bluuebunny/crossref_metadata_2025 huggingface dataset:
Effect of Prior Processing on the Performance of PH 13-8 Mo Stainless Steel Helicopter Components
Authors: Pepi Marc S. , Grendahl Scott M. , Champagne Victor K.
Published: May 2019

The purpose of this investigation was to determine the root cause of the differences noted in the fatigue test data of main rotor spindle assembly retaining rods fabricated from three different vendors, as part of a Second Source evaluation process. ARL performed dimensional verification, accessed overall workmanship, and measured the respective surface roughness of the rods in an effort to identify any discrepancies. Next, mechanical testing was performed, followed by optical and electron microscopy, and chemical analysis. Finally, ARL performed laboratory heat treatments at the required aging temperature and follow-up mechanical testing.
Fatigue Fracture of an Aluminum Main Support Bridge for a Helicopter
Authors: Champagne V.K.
Published: May 2019

This paper summarizes the results of a failure analysis investigation of a fractured main support bridge made of 7075 aluminum alloy from an army helicopter. The part, manufactured by “Contractor IT,” failed component fatigue testing while those of the original equipment manufacturer (OEM) passed. Metallurgical data collected during this investigation indicated that the difference in fatigue life between the components fabricated by IT and by OEM may be attributable to a difference in dimensions at the web where fatigue crack initiation occurred. The webs of the two OEM parts examined had cross-sectional thicknesses significantly larger than the web cross-sectional thicknesses of the IT components. Recommendations included changing the web reference dimension of 0.38 in. to include a tolerance range based upon a fracture mechanics model. Also, the shot peening process should be controlled especially at the critical areas of the web, to assure complete coverage and proper compressive residual stresses.
Ejection Seat Quick-Release Fitting: Quantitative Fractography and Estimation of Local Toughness Using the Topography of the Fracture Surface
Authors: Wolf K.
Published: May 2019

After a quick-release fitting of an ejection seat broke, an investigation was performed to determine the manner and cause of crack propagation. Most fractography-based investigations aim to characterize only qualitative characteristics, such as the fracture orientation and origin position, topology, and details of interactions with microstructural features. The aim of this investigation was to use quantitative fractography as a tool to extract information, including striation spacing and size of the stretched zone, in order to make a direct correlation with fracture mechanic concepts. As the crack propagated, striations were created on the fracture surface as a result of service-induced load changes. The size of the striations were measured to estimate crack propagation rate. Remaining lifetime estimates were also made. The dimensions of plastically stretched zones found at the tips of the cracks were evaluated using electron micrograph stereo image pairs to characterize local fracture toughness. To complete the failure analysis, nondestructive evaluation, metallographic examination, and chemical investigations were carried out. No secondary cracks could be found. Most of the broken parts showed that the microstructure, the hardness, and the chemical composition of the Al-alloy were within the specification, but some of the cracked parts were manufactured using a different material than that specified.
Material-Based Failure Analysis of a Helicopter Rotor Hub
Authors: Wanhill R.J.H.
Published: May 2019

A Lynx helicopter from the Royal Netherlands Navy lost a rotor blade during preparation for take-off. The blade loss was due to failure of a rotor hub arm by fatigue. The arm was integral to the titanium alloy rotor hub. An extensive material based failure analysis covered the hub manufacture, service damage, and estimates of service stresses. There was no evidence for failure due to poor material properties. However, fractographic and fracture mechanics analyses of the service failure, a full scale test failure, and specimen test failures indicated that the service fatigue stress history could have been more severe than anticipated. This possibility was subsequently supported by a separate investigation of the assumed and actual fatigue loads and stresses.
Metallurgical Evaluation of Inner Wall Softening in a Tow Flight Missile Case
Authors: Hickey Charles F.
Published: May 2019

Failure occurred in two TOW flight missile cases in unrelated launchings. After an extensive investigation, it was concluded that stress corrosion was the most likely cause of failure. Subsequent to this conclusion, inner wall softening was observed in an unfired TOW flight missile case. Questions arose as to how the softening occurred and whether or not it had contributed to the failures. This report contains the results of a study which resolved that inner wall softening could not have been present in the failed missile cases.
Failure Investigation of a Structural Component of the Main Landing Gear of a Transport Aircraft
Authors: Abdel-Latif A.M. , Roth M. , Yanishcvsky M.
Published: May 2019

The truck beam of the left main landing gear (MGL) of a Boeing 707 airplane collapsed on the ground just after the aircraft was unloaded and refueled. The investigation revealed that failure was caused by the propagation of an intergranular crack originating from the bottom of the pit. The crack reached the critical size and caused failure by stress-corrosion cracking (SCC) under static loading conditions in service. The failed beam was protected by a well adhering paint system. However, the presence of adequate amounts of corrosion preventive compound films (CPC) on the surfaces of the failed beam could not be conclusively established because of the long term service exposure and presence of lubricants.
Investigating an Aircraft Disaster
Authors: Barer Ralph D. , Sterling Thomas S.
Published: May 2019

Applying general techniques of failure analysis, the authors deduced that an in-flight explosion brought down a passenger plane. Other evidence pinpointed the location of the explosive, an important factor in establishing responsibility.
Failure in Aircraft Parts Made of Ultra-High-Strength Steel
Authors: Holshouser William L.
Published: May 2019

Service failures have occurred in a number of aircraft parts made of quenched and tempered steel heat treated to ultimate tensile strengths of 260,000 to 280,000 psi. Some of these failures have been attributed to “delayed cracking” as a result of hydrogen embrittlement or to stress-corrosion. Because of the serious nature of the failures and because the mechanism of the fracture initiation is not well understood, unusually complete laboratory investigations have been conducted. Three of these investigations are reviewed to illustrate the methods used in studying failures in aircraft parts. The results of the laboratory studies indicate that unusual care is necessary in the processing and fabrication of ultra-high-strength steel and in the design and maintenance of the structures in which it is used.
Helicopter Engine Connecting Rod Failures
Authors: Shah Jivan B.
Published: May 2019

In a helicopter engine connecting rod, high-cycle, low-stress fatigue fractures in bolts and arms progressed about 75% across the section before the final rupture. Factors involved were insufficient specified preload, inadequate tightening during assembly, and engine overspeed. The assigned main causes were design deficiency, improper maintenance during overhaul, and abnormal service operation. The problem can be solved by proper overhauling that ensures bolted assemblies are tightened evenly and accurately, in accordance with recommended torque values. Also, the manufacturer made various modifications, such as a thicker rod, fatigue resistant bolts, and more accurate preload measurements. The configuration of these rods were changed to a tongue-and-groove design to increase service life.
Overheating of Aircraft Engine Cylinders
Authors: Shah Jivan B.
Published: May 2019

Cylinder fatigue can result from abnormal heating in service. Fatigue can be experienced also by piston heads, exhaust valves, and turbosupercharger housings (castings). Pistons from different engines series can sometimes fit, but because of slight design modifications, they may not function properly. Circumferential cracks and fractures near the head-to- barrel junctions have occurred on numerous cylinders of reciprocating piston engines. In most instances, cracks were caused by high cyclic pressures and high temperatures resulting most probably from detonation. At times, fractures or cracks (or both) were also caused by a combination of unfavorable temperature distribution (and possibly excessive pressures around the cylinder barrel), un-nitrided internal surfaces of cylinder barrels, and inadequate thread contours, which caused high stress concentrations at the thread roots. One example of the most common type of cylinder failure is illustrated.
Brittle Fracture of Welds in Aircraft Components
Authors: Shah Jivan B.
Published: May 2019

Two examples involved brittle fracture promoted by small fatigue cracks owing to welding deficiencies. Other parts involving inadequate welding were a ski-wheel axle flange, ski fitting (brackets), and undercarriage shock strut stub assembly. In an attach fitting for an engine mount, weld cracks (severe stress concentrations) formed during repair welding. Cracks were severely oxidized. The main cause was incorrect repair and inadequate inspection of the fitting. In a cast CrNi alloy ski wheel axle, brittle fatigue failure emanated from welding cracks (notches). These welding cracks formed during the fabrication of the axle mounting plate. So-called all-purpose electrodes were used. Thus, the main cause for failure was a manufacturing deficiency-fatigue failure developed because of improper welding during fabrication of the axle. The proper electrode should have been used.
Corrosion Cracking of Aircraft Components
Authors: Shah Jivan B.
Published: May 2019

A 2000-T6 aluminum alloy bracket failed in a coastal environment because corrosive chlorides got between the bracket and attachment bolt. The material used for the part was susceptible to stress corrosion under the service conditions. Cracking may have been aggravated by galvanic action between aluminum alloy bracket and steel bolt. To preclude or minimize recurrences, fittings in service should be inspected periodically by dye penetrant for signs of cracking on the end face and within the fitting hole and protected with a suitable coating to exclude damaging chlorides. Also, a 2000-T6 aluminum alloy swivel fitting experienced intergranular corrosion fracture as the result of stress-accelerated corrosion. Corrosion began because of a loose fit between the aluminum swivel fitting and steel tube assembly, which caused fretting. Inadequate maintenance and/or abnormal service operation may have loosened the fitting.
Hydrogen Embrittlement of Aircraft Components
Authors: Shah Jivan B.
Published: May 2019

Brittle intergranular fracture, typical of a hydrogen-induced delayed failure, caused the failure of an AISI 4340 Cr-Mo-Ni landing gear beam. Corrosion resulting from protective coating damage released nascent hydrogen, which diffused into the steel under the influence of sustained tensile stresses. A second factor was a cluster of non-metallic inclusions which had ‘tributary’ cracks starting from them. Also, eyebolts broke when used to lift a light aircraft (about 7000 lb.). The bolt failure was a brittle intergranular fracture, very likely due to a hydrogen-induced delayed failure mechanism. As for the factors involved, cadmium plating, acid pickling, and steelmaking processes introduce hydrogen on part surfaces. As a second contributing factor, both bolts were 10 Rc points higher in hardness than specified (25 Rc), lessening ductility and notch toughness. A third factor was inadequate procedure, which resulted in bending moments being applied to the bolt threads.
Damaged Propeller Blades
Authors: Shah Jivan B.
Published: May 2019

This report covers case histories of failures in fixed-wing light airplane and helicopter components. In a 2025-T6 or 2219 aluminum alloy propeller blade that failed near the tip, cracks started on the leading edge at surface damage in the critical area-the zone between 4 and 10 in. from the tip of the blade. Incorrect dressing and inadequate pre-flight inspection were the two main causes. Two other types of propeller blade fatigue failures resulted mainly from propeller straightening operations, usually performed after previous blade bending damage. To eliminate blade tip failures, all surface-damaged material should be removed and polished smooth before further flight. The blade should be correctly dressed. Also, the tachometer should be calibrated to ensure the engine/propeller combination is not operated in the critical speed range at normal cruising speeds.
Failures in Landing Gear Spring Legs
Authors: Shah Jivan B.
Published: May 2019

In a spring leg of a main landing gear, large brittle fracture zones indicated a predominately cleavage pattern with some ductile dimples, and a tiny fatigue segment disclosed fine striations. Factors influencing failure were surface decarburization, notch sensitivity of the modified SAE 6150 spring steel, Canada's cold weather which may have had an embrittling effect on the steel, and cumulative fatigue damage from severe landing loads during service life. Replacement with heavier-duty spring legs will probably not eliminate this type of failure, but their use has reduced the number of failures substantially. Precautionary measures recommended to preclude accidents include removal of decarburization, proper operation of main landing gears, and adequate magnetic particle inspection of the legs at the beginning and end of the ski season to detect any fatigue cracks that might develop in attachment holes.
Failure of Steel Missile Launcher Attachment Bolts
Authors: Pepi M.
Published: May 2019

Aircraft missile launcher attachment bolts fabricated from cadmium-coated Hy-tuf steel were found broken. Subsequent analysis of the broken bolts indicated three causes of failure. First, the bolts had been carburized, which was not in conformance with the heat treating requirements. Second, macroetching showed that the bolts has been machined from stock rather than forged, and the threads cut rather than rolled. It was also determined that hydrogen-assisted stress-corrosion cracking also played a part in the failure of the high-strength bolts.
Failure of Maraging Steel Breech Bolt Assemblies
Authors: Pepi M.
Published: May 2019

Breech bolt assemblies from the Gatling guns used on fighter aircraft failed during firing tests. Metallography of the failed components revealed considerable decarburization which resulted in a loss of surface hardness. It was also determined that the maraging steel components were not in the nitrided condition as was required. This resulted in lower wear and fatigue resistance. These components also had a silicon content nearly double of that specified. The high silicon content lowered the notch tensile strength and toughness of the components.
Damaged Section of a Worm Drive
Authors: Kauczor Egon
Published: May 2019

A corrosion resistant chromium nickel steel (X 2 Cr-Ni-Mo 18 10) worm drive used in a chemical plant at 80 deg C and 100 to 200 atm pressure to transport media containing chloride failed during normal operation. Visual inspections showed that the entire surface of the gear was covered with fine branching cracks and was flaking off. Microscopic examination showed that the unetched polished material had disintegrated to an average depth of 1 mm below the surface. A micrograph of the etched surface revealed numerous deformation lines and transgranular cracking. The failure was thus due to stress-corrosion cracking and additional corrosion due to ventilation elements. Because austenitic chromium nickel steels are prone to stress-corrosion cracking, particularly in the presence of chlorine compounds at high temperatures, and because austenitic rust- and acid-resistant steels are prone to smearing and work hardening during machining, it was recommended that these types of steels be machined only with sharp, short tools mounted in rigid structures. In addition, residual stresses should be eliminated by post-process annealing in a protective atmosphere.
Failure of a Weld Seam in a Heat Exchanger of an Ammonia Synthesis Plant
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

A heat exchanger failed five years after going into service in an ammonia synthesis plant. Its container, made of Cr-Mo alloy steel (Material No. 1.7362), operated in an environment that did not exceed 400 deg C or 600 atm of hydrogen partial pressure. X-ray examination revealed a fissure in one of the welded seams, which according to microscopic examination, originated in the base material of the container. Higher magnification revealed a narrow zone adjacent to the weld seam permeated with intergranular cracks, the result of hydrogen attack. It also showed the structure to be completely martensitic. Thus, the failure was due to hardening of the base material during welding, and recommendation was made to temper or anneal the welded regions to reduce the effects of hydrogen under pressure.
Leaking Coil Made of Stainless Steel
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

Austenitic stainless steel (X 10 Cr-Ni-Mo-Ti 18 10, Material No. 1.4571) cooling coils were found leaking in 15 spots after eight weeks of service in an apparatus in which ammonium sulfide solution was converted into ammonium sulfate. The external temperature of the coil was approximately 175 deg C and it was cooled by water at 3 atm. Examination of two sections of the coil showed pinhead size pitting cavities at the exterior surface and partially parallel and partially angled array of fine cracks on external as well as the internal surfaces of the bend. Metallographic examination conducted on longitudinal and transverse sections showed predominantly transcrystalline cracks, originated from the pits at the external surfaces of the pipe. Their appearance suggested they were stress corrosion cracks that occur in austenitic steels under the combined effect of stresses and certain corrosion agents, especially chlorides. If chlorides were absent, hydrogen sulfide which causes similar pitting and is capable of causing cracks could be suspected. Favorable state of stresses, which could be residual or due to heat treating, bending or straightening operations, would be recommended for better behavior of the container.
Examination of Steel Specimens from an Ammonia Synthesis Installation
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

Unalloyed steels and the pure nickel steels frequently used in the past can sustain significant damage from hydrogen attack in ammoniacal environments. The attack causes decarburization that leads to a loosening of the structure due to the precipitation of methane along grain boundaries. It occurs between 200 and 300 deg C, depending on hydrogen pressure. Parts of an apparatus that operate in these types of environments must be checked constantly if they are not made from hydrogen-resistant steel. The results of two such examinations serve to illustrate the challenges.
Investigation of Distribution Manifolds from the Cooling Unit of an Ammonia Synthesis Plant
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

A cooler of an ammonia synthesis plant was destroyed after three years of service due to the rupture of a distribution manifold. Synthesis gas under high pressure and at about 300 deg C, consisting of 10% NH3 and unconverted gas of 25% N2 and 75% H2 content, was water-cooled externally to room temperature in this unit. The fracture had the typical flat-gray fibrous structure of a material destroyed by hydrogen. Specimens for the metallographic investigation showed that the structure appeared to have been loosened by intergranular separations. DVM notched impact specimens from the affected area yielded low specific impact energy values. These are the significant characteristics of hydrogen attack. The attack penetrated to a depth of 13 to 16 mm. It was recommended that the manifolds be made of hydrogen-resistant steel instead of the unalloyed steel used.
Pressure Vessel from a High-Pressure Vibratory Autoclave Burst by Explosion
Authors: Kauczor Egon
Published: May 2019

A forged pressure vessel made from high temperature austenitic steel X8Cr-Ni-MoVNb 16 13 K (DIN 1.4988) failed. The widest part of the burst had fine cracks on the internal wall running longitudinally. When the internal wall was cleaned, numerous even finer cracks were exposed. On the fracture surfaces in this region an irregularly formed zone was visible in the direction of the internal wall and a fibrous oriented fracture zone towards the external wall. The fracture was typical of stress-corrosion cracking in austenitic steels. Vanadium trichloride was present and tensile stresses were of necessity set up by the internal pressure. Stress-corrosion cracking does not occur if one of the basic requirements is lacking. Because the chloride agent and tensile stresses were inevitably present, the only possible way to prevent future reoccurrence is to forge the entire pressure vessel from a material immune to stress-corrosion cracking or to use interchangeable linings of such a material. A nickel alloy could be considered.
Screen Bars Destroyed by Intergranular Corrosion
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

Fragments of screen bars which as structural elements of a condenser had come into contact with cooling water from the mouth of a river were received. The screen bars were made of stainless austenitic Cr-Ni-Mo steel X 5 Cr-Ni-Mo18 10 (Material No. 1.4401). The bars were fractured repeatedly. The ruptures did not occur exclusively or even preferentially at the loops, but just as frequently at locations between them. The mistake made in this case was annealing the steel at a temperature in the critical region. This was probably done to relieve stresses that originated during cold-forming and led to damage by stress corrosion. This would have been the correct method for a ferritic steel, but not austenitic steel, which requires the special heat treatment indicated. When an anneal in the critical region is unavoidable and the indicated additional treatment is impossible or difficult, a type of steel has to be chosen which is resistant to intergranular corrosion.
Leaky Derusting Vessel Made of 18/8 Steel
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

A welded vessel made of acid resistant 18-8 steel used in a derusting operation started to leak after a long period due to the formation of cracks. The vessel was heated from the outside and did not come into direct contact with the flame. It was surrounded by a casing of unalloyed steel. Where the cracks had not eroded away, it was clear they ran transcrystalline, indicative of stress-corrosion cracking. Because the cracks propagated from the outer surface of the vessel, they were not caused by the derusting agent but by the external atmosphere in conjunction with welding stresses. The narrow gap between vessel and mild steel casing may have aggravated the situation in that it hindered ventilation and evaporation of condensation and favored the absorption and concentration of acids and salts. Contact and crevice corrosion due to deposition of rust from the mild steel casing may have contributed.
Failure Analysis of an Ammonia Refrigerant Condenser Tube
Authors: Muralidharan N.G. , Kaul R. , Kasiviswanathan K.V. , Jayakumar T. , Raj B.
Published: May 2019

A detailed failure analysis was conducted on an ammonia refrigerant condenser tube component that failed catastrophically during its initial hours of operation. Evidence collected clearly demonstrated that the weld between a pipe and a dished end contained a sharp unfused region at its root (lack of penetration). Component failure had started from this weld defect. The hydrogen absorbed during welding facilitated crack initiation from this weld defect during storage of the component after welding. Poor weld toughness at the low operating temperature facilitated crack growth during startup, culminating in catastrophic failure as soon as the crack exceeded critical length.
The Failure of Titanium Clad Tube Sheet in Heat Exchanger by Fatigue Cracking and Corrosion
Authors: Hsu C. H.
Published: May 2019

Corrosion failure occurred in a titanium clad tubesheet because of a corrosive tube-side gas-liquid mixture leaking through fatigue cracks in the seal welds at tube-to-tubesheet joints. The tubesheet was a carbon steel plate clad with titanium on the tube side face. The seal weld cracks were initiated by cyclic stress imposed by exchanger tubes. The gas-liquid mixture passed through cracks under tube-side pressure, resulting in severe corrosion of the steel backing plate. The failure started with the loosening of the expanded tube-to-tubesheet joints. Loose joints allowed the exchanger tubes to impose load on seal welds and the shell side cooling water entered the crevice between the tubesheet and the tubes. The cooling water in the crevice caused galvanic reaction and embrittlement of seal welds. Brittle crack opening and crack propagation in seal welds occurred due to the cyclic stress imposed by the tubes. The cyclic stress arised from the thermal cycling of the heat exchanger. The possible effects of material properties on the failure of the tubesheet are discussed.
Bacterial-Induced Corrosion of AISI Type 304 Stainless Steel Tanks
Authors: Kenny Philip J.
Published: May 2019

This investigation involved two AISI 304L acid storage tanks and one AISI 304L spent solvent tank from a sewage treatment facility. After installation, these tanks were hydrostatically tested using sewage effluent. No leaks were found and after a year or two, the tanks were drained and filled with nitric acid in preparation for service. Three weeks later the two acid tanks were found to be leaking from the bottom. Samples from the spent solvent tank revealed that pitting was located in a depressed area near a suction hole, beneath a black residue. It was concluded that the acid tanks failed by chloride-induced pitting initiated by microbial activity. Further, the spent solvent tank failed by a similar, but anaerobic mechanism. The use of the effluent for the hydrostatic test and the failure to remove it and clean and dry the tanks was the primary cause of failure. Localized carbide segregation in the original plate served as preferential corrosion sites. Had the tanks been hydrostatically tested in a proper manner, the pitting may not have occurred.
Failure Analysis for a Carbon Steel Vaporizer Coil
Authors: Lin Y. C. , Ellis F. V.
Published: May 2019

A root cause failure analysis was performed on a vaporizer coil removed from a horizontal forced circulation vaporizer. The carbon steel coil was wound in a right-hand helix with a coil centerline diameter of about 2 m. The vaporizer was gas fired and used Dowtherm A as the heat transfer fluid. Design conditions are based on annular fluid flow to cool the coil wall. NDE, metallographic and fractographic examinations were performed. Numerous, circumferentially oriented, OD initiating cracks were found near the crown for two coils near the non-fired end of the vaporizer. The cracking was confined to the inner diameter of the vaporizer coil at positions from 4:00 to 7:00. The cracking was characterized as transgranular and the fracture surface had beach marks. The failure mechanism was thermal fatigue. The heat transfer calculation predicted that dryout of the coil would occur for coils at the non-fired end of the vaporizer during low flow transients. Dryout results in rapid increase in the tube wall temperature. Thermal cycling of the coil is completed by liquid quenching resulting from resumption of normal flow rates and the return to annular flow. The probable root cause of failure was low flow transient operation.
Failure Analysis of a Steam Reformer Tube
Authors: Caceres P.G. , Habib K.
Published: May 2019

Microstructural examinations on transverse cross sections of a steam reformer tube, showed the presence of large macrovoids elongated in the radial direction and emanating from the internal surface of the tube. The macrovoids were located at the interdendritic regions, and were partially filled by a Mn-Fe bearing chromium oxide film. The areas adjacent to the oxide film were chemically depleted in C, Cr and Mn and rich in Fe and Ni. Associated with this depletion were a large concentration of microvoids. It was suggested that the dissolution of carbides in areas surrounding the macrovoids and the concentration of stresses at their tips, caused extensive localized plastic deformation which led to the formation of microvoids and subsequently to the spalling of the oxide film. The non-protective character of the film induced a progressive deterioration of the grain boundaries properties. Grain boundary sliding and dislocation motion were enhanced, causing a local increase in the steady state strain rate and the premature failure of the tube.
Oxidation Cracking and Residual Creep Life of an Incoloy 800H Bottom Manifold in a Steam Reformer at 800 °C
Authors: Gommans R.J. , Verheesen K.F. , Heerings J.H.
Published: May 2019

During a planned shut-down in 1990 it appeared that the bottom manifold parts made of wrought Incoloy 800H had undergone diametrical expansion of up to 2% due to creep. Further, cracking at the outer diam was found. It was decided to replace these parts. Microscopical investigations showed that the cracking could not be caused by creep. It was found that the cracking was confined to a 4-mm deep coarse-grained zone (ASTM 0-1) at the outer diameter. The cracking appeared to be caused by strain-induced intergranular oxidation. When the cracks reached the fine-grained material, the oxidation-cracks stopped. To determine the residual creep life of the sound (non-cracked) bottom manifold material, iso-stress creep tests were performed. It was found that tertiary creep started at 7% strain. The time-to-rupture was greater than 100,000 h. It was concluded that the bottom manifold (and thus the furnace) could be used safely during the foreseen production period.
Investigation of Worn Chain Links
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

Three links of a chain showing unusually strong wear were examined. Corresponding to the stress, the wear was strongest in the bends of the links, but it was especially pronounced in the bend in which the butt weld seam was located. Investigation showed the links were manufactured from an unkilled carbon-deficient steel, and were case hardened to a depth of 0.8 to 0.9 mm. The peripheral structure at the places not showing wear consisted of coarse acicular martensite with a high percentage of retained austenite. The links therefore were strongly overheated, probably directly heated during case hardening. The butt weld seams were not tight and were covered with oxide inclusions. Given that wear occurred preferentially at the welds it may be concluded that this weld defect contributed to the substantial wear. This leaves unanswered whether these chains could have withstood the high operating stress if they had been welded satisfactorily and hardened correctly, and whether it made any sense to case harden highly stressed chains of this type.
Fractures of Flat Wire Conveyor Belt Links of Glass Annealing Furnaces
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

The cross bars of conveyor belt links that served to transport glass containers through a stress relief furnace fractured in many cases. They consisted of wires of 5 mm diam made of low-carbon Siemens-Martin steel, while the interwoven longitudinal bars were made of strip steel of 4 x 2 sq mm. The furnace temperature was said to be 500 deg C. In addition to the fractures they also showed many more or less advanced cracks. These occurred in the circumferential grooves that recurred at regular intervals. The fractures were abraded and oxidized. They could have been fatigue fractures. The fracture probably was induced by the pressing-in or abrading of the sharp steel band edges into the surface of the cross bars. Torsion fatigue fractures may have started from these notches. Relaxation then contributed positively through recovery and recrystallization. Such damage occurs less frequently in round wire conveyor belt links because the round wire neither impresses so sharply nor abrades against the cross bars, and it also exerts less torsion than the flat wire.
Failure Analysis of Wire Rope
Authors: Miller Brett A.
Published: May 2019

Mechanical properties of wire ropes, their chemical composition, and the failure analysis process for them are described. The wires are manufactured from high-carbon, plain carbon steel, with high-strength ropes most often manufactured from AISI Grade 1074. During visual failure examination, the rope, strand, and wire diameters should all be measured. Examination should also address the presence or absence of lubricant, corrosion evidence, and gross mechanical damage. Failed wires can exhibit classic cup-and-cone ductile features, flat fatigue features, and various appearances in-between. However, wires are often mechanically damaged after failure. Most nondestructive evaluation (NDE) techniques are not applicable to wire rope failures. Electron microscope fractography of fracture surfaces is essential in failure analysis. Fatigue is the most important fracture mode in wire ropes. Metallographic features of wire ropes that failed because of ductile overload and fatigue are described.
An Analysis of Six Fatigue Failures in Cranes
Authors: Williams W. M. , Firth Mark
Published: May 2019

Crane collapse due to bolt fatigue and fatigue failure of a crane support column, crane tower, overhead yard crane, hoist rope, and overhead crane drive shaft are described. The first four examples relate to the structural integrity of cranes. However, equipment such as drive and hoist-train components are often subject to severe fatigue loading and are perhaps even more prone to fatigue failure. In all instances, the presence of fatigue cracks at least contributed to the failure. In most instances, fatigue was the sole cause. Further, in each case, with regular inspection, fatigue cracks probably would have been detected well before final failure.
Fractured Valve Spring
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

A steel valve spring meeting Steel-Iron-Test 1570 fractured during the high-stress condition of the operation of its valve. Metallographic examination of a transverse section adjacent to the fracture and a longitudinal section through the crack showed the steel was free of major defects and was of high purity, although a number of minor surface defects such as rolling laps were found. The spring was heat treated and its surface strengthened by shot-peening, but the surface was also decarburized to a depth of approximately 0.03 mm which resulted in a lowering of the surface hardness. The fracture of this valve spring is therefore primarily due to surface defects, and secondly perhaps also to weak surface decarburization. No recommendation resulted from the investigation except to note that comparatively minor effects suffice to cause fractures in highly stressed springs.
Broken Full Lift Disk of a Safety Valve
Authors: Kauczor Egon
Published: May 2019

A full lift disk, made of die cast brass, which served as a lifting aid in a safety valve, had cracked in service at a number of locations in the vicinity of the threaded hole. During microscopic examination, agglomeration of oxide inclusions were noted in the region of the cracks. Because the die cast brass was alloyed with aluminum, these inclusions consisted predominantly of aluminum oxide. The tolerable limit in pores and oxide inclusions was greatly exceeded in the lift disk under examination. Above all, the numerous oxide skins disrupted the cohesion of the microstructure and were primarily responsible for the failure of the lift disk.
Destroyed Needle Bearing of a Packing Machine
Authors: Naumann Friedrich Karl , Spies Ferdinand
Published: May 2019

A needle bearing from a filling and seating machine for milk cartons became unusable due to corrosion and fracture of a ring after only four weeks of operation of the machine in a Finnish milk packing plant. These bearings were subject to corrosion by water condensates in this type of environment because of constant temperature changes, and they normally are replaced after eight months. The bearings were lubricated by a molybdenum sulfide paste. Judging by their structure the needles probably consisted of ball bearing steel. They showed corroded initial cracks of the pitting type, i.e., shear-fatigue fractures due to excessive surface pressure. The needles too were overstressed by compression. It seemed that the higher pressure necessary for the pressing of thicker paper accelerated the corrosion, which lead to the crack initiations of the parts and possibly also to impaired lubrication. The machine manufacturer therefore switched to bearings with shells of a complex bronze.
A Survey of the Causes of Failure of Rolling Bearings
Authors: Hutchings F.R.
Published: May 2019

Factors which may lead to premature roller bearing failure in service include incorrect fitting, excessive pre-load during installation, insufficient or unsuitable lubrication, over-load, impact load vibration, excessive temperature, contamination by abrasive matter, ingress of harmful liquids, and stray electric currents. Most common modes of failure include flaking or pitting (fatigue), cracks or fractures, creep, smearing, wear, softening, indentation, fluting, and corrosion. The modes of failure are illustrated with examples from practice.
Wear Failure of a Leaded Bronze Bearing: Correlation Between Plant Experience and Laboratory Wear Test Data
Authors: Ahsan Q. , Haseeb A.S.M.A. , Haque E. , Celis J.P.
Published: May 2019

This paper describes an investigation on the failure of a large leaded bronze bearing that supports a nine-ton roller of a plastic calendering machine. At the end of the normal service life of a good bearing, which lasted for seven years, a new bearing was installed. However the new one failed catastrophically within a few days, generating a huge amount of metallic wear debris and causing pitting on the surface of the cast iron roller. Following the failure, samples were collected from both good and failed bearings. The samples were analyzed chemically and their microstructures examined. Both samples were subjected to accelerated wear tests in a laboratory type pin-on-disk apparatus. During the tests, the bearing materials acted as pins, which were pressed against a rotating cast iron disk. The wear behaviors of both bearing materials were studied using weight loss measurement. The worn surfaces of samples and the wear debris were examined by light optical microscope, SEM, and energy-dispersive x-ray microanalyzer. It was found that the laboratory pin-on-disk wear data correlated well with the plant experience. It is suggested that the higher lead content ~18%) of the good bearing compared with 7% lead of the failed bearing helped to establish a protective transfer layer on the worn surface. This transfer layer reduced metal-to-metal contact between the bearing and the roller and resulted in a lower wear rate. The lower lead content of the failed bearing does not allow the establishment of a well-protected transfer layer and leads to rapid wear.
Failure Analysis of Helical Suspension Springs under Compressor Start/Stop Conditions
Authors: Zaccone M.A.
Published: May 2019

During testing of compressors under start/stop conditions, several helical suspension springs failed. The ensuing failure investigation showed that the springs failed due to fatigue. The analysis showed that during start/stop testing the springs would undergo both a lateral and axial deflection, greatly increasing the torsional stresses on the spring. To understand the fatigue limits under these test conditions, a bench test was used to establish the fatigue strength of the springs. The bench tests showed that the failed springs had an unacceptable surface texture that reduced the fatigue life. Based on an understanding of the compressor motion, a Monte Carlo model was developed based on a linear damage theory to predict the fatigue life of the springs during start/stop conditions. The results of this model were compared to actual test data. The model showed that the design was marginal even for springs with acceptable surface texture. The model was then used to predict the fatigue life requirements on the bench test such that the reliability goals for the start/stop testing would be met, thus reducing the risk in qualifying the compressor.
Microstructural Analysis of the Brass Seat of a Valve from the 1907 Steam Tug ‘Hercules’
Authors: Brooks Charlie R. , Monday Dean
Published: May 2019

The steam tug Hercules was an ocean-going and bay tug for 55 years before being retired. It is now being restored by the National Park Service. A broken steam valve was obtained for microstructural examination. The body was gray cast iron, and the stem and seat were brass. The examination centered on corrosion of the brass components. The seat and shaft were alpha brass, with a hardness of 64 and 79 DPH, respectively. A nut held the shaft onto the seat, and was alpha-beta brass with a hardness of 197 DPH. Welded on the end of the shaft was a ring of hard (DPH 294) alpha-beta brass, which seated against the nut. The brass seat and stem show little corrosion. However, the alpha-beta brass nut and welded tip showed extensive dezincification. This process of removal of Zn and the retention of Cu began in the high Zn beta phase, but eventually both phases were attacked. The depth of penetration was consistent with dezincification rates reported in the literature for such brasses in salt water if the valve had been in service about 55 years.
Metallographic Characterization of Stress Corrosion Cracking in High Strength Bolts
Authors: Magner S.H. , Weins W.N.
Published: May 2019

Diagnosis of environmentally induced failures is greatly facilitated by metallographic analysis. As an example, a failure analysis of ASTM A574 material grade bolts is presented. The bolts served as bonnet screws in underground valves and failed due to stress-corrosion cracking. Metallographic methods were used to diagnose and provide solutions for the service failure. Included are photos showing crack propagation morphology and fracture surface appearance.
Failure of 17-4 PH Stainless Steel Bolts on a Titan Space Launch Vehicle
Authors: Raymond Louis , Kendall Ernest G.
Published: May 2019

Several stainless steel bolts used on a Titan Space Launch Vehicle broke at the shank and failure was attributed to stress-corrosion cracking. But results could not be duplicated in the laboratory with salt-solution immersion tests until the real culprit was established: the secondary effect of galvanic coupling, hydrogen embrittlement.
Fractography of Steel Drive Cables
Authors: Shemenski R. M.
Published: May 2019

Drive cables from a rubber processing machine were failing in less than 8 h of operation, the expected service life being much greater than 100 h. Comparison cables were tested to failure under known stress conditions, including tensile overload, torsional loading, reversed bending alternating stress, and buckling (compressive) cyclic loading. The mode of failure was found to be reversed bending fatigue caused by drive cables moving over guide pulleys of small radii. Modifications of the machinery and drive cable system were suggested.
Failure of Electric Motor Ball Bearing
Authors: Walton H.W.
Published: May 2019

Incorrect grounding of an electric motor resulted in electric current passing through a 52100 steel ball bearing and caused multiple arcing between the rolling elements. The multiple arcing developed a pattern on the outer race known as ‘fluting’. A section of ball race outer showed the distinct banding (fluting) resulting from spark discharges while the bearing was rotating. The severe distress of the surface resulted in unacceptable levels of vibration. An SEM photograph of the banded regions showed smoothing of the asperities from continued operation is evident. In the craters the residue of partial melting was seen.
Stress-Corrosion Cracking of a Brass Radiator Coil
Authors: Ogden Paul
Published: May 2019

An interstage radiator gas coil began leaking after only 45 days of service. The original brass coil with several aluminum fins was replaced three times but each replacement lasted less than a day. After removing the fins, leaks were found at circumferential cracks. A section of a tube was removed and split, revealing a series of cracks, evenly spaced. Crack spacing coincided with fin spacing, indicating that stresses incurred during installation of the fins promoted failure. Metallographic examination showed intergranular, branched cracking, characteristic of stress corrosion failures, with the cracks starting on the inside surfaces of the tubes. There was no known corrosive agent in the system, and no other corrosion damage could be found. Qualitative tests and spectrographic analysis gave a positive indication for mercury. The spacing of the cracks, the branched intergranular cracking, the rapid failure, and presence of mercury led to the conclusion of stress-corrosion cracking. It was impossible to remove mercury from the system so carbon steel coils were substituted for the brass ones. The carbon steel coils gave failure-free service for over nine years.
Corrosion-Erosion of a Carbon Steel Choke Body
Authors: Ogden Paul
Published: May 2019

A wall section of a carbon steel choke body in gas service at 4400 psig blew out three months after the use of a corrosion inhibitor was stopped. Corrosion damage occurred in ripples, leaving both smoothly polished and unattacked areas. The corrodent in condensate wells was principally carbon dioxide dissolved in water condensed from the gas stream, with organic acids possibly an aggravating factor. A gas analysis showed no other corrosive agents. No metallurgical or fabrication defects were found in the carbon steel part. The mode of attack was corrosion-erosion, caused by the corrosive, high velocity gas flow. The corrosion rate of either the inhibited or uninhibited gas stream was too high for equipment in high pressure gas service. Type 410 (12% Cr) stainless steel was recommended for the choke bodies because other equipment such as valves made of type 410 showed no evidence of corrosion damage after three years' exposure. This change was made five years ago and there have been no failures since.
Stress Corrosion Cracking Failures in Components Made of Austenitic Chromium Nickel Steels
Authors: Kauczor Egon
Published: May 2019

Practical examples of stress-corrosion cracking (SCC) and methods for its prevention were presented. Cracks in chloride-sensitive austenitic steels were very branched and transcrystalline. Etched cross sections of molybdenum-free samples showed chloride-induced cracks running out of the pitted areas. Alternatively polishing and etching micro-sections for viewing at high magnification made crack detail more visible. Optical and scanning electron micrographs showed cracking in austenitic cast steel and cast iron due to both internal tensile and critical residual stresses; the latter causes flake-like spalling. Measures to prevent SCC include stress reduction, use of austenitic steels or nickel alloys not susceptible to grain boundary attack, use of ferritic chromium steels, surface slag removal, control of temperature and chloride concentration, and cathodic protection.