bluuebunny/crossref_metadata_2025 huggingface dataset:
Label-Free Quantification (LFQ) of Fecal Proteins for Potential Pregnancy Detection in Polar Bears
Authors: Curry Erin , Philpott Megan E. , Wojtusik Jessye , Haffey Wendy D. , Wyder Michael A. , Greis Kenneth D. , Roth Terri L.
Published: May 2022

Reliable pregnancy diagnostics would be beneficial for monitoring polar bear (Ursus maritimus) populations both in situ and ex situ, but currently there is no method of non-invasive pregnancy detection in this species. Recent reports in several carnivore species described the identification of fecal proteins that may serve as pregnancy biomarkers; however, repeatability has been limited. The objective of the current analysis was to utilize an unbiased, antibody-free, label-free method for the identification and quantification of fecal proteins to determine if differences associated with pregnancy are detectable in polar bears. Protein was extracted from fecal samples (n = 48) obtained from parturient (n = 6) and non-parturient (n = 6) profiles each at four timepoints: pre-breeding season, embryonic diapause, early placental pregnancy, and mid-placental pregnancy. Protein was prepared and analyzed on the Thermo Orbitrap Eclipse nanoLC-MS/MS system. A total of 312 proteins was identified and quantified; however, coefficients of variation (CV) were high for both abundance ratio variability (384.8 ± 61.0% SEM) and within group variability (86.8 ± 1.5%). Results of this study suggest that the inconsistencies in specific protein concentrations revealed previously by antibody-based assays may not be due to that methodology’s limitations, but rather, are reflective of true variation that exists among samples.
The Highest Density of Phosphorylated Histone H1 Appeared in Prophase and Prometaphase in Parallel with Reduced H3K9me3, and HDAC1 Depletion Increased H1.2/H1.3 and H1.4 Serine 38 Phosphorylation
Authors: Legartová Soňa , Lochmanová Gabriela , Bártová Eva
Published: May 2022

Background: Variants of linker histone H1 are tissue-specific and are responsible for chromatin compaction accompanying cell differentiation, mitotic chromosome condensation, and apoptosis. Heterochromatinization, as the main feature of these processes, is also associated with pronounced trimethylation of histones H3 at the lysine 9 position (H3K9me3). Methods: By confocal microscopy, we analyzed cell cycle-dependent levels and distribution of phosphorylated histone H1 (H1ph) and H3K9me3. By mass spectrometry, we studied post-translational modifications of linker histones. Results: Phosphorylated histone H1, similarly to H3K9me3, has a comparable level in the G1, S, and G2 phases of the cell cycle. A high density of phosphorylated H1 was inside nucleoli of mouse embryonic stem cells (ESCs). H1ph was also abundant in prophase and prometaphase, while H1ph was absent in anaphase and telophase. H3K9me3 surrounded chromosomal DNA in telophase. This histone modification was barely detectable in the early phases of mitosis. Mass spectrometry revealed several ESC-specific phosphorylation sites of H1. HDAC1 depletion did not change H1 acetylation but potentiated phosphorylation of H1.2/H1.3 and H1.4 at serine 38 positions. Conclusions: Differences in the level and distribution of H1ph and H3K9me3 were revealed during mitotic phases. ESC-specific phosphorylation sites were identified in a linker histone.
Ciclopirox Hydroxypropyl Chitosan (CPX-HPCH) Nail Lacquer and Breathable Cosmetic Nail Polish: In Vitro Evaluation of Drug Transungual Permeation Following the Combined Application
Authors: Monti Daniela , Tampucci Silvia , Paganini Valentina , Burgalassi Susi , Chetoni Patrizia , Galván Jordi , Celandroni Francesco , Ghelardi Emilia
Published: May 2022

Background: Onychomycosis produces nail chromatic alterations that lead patients to mask them with cosmetic enamels. Objectives: Evaluate drug transungual permeation and antimycotic activity against selected strains after application of CPX-HPCH nail lacquer (NL) on the nail pre-covered with breathable cosmetic polish. Methods: CPX transungual permeation after applying CPX-HPCH NL once or twice a day on bovine hoof membranes pre-covered with a breathable cosmetic nail polish was compared to that obtained applying CPX-HPCH NL directly on the membrane. The relevant experimental permeates underwent an in vitro susceptibility test. Results: After CPX-HPCH NL application once a day, the drug transungual flux in the presence of cosmetic product tended to decrease while maintaining the antifungal activity. Two daily applications of CPX-HPCH NL on the membrane pre-covered with cosmetic polish exhibited the same permeation profile as daily application of the medicated lacquer directly on the nail as well as the same microbiological activity. Conclusions: The breathable cosmetic nail polish can be applied on the nail affected by onychomycosis in association with CPX-HPCH NL to mask the imperfections. The application of CPX-HPCH NL twice a day appears to be a good solution to obtain the same results as for a daily application without the presence of the cosmetic layer.
Impact of Internet of Things (IoT) on Inventory Management: A Literature Survey
Authors: Mashayekhy Yasaman , Babaei Amir , Yuan Xue-Ming , Xue Anrong
Published: May 2022

Background: The advancement of Industry 4.0 technologies has affected every aspect of supply chains. Recently, enterprises have tried to create more value for their businesses by tapping into these new technologies. Warehouses have been one of the most critical sections in a supply chain affected by Industry 4.0 technologies. Methods: By recognizing the role of inventory management in a supply chain and its importance, this paper aims to highlight the impact of IoT technologies on inventory management in supply chains and conducts a comprehensive study to identify the research gap of applying IoT to inventory management. The trend and potential opportunities of applying IoT to inventory management in the Industry 4.0 era are explored by analyzing the literature. Results: Our findings show that the research on this topic is growing in various industries. A broad range of journals is paying particular attention to this topic and publishing more articles in this research direction. Conclusions: Upgrading a supply chain into an integrated supply chain 4.0 is beneficial. Given the changes in fourth-generation technology compared to previous generations, the approach of conventional inventory replenishment policies seems not responsive enough to new technologies and is not able to cope with IoT systems well.
Algorithm for Determining Time Series of Phase Transformations in the Solid State Using Long-Short-Term Memory Neural Network
Authors: Wróbel Joanna , Kulawik Adam
Published: May 2022

In the numerical analysis of manufacturing processes of metal parts, many material properties depending on, for example, the temperature or stress state, must be taken into account. Often these data are dependent on the temperature changes over time. Strongly non-linear material property relationships are usually represented using diagrams. In numerical calculations, these diagrams are analyzed in order to take into account the coupling between the properties. An example of these types of material properties is the dependence of the kinetics of phase transformations in the solid state on the rate and history of temperature change. In literature, these data are visualized Continuous Heating Transformation (CHT) and Continuous Cooling Transformation (CCT) diagrams. Therefore, it can be concluded that time series analysis is important in numerical modeling. This analysis can also be performed using neural networks. This work presents a new approach to storing and analyzing the data contained in the discussed CCT diagrams. The application of Long-Short-Term Memory (LSTM) neural networks and their architecture to determine the correct values of phase fractions depending on the history of temperature change was analyzed. Moreover, an area of research was elements that determine what type of information should be stored by LSTM network coefficients, e.g., whether the network should store information about changes of single phase transformations, or whether it would be better to extract data from differences between several networks with similar architecture. The purpose of the studied network is strongly different from typical applications of artificial neural networks. The main goal of the network was to store information (even by overfitting the network) rather than some form of generalization that allows computation for unknown cases. Therefore, the authors primarily investigated in the ability of the layer-based LSTM network to store nonlinear time series data. The analyses presented in this paper are an extension of the issues presented in the paper entitled “Model of the Austenite Decomposition during Cooling of the Medium Carbon Steel Using LSTM Recurrent Neural Network”.
Crystallization Mechanism and Optical Properties of Antimony-Germanate-Silicate Glass-Ceramic Doped with Europium Ions
Authors: Golonko Piotr , Sadowska Karolina , Ragiń Tomasz , Kochanowicz Marcin , Miluski Piotr , Dorosz Jan , Kuwik Marta , Pisarski Wojciech , Pisarska Joanna , Leśniak Magdalena , Dorosz Dominik , Żmojda Jacek
Published: May 2022

Glass-ceramic is semi-novel material with many applications, but it is still problematic in obtaining fibers. This paper aims to develop a new glass-ceramic material that is a compromise between crystallization, thermal stability, and optical properties required for optical fiber technology. This compromise is made possible by an alternative method with a controlled crystallization process and a suitable choice of the chemical composition of the core material. In this way, the annealing process is eliminated, and the core material adopts a glass-ceramic character with high transparency directly in the drawing process. In the experiment, low phonon antimony-germanate-silicate glass (SGS) doped with Eu3+ ions and different concentrations of P2O5 were fabricated. The glass material crystallized during the cooling process under conditions similar to the drawing processes’. Thermal stability (DSC), X-ray photo analysis (XRD), and spectroscopic were measured. Eu3+ ions were used as spectral probes to determine the effect of P2O5 on the asymmetry ratio for the selected transitions (5D0 → 7F1 and 5D0 → 7F2). From the measurements, it was observed that the material produced exhibited amorphous or glass-ceramic properties, strongly dependent on the nucleator concentration. In addition, the conducted study confirmed that europium ions co-form the EuPO4 structure during the cooling process from 730 °C to room temperature. Moreover, the asymmetry ratio was changed from over 4 to under 1. The result obtained confirms that the developed material has properties typical of transparent glass-ceramic while maintaining high thermal stability, which will enable the fabrication of fibers with the glass-ceramic core.
Processing and Mechanical Properties of Highly Filled PP/GTR Compounds
Authors: Kościuszko Artur , Sykutera Dariusz , Czyżewski Piotr , Hoyer Stefan , Kroll Lothar , Szczupak Bogusław
Published: May 2022

Ground rubber from automobile tires is very difficult to recycle due to the cross-linking of the macromolecules and thus the lack of thermoplastic properties. The research consisted of assessing the processing possibility via the injection of highly filled PP/GTR compounds modified with 1.5 wt.% 2.5-dimethyl-2.5-di-(tert-butylperoxy)-hexane. GTR dosing ranged from 30 wt.% up to 90 wt.%. The evaluation of the processing properties of the obtained materials was carried out on the basis of the melt flow index test results and the signals recorded during processing by the injection molding by temperature and pressure sensors placed in the mold. The influence of the applied modifier on the changes in the mechanical properties of PP/GTR was determined with hardness, impact and static tensile tests. Moreover, thermal properties were obtained by the differential scanning calorimetry method. It has been found that it is possible to efficiently process compounds with high GTR content using injection molding. The presence of the filler allows to significantly reduce the cooling time in the injection mold and thus the time of the production cycle. It has been confirmed that 2.5-dimethyl-2.5-di-(tert-butylperoxy)-hexane modifies the rheological properties of PP and thus the PP/GTR composition. The lower viscosity of the matrix results in a more accurate bonding with the developed surface of the GTR grains, which results in better mechanical properties of the rubber-filled polypropylene.
Restirring and Reheating Effects on Microstructural Evolution of Al–Zn–Mg–Cu Alloy during Underwater Friction Stir Additive Manufacturing
Authors: Li Ying , He Changshu , Wei Jingxun , Zhang Zhiqiang , Tian Ni , Qin Gaowu , Zhao Xiang
Published: May 2022

Friction stir additive manufacturing (FSAM) can be potentially used for fabricating high-performance components owing to its advantages of solid-state processing. However, the inhomogeneous microstructures and mechanical properties of the build attributed to the complex process involving restirring and reheating deserve attention. This study is based on the previous research of the underwater FSAMed 7A04 aluminum alloy and adopts a quasi in situ experimental method, i.e., after each pass of the underwater FSAM, samples were taken from the build for microstructural observation to investigate the restirring and reheating effects on microstructural evolution during the underwater FSAM. Fine-grain microstructures were formed in the stir zone during the single-pass underwater FSAM. After restirring, the grain size at the bottom of the overlapping region decreased from 1.97 to 0.87 μm, the recrystallization degree reduced from 74.0% to 29.8%, and the initial random texture transformed into a strong shear texture composed of the C {110}<11¯0>. After reheating, static recrystallization occurred in the regions close to the new additive zones, increasing the grain size and recrystallization degree. This study not only revealed the microstructural evolution during the underwater FSAM but also provided a guideline for further optimization of the mechanical properties of the Al–Zn–Mg–Cu alloy build.
Non-Destruction Evaluation Method for Long-Term Oxidation Behavior of SiC/SiC Composites with Different Preforms in Wet Oxygen
Authors: Sun Guodong , Wu Yan , Luan Xin’gang , Xu Xinming , Cao Xinxin , Zhang Jiahao , Zhao Huan , Zhang Qing , Cheng Laifei
Published: May 2022

The implementation of SiC fiber reinforced SiC/SiC composites to aero-engine hot components has attracted wide attention, due to their many excellent properties. Along these lines, in order to predict the oxidation behavior of the material in extreme environments and to explore the effect of different preforms on the oxidative behavior of the composites, four SiC/SiC composites, with different preforms, were oxidized under environmental conditions of pressure of 12 kPa H2O:8 kPa O2:80 kPa Ar, at 1400 °C temperature. Moreover, the morphology and defect distribution of the samples were characterized by carrying out scanning electron microscopy, and micro-computed X-ray tomography measurements. Furthermore, the relation between the micro- and macro-scales was established, so as to be able to predict the oxidation behavior of the composites; not only the quantitative relationship between the mass change rate and the defect volume change rate, but also the combination of micro-computed X-ray images.
Characterization of the Effect of Hollow Glass Beads on the Mechanical Properties of Structural Adhesives
Authors: Santos João P. J. R. , Correia Daniel S. , Marques Eduardo A. S. , Carbas Ricardo J. C. , Gilbert Frida , da Silva Lucas F. M.
Published: May 2022

Adhesives are extensively used in the automotive and aeronautical industries as they enable the creation of durable and light weight joints, with exceptional strength to weight ratios. The constant search for the means of adapting the mechanical performance of adhesives to each application has led to the use of several types of fillers to change their properties. Following a study on the effect of inorganic fillers, i.e., hollow glass beads, in the failure mechanisms of single lap joint’s (SLJ), this work focuses on the response of the strength and fracture properties of structural adhesives to this filler. To this end, their tensile strength and mode I fracture properties were thoroughly analyzed by performing bulk tensile and double-cantilever beam (DCB) tests, at a quasi-static speed. The specimens were manufactured by adding different %v/v of filler to two epoxy-based crash resistant adhesives. Both adhesives have shown a negligible effect on the tensile strength, a decrease in strain at failure and critical energy release rate in mode I, as well as an increase of the Young’s modulus, for higher % in volume of hollow glass beads. These phenomena were further analyzed recurring to scanning electron microscopy, and the concept of rule of mixtures.
Anisotropic Piezoelectric Properties of Porous (Ba0.85Ca0.15)(Zr0.1Ti0.9)O3 Ceramics with Oriented Pores through TBA-Based Freeze-Casting Method
Authors: Ge Siyu , Zhang Junzhan , Zhang Ying , Shi Peng , Wang Honghui , Liu Shangyi , Tian Zhifeng , Shi Zongmo
Published: May 2022

Porous (Ba0.85Ca0.15)(Zr0.1Ti0.9)O3 (BCZT) piezoelectric ceramics with an oriented directional hole structure were prepared by using the tertbutyl alcohol (TBA)-based freeze-casting method. The influences of sintering temperatures on the microstructure and piezoelectric properties of porous BCZT ceramics were investigated both perpendicular and parallel to the freezing direction. With the increase in sintering temperatures and the porosities decreased from 58% to 42%, the compressive strength increased from 14.0 MPa to 25.0 MPa. In addition, the d33 value of 407 pC/N for the sample sintered at 1400 °C was obtained parallel to the freezing direction, which was 1.40 times that of the other direction.
Current Trends on Mechanical, Corrosion Resistance, and Antibacterial Properties of Metallic Materials
Authors: Conradi Marjetka , Kocijan Aleksandra
Published: May 2022

The scope of the Special Issue entitled “Mechanical, Corrosion Resistance, and Antibacterial Properties of Metallic Materials” includes research regarding the latest developments in materials’ mechanical properties and characterization, pure/applied corrosion phenomena, and advanced understanding of bacterial adhesion and the induced antibacterial properties of metallic materials [...]
Quality and Quantity Assessment of the Water Repellent Properties of Functional Clothing Materials after Washing
Authors: Kowalski Mateusz , Salerno-Kochan Renata , Kamińska Irena , Cieślak Małgorzata
Published: May 2022

The aim of the research was to evaluate the changes in the surface properties of five functional clothing materials with water-repellent finishes (including PFC-free finish) after 1, 5, and 10 washes with three detergents. A new approach to the interpretation of the water-repellent properties of textile materials is presented, based on two techniques, i.e., the spray test method and contact angle measurements. The results showed that washing materials with hydrophobic finishes can cause significant changes in their properties, which are mainly dependent on the composition and structure of the material, as well as the type of hydrophobic finish. The PFC-free finish is the least resistant to washing. For all materials with PFC finishes, the water repellency depends on the fluorine content on the surface and fabric topography. It was also found that increasing washing frequency resulted in a gradual decrease in water repellency. The loss of water repellency below an acceptable level (Grade 3) occurred after the fifth washing for all materials. Significant differences in the interpretation of the results of the spray test and contact angle measurements were observed. Using these methods separately provides information on the changes in the surface properties of the tested materials; however, their parallel application allows for obtaining complementary data, which is important for the proper interpretation of results.
The Cultural Heritage of “Black Stones” (Lapis Aequipondus/Martyrum) of Leopardi’s Child Home (Recanati, Italy)
Authors: Santi Patrizia , Pagnotta Stefano , Palleschi Vincenzo , Colombini Maria Perla , Renzulli Alberto
Published: May 2022

A macroscopic lithological study and physical (hardness, size, weight) investigations, coupled with laser-induced breakdown spectroscopy (LIBS) and X-ray fluorescence (XRF) chemical analyses of three egg- and one pear-shaped polished black stones, exposed in the library of the child home of the famous poet Giacomo Leopardi, at Recanati (Italy), were carried out. They are characterized by different sizes: two with the same weight of 16.9 kg and the two smaller ones of 5.6 kg each, corresponding to multiples of standard roman weights (drachma and scrupulum). These features and the presence of some grooves on the rock artefacts, probably for grappling hooks, suggest an original use as counterweight for the four black stones herein classified as amphibole-bearing serpentinites whose lithologies are far away from Recanati (probably coming from geological outcrops in Tuscany). The four serpentinite stones closely match with the so-called Lapis Aequipondus used in antiquity by the Romans as counterweights. Due to the presence of lead rings or iron hooks in these stones, Lapis Aequipondus were also used for martyrdoms during the persecution of Christians in the Roman period, attached to the necks of martyrs that were then thrown in the wells or attached to the ankles of hanging bodies. This is the reason why these stones are also known as Lapis Martyrum, venerated with the relative martyrs, in several churches of Rome. The four black stones investigated probably arrived at Recanati from Rome after the middle of the 19th century. In the past, Christians also called Lapis Martyrum the “devil’s stones” (Lapis Diaboli). This could also be the reason for the popular belief that black stones cannot be touched by people, except those of the Leopardi dynasty. This work contributes to the cultural heritage of Leopardi’s child home, as the four black stones had never been investigated.
The Electrical Response of Real Dielectrics: Using the Voltage Ramp Method as a Straightforward Diagnostic Tool for Polymeric Composites
Authors: Vitulo Paolo , Zanoletti Michele , Morina Riccardo , Callegari Daniele , Quartarone Eliana , Viola Riccardo , Comoretto Davide , Dulio Sergio , Mustarelli Piercarlo , Patrini Maddalena
Published: May 2022

An experimental method exploiting the capacitive response of most materials is here revised. The procedure called the “Voltage Ramp Method” (VRM) is based on applying proper voltage ramp cycles over time and measuring electrical current intensity flowing through the material sample. In the case of an ideal capacitor, a current plateau should be easily measured, and the capacitance value precisely determined. However, most media, e.g., semiconductors and insulating polymers, show dielectric absorption and hence electric leakage effects. Therefore, the VRM method allows simultaneous determination of their equivalent capacitance and resistance. Some case studies are discussed as concerning the application of VRM to both standard and actual media. A figure of merit of the method is the percentage difference between 2.5% and 1.5% with respect to the nominal values of a commercial capacitor and resistor, respectively. The simulation modeling of the material electrical response is compared to the experimental data also on polymer nanocomposites suitable for energy harvesting.
Optimization of the Heat Dissipation Performance of a Lithium-Ion Battery Thermal Management System with CPCM/Liquid Cooling
Authors: Zeng Xiaoping , Men Zhengxing , Deng Fang , Chen Cheng
Published: May 2022

In view of the harsh conditions of rapid charging and discharging of electric vehicles, a hybrid lithium-ion battery thermal management system combining composite phase change material (PCM) with liquid cooling was proposed. Based on the numerical heat transfer model, a simulation experiment for the battery thermal management system was carried out. Taking the maximum temperature and temperature difference of the battery module as the objectives, the effects of PCM thickness, the liquid flow rate and the cross-sectional area of the liquid channel on the temperature of the battery module were analyzed using response surface methodology (RSM). The results show that 31 groups of candidate parameter combinations can be obtained through response surface analysis, and phase change material (PCM) thickness should be minimized in order to improve space utilization in the battery module. The optimal parameter combination is a flow rate of 0.4 m/s and a PCM thickness of 5.58 mm, with the cross-sectional area of the liquid channel as 3.35 mm2.
Silver Nanoparticles Inhibit Metastasis of 4T1 Tumor in Mice after Intragastric but Not Intravenous Administration
Authors: Brzóska Kamil , Wojewódzka Maria , Szczygiel Małgorzata , Drzał Agnieszka , Sniegocka Martyna , Michalczyk-Wetula Dominika , Biela Eva , Elas Martyna , Kucińska Małgorzata , Piotrowska-Kempisty Hanna , Kapka-Skrzypczak Lucyna , Murias Marek , Urbańska Krystyna , Kruszewski Marcin
Published: May 2022

The potential anticancer activity of different silver nanoformulations is increasingly recognized. In the present work, we use the model of 4T1 tumor in BALB/ccmdb immunocompetent mice to analyze the impact of citrate- and PEG-coated silver nanoparticles (AgNPs) on the development and metastatic potential of breast cancer. One group of mice was intragastrically administered with 1 mg/kg body weight (b.w.) of AgNPs daily from day 1 to day 14 after cancer cells implantation (total dose 14 mg/kg b.w.). The second group was intravenously administered twice with 1 or 5 mg/kg b.w. of AgNPs. A tendency for lowering tumor volume on day 21 (mean volumes 491.31, 428.88, and 386.83 mm3 for control, AgNPs-PEG, and AgNPs-citrate, respectively) and day 26 (mean volumes 903.20, 764.27, and 672.62 mm3 for control, AgNPs-PEG, and AgNPs-citrate, respectively) has been observed in mice treated intragastrically, but the effect did not reach the level of statistical significance. Interestingly, in mice treated intragastrically with citrate-coated AgNPs, the number of lung metastases was significantly lower, as compared to control mice (the mean number of metastases 18.89, 14.90, and 8.03 for control, AgNPs-PEG, and AgNPs-citrate, respectively). No effect of AgNPs treatment on the number of lung metastases was observed after intravenous administration (the mean number of metastases 12.44, 9.86, 12.88, 11.05, and 10.5 for control, AgNPs-PEG 1 mg/kg, AgNPs-PEG 5 mg/kg, AgNPs-citrate 1 mg/kg, and AgNPs-citrate 5 mg/kg, respectively). Surprisingly, inhibition of metastasis was not accompanied by changes in the expression of genes associated with epithelial–mesenchymal transition. Instead, changes in the expression of inflammation-related genes were observed. The presented results support the antitumor activity of AgNPs in vivo, but the effect was limited to the inhibition of metastasis. Moreover, our results clearly point to the importance of AgNPs coating and route of administration for its anticancer activity. Finally, our study supports the previous findings that antitumor AgNPs activity may depend on the activation of the immune system and not on the direct action of AgNPs on cancer cells.
Prediction Model of Sound Signal in High-Speed Milling of Wood–Plastic Composites
Authors: Wei Weihua , Shang Yunyue , Peng You , Cong Rui
Published: May 2022

The accuracy of the acoustic signal prediction model for wood–plastic composites milling has an important influence on the condition monitoring of the cutting process and the improvement of the machining environment. To establish a high-precision prediction model of sound signal in the high-speed milling of wood–plastic composites, high-speed milling experiments on self-developed wood–plastic composites were carried out with cemented carbide tools. A mathematical model of the relationship of the four milling parameters, including axial cutting depth, radial cutting depth, feed rate and cutting speed, and the sound signal of wood–plastic composites milling, was established by using the full-factor test method. The experimental data obtained by the orthogonal test method were used as the test samples in the mathematical model. Test results show that the prediction accuracy of the mathematical model of the sound signal in the milling of wood–plastic composites exceeds 95.4%. To further improve the prediction accuracy of the sound signal in the milling of wood–plastic composites, a prediction model was established using back propagation (BP) neural network. Then, the particle swarm optimization (PSO) algorithm was used to optimize the BP neural network, obtaining the PSO–BP neural network prediction model. The test results show that the prediction accuracy of the PSO–BP prediction model for the sound signal in the high-speed milling of wood–plastic composites exceeds 97.5%. The PSO–BP model has a better global approximation ability and higher prediction accuracy than the BP model. The research results can provide a reference basis for sound signal prediction in the high-speed milling of wood–plastic composites.
Effect of Candida albicans Suspension on the Mechanical Properties of Denture Base Acrylic Resin
Authors: Chladek Grzegorz , Nowak Michał , Pakieła Wojciech , Mertas Anna
Published: May 2022

Yeast-like fungi such as Candida albicans (C. albicans) are the primary pathogenic microorganism in the oral cavity of denture wearers. The research available so far, conducted according to a protocol based on the exposure of specimens to a C. albicans suspension and their cutting with water cooling, shows that hard polymethyl methacrylate (PMMA) prosthetic materials are not only surface colonized, but also penetrated by microorganisms in a short time. This justifies the hypothesis that exposure to a suspension of the C. albicans strain causes the changes in mechanical properties due to surface colonization and/or penetration of the samples. In the current study, the chosen mechanical properties (flexural strength, flexural modulus, tensile strength, impact strength, ball indentation hardness, and surface Vickers hardness at 300 g load) of the PMMA denture base material Vertex RS (Vertex-Dental, The Netherlands) exposed for 30, 60, and 90 days to a suspension of C. albicans were investigated. The potential penetration of yeast was examined on the fractured surfaces (interior of specimens) to eliminate the risk of the contamination of samples during cutting. There was no influence on the flexural strength, flexural modulus, tensile strength, impact strength, or ball indentation hardness, but a significant decrease in surface hardness was registered. Microscopic observations did not confirm the penetration of C. albicans. On the surface, blastospores and pseudohyphae were observed in crystallized structures and in traces after grinding, which indicates that in clinical conditions, it is not penetration but the deterioration of surface quality, which may lead to the formation of microareas that are difficult to disinfect, causing rapid recolonization.
Bending Behaviour of Prestressed T-Shaped Concrete Beams Reinforced with FRP—Experimental and Analytical Investigations
Authors: Hammerl Mathias , Kromoser Benjamin
Published: May 2022

Materials such as high performance (HPC) or ultra-high performance concrete (UHPC), and fibre-reinforced polymer (FRP) reinforcement can be used to improve the resource efficiency in concrete construction by, for example, enabling the production of thin-walled structures. When building filigree concrete beams two essential factors must be considered: the low stiffness of the structure and the bond between the materials. By prestressing the structural stiffness is improved while an adequate concrete cover ensures sufficient bond strength. Based on this the bending behaviour of prestressed T-shaped beams reinforced with FRP, focussing on determining the influence of four parameters on the bearing capacity, bond behaviour and failure mode, is investigated in this paper. Comprehensive experimental investigations prove the potential of the approach and show that a reduction of the web thickness down to 40 mm, a lower concrete quality, and the use of glass FRP instead of carbon FRP allow a more resource-efficient structure while the applied prestressing leads to a higher utilisation of the high performance materials.
Ni–Cr Powders Modified with Rhenium as a Novel Coating Material—Physical Properties, Microstructure, and Behavior in Plasma Plume
Authors: Wrona Adriana , Lis Marcin , Pęcak Krzysztof , Kalemba-Rec Izabela , Dymek Stanisław , Wróbel Mirosław , Bilewska Katarzyna , Kustra Katarzyna , Węglowski Marek Stanisław , Śliwiński Piotr
Published: May 2022

The aim of this work was to develop a new coating material based on Ni20Cr alloy modified with up to 50%wt. rhenium. The modification was carried out by the mechanical mixing of the base powder and ammonium perrhenate with the subsequent thermoreduction in an H2 atmosphere. The obtained powder consists of a nickel–chromium core surrounded by a rhenium shell. The characterization of the powders—including their microstructure, phase and chemical composition, density, flowability, particle size distribution, and specific surface area—was performed. The influence of plasma current intensity and hydrogen gas flow on in-flight particle temperature and velocity were investigated. The results indicate that there is interdiffusion between the base Ni20Cr and the rhenium shell, resulting in intermediary solid solution(s). The modified powders have a higher specific surface area and a lower flowability, but this does not prevent them from being used as feedstock in plasma spraying. In-flight measurements reveal that increasing the content of rhenium allows for the higher temperature of particles, though it also reduces their speed.
CdS-Decorated Porous Anodic SnOx Photoanodes with Enhanced Performance under Visible Light
Authors: Gawlak Karolina , Popiołek Dominika , Pisarek Marcin , Sulka Grzegorz D. , Zaraska Leszek
Published: May 2022

Electrochemically generated nanoporous tin oxide films have already been studied as photoanodes in photoelectrochemical water splitting systems. However, up to now, the most significant drawback of such materials was their relatively wide band gap (ca. 3.0 eV), which limits their effective performance in the UV light range. Therefore, here, we present for the first time an effective strategy for sensitization of porous anodic SnOx films with another narrow band gap semiconductor. Nanoporous tin oxide layers were obtained by simple one-step anodic oxidation of metallic Sn in 1 M NaOH followed by further surface decoration with CdS by the successive ionic layer adsorption and reaction (SILAR) method. It was found that the nanoporous morphology of as-anodized SnOx is still preserved after CdS deposition. Such SnOx/CdS photoanodes exhibited enhanced photoelectrochemical activity in the visible range compared to unmodified SnOx. However, the thermal treatment at 200 °C before the SILAR process was found to be a key factor responsible for the optimal photoresponse of the material.
The Effect of Fit Clearance between Outer Race and Housing on Vibration Characteristics of a Cylindrical Roller Bearing with Localized Defects
Authors: Wang Fengtao , Ling Xin , Zhang Zhen , Dai Peng , Yan Shuping , Wang Lei
Published: May 2022

Due to bolt looseness or operating ambient temperature, fit clearance can often be found between the outer ring and housing. The vibration characteristics of a cylindrical roller bearing with localized defects are greatly affected by the fit clearance and the accuracy of bearing fault diagnosis may be reduced. Thus, a mathematical model for a cylindrical roller bearing was constructed and the interaction between the outer ring and housing was described. The classical localized defects were modeled, such as the inner ring defect, outer ring defect and roller defect. The relative experiments were conducted to check the constructed model. Then, it was found that the RMS (Root Mean Square) of housing acceleration decreased with increasing housing stiffness and viscous damping. When the fit clearance and friction coefficient increased, the RMS values increased. Except for housing stiffness and viscous damping, there were no uniform change rules of defect frequency amplitudes for other conditions. In the bearing with an outer ring defect or roller defect, the shock times of housing acceleration and the contact force between outer ring and housing were delayed, while fit clearance decreased. However, contrary variation trends were found for the inner ring defect. If the phase difference between defect location and rotor unbalanced force increased, the RMS and acceleration fluctuation amplitudes for the inner ring defect decreased. When the location angle of the outer ring defect increased, RMS and frequency amplitudes increased and RMSy/RMS decreased. The calculated results may provide the theoretical foundation for condition monitoring rotating machinery systems.
Numerical Simulation on Windage Power Loss of High-Speed Spur Gear with Baffles
Authors: Zhang Yuzhe , Hou Xiangying , Zhang Hong , Zhao Jiang
Published: May 2022

Windage power loss (WPL) is significant and cannot be neglected in a study on transmission efficiency and reducing the energy consumption of high-speed gear. The influence mechanism of the baffle on the reduction of WPL needs to be further studied. Based on computational fluid dynamics (CFD) technology, this paper puts stress on analyzing the influence of axial and radial baffles on viscous and pressure effects in WPL and the influence of baffles with groove structures on reducing WPL. The numerical calculation model of windage torque considering the baffle’s regulation is established, and the calculation results of WPL with different baffle configurations are obtained. The results indicate that the radial baffle mainly reduces pressure loss, while power loss caused by the viscous effect is mainly affected by the axial baffle. The baffle with the smallest clearance achieves the most significant suppression effect on windage. On this basis, adding groove structures to a smooth baffle can have a positive or negative impact on reducing WPL, and the baffles with circular grooves can further promote the reduction of WPL by 8.2%, compared with smooth baffles. This paper provides a reference for the optimal design of baffles in engineering applications.
Study on the Digital Hydraulic Driving System of the Belt Conveyor
Authors: Yang Meisheng
Published: May 2022

The electrohydraulic equipment of the coal gangue belt conveyor has been widely studied in recent years, but studies have been limited to the traditional hydraulic system with proportional valve and servo valve as control elements. Because of their own structural characteristics, proportional valves and servo valves have inherent defects such as low reliability, high cost and a long debugging cycle. It is necessary to carry out technological innovation and upgrading. This paper presents a hydraulic system scheme which uses digital valves instead of proportional valves and servo valves to control the belt conveyor propulsion system. Firstly, the system scheme is described in detail. Secondly, the simulation model of the control element digital valve is established, and its dynamic characteristics are analyzed in detail. Finally, the displacement tracking control of the new system is carried out to verify the feasibility of the proposed control scheme. The results show that the new digital hydraulic control system can effectively achieve the displacement control function of the belt conveyor propulsion system.
Effect of the Gap Matching Relation on the Pressure Pulsation Characteristics at Blade’s Surface of the Multiphase Pump
Authors: Shi Guangtai , Zhu Zheyu , Wang Binxin , Wen Haigang
Published: May 2022

The pressure pulsation characteristics of the blade’s surface have an impact on the lifespan of the multiphase pump impeller. To explore the influence of the gap matching relation on the pressure pulsation characteristics at blade’s surface of the pump, the axial clearance coefficient (ACC) between the impeller and diffuser and the relative tip clearance of the impeller were defined. By combining of numerical simulation and experiment, the pressure pulsation characteristics at blade’s surface of the single pressurization unit of the pump were studied under different gap matching relations. The results show that the size of tip leakage flow and the strength of rotor-stator interaction caused by different relative tip clearances have a decisive influence on the pressure pulsation characteristics in the impeller. With the increase of tip clearance, the internal flow field distribution law was greatly changed, which had a great impact on the pressure pulsation peak-to-peak value and dominant frequency amplitude of the suction surface. In addition, the pressure pulsation characteristics of the diffuser were mainly affected by the strength of rotor-stator interaction. When the strength of rotor-stator interaction weakened, the amplitude of the dominant frequency pulsation was decreased by degrees. As the ACC increased, the variation of the pressure pulsation peak-to-peak value and the dominant frequency amplitude coefficient were gradually slowed down in the diffuser, and the dominant frequency amplitude of the monitoring points were most sensitive to change in the ACC. The research results can provide a theoretical reference for the optimal design of the multiphase pump blades.
Design, Assembly, and Simulation of Flexure-Based Modular Micro-Positioning Stages
Authors: Liao Shufan , Ding Bingxiao , Li Yangmin
Published: May 2022

With flexure-based micro-positioning stages (MPSs) being in high demand for high-precision applications, the performance and cost of flexure-based MPSs are two issues that urgently need to be addressed. In addition, the current MPSs are being developed toward complex spatial configurations, which further precludes monolithic fabrication. To address the aforementioned issues, modular MPSs using designed standardized modules are introduced in this paper. Firstly, the motivations are described, followed by the modular design. In addition, a new assembly concept analogy with composing compounds is proposed for guiding module assembly, including some proposed planar and spatial configurations. For validation, the static and dynamic performances of modular MPSs with respect to different modules and materials are presented as case studies. The proposed modular MPSs can provide better flexibility and functionality for further applications.
Adaptive Swarm Fuzzy Logic Controller of Multi-Joint Lower Limb Assistive Robot
Authors: Amiri Mohammad Soleimani , Ramli Rizauddin , Aliman Norazam
Published: May 2022

The idea of developing a multi-joint rehabilitation robot is to satisfy the demands for recovery of lower limb functionality in hemiplegic impairments and assist the physiotherapists with their therapy plans. This work aims at to implement the Lyapunov Adaptive and Swarm-Fuzzy Logic Control (LASFC) strategy of 4-degree of freedom (4-DoF) Lower Limb Assistive Robot (LLAR) application, in which the control law is an integration of swarm-fuzzy logic control (SFLC) and Lyapunov adaptive control (LAC) with particle swarm optimization (PSO). The controller is established based on the sliding filtered steady-state error for SFLC. Its parameters are tuned by using PSO for the mathematical model of LLAR. The fuzzy defuzzification membership is set based on the tuned parameters for the real-time control system. LAC strategy is determined using stability analysis of the system to choose the controller’s parameters by observation of the system’s output and reference. The control law implemented in LLAR is the integration of SFLC and LAC to adjust the input voltage of joints. The parameters tuned by PSO are compared with the genetic algorithm (GA) statistically. In addition, the real-time trajectory tracking of the proposed controller for each joint is compared with LAC and SFLC separately. The experiment revealed that the LASFC has superior performance to the other two methods in trajectory tracking. For example, the average error for left hip by LASFC is 53.57% and 68% lower than SFLC and LAC, respectively. By the statistical analysis, it can be ascertained that the LASFC strategy performed efficiently for real-time control of the joint trajectory tracking.
Temperature-Sensitive Point Selection and Thermal Error Model Adaptive Update Method of CNC Machine Tools
Authors: Liu Hui , Miao Enming , Wang Jingfan , Zhang Liyin , Zhao Siyu
Published: May 2022

The thermal error of CNC machine tools can be reduced by compensation, where a thermal error model is required to provide compensation values. The thermal error model adaptive update method can correct the thermal error model by supplementing new data, which fundamentally solves the problem of model robustness. Certain problems associated with this method in temperature-sensitive point (TSP) selection and model update algorithms are investigated in this study. It was found that when the TSPs were selected frequently, the selection results may be different, that is, there was a variability problem in TSPs. Further, it was found that the variability of TSPs is mainly due to some problems with the TSP selection method, (1) the conflict between the collinearity among TSPs and the correlation of TSPs with thermal error is ignored, (2) the stability of the correlation is not considered. Then, a stable TSP selection method that can choose more stable TSPs with less variability was proposed. For the model update algorithm, this study proposed a novel regression algorithm which could effectively combine the new data with the old model. It has advantages for a model update, (1) fewer data are needed for the model update, (2) the model accuracy is greatly improved. The effectiveness of the proposed method was verified by 20 batches of thermal error measurement experiments in the real cutting state of the machine tool.
The Investigation of Coupled Vibration of Automobile Transmission System and Its Intelligent Design
Authors: Liu Xiaogang , Xiang Dongshan , Zeng Chunhui , Huang Fengyun
Published: May 2022

Intelligent manufacturing is developing rapidly nowadays, promoting the efficiency of manufacturing. In comparison, the design process has become a bottleneck in the product life cycle. In order to address this problem, this research develops an intelligent design method based on the automobile transmission system. Firstly, a mathematical model of the coupled vibration between the drive shaft and the main reducer was developed, and the vibration responses of the transmission system were simulated based on this mathematical model. Then, a test rig was developed to measure the vibration responses of the system; the measured results correlated well with the simulation results, indicating that the mathematical model can be used to investigate the coupled vibration between the drive shaft and the main reducer. Furthermore, the multiple parameters of the transmission system were optimized based on the mathematical model using the intelligent optimization algorithm. In particular, software was developed based on the intelligent optimization algorithm for the convenience of analysis, and the optimized results were acquired. The analysis results show that the vibration responses can be reduced when the optimized parameters are applied, indicating that the intelligent design method developed in this research is effective for the intelligent design of transmission system.