bluuebunny/crossref_metadata_2025 huggingface dataset:
Continuous Positive Airway Pressure Reduces Plasma Neurochemical Levels in Patients with OSA: A Pilot Study
Authors: Liu Wen-Te , Huang Huei-Tyng , Hung Hsin-Yi , Lin Shang-Yang , Hsu Wen-Hua , Lee Fang-Yu , Kuan Yi-Chun , Lin Yin-Tzu , Hsu Chia-Rung , Stettler Marc , Yang Chien-Ming , Wang Jieni , Duh Ping-Jung , Lee Kang-Yun , Wu Dean , Lee Hsin-Chien , Kang Jiunn-Horng , Lee Szu-Szu , Wong Hsiu-Jui , Tsai Cheng-Yu , Majumdar Arnab
Published: February 2023

Obstructive sleep apnea (OSA) is a risk factor for neurodegenerative diseases. This study determined whether continuous positive airway pressure (CPAP), which can alleviate OSA symptoms, can reduce neurochemical biomarker levels. Thirty patients with OSA and normal cognitive function were recruited and divided into the control (n = 10) and CPAP (n = 20) groups. Next, we examined their in-lab sleep data (polysomnography and CPAP titration), sleep-related questionnaire outcomes, and neurochemical biomarker levels at baseline and the 3-month follow-up. The paired t-test and Wilcoxon signed-rank test were used to examine changes. Analysis of covariance (ANCOVA) was performed to increase the robustness of outcomes. The Epworth Sleepiness Scale and Pittsburgh Sleep Quality Index scores were significantly decreased in the CPAP group. The mean levels of total tau (T-Tau), amyloid-beta-42 (Aβ42), and the product of the two (Aβ42 × T-Tau) increased considerably in the control group (ΔT-Tau: 2.31 pg/mL; ΔAβ42: 0.58 pg/mL; ΔAβ42 × T-Tau: 48.73 pg2/mL2), whereas the mean levels of T-Tau and the product of T-Tau and Aβ42 decreased considerably in the CPAP group (ΔT-Tau: −2.22 pg/mL; ΔAβ42 × T-Tau: −44.35 pg2/mL2). The results of ANCOVA with adjustment for age, sex, body mass index, baseline measurements, and apnea–hypopnea index demonstrated significant differences in neurochemical biomarker levels between the CPAP and control groups. The findings indicate that CPAP may reduce neurochemical biomarker levels by alleviating OSA symptoms.
Resonance Scanning as an Efficiency Enhancer for EEG-Guided Adaptive Neurostimulation
Authors: Fedotchev Alexander I. , Parin Sergey B. , Polevaya Sofia A.
Published: February 2023

Electroencephalogram (EEG)-guided adaptive neurostimulation is an innovative kind of non-invasive closed-loop brain stimulation technique that uses audio–visual stimulation on-line modulated by rhythmical EEG components of the individual. However, the opportunity to enhance its effectiveness is a challenging task and needs further investigation. The present study aims to experimentally test whether it is possible to increase the efficiency of EEG-guided adaptive neurostimulation by pre- strengthening the modulating factor (subject’s EEG) through the procedure of resonance scanning, i.e., LED photostimulation with the frequency gradually increasing in the range of main EEG rhythms (4–20 Hz). Thirty-six university students in a state of exam stress were randomly assigned to two matched groups. One group was presented with the EEG-guided adaptive neurostimulation alone, whereas another matched group was presented with the combination of resonance scanning and EEG-guided adaptive neurostimulation. The changes in psychophysiological indicators after stimulation relative to the initial level were used. Although both types of stimulation led to an increase in the power of EEG rhythms, accompanied by a decrease in the number of errors in the word recognition test and a decrease in the degree of emotional maladjustment, these changes reached the level of significance only in experiments with preliminary resonance scanning. Resonance scanning increases the brain’s responsiveness to subsequent EEG-guided adaptive neurostimulation, acting as a tool to enhance its efficiency. The results obtained clearly indicate that the combination of resonance scanning and EEG-guided adaptive neurostimulation is an effective way to reach the signs of cognitive improvement in stressed individuals.
Miniaturization of Non-Assembly Metallic Pin-Joints by LPBF-Based Additive Manufacturing as Perfect Pivots for Pantographic Metamaterials
Authors: Gutmann Florian , Stilz Maximilian , Patil Sankalp , Fischer Frank , Hoschke Klaus , Ganzenmüller Georg , Hiermaier Stefan
Published: February 2023

This work introduced additively manufactured non-assembly, miniaturized pin-joints for pantographic metamaterials as perfect pivots. The titanium alloy Ti6Al4V was utilized with laser powder bed fusion technology. The pin-joints were produced using optimized process parameters required for manufacturing miniaturized joints, and they were printed at a particular angle to the build platform. Additionally, this process optimization will eliminate the requirement to geometrically compensate the computer-aided design model, allowing for even further miniaturization. In this work, pin-joint lattice structures known as pantographic metamaterials were taken into consideration. The mechanical behavior of the metamaterial was characterized by bias extension tests and cyclic fatigue experiments, showing superior levels of performance (no sign of fatigue for 100 cycles of an elongation of approximately 20%) in comparison to classic pantographic metamaterials made with rigid pivots. The individual pin-joints, with a pin diameter of 350 to 670 µm, were analyzed using computed tomography scans, indicating that the mechanism of the rotational joint functions well even though the clearance of 115 to 132 µm between the moving parts is comparable to the nominal spatial resolution of the printing process. Our findings emphasize new possibilities to develop novel mechanical metamaterials with actual moving joints on a small scale. The results will also support stiffness-optimized metamaterials with variable-resistance torque for non-assembly pin-joints in the future.
Optimization of Coherent Dynamics of Localized Surface Plasmons in Gold and Silver Nanospheres; Large Size Effects
Authors: Kolwas Krystyna
Published: February 2023

Noble metal nanoparticles have attracted attention in recent years due to a number of their exciting applications in plasmonic applications, e.g., in sensing, high-gain antennas, structural colour printing, solar energy management, nanoscale lasing, and biomedicines. The report embraces the electromagnetic description of inherent properties of spherical nanoparticles, which enable resonant excitation of Localized Surface Plasmons (defined as collective excitations of free electrons), and the complementary model in which plasmonic nanoparticles are treated as quantum quasi-particles with discrete electronic energy levels. A quantum picture including plasmon damping processes due to the irreversible coupling to the environment enables us to distinguish between the dephasing of coherent electron motion and the decay of populations of electronic states. Using the link between classical EM and the quantum picture, the explicit dependence of the population and coherence damping rates as a function of NP size is given. Contrary to the usual expectations, such dependence for Au and Ag NPs is not a monotonically growing function, which provides a new perspective for tailoring plasmonic properties in larger-sized nanoparticles, which are still hardly available experimentally. The practical tools for comparing the plasmonic performance of gold and silver nanoparticles of the same radii in an extensive range of sizes are also given.
Effects of Rotational Speed on the Microstructure and Mechanical Properties of 2198-T8 Al-Li Alloy Processed by Friction Spot Welding
Authors: Pang Zheng , Yang Jin , Cai Yangchuan
Published: February 2023

The friction spot welding (FSpW) method was used to weld 2198-T8 Al-Li alloy at rotational speeds of 500 rpm, 1000 rpm, and 1800 rpm. It was shown that the grains in the FSpW joints were transformed from “pancake” grains to fine equiaxed grains by the heat input of welding, and the reinforcing phases of S’ and θ were all redissolved into the Al matrix. This leads to a decrease in the tensile strength of the FsPW joint compared to the base material and a change in the fracture mechanism from mixed ductile-brittle fracture to ductile fracture. Finally, the tensile properties of the welded joint depend on the size and morphology of the grains and their dislocation density. At the rotational speed setting of 1000 rpm in this paper, the mechanical properties of welded joints consisting of fine and uniformly distributed equiaxed grains are best. Therefore, a reasonable set of the rotational speed of FSpW can improve the mechanical properties of the welded joints of 2198-T8 Al-Li alloy.
An Image-Based Framework for Measuring the Prestress Level in CFRP Laminates: Experimental Validation
Authors: Valença Jónatas , Ferreira Cláudia , Araújo André G. , Júlio Eduardo
Published: February 2023

Image-based methods have been applied to support structural monitoring, product and material testing, and quality control. Lately, deep learning for compute vision is the trend, requiring large and labelled datasets for training and validation, which is often difficult to obtain. The use of synthetic datasets is often applying for data augmentation in different fields. An architecture based on computer vision was proposed to measure strain during prestressing in CFRP laminates. The contact-free architecture was fed by synthetic image datasets and benchmarked for machine learning and deep learning algorithms. The use of these data for monitoring real applications will contribute towards spreading the new monitoring approach, increasing the quality control of the material and application procedure, as well as structural safety. In this paper, the best architecture was validated during experimental tests, to evaluate the performance in real applications from pre-trained synthetic data. The results demonstrate that the architecture implemented enables estimating intermediate strain values, i.e., within the range of training dataset values, but it does not allow for estimating strain values outside those range. The architecture allowed for estimating the strain in real images with an error ∼0.5%, higher than that obtained with synthetic images. Finally, it was not possible to estimate the strain in real cases from the training performed with the synthetic dataset.
Zero-Waste Approach for Heavy Metals’ Removal from Water with an Enhanced Multi-Stage Hybrid Treatment System
Authors: Urbancl Danijela , Goricanec Darko , Simonic Marjana
Published: February 2023

The aim of the work was to develop a zero-waste technological solution for hybrid removal of heavy metals from river sediments. The proposed technological process consists of sample preparation, sediment washing (a physicochemical process for sediment purification), and purification of the wastewater produced as a by-product. A suitable solvent for heavy metal washing and the effectiveness of heavy metal removal were determined by testing EDTA and citric acid. The process for removing heavy metals from the samples worked best with citric acid when the 2% sample suspension was washed over a 5-h period. The method was chosen of the adsorption of heavy metals from the exhausting washing solution on natural clay. Analyses were performed of the three main heavy metals, Cu(II), Cr(VI), and Ni(II), in the washing solution. Based on the laboratory experiments, a technological plan was prepared for the purification of 100,000 tons of material per year.
Efficiency Improvement of Industrial Silicon Solar Cells by the POCl3 Diffusion Process
Authors: Xu Xiaodong , Wu Wangping , Wang Qinqin
Published: February 2023

To improve the efficiency of polycrystalline silicon solar cells, process optimization is a key technology in the photovoltaic industry. Despite the efficiency of this technique to be reproducible, economic, and simple, it presents a major inconvenience to have a heavily doped region near the surface which induces a high minority carrier recombination. To limit this effect, an optimization of diffused phosphorous profiles is required. A “low-high-low” temperature step of the POCl3 diffusion process was developed to improve the efficiency of industrial-type polycrystalline silicon solar cells. The low surface concentration of phosphorus doping of 4.54 × 1020 atoms/cm3 and junction depth of 0.31 μm at a dopant concentration of N = 1017 atoms/cm3 were obtained. The open-circuit voltage and fill factor of solar cells increased up to 1 mV and 0.30%, compared with the online low-temperature diffusion process, respectively. The efficiency of solar cells and the power of PV cells were increased by 0.1% and 1 W, respectively. This POCl3 diffusion process effectively improved the overall efficiency of industrial-type polycrystalline silicon solar cells in this solar field.
Ti–15Zr and Ti–15Zr–5Mo Biomaterials Alloys: An Analysis of Corrosion and Tribocorrosion Behavior in Phosphate-Buffered Saline Solution
Authors: Santos Adriana Alencar , Teixeira Jean Valdir Uchôa , Pintão Carlos Alberto Fonzar , Correa Diego Rafael Nespeque , Grandini Carlos Roberto , Lisboa-Filho Paulo Noronha
Published: February 2023

It is crucial for clinical needs to develop novel titanium alloys feasible for long-term use as orthopedic and dental prostheses to prevent adverse implications and further expensive procedures. The primary purpose of this research was to investigate the corrosion and tribocorrosion behavior in the phosphate buffered saline (PBS) of two recently developed titanium alloys, Ti–15Zr and Ti–15Zr–5Mo (wt.%) and compare them with the commercially pure titanium grade 4 (CP–Ti G4). Density, XRF, XRD, OM, SEM, and Vickers microhardness analyses were conducted to give details about the phase composition and the mechanical properties. Additionally, electrochemical impedance spectroscopy was used to supplement the corrosion studies, while confocal microscopy and SEM imaging of the wear track were used to evaluate the tribocorrosion mechanisms. As a result, the Ti–15Zr (α + α′ phase) and Ti–15Zr–5Mo (α″ + β phase) samples exhibited advantageous properties compared to CP–Ti G4 in the electrochemical and tribocorrosion tests. Moreover, a better recovery capacity of the passive oxide layer was observed in the studied alloys. These results open new horizons for biomedical applications of Ti–Zr–Mo alloys, such as dental and orthopedical prostheses.
Molecular Sieve, Halloysite, Sepiolite and Expanded Clay as a Tool in Reducing the Content of Trace Elements in Helianthus annuus L. on Copper-Contaminated Soil
Authors: Wyszkowski Mirosław , Wyszkowska Jadwiga , Kordala Natalia , Zaborowska Magdalena
Published: February 2023

The aim of this study was to determine the effect of copper soil contamination on the trace element content of sunflower aerial parts and in roots. Another aim was to assess whether the introduction of selected neutralizing substances (molecular sieve, halloysite, sepiolite and expanded clay) into the soil could reduce the impact of copper on the chemical composition of sunflower plants. Copper soil contamination with 150 mg Cu2+ kg−1 of soil and 10 g of each adsorbent per kg of soil were used. Soil contamination with copper caused a significant increase in the content of this element in the aerial parts (by 37%) and roots (by 144%) of sunflower. Enriching the soil with the mineral substances reduced the amount of copper in the aerial parts of sunflower. Halloysite had the greatest effect (35%), while expanded clay had the smallest effect (10%). An opposite relationship was found in the roots of this plant. In copper-contaminated objects, a decrease in the content of cadmium and iron and an increase in the concentrations of nickel, lead and cobalt in the aerial parts and roots of sunflower were observed. The applied materials reduced the content of the remaining trace elements more strongly in the aerial organs than in the roots of sunflower. Molecular sieve had the greatest reducing effect on the content of trace elements in sunflower aerial organs, followed by sepiolite, while expanded clay had the least impact. The molecular sieve also reduced the content of iron, nickel, cadmium, chromium, zinc and, especially, manganese, whereas sepiolite reduced the content of zinc, iron, cobalt, manganese and chromium in sunflower aerial parts. Molecular sieve contributed to a slight increase in the content of cobalt, while sepiolite had the same effect on the content of nickel, lead and cadmium in the aerial parts of sunflower. All materials decreased the content of chromium in sunflower roots, molecular sieve—zinc, halloysite—manganese, and sepiolite—manganese and nickel. The materials used in the experiment, especially the molecular sieve and to a lesser extent sepiolite, can be used effectively to reduce the content of copper and some other trace elements, particularly in the aerial parts of sunflower.
Phase Relations in the Ln2O3–Cr2O3–B2O3 (Ln = Gd–Lu) Ternary Oxide Systems
Authors: Kuzmin Nikolai , Maltsev Victor , Mikliaeva Elizaveta , Volkova Elena , Boldyrev Kirill , Koporulina Elizaveta
Published: February 2023

In this work, isothermal sections of the Ln2O3–Cr2O3–B2O3 (Ln = Gd–Lu) ternary oxide systems at 900, 1000, and 1100 °C were constructed by determining the phase relations by using a powder X-ray diffraction technique. As a result, these systems were divided into subsidiary subsystems. Two types of double borates, LnCr3(BO3)4 (Ln = Gd–Er) and LnCr(BO3)2 (Ln = Ho–Lu), were observed in the investigated systems. Regions of phase stability for LnCr3(BO3)4 and LnCr(BO3)2 were determined. It was shown that the LnCr3(BO3)4 compounds crystallized in rhombohedral and monoclinic polytype modifications up to 1100 °C; above this temperature and up to the melting points, the monoclinic modification was predominantly formed. The LnCr3(BO3)4 (Ln = Gd–Er) and LnCr(BO3)2 (Ln = Ho–Lu) compounds were characterized by using a powder X-ray diffraction method and thermal analysis.
Allergenicity and Bioavailability of Nickel Nanoparticles Compared to Nickel Microparticles in Mice
Authors: Tsuchida Dai , Matsuki Yuko , Tsuchida Jin , Iijima Masahiro , Tanaka Maki
Published: February 2023

Metal allergy is a common disease that afflicts many people. Nevertheless, the mechanism underlying metal allergy development has not been completely elucidated. Metal nanoparticles might be involved in the development of a metal allergy, but the associated details are unknown. In this study, we evaluated the pharmacokinetics and allergenicity of nickel nanoparticles (Ni-NPs) compared with those of nickel microparticles (Ni-MPs) and nickel ions. After characterizing each particle, the particles were suspended in phosphate-buffered saline and sonicated to prepare a dispersion. We assumed the presence of nickel ions for each particle dispersion and positive control and orally administered nickel chloride to BALB/c mice repeatedly for 28 days. Results showed that compared with those in the Ni-MP administration group (MP group), the Ni-NP administration group (NP group) showed intestinal epithelial tissue damage, elevated serum interleukin (IL)-17 and IL-1β levels, and higher nickel accumulation in the liver and kidney. Additionally, transmission electron microscopy confirmed the accumulation of Ni-NPs in the livers of both the NP and nickel ion administration groups. Furthermore, we intraperitoneally administered a mixed solution of each particle dispersion and lipopolysaccharide to mice and then intradermally administered nickel chloride solution to the auricle after 7 days. Swelling of the auricle was observed in both the NP and MP groups, and an allergic reaction to nickel was induced. Particularly in the NP group, significant lymphocytic infiltration into the auricular tissue was observed, and serum IL-6 and IL-17 levels were increased. The results of this study showed that in mice, Ni-NP accumulation in each tissue was increased after oral administration and toxicity was enhanced, as compared to those with Ni-MPs. Orally administered nickel ions transformed into nanoparticles with a crystalline structure and accumulated in tissues. Furthermore, Ni-NPs and Ni-MPs induced sensitization and nickel allergy reactions in the same manner as that with nickel ions, but Ni-NPs induced stronger sensitization. Additionally, the involvement of Th17 cells was suspected in Ni-NP-induced toxicity and allergic reactions. In conclusion, oral exposure to Ni-NPs results in more serious biotoxicity and accumulation in tissues than Ni-MPs, suggesting that the probability of developing an allergy might increase.
Cardiovascular Magnetic Resonance Imaging in Familial Dilated Cardiomyopathy
Authors: Lau Clement , Gul Uzma , Liu Boyang , Captur Gabriella , Hothi Sandeep S.
Published: February 2023

Dilated cardiomyopathy (DCM) is a common cause of non-ischaemic heart failure, conferring high morbidity and mortality, including sudden cardiac death due to systolic dysfunction or arrhythmic sudden death. Within the DCM cohort exists a group of patients with familial disease. In this article we review the pathophysiology and cardiac imaging findings of familial DCM, with specific attention to known disease subtypes. The role of advanced cardiac imaging cardiovascular magnetic resonance is still accumulating, and there remains much to be elucidated. We discuss its potential clinical roles as currently known, with respect to diagnostic utility and risk stratification. Advances in such risk stratification may help target pharmacological and device therapies to those at highest risk.
Extracorporeal Circulation and Optic Nerve Ultrasound: A Pilot Study
Authors: Taşkın Öztürk , Demir Ufuk
Published: February 2023

Background and Objectives: Cardiopulmonary bypass (CPB) is an extracorporeal circuit that provides surgical access to an immobile and bloodless area, allowing for technical and procedural advances in cardiothoracic surgery. CBP can alter the integrity of the blood–brain barrier and cause changes in intracranial pressure (ICP) postoperatively. Optical nerve sheath diameter (ONSD) measurement is among the alternative non-invasive methods for ICP monitoring. In this study, we aimed to evaluate the optic nerve sheath diameter measurements under the guidance of ultrasonography for ICP changes during the extracorporeal circulation process. Materials and Methods: The study population included 21 patients over 18 years of age who required extracorporeal circulation. Demographic data of the patients, such as age, gender, comorbidity, American Society of Anesthesiologists (ASA) classification and reason for operation (coronary artery disease or mitral or aortic valve disease) were recorded. The ONSD was measured and evaluated before the extracorporeal circulation (first time) and at the 30th minute (second time), 60th minute (third time) and 90th minute (fourth time) of the extracorporeal circulation. Non-invasive ICP (ICP ONSD) values were calculated based on the ONSD values found. Results: The mean ONSD values measured before the extracorporeal circulation of the patients were found to be 4.13 mm (3.8–4.6) for the right eye and 4.36 mm (4.1–4.7) for the left eye. Calculated nICPONSD values of 11.0 mm Hg (1.0–21.0) for the right eye and 10.89 mm Hg (1.0–21.0) for the left eye were found. It was observed that there was a significant increase in the ONSD and nlCPONSD values recorded during the extracorporeal circulation of all patients compared to the baseline values (p < 0.005). Conclusions: During extracorporeal circulation, ultrasound-guided ONSD measurement is an easy, inexpensive and low-complication method that can be performed at the bedside during the operation to monitor ICP changes.
Membrane Progesterone Receptors (mPRs/PAQRs) Are Going beyond Its Initial Definitions
Authors: Aickareth Justin , Hawwar Majd , Sanchez Nickolas , Gnanasekaran Revathi , Zhang Jun
Published: February 2023

Progesterone (PRG) is a key cyclical reproductive hormone that has a significant impact on female organs in vertebrates. It is mainly produced by the corpus luteum of the ovaries, but can also be generated from other sources such as the adrenal cortex, Leydig cells of the testes and neuronal and glial cells. PRG has wide-ranging physiological effects, including impacts on metabolic systems, central nervous systems and reproductive systems in both genders. It was first purified as an ovarian steroid with hormonal function for pregnancy, and is known to play a role in pro-gestational proliferation during pregnancy. The main function of PRG is exerted through its binding to progesterone receptors (nPRs, mPRs/PAQRs) to evoke cellular responses through genomic or non-genomic signaling cascades. Most of the existing research on PRG focuses on classic PRG-nPR-paired actions such as nuclear transcriptional factors, but new evidence suggests that PRG also exerts a wide range of PRG actions through non-classic membrane PRG receptors, which can be divided into two sub-classes: mPRs/PAQRs and PGRMCs. The review will concentrate on recently found non-classical membrane progesterone receptors (mainly mPRs/PAQRs) and speculate their connections, utilizing the present comprehension of progesterone receptors.
Pressure Drop and Gas Flow in an Oxygen Blast Furnace Analyzed by a Combination of Experimentation and a Porous Model
Authors: Li Cong , Xue Qingguo , Zuo Haibin , Wang Jingsong , Wang Guang
Published: February 2023

As a modification of the conventional blast furnace (BF), the top gas recycling-oxygen blast furnace (TGR-OBF) has been continuously studied in the context of the technological transformation of low-carbon metallurgy. As it has a set of new gas inlets in the stack and changes the blast operation system in the hearth, the pressure drop and the in-furnace gas flow are the primary problems to be solved in the TGR-OBF’s industrialization. In this paper, a two-dimensional model of a whole blast furnace, based on a softening-and-melting experiment and porous-medium theory, is established. The in-furnace pressure drop and the gas velocity with different oxygen concentrations and tuyere heights are studied. The results show that the suitable height of the stack tuyere is the same as that of the elevation as the cohesive zone inside the furnace. With the gradual increase in oxygen enrichment, the permeability of the cohesive ore layer (COL) increases, while the gas flow through the coke layer (CL) decreases gradually up to 10%. The simulation results provide a theoretical basis for the TGR-OBF to reduce the coke rate and keep the pressure drop from increasing, or even to enable it to decrease.
Effect of Filler Wire Feed Rate on the Formation of Porosity in Laser Welded Joints of Magnesium Alloy AZ31B–H24
Authors: Vyskoč Maroš
Published: February 2023

In this work, the effect of a filler wire feed rate was studied with special attention to the proportion of porosity volume in the weld metal, microstructure, and mechanical properties. Butt laser weld joints were created using the Nd:YAG laser. Weld joints were produced with the AZ31 filler wire with a diameter of 1.2 mm. Decreasing the filler wire feed rate of the filler wire led to an increase in the porosity of the weld metal. Therefore, porosity is more likely to occur in laser welding without the use of a filler wire. Clear segregation of aluminium, manganese, and zinc was observed in the EDS maps and the local EDS line profile measurements. The precipitates formed were rich in Al and Mn or Al and Zn, compared to the matrix. They also show a large decrease in Mg content to minimum values ranging from 10 to 60 wt.% in the precipitates. To investigate pores in the weld metal of the weld joint, computed tomography was used. The highest volume of porosity was measured in weld joint no. 3. (0.63 mm3). On the contrary, the lowest porosity volume was detected in weld joint no. 1. (0.06 mm3). The largest width of the weld metal (2.25 mm) was measured if the filler wire feed rate was 130 cm/min. The highest average microhardness (82.5 HV0.1) was recorded in the weld metal of weld joint no. 1. In weld joint no. 3, a fracture occurred in the weld metal and the measured tensile strength was only 154 MPa.
The Microstructure Characteristics Evolution of Bulk High-Purity Silver for High Relief Application
Authors: Liang Pei , Zhang Jie , Kong Ning , Li Hongbo , Zhu Hengfei
Published: February 2023

Silver products with high relief have become popular in the silver decoration industry. However, it is difficult to obtain these products through conventional processing at ambient temperature. The aim of this work is to solve this problem by increasing the deformation temperature. Detailed studies were conducted on the evolution of microstructure characteristics in bulk high-purity silver by electron backscatter diffraction (EBSD) to achieve high-relief applications at elevated temperatures. The high temperature sample is mainly composed of recrystallized and substructured grains, exhibiting a more stable state than the ambient temperature sample. More than 70% annealing twins are observed in the hot-working sample. They are characterized by the amount of Σ3n-type triple grain boundary junctions within large grain clusters formed by multiple twinning. These particular boundaries improve the intergranular corrosion resistance and degradation, which is significantly essential for high-purity silver jewelry exposed to sweat and air. The closed multi-coining processes at different temperatures were conducted subsequently. The performance of workpieces demonstrates that increasing the deformation temperature is a viable alternative for producing durable high-relief silver products.
Antimicrobial Peptides Relieve Transportation Stress in Ragdoll Cats by Regulating the Gut Microbiota
Authors: He Shansong , Yang Kang , Wen Jiawei , Kuang Tao , Cao Zhihao , Zhang Lingna , Han Sufang , Jian Shiyan , Chen Xin , Zhang Limeng , Deng Jinping , Deng Baichuan
Published: February 2023

Transportation is common in cats and often causes stress and intestinal disorders. Antimicrobial peptides (AMPs) exhibit a broad spectrum of antibacterial activity, and they may have the capacity for antioxidant and immune regulation. The objective of this study was to investigate the effects of dietary supplementation with AMPs on stress response, gut microbiota and metabolites of cats that have undergone transport stress. A total of 14 Ragdoll cats were randomly allocated into 2 treatments: basal diet (CON) and a basal diet supplemented with 0.3% AMPs. After a 6-week feeding period, all cats were transported for 3 h and, then, fed for another week. The results show that the diarrhea rate of cats was markedly reduced by supplementation with AMPs throughout the trial period (p < 0.05). In addition, AMPs significantly reduced serum cortisol and serum amyloid A (p < 0.05) and increased apolipoprotein 1 after transportation (p < 0.05). Moreover, AMPs reduced the level of inflammatory factors in the serum caused by transportation stress, including tumor necrosis factor-alpha (TNF-α) and interleukin-1 beta (IL-1β) (p < 0.05). The AMPs enhanced the activities of glutathione peroxidase (p < 0.01) and superoxide dismutase (p < 0.05). Furthermore, cats fed AMPs had higher levels of branched chain fatty acids (BCFAs) and a relative abundance of Blautia and a lower relative abundance of Negativibacillus after transportation (p < 0.05). The serum metabolome analysis further revealed that AMPs markedly regulated lipid metabolism by upregulating cholic acid expression. In conclusion, AMP supplementation alleviated oxidative stress and inflammatory response in transportation by regulating the gut microbiota and metabolites, thereby relieving stress-induced diarrhea and supporting gut and host health in cats.
Acoustic Sensing Performance Investigation Based on Grooves Etched in the Ring Resonators
Authors: Han Yuan , Zheng Yongqiu , Li Nan , Luo Yifan , Xue Chenyang , Bai Jiandong , Chen Jiamin
Published: February 2023

Acoustic detection based on optical technology has moved in the direction of high sensitivity and resolution. In this study, an optical waveguide acoustic sensor based on a ring resonator with the evanescent field is proposed. Grooves are introduced into the ring resonators as a direct sensitive structure to excite the evanescent field. A series of resonators with diverse grooves are fabricated for a comparative analysis of acoustic performance. The acoustic parameters of bandwidth, sensitivity, and signal-to-noise ratio (SNR) vary with different grooves indicated by the Q-factor. The results show that the ring resonators with variable-sized grooves exhibit excellent capability of acoustics detection. A maximum frequency of 160 kHz and a high sensitivity of 60.075 mV/Pa is achieved, with the minimum detectable sound pressure being 131.34 µPa/Hz1/2. Furthermore, the resonators with high Q-factors represent a remarkable sound resolution reaching 0.2 Hz. This work is of great significance for optimizing acoustic sensors and broadening the application range.
Design and Test of a Spatial Nanopositioner for Evaluating the Out-of-Focus-Plane Performance of Micro-Vision
Authors: Wang Ruizhou , Wu Heng
Published: February 2023

Micro-vision possesses high in-focus-plane motion tracking accuracy. Unfortunately, out-of-focus-plane displacements cannot be avoided, decreasing the in-focus-plane tracking accuracy of micro-vision. In this paper, a spatial nanopositioner is proposed to evaluate the out-of-focus-plane performance of a micro-vision system. A piezoelectric-actuated spatial multi-degree-of-freedom (multi-DOF) nanopositioner is introduced. Three in-plane Revolute-Revolute-Revolute-Revolute (RRRR) compliant parallel branched chains produce in-focus-plane motions. Three out-of-plane RRRR chains generate out-of-focus-plane motions. A typical micro-vision motion tracking algorithm is presented. A general grayscale template matching (GTM) approach is combined with the region of interest (ROI) method. The in-focus-plane motion tracking accuracy of the micro-vision system is tested. Different out-of-focus-plane displacements are generated using the proposed nanopositioner. The accuracy degradation of the in-focus-plane motion tracking is evaluated. The experimental results verify the evaluation ability of the proposed nanopositioner.
ScAlN Film-Based Piezoelectric Micromechanical Ultrasonic Transducers with Dual-Ring Structure for Distance Sensing
Authors: Zhang Yuchao , Miao Bin , Wang Guanghua , Zhou Hongyu , Zhang Shiqin , Hu Yimin , Wu Junfeng , Yu Xuechao , Li Jiadong
Published: February 2023

Piezoelectric micromechanical ultrasonic transducers (pMUTs) are new types of distance sensors with great potential for applications in automotive, unmanned aerial vehicle, robotics, and smart homes. However, previously reported pMUTs are limited by a short sensing distance due to lower output sound pressure. In this work, a pMUT with a special dual-ring structure based on scandium-doped aluminum nitride (ScAlN) is proposed. The combination of a dual-ring structure with pinned boundary conditions and a high piezoelectric performance ScAlN film allows the pMUT to achieve a large dynamic displacement of 2.87 μm/V and a high electromechanical coupling coefficient (kt2) of 8.92%. The results of ranging experiments show that a single pMUT achieves a distance sensing of 6 m at a resonant frequency of 91 kHz, the farthest distance sensing registered to date. This pMUT provides surprisingly fertile ground for various distance sensing applications.
Structural Design and Experimental Studies of Resonant Fiber Optic Scanner Driven by Co-Fired Multilayer Piezoelectric Ceramics
Authors: He Liyuan , Wen Zhiyi , Wang Boquan , Li Xiaoniu , Wu Dawei
Published: February 2023

Piezo-driven resonant fiber optic scanners are gaining more and more attention due to their simple structure, weak electromagnetic radiation, and non-friction loss. Conventional piezo-driven resonant fiber optic scanners typically use quadrature piezoelectric tubes (piezo tubes) operating in 31-mode with high drive voltage and low excitation efficiency. In order to solve the abovementioned problem, a resonant fiber scanner driven by co-fired multilayer piezoelectric ceramics (CMPCs) is proposed in which four CMPCs drive a cantilevered fiber optic in the first-order bending mode to achieve efficient and fast space-filling scanning. In this paper, the cantilever beam vibration model with base displacement excitation was derived to provide a theoretical basis for the design of the fiber optic scanner. The finite element method was used to guide the dynamic design of the scanner. Finally, the dynamics characteristics and scanning trajectory of the prepared scanner prototype were tested and compared with the theoretical and simulation calculation results. Experimental results showed that the scanner can achieve three types of space-filling scanning: spiral, Lissajous, and propeller. Compared with the structure using piezo tubes, the designed scanner achieved the same scanning range with smaller axial dimensions, lower drive voltage, and higher efficiency. The scanner can achieve a free end displacement of 10 mm in both horizontal and vertical directions under a sinusoidal excitation signal of 50 Vp-p and 200 Hz. The theoretical, simulation and experimental results validate the feasibility of the proposed scanner structure and provide new ideas for the design of resonant fiber optic scanners.
A Compact UWB Monopole Antenna with Triple Band Notches
Authors: Lin Han , Lu Zhongyuan , Wang Zhonggen , Mu Weidong
Published: February 2023

This article presents an ultra-wideband (UWB) monopole antenna with triple band notch characteristics. The proposed antenna consists of an octagonal patch, fed with a 50 Ω line, which occupies a compact size of 40 mm × 29 mm (0.36λ × 0.26λ, λ is computed using 2.7 GHz frequency) and resonances at a relatively low frequency (2.94 GHz). Specifically, an L-shaped stub, an inverted C-shaped slot, and a pair of U-shaped resonating structures are introduced into the design, which allow antenna to generate three band notches at 3.22–3.83 GHz, 4.49–5.05 GHz and 7.49–8.02 GHz, corresponding to WiMAX band, Indian national satellite (INSAT) band, and X-band satellite frequencies, respectively. In the center of the notched band, the antenna has lower efficiency and gain, essentially indicating that the antenna has good interference rejection performance. To evaluate its performance, the proposed antenna has been fabricated and measured, and the relevant functional parameters, such as S-parameters, voltage standing wave ratio (VSWR) and radiation property, have been studied.
Numerical Study on the Hydraulic Fracturing Pattern in the Hard Roof in Response to Mining-Induced Stress
Authors: Chen Junchao , Qu Zhengzhen , Zhou Lei , Su Xiaopeng
Published: February 2023

A hard roof can cause serious issues corelated with the stability of the panel including large deformation of the roadway in the gob, rock burst, coal and gas outbursts, etc. Currently, hydraulic fracturing has ever-increasingly been used to help control these above-mentioned issues in many engineering cases. This paper presents a series of numerical simulations for hydraulic fracturing with a recently developed model to examine the weakening effect of this pre-conditioning measure on a hard roof. The results show that large deflections in the principal stress direction occur above the coal seam after mining, which can be progressively enhanced as the working face continuously advances. This further could significantly affect the hydraulic fracturing pattern and result in arc-shaped fracture propagation, especially for the hydraulic fracture in stress-descending areas. The obtained results suggest that the hydraulic fracturing operation in a hard roof is preferable in the areas close to the middle of the gob where the created fractures would be deflected more. At last, sensitivity analysis shows that geological conditions have great influence on the hydraulic fracturing pattern. Among the factors analyzed in this paper, the difference between the maximum and minimum stress has the largest influence and should be fully considered. This study could provide a theoretical basis for the practical hydraulic fracturing operation in a hard roof.
Characterization of Extracellular Polymeric Substances Produced by an Acidianus Species and Their Relevance to Bioleaching
Authors: Castro Camila , Donati Edgardo R. , Vera Mario
Published: February 2023

Extracellular polymeric substances (EPS) produced by microorganisms play a crucial role in various bioprocesses, including bioleaching. The microbial leaching of metal sulfides requires an initial cell attachment, which is facilitated by EPS. These substances are mixtures of polysaccharides, proteins, lipids, and other compounds, and their composition and properties can vary depending on the species, growth conditions, and environmental factors. Despite the significance of iron/sulfur oxidizing species in biomining processes, the knowledge of the interfacial processes between thermoacidophilic archaeal species and mineral surfaces is limited. This study examines the cell surface characteristics and EPS produced by an Acidianus strain. The research was conducted using microscopic techniques, Zeta-potential measurements, spectrophotometric methods, Fourier transform infrared spectroscopy, and fluorescence lectin-binding analysis. The results suggest that non-soluble substrates, such as sulfur or pyrite, induce changes in cell surface structures, including the presence of cell appendages, wider cell envelopes, higher hydrophobicities, and increased EPS production, compared to cells grown with soluble substrates such as tetrathionate or ferrous iron. The EPS mainly consist of proteins and carbohydrates, including glucose, manose, N-acetylgalactosamine, and N-acetylglucosamine residues. This study contributes to a better understanding of the relationship between thermophilic archaea and mineral surfaces in biomining processes.
Silica Coated Bi2Se3 Topological Insulator Nanoparticles: An Alternative Route to Retain Their Optical Properties and Make Them Biocompatible
Authors: Belec Blaž , Kostevšek Nina , Pelle Giulia Della , Nemec Sebastjan , Kralj Slavko , Bergant Marušič Martina , Gardonio Sandra , Fanetti Mattia , Valant Matjaž
Published: February 2023

Localized surface plasmon resonance (LSPR) is the cause of the photo-thermal effect observed in topological insulator (TI) bismuth selenide (Bi2Se3) nanoparticles. These plasmonic properties, which are thought to be caused by its particular topological surface state (TSS), make the material interesting for application in the field of medical diagnosis and therapy. However, to be applied, the nanoparticles have to be coated with a protective surface layer, which prevents agglomeration and dissolution in the physiological medium. In this work, we investigated the possibility of using silica as a biocompatible coating for Bi2Se3 nanoparticles, instead of the commonly used ethylene-glycol, which, as is presented in this work, is not biocompatible and alters/masks the optical properties of TI. We successfully prepared Bi2Se3 nanoparticles coated with different silica layer thicknesses. Such nanoparticles, except those with a thick, ≈200 nm silica layer, retained their optical properties. Compared to ethylene-glycol coated nanoparticles, these silica coated nanoparticles displayed an improved photo-thermal conversion, which increased with the increasing thickness of the silica layer. To reach the desired temperatures, a 10–100 times lower concentration of photo-thermal nanoparticles was needed. In vitro experiments on erythrocytes and HeLa cells showed that, unlike ethylene glycol coated nanoparticles, silica coated nanoparticles are biocompatible.
Effect of Au Nanoparticle Agglomeration on SERS Signal Amplification
Authors: Khabarov Kirill , Filalova Emiliia , Nouraldeen Messan , Kameneva Ekaterina , Musaev Andrey , Tikhonov Sergei , Ivanov Victor
Published: February 2023

An analyzed substance’s signal intensity and detection sensitivity in surface-enhanced Raman spectroscopy (SERS) significantly depend on the size and agglomeration degree of nanoparticles (NPs) forming the enhancing structure. Structures were manufactured by aerosol dry printing (ADP), where NPs’ agglomeration depends on printing conditions and additional particle modification techniques. The influence of agglomeration degree on SERS signal enhancement was studied in three types of printed structures using the methylene blue model molecule as an analyte. We demonstrated that the ratio between individual NPs and agglomerates in a studied structure strongly affects SERS signal amplification, and structures formed mainly from non-agglomerated NPs enhance the signal better. In this sense, aerosol NPs modified by pulsed laser radiation provide better results than thermally modified NPs, since in laser modification a larger number of individual NPs is observed due to the absence of secondary agglomeration effects in the gas stream. However, increasing gas flow may minimize the secondary agglomeration, since the time allotted for the agglomeration processes is reduced. In this paper, we show how different NPs’ agglomeration tendencies influence SERS enhancement to demonstrate the process of using ADP to form inexpensive and highly efficient SERS substrates with huge application potential.
Single-Layer Transmissive Chiral Plasma Metasurface with High Circular Polarization Extinction Ratio in Visible Wavelength
Authors: Zhang Ran , Zhang Zhichao , Fan Yuanyi , Zhang Hao , Chu Jinkui
Published: February 2023

Chiral metamaterials are extensively applied in the fields of photoelectric detection, biomedical diagnostics and micro-nano polarization imaging. Currently, single-layer chiral metamaterials are unfortunately limited by several issues, such as a weaker circular polarization extinction ratio and circular polarization transmittance difference. To tackle these issues, a single-layer transmissive chiral plasma metasurface (SCPMs) suitable for visible wavelength is proposed in this paper. Its basic unit is composed of double orthogonal rectangular slots and a spatial π/4 inclined arrangement of the rectangular slot to constitute a chiral structure. Each rectangular slot structure has characteristics that enable the SCPMs to easily achieve a high circular polarization extinction ratio and strong circular polarization transmittance difference. Both the circular polarization extinction ratio and circular polarization transmittance difference of the SCPMs reach over 1000 and 0.28 at a wavelength of 532 nm, respectively. In addition, the SCPMs is fabricated via the thermally evaporated deposition technique and focused ion beam system. This compact structure coupled with a simple process and excellent properties enhances its applicability for the control and detection of polarization, especially during integration with linear polarizers, to achieve the fabrication of a division-of-focal-plane full-Stokes polarimeter.
Highly Porous Carbon Aerogels for High-Performance Supercapacitor Electrodes
Authors: Lee Jong-Hoon , Lee Seul-Yi , Park Soo-Jin
Published: February 2023

In recent years, porous carbon materials with high specific surface area and porosity have been developed to meet the commercial demands of supercapacitor applications. Carbon aerogels (CAs) with three-dimensional porous networks are promising materials for electrochemical energy storage applications. Physical activation using gaseous reagents provides controllable and eco-friendly processes due to homogeneous gas phase reaction and removal of unnecessary residue, whereas chemical activation produced wastes. In this work, we have prepared porous CAs activated by gaseous carbon dioxide, with efficient collisions between the carbon surface and the activating agent. Prepared CAs display botryoidal shapes resulting from aggregation of spherical carbon particles, whereas activated CAs (ACAs) display hollow space and irregular particles from activation reactions. ACAs have high specific surface areas (2503 m2 g−1) and large total pore volumes (1.604 cm3 g−1), which are key factors for achieving a high electrical double-layer capacitance. The present ACAs achieved a specific gravimetric capacitance of up to 89.1 F g−1 at a current density of 1 A g−1, along with a high capacitance retention of 93.2% after 3000 cycles.