georgian high schools the quantitative approach (4-point Likert scale questionnaire) was applied. Eight schools from different regions of Georgia were involved in the research. The results from the research are positive enough: more than the half of the high school students in Georgian schools both in public and in private ones consider their classroom and the whole educational management more student-centered than teacher-centered. However, there is still much to be done for fostering and enhancing theses tendencies for making students learn in a really student-centered classroom environment and to make them more self-actualized.