bluuebunny/crossref_metadata_2025 huggingface dataset:
Strength and Microscopic Mechanism of Cement–Fly Ash–Slag–Desulfurization Gypsum Solidified Mica Schist Weathered Soil
Authors: Shang Yunzhi , Cui Zhenglong , Li Yongjing , Zhang Yannian , Cheng Yaohui
Published: October 2023

Mica schist weathered soil possesses a number of poor engineering characteristics, which make it difficult to use as a subgrade material for resource utilization. Therefore, in this study, a new type of curing agent, CFSD (cement–fly ash–slag–desulfurized gypsum), is proposed for this soil. The effects of different curing agent dosages, age of preservation, and confining pressure on the stress–strain curves were analyzed via the uniaxial compression test and triaxial compression test, while the micromorphological characteristics of cured soil were analyzed via X-ray diffraction analysis and the SEM test combined with Image J software. In this paper, we also establish a microscopic mechanism model to determine how curing agents increase the strength of mica schists. The results reveal that the compressive strength of solidified soil increases rapidly within 28 days; the CFSD dosage of 4% at 7 d increased by 103.23% by 28 d. After 28 d, the trend of compressive strength growth was flat. The CFSD dosage of 4% at 7 d increased by 128.34% by 90 d; with the increase in the dosage, the curve transformed from flat to steep. These results suggest that the CFSD dosage is positively correlated with the damage strain and damage bias stress of solidified soil. The curves for the strain softening type with a 4% dosage as the initial effective confining pressure increased from 50 kPa to 300 kPa; the failure stress and failure strain increased by 202.09% and 90.85%, respectively. With the increase in curing agent dosage and maintenance age, the pore size of 2~5 μm, >5 μm interval decreased from 56.46% to 27.92%, the porosity decreased from 12.51% to 4.6%, and the hydrate produced by the curing agent cemented and filled up the pore space between the loose particles of the soil body. Thus, the large pore space became microporous, and the pore structure densification was greatly improved.
Microstructure and Mechanical Properties of Stainless Steel/6082 Aluminum Alloy Heterogeneous Laser Welded Joint
Authors: Kang Lei , Li Xin , Chen Jing , Zhang Yu , Wang Ting
Published: October 2023

The microstructures and mechanical properties of laser penetration welded joints of overlap steel-on-aluminum were investigated. The structure of the intermetallic compound layer without interlayer consists of FeAl and FeAl3 phases. After the Ni-foil was added, the thickness of the intermetallic compound layer and the content of the brittle and hard Al-Fe phase decreased significantly, and some new phases of Al0.9Ni1.1 and FeNi were formed. It was found that the Ni interlayer enhanced the tensile property of the joint by about 40% and decreased the microhardness of the intermetallic compounds, which is attributed to the improvement of the toughness of the welded joint made by the Ni interlayer. It is an effective way to improve the mechanical properties of the laser welding joint by adding a nickel interlayer to improve the metallurgical reaction.
Anisotropy in the Liquefaction Resistance of Fibre Reinforced Sand
Authors: Zhang Xidong , Zhuang Yan , Wang Zhen’ang , Yang Changxing , Hu Shunlei
Published: October 2023

Adding discrete fibres to sand has been seen as a feasible technique to improve sand’s strength as well as liquefaction resistance. Considering the anisotropic distribution of fibre orientations, the anisotropy in the liquefaction resistance of the reinforced sand is also introduced using fibres. Here, the triaxial compression and extension test results of unreinforced and fibre-reinforced sand in different density states are provided, from which the anisotropy in the liquefaction resistance of fibre-reinforced sand is demonstrated. Fibre reinforcement improves the liquefaction resistance of sand by introducing both the densifying effect and the confining effect. The inclusion of fibres increases both the slope and the intercept of the strength envelope in comparison with the unreinforced sand under triaxial compression, while the strength envelope is not affected by fibres under triaxial extension. Stress contribution of fibres makes the ESP of the composite under undrained loading reverse its direction to develop even though the phase transformation is absent. The stress ratio initiating the ESP reversal is irrespective of the fibre content but dependent on the density state under triaxial compression. Under triaxial extension, the stress ratio initiating the ESP reversal remains the same in the samples with varied density states and fibre contents. The mechanism correlating to the strength envelope and ESP reversal of the fibre-reinforced sand was demonstrated following a rule of mixture based constitutive modelling framework. By introducing an alternatively defined pore pressure ratio that incorporates the stress contribution of fibres, the liquefaction state of the fibre reinforced sand is reasonably assessed. Liquefaction remains absent in the sand once the fibres are mixed. The anisotropy in the liquefaction resistance of fibre-reinforced sand arises, as the predominant role played by the fibres to suppress the liquefaction is different when varied loading paths are involved, which is sourced from the anisotropic distribution of fibre orientations.
A Simplified Method for the Preparation of Highly Conductive and Flexible Silk Nanofibrils/MXene Membrane
Authors: Ding Bohan , Teng Chao , Wang Yanxiang , Wang Yongbo , Jiang Haotian , Sun Yue , Guo Jinghe , Dai Shichao
Published: October 2023

Silk nanofibers (SNF) have great applications in high-performance functional nanocomposites due to their excellent mechanical properties, biocompatibility, and degradability. However, the preparation of SNF by traditional methods often requires the use of some environmentally harmful or toxic reagents, limiting its application in green chemistry. In this paper, we successfully prepared SNF using natural silk as raw material and solvent stripping technology by adjusting the solvent concentration and solution ratio (the diameter of about 120 nm). Using the above SNFs as raw materials, SNF membranes were prepared by vacuum filtration technology. In addition, we prepared an SNF/MXene nanocomposite material with excellent humidity sensitivity by simply coating MXene nanosheets with silk fibers. The conductivity of the material can approach 1400.6 S m−1 with excellent mechanical strength (51.34 MPa). The SNF/MXene nanocomposite material with high mechanical properties, high conductivity, and green degradability can be potentially applied in the field of electromagnetic interference (EMI) shielding, providing a feasible approach for the development of functional nanocomposite materials.
In Vitro Comparison of Internal and Marginal Adaptation between Printed and Milled Onlays
Authors: Cantó-Navés Oriol , Michels Kyra , Figueras-Alvarez Oscar , Fernández-Villar Sandra , Cabratosa-Termes Josep , Roig Miguel
Published: October 2023

Statement of problem: Nowadays, milling is still the gold standard for fabricating indirect restorations, but to overcome its disadvantages, there are alternatives, such as 3D printing. Purpose: This study aimed to compare the gaps between the prepared tooth and milled and printed onlays fabricated with the same CAD design. It also aimed to determine the gap reproducibility across onlays fabricated by 3D printing and milling. Methods: A resin tooth was prepared for an onlay. After scanning the preparation, an onlay was designed with proprietary dental software. Next, 22 onlays were milled in a graphene-reinforced PMMA disc (Group 1), and 22 onlays were 3D-printed with a hybrid composite material (Group 2). After that, all fabricated restorations were scanned and superimposed on the scanned prepared resin tooth. Subsequently, a specific software was used to measure the margin, central, and intaglio-located gap between the milled or printed restoration and the preparation. Finally, measurements were compared with a multifactor analysis of variance. Results: The results demonstrated that printed onlays (Group 2) adapted better to the prepared tooth than the milled ones (Group 1) (p < 0.05). The comparison of standard deviations showed the better gap reproducibility of printed onlays (p < 0.05). Conclusion: This study concluded that the printed onlays adapted significantly better to the prepared tooth than the milled onlays. Printed onlays also showed significantly better gap reproducibility.
Effect of Welding Process Parameters on the Strength of Dissimilar Joints of S355 and Strenx 700 Steels Used in the Manufacture of Agricultural Machinery
Authors: Szusta Jarosław , Derpeński Łukasz , Karakaş Özler , Tüzün Nail , Dobrzański Sławomir
Published: October 2023

The paper evaluates the possibility of using dissimilar materials joined by welding technology in the construction of agricultural machinery. The desire to design larger and more efficient structures requires designers to combine materials with different mechanical and structural properties. In such a case, it is very important to properly select welding parameters so that, on the one hand, the quality of the joint meets the standard requirements, and on the other, the welding process is not too energy-intensive. In this paper, overlay joints connecting S355 steel with Strenx 700 steel were analyzed in terms of strength for three different values of welding parameters and different thicknesses. The starting point was the reference parameters recommended by the company’s welding technologists, which were reduced by 10 and 20% according to the linear welding energy. The study compared the strength, ductility and macrostructure of the joints, as well as the energy intensity of the process. The proposed dissimilar joints achieved approximately a 10% increase in the strength limit of the components in comparison to the previously recommended welding parameters. Additionally, finite element analysis calculations of the improved designs showed significant weight reduction (up to 40%) for the relevant agricultural machinery components.
Advancements in the Evolution of Engineering Characteristics and Reinforcement Technologies for Subgrade Silt
Authors: Liu Xiaoyan , Zhao Jinpeng , Liu Lulu
Published: October 2023

Technical challenges associated with the treatment of silt subgrades frequently arise in coastal and river delta areas. Given the importance of environmental sustainability, the selection of efficient, cost-effective, and eco-friendly techniques for silt subgrade stabilization is paramount. While recycled polyester fibers primarily sourced from discarded polyester bottles have not yet been systematically employed in silt subgrade reinforcement, their potential is considerable. This paper offers a comprehensive review of the existing literature on the microstructural, physicochemical, and mechanical properties of silt, summarizing prior advancements in silt stabilization methodologies. Building upon this foundation, we introduce a novel approach utilizing recycled polyester fibers for silt subgrade improvement, outlining both its application prospects and challenges, which require further investigation. The findings of this study serve as a robust scientific foundation for the broader adoption and engineering implementation of this technology.
Enhancing Mechanical Properties: Exploring the Effect of Annealing Temperature on Wire Arc Additively Manufactured High-Strength Steel
Authors: Chen Yi , Hao Zhizhuang , Li Yang , Liu Chao , Liu Yongkang , Luo Zhen , Ao Sansan
Published: October 2023

This study investigates the mechanical properties of exceptionally high-strength steel produced by wire and arc additive manufacturing (WAAM), using the 304 stainless steel wire and the low carbon wire (LCS). The study found that annealing treatment can enhance the steel’s mechanical properties. The microstructure in the LCS layer changed from ferrite to bainite and then to a mixture of austenite, pearlite, and bainite with increasing annealing temperature. In contrast, the SS layer retained its martensitic structure, albeit with altered lath sizes. The annealing treatment also improved the orientation of the grains in the steel. The optimal annealing temperature observed for the steel was 900 ℃, which resulted in a maximum tensile strength of 1176 MPa along the Y direction and 1255 MPa along the Z direction. Despite the superior mechanical properties, the LCS layer still exhibited failure during tensile testing due to its lower hardness. The study suggests that annealing treatment can be a useful technique for enhancing the mechanical properties of high-strength steel in WAAM applications.
Strengthening of Reinforced Concrete Non-Circular Columns with FRP
Authors: Yardim Yavuz , Yilmaz Salih , Corradi Marco , Thanoon Waleed A.
Published: October 2023

Fiber reinforced polymer (FRP) strengthening in circular columns is known to be more effective than in rectangular and square columns because of the uniform distribution of confining pressure. This study explores the effectiveness of using carbon-FRP anchors to improve the confinement of square reinforced concrete (RC) columns strengthened with FRP. Sharp corners in non-circular columns cause stress concentration on the corners, reducing the effectiveness of strengthening. To address this, the study examines the impact of three different anchor configurations on two sizes of FRP-strengthened square columns. The results show that the proposed anchors distribute stresses to a greater extent, resulting in a more uniform distribution of stresses and better confinement. For the best performance, it is proposed that the anchor fans surround the corners of the cross section. Experimental findings and finite element analysis results using the Concrete Damage Plasticity model in the ABAQUS material library match.
Successful Ultrasound-Guided Superficial Cervical Plexus Block Treatment for Head and Neck Pain with an Unusually Delayed Onset Following Ventriculoperitoneal Shunt: A Case Report
Authors: Hu Ching-Yuan , Huang Ying-Zhen , Tsai Sheng-Tzung , Wang Po-Kai
Published: October 2023

Background and Objectives: Ventriculoperitoneal (VP) shunt placement is the most common treatment for cerebrospinal fluid diversion. Head and neck pain occurring after a long period following VP shunt insertion is rarely reported. Here, we present a rare case of head and neck pain occurring 2 years after surgery due to irritation of the superficial cervical plexus by the VP shunt. Case Description: A 46-year-old female patient received VP shunt placement surgery. Two years after the surgery, she experienced a left temporal headache with neck pain on the left side, which extended to the left para-auricular and fascial region. Ultrasound (US) scanning revealed that the VP shunt passed within the superficial cervical fascia and through the left sternocleidomastoid muscle (SCM). Additionally, friction of the branches of the superficial cervical plexus and of the greater auricular and lesser occipital nerves caused by the VP shunt was found underneath the lateral border of the SCM. Subsequently, the blocking and hydro-release of the left superficial cervical plexus were performed. After four series of treatments, the patient’s head and neck pain vanished, and the frequency of the headaches was substantially reduced. The patient was regularly followed-up in the outpatient department of neurosurgery. Conclusions: Head and neck pain caused by the malpositioning of a VP shunt catheter with an unusually delayed onset is a rarely reported complication and could be easily neglected. Patients with head and neck pain following VP shunt insertion should be checked using US scanning to identify the potential origin of the pain and receive adequate treatments. Intraoperative US-guided tunnelling is suggested to avoid the malpositioning of the VP shunt catheter.
Importance of Determining Vascular Endothelial Growth Factor Serum Levels in Children with Infantile Hemangioma
Authors: Rešić Arnes , Benco Kordić Nikolina , Obuljen Jasna , Bašković Marko
Published: October 2023

Background and Objectives: A potential role of vascular endothelial growth factor (VEGF) in the pathophysiology of infantile hemangiomas (IH) is thought to be plausible. The primary objective of this study was to investigate the importance of determining VEGF serum levels at various stages of IH growth in children. Materials and Methods: A nested case–control study was conducted. For the purposes of the researched target group, samples of fifty (N = 50) children with IH without associated diseases at different stages of hemangioma growth (proliferative and involutional stages) were used. The control group consisted of one hundred (N = 100) healthy children comparable in terms of age and sex, in whom the existence of IH and vascular malformations was ruled out via clinical examination. An immunoassay (ELISA) was used to determine VEGF serum levels in hemangioma growth’s proliferation and involution phases. Results: A comparison of serum levels of VEGF in the phases of proliferation and involution in the group of patients with IH did not show a statistically significant difference (p = 0.171). The control group had significantly higher serum VEGF levels than the patient group in both the proliferation phase (p = 0.009) and the involution phase (p = 0.019). In the proliferation phase, a multivariate regression model explained 15% of the variance in the dependent variable, without significant predictor variables, while in the involution phase, it explained 21% of the variance in the dependent variable, and the history of invasive prenatal procedures stood out as a significant predictor variable positively associated with serum VEGF levels (beta coefficient = 0.33; p = 0.043). Conclusions: Although IH is thought to be the result of the dysregulation of angiogenesis and vasculogenesis under the influence of angiogenic factors, especially VEGF, this study did not demonstrate that VEGF serum levels in the proliferation phase of hemangioma growth were higher than those in the involution phase, or in relation to the control group.
General Clinico-Pathological Characteristics in Glioblastomas in Correlation with p53 and Ki67
Authors: Sipos Tamás-Csaba , Kövecsi Attila , Ovidiu-Ioan Șușu , Zsuzsánna Pap
Published: October 2023

Introduction: A glioblastoma is an intra-axial brain tumour of glial origin that belongs to the category of diffuse gliomas and is the most common malignant neoplasia of the central nervous system. The rate of survival at 5 years, from the moment of diagnosis, is not higher than 10%. Materials and methods: In this retrospective study, fifty-four patients diagnosed with glioblastoma, from the Pathology Department of the County Emergency Clinical Hospital of Târgu Mureș, between 2014 and 2017 were included. We studied the clinico-pathological data (age, gender, location, and laterality) and, respectively, the immunoexpression of p53, Ki67, ATRX, and IDH-1 proteins. Results: We observed a statistically significant association between the laterality of the tumour according to the age groups, with the localization on the right side being more frequent in the age group below 65 years of age, while the involvement of the left hemisphere was more prevalent in those over 65 years. Out of the total 54 cases, 87.04% were found to be primary glioblastomas; more than 70% of the cases were ATRX immunopositive; almost 80% of the glioblastomas studied had wild-type p53 profile; and 35% of the cases were found to have a Ki67 index greater than 20%. A statistically significant association between gender and ATRX mutation was found; female cases were ATRX immunopositive in 92% of the cases. Almost 70% of the cases were both IDH-1 and p53 wild-type, and we observed the presence of both mutations in only 3.7% of the cases. Approximately 83% of primary glioblastomas were ATRX positive, respectively, and all IDH-1 mutant cases were ATRX negative. Conclusions: Glioblastomas still represent a multidisciplinary challenge considering their reserved prognosis. In this study, we described the most common clinico-pathological characteristics and IHC marker expression profiles, highlighting a variety of percentage ranges in primary and secondary glioblastomas. Given the small number of studied cases, further prospective studies on larger cohorts are needed in the future to evaluate the role of these immunohistochemical markers as prognostic factors for survival or recurrence.
Single-Event Multi-Level Surgery in Cerebral Palsy: A Bibliometric Analysis
Authors: Ma Norine , Gould Daniel , Camathias Carlo , Graham Kerr , Rutz Erich
Published: October 2023

Background and Objectives: Single-Event Multi-Level Surgery (SEMLS) is a complex surgical programme in which soft tissue contractures and bony torsional deformities at the ankle, knee and hip, in both lower limbs are surgically corrected during a single operative session, requiring one hospital admission and one period of rehabilitation. The aim of SEMLS is to improve gait and function in ambulant children with cerebral palsy. Utilisation of the SEMLS concept can reduce the number of surgical events, hospital inpatient stays and reduce rehabilitation requirements to a single intensive episode. Three-dimensional gait analysis is a pre-requisite to plan intervention at multiple anatomic levels to correct fixed deformities and to improve gait and function. Materials and Methods: This study was a bibliometric analysis of SEMLS in cerebral palsy using the Clarivate Web of Science Core Collection database from 1900 to 29 May 2023. Results: A total of 84 studies met the inclusion criteria. The most highly cited article was “Correction of severe crouch gait in patients with spastic diplegia with use of multilevel orthopaedic surgery” by Rodda et al. (2006) with 141 citations. The most productive institutions by number of articles were the Royal Children’s Hospital Melbourne (Australia), Murdoch Children’s Research Institute (Australia) and University of Melbourne (Australia). The most productive author by number of citations was HK Graham (Australia). Conclusions: The literature base for SEMLS consists largely of retrospective cohort studies. The aforementioned three institutes in Melbourne, Australia, which frequently collaborate together, have contributed the greatest number of studies in this field.
Obtaining Excellent Mechanical Properties in an Ultrahigh-Strength Stainless Bearing Steel via Solution Treatment
Authors: Zheng Kai , Zhong Zhenqian , Wang Hui , Xu Haifeng , Yu Feng , Wang Cunyu , Wu Guilin , Liang Jianxiong , Godfrey Andy , Cao Wenquan
Published: October 2023

A novel versatile ultrahigh-strength stainless bearing steel was prepared by first solution treating the steel at temperatures between 1000 °C and 1100 °C for 1 h, followed by performing cryogenic treatment at −73 °C for 2 h, and tempering at 500 °C for 2 h, with the cryogenic and tempering treatments being repeated twice. The microstructures were characterized using multiscale techniques, and the mechanical properties were investigated using tensile testing, as well as via Rockwell hardness and impact toughness measurements. Tensile strength was found to be independent of solution temperature, with a value of about 1800 MPa. In contrast, yield strength decreased from 1530 MPa to 1033 MPa with increasing solution temperature, while tensile elongation increased from 15.3% to 20.5%. This resulted in an excellent combined product of tensile strength and elongation for steels initially treated at 1080 °C and 1100 °C, with values of 33.9 GPa·% and 37.0 GPa·%, respectively. Furthermore, the steels showed excellent impact toughness, increasing from 37.0 J to 86.2 J with increasing solution temperature. The microstructural and mechanical investigations reveal that the excellent mechanical properties and impact toughness are related to three factors, namely (i) a transformation-induced plasticity effect, mainly attributed to a high volume fraction of retained austenite, (ii) a high strengthening capacity arising from a high dislocation density, and (iii) a synergistic effect due to cobalt additions and the nanoprecipitation of M2C and M6C carbides.
Electrophoretic Deposition of Chitosan–Hydroxyapatite Films and Their Electrochemical Behavior in Artificial Plasma
Authors: Mata-Davila J. P. , Arrieta-Gonzalez C. D. , Perez-Arizmendi F. J. , Dorta-Leon M. A. , Brown-Bojorquez F. , Porcayo-Calderon J.
Published: October 2023

The electrochemical behavior of chitosan–hydroxyapatite films deposited on Ti CP was evaluated. Hydroxyapatite was synthesized from eggshell at different precipitation pH conditions. The films were deposited on the Ti CP surface from chitosan–hydroxyapatite solutions by means of electrophoretic deposition. The hydroxyapatite content of the solutions varied from 0 to 20 g/L. The different films obtained were evaluated by means of electrochemical measurements such as polarization curves, open circuit potential measurements, polarization resistance, and electrochemical impedance. The results obtained showed that regardless of the precipitation pH, it is possible to obtain pure hydroxyapatite from a waste such as eggshell. The incorporation of hydroxyapatite within the chitosan structure allows for improvement of the electrochemical performance of the bare Ti CP surface. It was observed that the passive zone was achieved at lower current densities, and that the stability zone of the passive layer increased. Electrochemical impedance analyzes showed that there is an improvement in corrosion resistance due to a more controlled growth of the passive layer that allows for the formation of a dense and compact film.
Study on the Common Molecular Mechanism of Metabolic Acidosis and Myocardial Damage Complicated by Neonatal Pneumonia
Authors: Zhan Yifei , Wang Huaiyan , Wu Zeying , Zeng Zhongda
Published: October 2023

Pneumonia is a common clinical disease in the neonatal period and poses a serious risk to infant health. Therefore, the understanding of molecular mechanisms is of great importance for the development of methods for the rapid and accurate identification, classification and staging, and even disease diagnosis and therapy of pneumonia. In this study, a nontargeted metabonomic method was developed and applied for the analysis of serum samples collected from 20 cases in the pneumonia control group (PN) and 20 and 10 cases of pneumonia patients with metabolic acidosis (MA) and myocardial damage (MD), respectively, with the help of ultrahigh-performance liquid chromatography–high-resolution mass spectrometry (UPLC–HRMS). The results showed that compared with the pneumonia group, 23 and 21 differential metabolites were identified in pneumonia with two complications. They showed high sensitivity and specificity, with the area under the curve (ROC) of the receiver operating characteristic curve (ROC) larger than 0.7 for each differential molecule. There were 14 metabolites and three metabolic pathways of sphingolipid metabolism, porphyrin and chlorophyll metabolism, and glycerophospholipid metabolism existing in both groups of PN and MA, and PN and MD, all involving significant changes in pathways closely related to amino acid metabolism disorders, abnormal cell apoptosis, and inflammatory responses. These findings of molecular mechanisms should help a lot to fully understand and even treat the complications of pneumonia in infants.
A 14-Bit, 12 V-to-100 V Voltage Compliance Electrical Stimulator with Redundant Digital Calibration
Authors: Su Kangyu , Qiu Zhang , Xu Jian
Published: October 2023

Electrical stimulation is an important technique for modulating the functions of the nervous system through electrical stimulus. To implement a more competitive prototype that can tackle the domain-specific difficulties of existing electrical stimulators, three key techniques are proposed in this work. Firstly, a load-adaptive power saving technique called over-voltage detection is implemented to automatically adjust the supply voltage. Secondly, redundant digital calibration (RDC) is proposed to improve current accuracy and ensure safety during long-term electrical stimulation without costing too much circuit area and power. Thirdly, a flexible waveform generator is designed to provide arbitrary stimulus waveforms for particular applications. Measurement results show the stimulator can adjust the supply voltage from 12 V to 100 V automatically, and the measured effective resolution of the stimulation current reaches 14 bits in a full range of 6.5 mA. Without applying charge balancing techniques, the average mismatch between the cathodic and anodic current pulses in biphasic stimulus is 0.0427%. The proposed electrical stimulator can generate arbitrary stimulus waveforms, including sine, triangle, rectangle, etc., and it is supposed to be competitive for implantable and wearable devices.
Bond Wire Fatigue of Au, Cu, and PCC in Power LED Packages
Authors: Czerny Bernhard , Schuh Sebastian
Published: October 2023

Bond wire failure, primarily wire neck breakage, in power LED devices due to thermomechanical fatigue is one of the main reliability issues in power LED devices. Currently, the standard testing methods to evaluate the device’s lifetime involve time-consuming thermal cycling or thermal shock tests. While numerical or simulation methods are used as convenient and quick alternatives, obtaining data from material lifetime models with accurate reliability and without experimental fatigue has proven challenging. To address this issue, a mechanical fatigue testing system was developed with the purpose of inducing mechanical stresses in the critical region of the bond wire connection above the ball bond. The aim was to accelerate fatigue cracks at this bottleneck, inducing a similar failure mode as observed during thermal tests. Experimental investigations were conducted on Au, Cu, and Pd-coated Cu bonding wires, each with a diameter of 25 µm, using both low- and high-frequency excitation. The lifetime of the wire bond obtained from these tests ranged from 100 to 1,000,000 cycles. This proposed testing method offers material lifetime data in a significantly shorter timeframe and requires minimal sample preparation. Additionally, finite element simulations were performed to quantify the stresses at the wire neck, facilitating comparisons to conventional testing methods, fatigue test results under various operating conditions, material models, and design evaluations of the fine wire bond reliability in LED and microelectronic packages.
Towards High-Temperature MEMS: Two-Step Annealing Suppressed Recrystallization in Thin Multilayer Pt-Rh/Zr Films
Authors: Pleshakov Georgii A. , Kalinin Ivan A. , Ivanov Alexey V. , Roslyakov Ilya V. , Yaminsky Igor V. , Napolskii Kirill S.
Published: October 2023

Platinum-based thin films are widely used to create microelectronic devices operating at temperatures above 500 °C. One of the most effective ways to increase the high-temperature stability of platinum-based films involves incorporating refractory metal oxides (e.g., ZrO2, HfO2). In such structures, refractory oxide is located along the metal grain boundaries and hinders the mobility of Pt atoms. However, the effect of annealing conditions on the morphology and functional properties of such multiphase systems is rarely studied. Here, we show that the two-step annealing of 250-nm-thick Pt-Rh/Zr multilayer films instead of the widely used isothermal annealing leads to a more uniform film morphology without voids and hillocks. The composition and morphology of as-deposited and annealed films were investigated using X-ray diffraction and scanning electron microscopy, combined with energy-dispersive X-ray spectroscopy. At the first annealing step at 450 °C, zirconium oxidation was observed. The second high-temperature annealing at 800–1000 °C resulted in the recrystallization of the Pt-Rh alloy. In comparison to the one-step annealing of Pt-Rh and Pt-Rh/Zr films, after two-step annealing, the metal phase in the Pt-Rh/Zr films has a smaller grain size and a less pronounced texture in the <111> direction, manifesting enhanced high-temperature stability. After two-step annealing at 450/900 °C, the Pt-Rh/Zr thin film possessed a grain size of 60 ± 27 nm and a resistivity of 17 × 10−6 Ω·m. The proposed annealing protocol can be used to create thin-film MEMS devices for operation at elevated temperatures, e.g., microheater-based gas sensors.
Design of Trench MIS Field Plate Structure for Edge Termination of GaN Vertical PN Diode
Authors: Lee Sung-Hoon , Cha Ho-Young
Published: October 2023

In this study, we developed an analytic model to design a trench metal–insulator–semiconductor (MIS) field plate (FP) structure for the edge termination of a vertical GaN PN diode. The key parameters considered in the trench MIS FP structure include trench depth, MIS dielectric material and thickness, and interface charge density of MIS. The boundary conditions are defined based on the maximum allowed electric field strengths at the dielectric and semiconductor regions. The developed model was validated using TCAD simulations. As an example, a 1 kV GaN vertical PN diode was designed using the optimized FP structure, which exhibited the same breakdown voltage characteristics as an ideal one-dimensional PN diode structure without edge effects. This proposed simple analytic model offers a design guideline for the trench MIS FP for the edge termination of vertical PN diodes, enabling efficient design without the need for extensive TCAD simulations, thus saving significant time and effort.
Graphene-Enabled Tunable Phase Gradient Metasurface for Broadband Dispersion Manipulation of Terahertz Wave
Authors: Zhang Yin , Feng Yijun , Zhao Junming
Published: October 2023

With the increasing demand for the miniaturization and flexibility of optical devices, graphene-based metasurfaces have emerged as a promising ideal design platform for realizing planar and tunable electromagnetic or optical devices. In this paper, we propose a tunable metasurface with low-dispersion phase gradient characteristics that is composed of an array of double-layer graphene ribbons sandwiched with a thin insulating layer and a polymer substrate layer with a gold ground plane. As two typical proof-of-concept examples, metasurfaces act as a planar prism and a planar lens, respectively, and the corresponding performances of tunable broadband dispersion are demonstrated through full-wave simulation experiments. By changing the Fermi level of each graphene ribbon individually to introduce abrupt phase shifts along the metasurface, the broadband continuous dispersion effect of abnormal reflection and beam focusing is achieved within a terahertz (THz) frequency region from 3.0 THz to 4.0 THz, and the dispersion results can be freely regulated by reconfiguring the sequence of Fermi levels via the bias voltage. The presented graphene metasurface provides an avenue for the dispersion manipulation of a broadband terahertz wave and may have great prospects in the fields of optics, imaging, and wireless communication.
Study of a High-Precision Read-Out Integrated Circuit for Bridge Sensors
Authors: Li Xiangyu , Wang Pengjun , Ye Hao , He Haonan , Zhang Xiaowei
Published: October 2023

Bridge sensors are widely used in military and civilian fields, and their demand gradually increases each year. Digital sensors are widely used in the military and civilian fields. High-precision and low-power analog-to-digital converters (ADCs) as sensor read-out circuits are a research hotspot. Sigma-delta ADC circuits based on switched-capacitor topology have the advantages of high signal-to-noise ratio (SNR), good linearity, and better compatibility with CMOS processes. In this work, a fourth-order feed-forward sigma-delta modulator and a digital decimation filter are designed and implemented with a correlated double sampling technique (CDS) to suppress pre-integrator low-frequency noise. This work used an active pre-compensator circuit for deep phase compensation to improve the system’s stability in the sigma-delta modulator. The modulator’s local feedback factor is designed to be adjustable off-chip to eliminate the effect of process errors. A three-stage cascade structure was chosen for the post-stage digital filter, significantly reducing the number of operations and the required memory cells in the digital circuit. Finally, the layout design and engineering circuit were fabricated by a standard 0.35 μm CMOS process from Shanghai Hua Hong with a chip area of 9 mm2. At a 5 V voltage supply and sampling frequency of 6.144 MHz, the modulator power consumption is 13 mW, the maximum input signal amplitude is −3 dBFs, the 1 Hz dynamic range is about 118 dB, the modulator signal-to-noise ratio can reach 110.5 dB when the signal bandwidth is 24 kHz, the practical bit is about 18.05 bits, and the harmonic distortion is about −113 dB, which meets the design requirements. The output bit stream is 24 bits.
Simulating Synaptic Behaviors through Frequency Modulation in a Capacitor–Memristor Circuit
Authors: Yin Kuibo , Li Jingcang , Xiong Yuwei , Zhu Mingyun , Tan Zhiyuan , Jin Zhanrui
Published: October 2023

Memristors, known for their adjustable and non-volatile resistance, offer a promising avenue for emulating synapses. However, achieving pulse frequency-dependent synaptic plasticity in memristors or memristive systems necessitates further exploration. In this study, we present a novel approach to modulate the conductance of a memristor in a capacitor–memristor circuit by finely tuning the frequency of input pulses. Our experimental results demonstrate that these phenomena align with the long-term depression (LTD) and long-term potentiation (LTP) observed in synapses, which are induced by the frequency of action potentials. Additionally, we successfully implement a Hebbian-like learning mechanism in a simple circuit that connects a pair of memristors to a capacitor, resulting in observed associative memory formation and forgetting processes. Our findings highlight the potential of capacitor–memristor circuits in faithfully replicating the frequency-dependent behavior of synapses, thereby offering a valuable contribution to the development of brain-inspired neural networks.
Surface Roughness Prediction in Ultra-Precision Milling: An Extreme Learning Machine Method with Data Fusion
Authors: Shang Suiyan , Wang Chunjin , Liang Xiaoliang , Cheung Chi Fai , Zheng Pai
Published: October 2023

This paper pioneers the use of the extreme learning machine (ELM) approach for surface roughness prediction in ultra-precision milling, leveraging the excellent fitting ability with small datasets and the fast learning speed of the extreme learning machine method. By providing abundant machining information, the machining parameters and force signal data are fused on the feature level to further improve ELM prediction accuracy. An ultra-precision milling experiment was designed and conducted to verify our proposed data-fusion-based ELM method. The results show that the ELM with data fusion outperforms other state-of-art methods in surface roughness prediction. It achieves an impressively low mean absolute percentage error of 1.6% while requiring a mere 18 s for model training.
Tensile Property of 7075 Aluminum Alloy with Strengthening Layer by Laser Remelting-Cladding Treatment
Authors: Sui Qi , Hu Ning , Su Yingrui , Wang Yan , Song Xiaolei
Published: October 2023

The Ni60-SiC-CeO2 strengthening layer with deep remelting pools was constructed on the surface of 7075 aluminum alloy using the laser remelting-cladding processing method, and a soft and hard interphase was prepared on the matrix by the interval of laser remelting, which was inspired by soft–hard interphase structure with excellent crack inhibition performance from the natural world. The microstructure and microhardness of the remelting region and the remelting-cladding region of the strengthening layer were studied. The tensile characteristics of two distinct strengthening layers were investigated in the laboratory. The results showed that the grain size of remelting pools is finer, and the microhardness is higher than that of the matrix, which makes crack propagation more difficult. In addition, the results show that the strengthening layer has compact and flawless microstructure and has been metallurgically integrated with the matrix, and the microhardness of the regions treated by laser cladding and laser remelting-cladding has been improved obviously. Toughness has improved, as has the problem of toughness reduction after cladding ceramic particles. The sample’s strength is also significantly greater than that of the untreated sample.
Compact Physics Hot-Carrier Degradation Model Valid over a Wide Bias Range
Authors: Tyaginov Stanislav , Bury Erik , Grill Alexander , Yu Zhuoqing , Makarov Alexander , De Keersgieter An , Vexler Mikhail , Vandemaele Michiel , Wang Runsheng , Spessot Alessio , Chasin Adrian , Kaczer Ben
Published: October 2023

We develop a compact physics model for hot-carrier degradation (HCD) that is valid over a wide range of gate and drain voltages (Vgs and Vds, respectively). Special attention is paid to the contribution of secondary carriers (generated by impact ionization) to HCD, which was shown to be significant under stress conditions with low Vgs and relatively high Vds. Implementation of this contribution is based on refined modeling of carrier transport for both primary and secondary carriers. To validate the model, we employ foundry-quality n-channel transistors and a broad range of stress voltages {Vgs,Vds}.
An Exploratory Study of Laser Scribing Quality through Cross-Section Scribing Profiles
Authors: Chen Ruqi , Chang Shing , Lei Shuting
Published: October 2023

This article presents a novel approach for evaluating laser scribing quality through cross-section profiles generated from a three-dimensional optical profiler. Existing methods for assessing scribing quality only consider the width and depth of a scribe profile. The proposed method uses a cubic spline model for cross-section profiles. Two quality characteristics are proposed to assess scribing accuracy and consistency. Accuracy is measured by the ratio of the actual laser-scribed area to the target area (RA), which reflects the deviation from the desired profile. The mean square error (MSE) is a measure of how close each scribed cross-section under the same scribing conditions is to the fitted cubic spline model. Over 1370 cross-section profiles were generated under 171 scribing conditions. Two response surface polynomial models for RA and MSE were built with 18 scribing conditions with acceptable scribing depth and RA values. Both RA and MSE were considered simultaneously via contour plots. A scatter plot of RA and MSE was then used for Pareto optimization. It was found that the cross-sectional profile of a laser scribe could be accurately represented by a cubic spline model. A multivariate nonlinear regression model for RA and MSE identified pulse energy and repetition rate as the two dominant laser parameters. A Pareto optimization analysis further established a Pareto front, where the best compromised solution could be found.
Structural Control of Nanofibers According to Electrospinning Process Conditions and Their Applications
Authors: Nguyen Trong Danh , Roh Sojeong , Nguyen My Thi Ngoc , Lee Jun Seop
Published: October 2023

Nanofibers have gained much attention because of the large surface area they can provide. Thus, many fabrication methods that produce nanofiber materials have been proposed. Electrospinning is a spinning technique that can use an electric field to continuously and uniformly generate polymer and composite nanofibers. The structure of the electrospinning system can be modified, thus making changes to the structure, and also the alignment of nanofibers. Moreover, the nanofibers can also be treated, modifying the nanofiber structure. This paper thoroughly reviews the efforts to change the configuration of the electrospinning system and the effects of these configurations on the nanofibers. Excellent works in different fields of application that use electrospun nanofibers are also introduced. The studied materials functioned effectively in their application, thereby proving the potential for the future development of electrospinning nanofiber materials.
An Aging Small-Signal Model for Degradation Prediction of Microwave Heterojunction Bipolar Transistor S-Parameters Based on Prior Knowledge Neural Network
Authors: Cheng Lin , Lu Hongliang , Yan Silu , Liu Chen , Qiao Jiantao , Qi Junjun , Cheng Wei , Zhang Yimen , Zhang Yuming
Published: October 2023

In this paper, an aging small-signal model for degradation prediction of microwave heterojunction bipolar transistor (HBT) S-parameters based on prior knowledge neural networks (PKNNs) is explored. A dual-extreme learning machine (D-ELM) structure with an adaptive genetic algorithm (AGA) optimization process is used to simulate the fresh S-parameters of InP HBT devices and the degradation of S-parameters after accelerated aging, respectively. In addition to the reliability parametric inputs of the original aging problem, the S-parameter degradation trend obtained from the aging small-signal equivalent circuit is used as additional information to inject into the D-ELM structure. Good agreement was achieved between measured and predicted results of the degradation of S-parameters within a frequency range of 0.1 to 40 GHz.
Research Progress in Tunable Fiber Lasers Based on Multimode Interference Filters
Authors: Zhang Liqiang , Zhu Kexin , Yao Yicun , Tian Xiuying , Xu Hailong , Nie Zhaogang
Published: October 2023

Tunable fiber lasers have the advantages of good beam quality, high integration, and adjustable output wavelength, and they are widely used in fields such as optical fiber communication and optical fiber sensing. The fiber filter is one of the key components of tunable fiber lasers. Among the various filters currently used, multimode interference filters have the advantages of simple structure, convenient implementation, flexible tuning methods, and convenient spectral range design. The structures of multimode interference filters based on multimode fibers, no-core fibers, multi-core fibers, tapered fibers, and other special fibers are introduced in this paper. The working principles and tuning methods are analyzed and the research progress of tunable fiber lasers based on these filters is summarized. Finally, the development trend of tunable fiber lasers based on multimode interference filters is discussed. The rapid development and applications of multimode interference filters can help improve the performance of continuous and pulse lasers as well as promote the practicality of tunable fiber lasers.