bluuebunny/crossref_metadata_2025_split huggingface dataset:
PRODUKSI BIODIESEL DARI LEMAK SAPI DENGAN PROSES TRANSESTERIFIKASI DENGAN KATALIS BASA NaOH
Authors: Ranggita Dwi Nindya Affandi  , Toni Rizki Aruan  , Taslim  , Iriany  
Published: October 2019

Biodiesel is an alternative fuel commonly produced from vegetable oil or animal fat with methanol through transesterification. Beef tallow was used as a raw material of transesterification to make biodiesel, because the price of beef tallow was driven down by the market and to reduce the pollution to the surrounding. In this research variable observed were reaction temperature, reaction time and amount of catalyst. Transesterification was carried out in a three necked spherical Pyrex vessel equipped with reflux condenser, stirrer and thermometer. In the present investigation an attempt has been made to use beef tallow as low cost sustainable potential feedstock for biodiesel production by single step transesterification process. Under optimal condition, the maximum yield of 95,67 % beef tallow methyl ester was obtained by using 6 : 1 molar ratio of beef tallow to methanol at 50 oC for a reaction time 30 minutes in the presence of 0,8 wt% of NaOH catalyst. The biodiesel properties were comparable to Indonesian National Standard (SNI). The results of this work showed that the use of beef tallow is suitable for feedstock of biodiesel production with low cost.
PENGARUH WAKTU POLIMERISASI PADA PROSES PEMBUATAN POLIESTER DARI ASAM LEMAK SAWIT DISTILAT (ALSD)
Authors: Ahmad Rozi Tanjung  , Ida Ayuningrum  , Renita Manurung  
Published: October 2019

Palm Fatty Acid Distillate (PFAD) can be used as raw material for synthesis polyester. The aim of this research is to synthesis of polyester and to determine the effect of reaction time on polymerization methyl ester PFAD. The esterification stage was done at temperature 70oC, reactiontime 120 minute, reactant ratio 1:8 (PFAD:methanol), concentration of catalyst (H2SO4) 1% (w/w) PFAD;polymerization stage was done at temperature 126-132°C, concentration ofcatalyst (BF3-diethyl etherate) 9.2 % (w/w), variation of polymerization reaction time3, 4, and 5 hours; and polyesterification stage was done at temperature 175-200 oC,reactant ratios (w/w) 1:1 (polymerized ME : ethylene glycol), reaction time 4 hours and all ofstage was stirred at 150 rpm. The results showed, in the esterification stage wasobtained methyl ester with iodine value 77.29 g I2/100 g, viscosity 6.90 cP,density 859.91 kg/m3 and analysis byusing GC-MS showed that the purity of methyl ester was 82.23% andmolecular weight 267.97 g/mol. Decreasing in iodine value from 77.294 I2 g/100 g to 63.45-61.14 gI2/100 g indicated that the polymerization process had takenplace. In polyesterification stage wasobtained gel polyester, viscous, dark brown colored solid at room temperature with acid value from13.13 to 21.65 mg KOH/g, viscosity from 14.3 to 19.1 P, and molecular weight 995.03 to 1,522.07g/mol which is more suitable for application of modified polyester. Analysis by using GC showed that the purity of polyester is equal to 65.49%.
PEMANFAATAN KITOSAN DARI CANGKANG RAJUNGAN (Portonus sanginolentus L.) SEBAGAI PENGAWET IKAN KEMBUNG (Rastrelliger sp) DAN IKAN LELE (Clarias Batrachus)
Authors: Rika Silvia  , Sari Wahyu Waryani  , Farida Hanum  
Published: October 2019

The use of appropriate anti-microbial compounds can extend the shelf life of a product as well as ensure the safety of the product. That requires a material that is naturally anti-microbial so as not harmful to health. The use of chitosan to inhibit microbial activity on mackerel (Rastrelliger sp) and catfish (Clarias batrachus) to test it's effectiveness. In this research chitosan that used as an anti-microbial extracted from the shells of crabs (Portunus sanginolentus L.). Chitin and chitosan that were successfully extracted were characterized it's results includes moisture content testing, ash content, and degrees of deacetylation. Characterized chitosan, were used as an anti-microbial mackerel (Rastrelliger sp) and catfish (Clarias batrachus). Chitosan was dissolved in 1% acetic acid with varying concentrations of chitosan as 1%, 1.5%, 2%, and 2.5%. The storage time of fish: 0 hours, 10 hours, 15 hours, 20 hours, and 25 hours. The results of research chitosan form as granules / powder, 5% moisture content, ash content 2% and the degree of deacetylation which amounted to 61,08%. Chitosan solution test results on fish showed that fish preservation by soaking with chitosan addition of 1.5% was the best variable and could extend the shelf life of fish more than 5 hours while fish preservation by spraying gave the best variable with addition of chitosan 2.5% and could extend the shelf life of fish less than 5 hours.
PENGARUH PENAMBAHAN RESORSINOL PADA PEMBUATAN PEREKAT LIKUIDA SABUT KELAPA
Authors: Mutiara Istiqomah  , Netti Herlina  
Published: October 2019

Liquid adhesive coconut coir is the result of a reaction between lignin powder material used with aromatic compounds at high temperatures in order to obtain a solution that can be used as an adhesive. This study aims to investigate the characteristics of liquid adhesive of coconut coir (LACC) qualities and determine the effect of resorcinol in the manufacture of adhesives LACC. The study was conducted in three phases: the first stage of coir manufacturing particles, which at this stage coir made into particles of 100 mesh, adhesive manufacturing second stage LACC which at this stage there are two stages of the liquefaction reaction coir and polymerization, and the third stage addition of resorcinol LACC into the adhesive. The variables used in this study is the addition of variable rate resorcinol at 10, 20, 30% by weight. Variables - variables that were analyzed pH, viscosity, spesific gravity, solid content, formaldehyde-free rate and compound analysis using FT-IR adhesive LACC to conditions without the addition of resorcinol and with the addition of 30% resorcinol. The results showed that the addition of resorcinol LACC influence on the resulting adhesive, which has a liquid form, the pH ranged from 12.6 to 10.6, 43,867- 131.712 cps viscosity, specific gravity of 1.252 to 1.258, solid content 46.67 to 80%, from 1.952 to 1.051% formaldehyde content. FT-IR results showed similarity LACC adhesive force phenol formaldehyde resin, namely the presence of the OH group, C = H of the aromatic ring, of methylene CH, CO from ether and fenolic compound.
PENGHILANGAN TINTA PADA KERTAS THERMAL BEKAS : PENGARUH KONSISTENSI DAN KONSENTRASI PENDISPERSI FLOTASI
Authors: Sulastri Dewanti  , Elisabet Aprilyanti  , Taslim  
Published: October 2019

Recycling of wastepaper is a solution for paper industry to overcome the scarcity and the limited presence of the virgin pulp sources. Thermal paper is a highly engineered product coated with a thermal sensitive layer that reacts in the presence of heat to create the printed image. The purpose of this research is to study the effect of pulp consistency and dispersant concentration on the removal of ink in the thermal paper. There are 3 steps in this research which are immersing, pulping and flotation. The results of this research were measured according to TAPPI and SNI to determine the brightness and tensile strength of the recycled paper, respectively. The excellent conditions were obtained at pulp consistency of 0.8%, dispersant concentration of 1.5%, flotation temperature of 50 °C and flotation time of 40 minutes. In these conditions, the brightness was 72,17% and tensile strength was 3.7 kN/m.
PENGARUH KONSENTRASI PEREKAT TEPUNG TAPIOKA DAN PENAMBAHAN KAPUR DALAM PEMBUATAN BRIKET ARANG BERBAHAN BAKU PELEPAH AREN (Arenga pinnata)
Authors: Julham Prasetya Pane  , Erwin Junary  , Netti Herlina  
Published: October 2019

The demand of renewable energy resources has been increasing. Briquette is one of the alternative energy resource which can be produced from utilization of biomass. This research aims to obtain a briquette from sugar palm frond, to obtain the effect of adhesive concentration of cassava starch and addition of lime on the quality of briquettes. This research used the batch method. Research variabels are the adhesive concentration of cassava starch in 0%, 10%, 20% and 30% (w/w) and the addition of lime in 0%, 1%, 3% and 5% (w/w) based on the weight of char powder. General materials are sugar palm (Arenga pinnata) frond, cassava starch and lime, and the general tools are furnace, briquette printer, oven, moisture analyzer, universal testing machine and bomb calorimeter. Briquetting process was started with sugar palm fronds preparation then they’re carbonized at 350 oC for 2 hours. Product of carbonization as a charcoal which is added by a cassava starch adhesive and lime then they’re printed or shaped and dried to be a briquette. Analysis used is the proximate analysis of the test parameters moisture content, ash content, volatile combustion matter content, carbon content, calorific value and compressive strength. The best briquette is with adhesive concentration in 0% and addition of lime in 5% with the calorific value 6502,379 cal/g, 45,56% fixed carbon, 6,44% moisture, 18,00% ash, 30,00% volatile combustion matter and 59,141 kg/cm2 compressive strength.
PENGARUH LIMBAH ABU PEMBAKARAN BIOMASSA KELAPA SAWIT TERHADAP SIFAT-SIFAT FISIKA DAN MEKANIK HIGH IMPACT POLYSTYRENE
Authors: Fadhilla Asyri  , Kartini Noor Hafni  , A. Haris Simamora  
Published: October 2019

This study aims was to determine the effect of palm oil fuel ash (POFA) composite as filler on the physical and mechanical properties of high impact polystyrene (HIPS) composites. The research methodology included preparation of raw materials, treatment POFA (hydration process of POFA), mixing using tumbler and then extruder, molding composite specimens, and testing. The variables used were weight ratio of HIPS with 140 mesh POFA at 95/5; 92.5/7.5; 90/10. The composites were tested by Fourier Transform Infrared (FTIR), ash content, specific gravity, tensile strength, elongation at break, impact strength, hardness test, and Scanning Electron Microscopy (SEM). The results of FTIR characterization shows the formation of –OH bonding that was suspected as Si-OH or Si-hydrat. Results of physical and mechanical properties of the composites shows that increase of the filler composition in HIPS-POFA composites until the ratio of 90/10, increase the specific gravity to 7.2% of the original, tensile strength did not change significantly to 28.4 MPa, elongation at break decreased to 2.7%, impact strength decreased to 3.183 KJ/m2, and the hardness increased to 110.5, and Scanning Electron Microscopy (SEM) test show the transformation of POFA structure on treated POFA and intercalation between the matrix and POFA.
EKSTRAKSI MULTI TAHAP KURKUMIN DARI KUNYIT (Curcuma domestica Valet) MENGGUNAKAN PELARUT ETANOL
Authors: Rajian Sobri Rezki  , Dwimas Anggoro  , Siswarni MZ  
Published: October 2019

Curcumin is a pigment in Curcuma domestica Valet, which has an orange-yellow crystal appearance, and commonly being used as a colouring agent. Extraction method which is used in extracting curcumin from Curcuma domestica Valet is one stage extraction. This research studied a multi stages extraction of curcumin from Curcuma domestica Valet. The purposes of this research is to find the best condition in extracting curcumin using multi stages extraction method, to increase the efficiency rate in curcumin extraction. This research used ethanol as a solvent, and effect from variables such as extraction time, solvent concentration, and number of extraction stages are observed. Extraction times are 60 minutes, 120 minutes, and 180 minutes. Variations of ethanol concentration are 50%, 70%, and 96%. Stage numbers of extraction are two stages extraction and three stages extraction. Extracts of curcumin are examined with qualitative analysis and quantitative analysis. The best condition of multi stages curcumin extraction is determined based on yield and content of curcumin. The maximum yield obtained in this study was 12% with conditions 180 minutes extraction time, 96% ethanol concentration, and two stages extraction. The highest content of curcumin obtained is 16% with conditions 180 minutes extraction time, 96% ethanol concentration, and three stages extraction. Content means a fraction of yield. These results show that increase in extraction time, solvent concentration, and stage numbers of extraction will increase the yield and content of curcumin extracted from Curcuma domestica Valet.
PEMBUATAN GLISEROL TRIBENZOAT DENGAN PROSES ESTERIFIKASI MENGGUNAKAN KATALIS H-ZEOLIT TERAKTIVASI OLEH ASAM KLORIDA DAN ASAM SULFAT
Authors: Mutiara Valentina M  , Ekelesia Martina  , Zuhrina Masyithah  
Published: October 2019

Esterification is one method that is often used in converting glycerol. Glycerol tribenzoate is a derivative product of glycerol which used as a plasticizer for polymer industry, food additives, water repellent material on printer ink, and many more. This research aims to study the making of glycerol tribenzoate through esterification process by using natural zeolit catalyst which is activated with hydrochloric acid, in order to obtain the optimum catalyst % weight (w/w glycerol), and also to see the potential of recycling the zeolit. Zeolit is activated by 4M for 6 hours, and then calcined in the furnace at 500 oC for 5 hours. Then continued to esterification process, glycerol 90% reacted with benzoic acid which dissolved in metanol, with mole ratio of benzoic acid and glycerol at 3,5:1, reaction temperature at 65 oC, and the stirrer speed of 200 rpm, the catalyst % weight is varied at 5 %, 6%, 7%, and 8%, and catalyst recycling is performed 3 times. FTIR characterization result a close match, shows that the product is glycerol tribenzoate. The highest yield of zeolite which activated by HCl is obtained at 6% catalyst % weight i.e 68,992%, while zeolite that activated by H2SO4 is obtained at 8% catalyst % weight i.e 69,678%, H- zeolit catalyst is still feasible to use up to 3 times recycling, with percent of yield reduction for each recycle is ≤ 8%.
PENGARUH KONSENTRASI RAGI DAN WAKTU FERMENTASI PADA PEMBUATAN BIOETANOL DARI BIJI CEMPEDAK (Artocarpus champeden spreng)
Authors: Irvan  , Ayu Wandira Putri  , Sri Ulina Surbakti  , Bambang Trisakti  
Published: October 2019

Needs fuel as a source of energy every day is increasing, while the energy reserves of petroleum (fossil) dwindling, therefore, to meet the needs of the fuel it is necessary to develop alternative fuels that are renewable and home environment (renewable ). Etonal Bioethanol is made from plants containing starch, sugar and other plant cellulose. Where in this study using jackfruit seeds that contain high enough carbohydrates as raw materials. This research aims to make bioethanol from cempedak seeds with various concentrations of yeast and fermentation time. The main process is hydrolysis; fermentation using yeast Saccharomyces Cereviciae; and purification by distillation and condensation. Variables used are changes in the concentration of yeast 3%, 6%, 9% and 2 days, 3 days, 4 days fermentation period. From the analysis of the research results obtained bioethanol yield per amount of raw materials is the best starting 12,5 ml/kg with a density of 0.962 g/ml and the calorific value sebasar 181.925 kcal/kg, which is the variation of the concentration of 9% and 3 days of fermentation period.
ISOLASI PROTEIN SELAMA PROSES PENGAMBILAN KITIN DARI KULIT UDANG
Authors: Kherliyanda Febriani  , Fitri Hariani Nurza  , Iriany  
Published: October 2019

Shrimp is one of the Indonesia fishery commodities with high economic value. The production of shrimp shells is usually 40-45% from crude shrimp. Shrimp shell contain protein, chitin, minerals and carotenoids. It is very potential to be used as materials for isolation of protein.This experiment is to determine factors that effect protein recovery and optimize deproteination processconditions to produce high yield of protein. The design of experiment used response surface methodology. It is 2 steps consist of deproteination and protein extraction process using shrimp shells and KOH solution in comparison 1:10 (w/v). The concentration of KOH are1,3 M; 2 M; 3 M; 4 M; 4,7 M. The reaction temperatures are37 oC; 40 oC; 45 oC; 50 oC; 53 oCand the reaction times are 40 minutes, 60 minutes, 90 minutes, 120 minutes, 140 minutes. Reaction temperature is the main factor influence protein recovery process. The highest protein yield obtained is 64,5826 % with protein content is 86,24% using KOH solution 2,98 M, reaction temperature 45,76 ºC and reaction time 90,51 minute. Economic potential by protein recovery during isolation of chitin from shrimp shells is profitable.
PENGARUH WAKTU FERMENTASI TERHADAP VOLUME GAS BIO DAN PENYISIHAN COD DENGAN METODE PERLAKUANAWAL MENGGUNAKAN KALIUMHIDROKSIDA(KOH) PADA ECENG GONDOK (Eichhornia crassipes)
Authors: Setiaty Pandia  , Amin Trisnawati  
Published: October 2019

The purpose of this study was to determine the effect of alkali pre-treatment methods on the quality and quantity of biogas. The study was doneby fermentation process the water hyacinth with KOH in a concentration of 6,7 M; 4 M;3 M; and 2,95 (M) with water in ratio hyacinth: water 70:30; 50:50; 30:70 and 100:0 (v/v) mixed with cow dung starter in an anaerobic digester batch system of 2,5 L capacity. In this study the highest biogas production at KOH concentration 4 M was in ratio of 50:50 (v/v)with yield biogas volume 449 mL and 86,52% of COD revomal, 92,42% of TSS removal. The lowest biogas production at KOH concentration 6,7 M was in ratio of 70:30 (v/v) with yield biogas volume 132 mL and 86,55% of COD removal and 88,65%of TSS removal.
PENGARUH AERASI PADA FERMENTASI PADAT TANDAN KOSONG KELAPA SAWIT OLEH Aspergillus niger TERHADAP PRODUKSI GULA SEDERHANA
Authors: Himmatun Wisda  , Wahyudi Budi Sediawan  , Sarto  
Published: October 2019

The effects of aeration on production of simple sugars by Aspergillus niger were investigated using oil palm empty fruit bunch (OPEFB) by solid state fermentation using Aspergillus niger. Simple sugars can further be fermented to produce bioethanol. OPEFB is renewable cellulosic biomass and largely available in Indonesia. Before being fermented, OPEFB needs to be pretreated. It was done by NaOH 1% solution at 150 ºC for 2 hours. The concentrations simple sugars produced by hydrolysis were analyzed by Dinitrosalicylic acid (DNS). It turned out that the highest concentration of sugars was to be 9,102 g/L, and it was obtained on the 3rd day of fermentation. Some parts of the sugars produced were consumed by Aspergillus niger itself for growth and maintenance. The experiment showed that aeration increased the simple sugars concentration. Modelling of reaction kinetic assumed to hydrolisis process and simple sugar consumed. Simply modelling can describe in quantitative fermentation of OPEFB. Moreover, get parameters value at equation of reaction kinetic.
PEMBUATAN BIOBRIKET DARI PELEPAH DAN CANGKANG KELAPA SAWIT: PENGARUH VARIASI KOMPOSISI BAHAN BAKU DAN WAKTU KARBONISASI TERHADAP KUALITAS BRIKET
Authors: Iriany  , Cindy Carnella  , Cici Novita Sari  
Published: October 2019

Briquette was a product of the compaction process of biomass residue used as fuel and it is formed using binder. Briquette from biomass has a high heating value. The quality of briquettes influenced by raw material composition and the time of carbonization. The carbonization process in the manufacture of briquettes could improve heating value and reduce smoke produced from burning briquette. This research is aim to study the effect of variations in the composition of raw materials and carbonization time on the heating value and the characteristics of the resulting briquettes. The materials used are palm fronds, palm shells, starch, used oil, H2SO4 and Tri Ethyl Amine (TEA). The ratios of palm frond and palm shell charcoal in this research is 1: 2, 1: 4, 1: 6 and 1: 8 with variation of carbonization time 30 minutes, 60 minutes, 90 minutes and 120 minutes. The research began with the carbonization process of the raw materials. Then charcoal product of carbonization was pressed using an binder starch and used oil as much as 20% based on the weight of raw materials at the ratio of 1: 1. The best quality from this research is obtained at the ratio palm fronds and oil palm shell 1: 8 with carbonization time of 120 minutes, heating value 15107,138 cal/g, moisture content 6%, ash content of 5,185%, volatile matter 39,226%, fixed carbon 70,955%, density 0,442 g/cm3, burning rate 0,273 g/min, and compressive strength 0,046 N / mm2. The result shows the briquettes produced had a strong structure, it was not easily broken and it was not moldy when stored.
O papel da Internet na constituição de redes sociais transnacionais de sociabilidade e mobilização dos estudantes brasileiros no ensino superior em Portugal
Authors: Iorio Juliana Chatti , Fonseca Maria Lucinda Cruz dos Santos 
Published: October 2019

Na era da globalização, o papel da Internet tem sido fundamental para a formação de redes de contatos além-fronteiras. Com a introdução das chamadas redes sociais online de relacionamento (Facebook, Twitter, Instagram, Google+, Youtube, MySpace, Badoo, etc), a facilidade em comunicar e obter informações de qualquer parte do globo aumentou ainda mais, apesar do acesso a essas novas mídias ainda não ser igual para todos.Tendo como base as entrevistas qualitativas realizadas no âmbito do projeto de doutorado em desenvolvimento sobre as trajetórias de mobilidade dos estudantes brasileiros no ensino superior em Portugal, pretende-se discorrer sobre a importância do Facebook na constituição de redes de contatos entre Brasil e Portugal. Os resultados preliminares têm apontado esta rede social online como uma das grandes facilitadoras deste tipo de mobilidade.
El desarrollo profesional de los maestrantes del programa de la Maestría en Educación de la Universidad de Cienfuegos, Cuba
Authors: Lara Díaz Lidia Mercedes , Sánchez Arce Luís , Bravo López Gisela 
Published: October 2019

La Maestría en Educación que se desarrolla por el Centro de Estudios de la Didáctica y Dirección de la Educación Superior de la Universidad de Cienfuegos, Cuba, considera entre sus objetivos esenciales la formación de master con una concepción ética y responsabilidad expresadas en la autonomía y el compromiso de su función educativa, propósito que se logra en la medida en que el programa contribuye al desarrollo profesional docente de los maestrantes.
El propósito del artículo es exponer la contribución de la Maestría en Educación, en sus dos modalidades (presencial y semipresencial), al desarrollo profesional docente de los maestrantes matriculados en el programa; concebido este como un proceso que genera aprendizajes, desde la reflexión, la indagación y la trasformación de su propia práctica, incidiendo en la calidad de su desempeño, sobre la base de un clima de diálogo y participación en su contexto de actuación.
Los resultados de la investigación evidencian que la Maestría en Educación contribuye al desarrollo profesional docente de los maestrantes, orientada tanto al ámbito profesional, como al personal y social.
Los indicadores del desarrollo profesional docente de los maestrantes se agrupan en atención al vínculo con: la actividad académica, el trabajo metodológico, la gestión del proceso formativo, la investigación y la reflexión de su propia práctica.