bluuebunny/crossref_metadata_2025 huggingface dataset:
Ceramic Scaffolds for Bone Augmentation: Design and Characterization with SEM and Confocal Microscopy
Authors: Gabor Alin Gabriel , Duma Virgil-Florin , Fabricky Mihai M. C. , Marsavina Liviu , Tudor Anca , Vancea Cosmin , Negrea Petru , Sinescu Cosmin
Published: July 2022

Bone scaffolds must fulfil numerous and sometimes contradictory characteristics: biocompatibility, bioactivity, high porosity, and appropriate mechanical strength. To tackle some of these issues, this study has several aims for the development of such scaffolds for dentistry applications: (i) to utilize appropriate materials (ceramics and sponges) and to introduce a novel, potentially performant ceramic material; (ii) to characterize the obtained scaffolds by using a range of methods; (iii) to compare and to correlate the assessment results with the scope to validate them reciprocally. There are two commercially available dental ceramics (i.e., Ceramco iC Natural Enamel (E) and Ceramco iC Natural Dentine (D), (DeguDent GmbH, Hanau-Wolfgang, Deutschland)) that are considered, as well as a new-developed porcelain (ceramic C). To obtain porous structures of scaffolds, each ceramic is introduced in two different sponges: a denser one, green (G) and a less dense one, blue (B). A total of 60 samples are manufactured and divided in six study groups, obtained by combining the above materials: GE, BE, GD, BD, GC, and BC (where the first letter represents the sponge type and the second one the utilized ceramic). Several methods are applied to characterize their chemical composition, as well as their macro- and micro-porosity: X-ray Diffraction (XRD), apparent porosity measurements, scanning electronic microscopy (SEM), and confocal microscopy (CM). The latter two methods image the inner (porous) and the outer/cortical (denser) areas of the samples. The results show a good porosity (i.e., dimensions and uniformity of pores) of around 65% for the final group BC, with satisfactory values of around 51% for BD and GC. A certain correlation is made between SEM, CM, and the apparent porosity results. The biocompatibility of the new ceramic C is demonstrated. Finally, a necessary trade-off is made with the mechanical strength of the obtained scaffolds, which was also evaluated. From this point of view, Group BD has the highest compressive strength of around 4 MPa, while Group BC comes second, with around 2 MPa. This trade-off between porosity and mechanical strength suggests a choice between Groups BC and BD, which are the best with regard to the porosity and mechanical strength criterium, respectively.
Removal of Cr(VI) from Wastewater Using Graphene Oxide Chitosan Microspheres Modified with α–FeO(OH)
Authors: Liu Yunquan , Shan Huimei , Zeng Chunya , Zhan Hongbin , Pang Yanyue
Published: July 2022

Graphene oxide and chitosan microspheres modified with α–FeO(OH) (α–FeO(OH)/GOCS) are prepared and utilized to investigate the performance and mechanism for Cr(VI) removal from aqueous solutions and the possibility of Fe secondary pollution. Batch experiments were carried out to identify the effects of pH, mass, and volume ratio (m/v), coexisting ions, time (t), temperature (T), and Cr(VI) initial concentration (C0) on Cr(VI) removal, and to evaluate adsorption kinetics, equilibrium isotherm, and thermodynamics, as well as the possibility of Fe secondary pollution. The results showed that Cr(VI) adsorption increased with C0, t, and T but decreased with increasing pH and m/v. Coexisting ions inhibited Cr(VI) adsorption, and this inhibition increased with increasing concentration. The influence degrees of anions and cations on the Cr(VI) adsorption in descending order were SO42− > PO42− > NO3− > Cl− and Ca2+ > Mg2+ > Mn2+, respectively. The equilibrium adsorption capacity of Cr(VI) was the highest at 24.16 mg/g, and the removal rate was 97.69% under pH = 3, m/v = 1.0 g/L, T = 298.15 K, and C0 = 25 mg/L. Cr(VI) adsorption was well fitted to a pseudo-second-order kinetic model and was spontaneous and endothermic. The best fit of Cr(VI) adsorption with the Langmuir and Sips models indicated that it was a monolayer and heterogeneous adsorption. The fitted maximum adsorption capacity was 63.19 mg/g using the Sips model under 308.15 K. Cr(VI) removal mainly included electrostatic attraction between Cr(VI) oxyanions with surface Fe–OH2+, and the adsorbed Cr(VI) was partially reduced to Cr(III) and then precipitated on the surface. In addition, there was no Fe secondary pollution during Cr(VI) adsorption.
Effect of the Type of Inorganic Binder on the Microstructure and Properties of AlSi7Mg Alloy Castings Made by Ablation Casting Technology
Authors: Kamińska Jadwiga , Angrecki Michał , Puzio Sabina
Published: July 2022

The results of studies on the effect that the type of binder and casting technology exert on the microstructure and properties of AlSi7Mg alloy castings are discussed in this paper. Comparative tests were carried out on three casting manufacturing technologies, i.e., conventional sand mould casting and cooling process, metal mould (die) casting, and sand mould casting with ablation breakdown of mould and cooling of castings. Moulds were made from four different sand mixtures with inorganic binders hardened by various technologies. The microstructure of test castings was examined at three different levels, i.e., in the upper part, central part, and lower part of each casting. The tensile test at room temperature was carried out in accordance with standards. The experimental results showed differences in the microstructure of castings. The differences resulted from changes in the crystallisation path due to the use of three different casting technologies, ensuring different rates of heat dissipation from castings; they were also due to the shape of castings. It has been shown that castings made by ablation technology are characterised by a high degree of the microstructure refinement (SDAS reduced by 18–30%), which gives higher strength properties than the properties of castings made in conventional sand moulds. Samples taken from castings made by the ablation technology in moulds with phosphate binder and microwave-hardened geopolymer binder were characterised by the mechanical properties comparable to gravity die castings.
Evaluation of Solidified Wastewater Treatment Sludge as a Potential SCM in Pervious Concrete Pavements
Authors: Govedarica Ognjen , Aškrabić Marina , Hadnađev-Kostić Milica , Vulić Tatjana , Lekić Branislava , Rajaković-Ognjanović Vladana , Zakić Dimitrije
Published: July 2022

Waste and recycled materials have recently been used in the construction industry to comply with the principles of circular economy and sustainable development. The aim of this paper is to examine the potentials of solidified wastewater treatment sludge (SWWTS) as a supplementary cementitious material (SCM) in the production of lightweight pervious concrete pavers (LWPCP) suitable for pedestrian trails and rooftops (green) that comply with EU standards. Detailed characterization of SWWTS was performed, in order to understand its properties related to application as SCM, which led to the conclusion that it may be applied only as a filler, having 89.5% of Ca(OH)2. After thorough characterization, LWPCP samples were prepared and testing of physical and mechanical properties was conducted. The research showed that partial replacement of cement with SWWTS led to the decrease of all mechanical properties, ranging between 3.91 and 5.81 MPa for compressive strength and 0.97 to 1.23 MPa for flexural strength. However, all of the investigated mixtures showed a value higher than 3.5 MPa, which was defined as the lowest compressive strength in the range of pervious concrete properties. The addition of SWWTS led to a slight decrease in bulk density of the mixtures and an increase in water absorption. This could be explained by the reduction in hydration products that would fill in the micropores of the matrix, since SWWTS showed no pozzolanic reactivity. Pore sizes that prevail in the tested binder matrices are in accordance with the results measured on ordinary pervious concrete (the largest fraction of pores had a diameter between 0.02 and 0.2 μm). Low thermal conductivity nominates produced pavers as potential rooftop elements.
Editorial for “Mechanical Behavior of Concrete Materials and Structures: Experimental Evidence and Analytical Models”
Authors: De Domenico Dario , Bernardo Luís F. A.
Published: July 2022

Concrete is one of the most widespread materials in the civil engineering field due to its versatility for both structural and non-structural applications depending on the density range, competitiveness in terms of durability and manufacturing costs, as well as ease in finding raw constituent elements [...]
Dynamic Modeling, Workspace Analysis and Multi-Objective Structural Optimization of the Large-Span High-Speed Cable-Driven Parallel Camera Robot
Authors: Su Yu , Qiu Yuanying , Liu Peng , Tian Junwei , Wang Qin , Wang Xingang
Published: July 2022

Since most of the cable-driven parallel manipulators (CDPMs) are small in dimension or low in speed, the self-weight or inertia of the cable is neglected when dealing with the problems of kinematics, dynamics and workspace. The cable is treated as a massless straight line, and the inertia of the cable is not discussed. However, the camera robot is a large-span high-speed CDPM. Thus, the self-weight and inertia of the cable cannot be negligible. The curved cable due to the self-weight is modeled as a catenary to accurately account for its sagging effect. Moreover, the dynamic model of the camera robot is derived by decomposing the motion of the cable into an in-plane motion and an out-plane motion, based on which an iterative-based tension distribution algorithm and a workspace generation algorithm are presented. An optimization model is presented to simultaneously improve the workspace volume, anti-wind disturbance ability and impulse of tensions on the camera and pan–tilt device system (CPTDS) by selecting the proper optimal variables under the linear and nonlinear constraints. An improved genetic algorithm (GA) is proposed, and the simulation results demonstrate that the improved GA offers a stronger ability in global optimization compared to the standard genetic algorithm (SGA). The ideal-point method is employed to avoid the subjective influence of the designer when performing the multi-objective optimization, and a remarkable improvement of the performance is obtained through the optimization. Furthermore, the distribution characteristics of the optimization objects are studied, and some valuable conclusions are summarized, which will provide some valuable references in designing large-span high-speed CDPMs.
A Review of Key Technologies for Friction Nonlinearity in an Electro-Hydraulic Servo System
Authors: Gao Bingwei , Shen Wei , Zheng Lintao , Zhang Wei , Zhao Hongjian
Published: July 2022

In a high-precision servo system, the nonlinear friction link is the key factor affecting the system performance. Reasonable solving of the friction link in servo systems has become a focus of current research. This paper summarizes the friction nonlinearity that affects the control performance of servo systems. First, the characteristics of friction are summarized, and the advantages and disadvantages of typical friction models in recent years are analyzed. Subsequently, existing friction model parameter identification methods are introduced and evaluated. On this basis, the development level of the friction nonlinear control strategy is analyzed from three aspects: friction model-based control, friction model-free control, and compound control. Finally, the objective advantages and disadvantages of the existing technology are summarized, and the future development direction of the friction model and selection reference for the nonlinear friction control strategy are comprehensively discussed.
Matrix Summability of Walsh–Fourier Series
Authors: Goginava Ushangi , Nagy Károly
Published: July 2022

The presented paper discusses the matrix summability of the Walsh–Fourier series. In particular, we discuss the convergence of matrix transforms in L1 space and in CW space in terms of modulus of continuity and matrix transform variation. Moreover, we show the sharpness of our result. We also discuss some properties of the maximal operator t∗(f) of the matrix transform of the Walsh–Fourier series. As a consequence, we obtain the sufficient condition so that the matrix transforms tn(f) of the Walsh–Fourier series are convergent almost everywhere to the function f. The problems listed above are related to the corresponding Lebesgue constant of the matrix transformations. The paper sets out two-sides estimates for Lebesgue constants. The proven theorems can be used in the case of a variety of summability methods. Specifically, the proven theorems are used in the case of Cesàro means with varying parameters.
Modelling and Fault Detection for Specific Cavitation Damage Based on the Discharge Pressure of Axial Piston Pumps
Authors: Xia Shiqi , Xia Yimin , Xiang Jiawei
Published: July 2022

Cavitation will increase the leakage and discharge pressure fluctuation of axial piston pumps. In particular, specific cavitation damage may aggravate the pressure impact and performance degradation. The influence of the specific cavitation damage on the discharge pressure is unclear, and the need for fault detection of this damage is urgent. In this paper, we propose a discharge pressure-based model and fault detection methodology for the specific cavitation damage of axial piston pumps. The discharge pressure model with specific damage is constructed using a slender hole. The simulation model is solved through numerical integration. Experimental investigation of cavitation damage detection is carried out. Discharge pressure features in the time domain and frequency domain are compared. The results show that waveform distortions, spectrum energy relocation, generation of new frequencies and sidebands can be used as features for fault detection regarding the specific cavitation damage of axial piston pumps.
Regional Variety of Reduction in Retinal Thickness of Diabetic Macular Edema after Anti-VEGF Treatment
Authors: Yamada Yutaka , Takamura Yoshihiro , Matsumura Takehiro , Gozawa Makoto , Morioka Masakazu , Inatani Masaru
Published: July 2022

Background and Objectives: The presence of refractory cases resistant to anti-vascular endothelial growth factor (VEGF) therapy for diabetic macular edema (DME) is a problem in clinical practice. This study aimed to explore the less responsive area of optical coherence tomography (OCT) 3D map the characteristics of naïve DME cases after their first anti-VEGF. Materials and Methods: In 46 patients with DME who received an intravitreal injection of anti-VEGF agents, retinal thickness in 100 sections of the macular area was measured by 3D-mapping mode using OCT before and 1 month after injection. The density of the microaneurysm (MA) was calculated using merged images of the OCT map and fluorescein angiography. Results: One month after injection, the central retinal thickness significantly decreased (p < 0.0001). In severe edema (retinal thickness more than 500 µm), the area percentages with a reduction rate of the retinal thickness greater than 30% and less than 5% were 6.4 ± 6.6% and 10.1 ± 4.6%, respectively. The reduction rate of the retinal thickness varied from section to section. The mutual distance between the areas of maximum thickness before and after the injection averaged 1.22 ± 0.62 mm apart. The reduction rate of retinal thickness in the thickest region before injection was significantly higher (p = 0.02), and that in the thickest region after injection was lower (p = 0.001) than in the other regions. MA density in the residual edema was significantly higher than in the edema-absorbed area (p = 0.03). Conclusion: DME has areas that show low response to the reduction in retinal thickness with anti-VEGF therapy. A high density of MA may be associated with this pathogenesis.
Associations between Workers’ Health and Working Conditions: Would the Physical and Mental Health of Nonregular Employees Improve If Their Income Was Adjusted?
Authors: Nishikitani Mariko , Nakao Mutsuhiro , Inoue Mariko , Tsurugano Shinobu , Yano Eiji
Published: July 2022

Precarious employment can negatively affect health, but workers may be healthy if they earn enough income. This study uses equivalent disposable income and examines the interaction between income classes and employment types to clarify whether workers’ health improves as the income classes rise. In Japan, nonstandard workers, called nonregular employees, have remained high since 2013. Therefore, using data from the national cross-sectional Comprehensive Survey of Living Conditions 2013, an official survey performed in Japan, we targeted a sample of employees aged 18 to 45 who graduated during the economic recession. Our final sample included 8282 employees (4444 males and 3838 females). The health (general and mental) status indicators used the dichotomized self-rated health and scores of the K6 questionnaires scored in the national survey. The association between income and health was almost proportional. Female workers tended to improve their health as their income class increased; however, this tendency was not observed in male workers, especially nonregular employees. Although the associations were weakened by added income information on the regression models, nonregular employees always showed inferior health to regular employees. The health status of nonregular employees, especially female nonregular employees, is statistically significantly lower than that of regular employees, even when the economic class is similar. In conclusion, improving low incomes for nonregular employees could improve health challenges, but income alone may not result in the same health status for regular and nonregular employees.
Impact of Leavening Agent and Wheat Variety on Bread Organoleptic and Nutritional Quality
Authors: Mietton Lauriane , Samson Marie-Françoise , Marlin Thérèse , Godet Teddy , Nolleau Valérie , Guezenec Stéphane , Segond Diego , Nidelet Thibault , Desclaux Dominique , Sicard Delphine
Published: July 2022

Leavened bread can be made with different wheat varieties and leavening agents. Several studies have now demonstrated that each of these factors can play a role in bread quality. However, their relative impact in artisanal bread making remains to be elucidated. Here, we assessed the impact of two wheat varieties as well as the impact of sourdoughs and yeasts on multiple components of bread organoleptic and nutritional quality. Using a participatory research approach including scientists and bakers, we compared breads leavened with three different sourdoughs and three different commercial yeasts as well as a mix of sourdough and yeast. Breads were made from two wheat varieties commonly used in organic farming: the variety “Renan” and the landrace “Barbu”. Except for bread minerals contents that mostly depended on wheat variety, bread quality was mostly driven by the fermenting agent. Sourdough breads had lower sugar and organic acids contents. These differences were mostly attributable to lower amounts of maltose and malate. They also had a higher proportion of soluble proteins than yeast breads, with specific aroma profiles. Finally, their aroma profiles were specific and more diverse compared to yeast breads. Interestingly, we also found significant nutritional and organoleptic quality differences between sourdough breads. These results highlight the value of sourdough bread and the role of sourdough microbial diversity in bread nutritional and organoleptic quality.
Paraprobiotics and Postbiotics of Lactobacillus delbrueckii CIDCA 133 Mitigate 5-FU-Induced Intestinal Inflammation
Authors: Batista Viviane Lima , De Jesus Luís Cláudio Lima , Tavares Laísa Macedo , Barroso Fernanda Lima Alvarenga , Fernandes Lucas Jorge da Silva , Freitas Andria dos Santos , Americo Monique Ferrary , Drumond Mariana Martins , Mancha-Agresti Pamela , Ferreira Enio , Laguna Juliana Guimarães , Alcantara Luiz Carlos Júnior , Azevedo Vasco
Published: July 2022

Intestinal mucositis is a commonly reported side effect in oncology practice. Probiotics are considered an excellent alternative therapeutic approach to this debilitating condition; however, there are safety questions regarding the viable consumption of probiotics in clinical practice due to the risks of systemic infections, especially in immune-compromised patients. The use of heat-killed or cell-free supernatants derived from probiotic strains has been evaluated to minimize these adverse effects. Thus, this work evaluated the anti-inflammatory properties of paraprobiotics (heat-killed) and postbiotics (cell-free supernatant) of the probiotic Lactobacillus delbrueckii CIDCA 133 strain in a mouse model of 5-Fluorouracil drug-induced mucositis. Administration of paraprobiotics and postbiotics reduced the neutrophil cells infiltrating into the small intestinal mucosa and ameliorated the intestinal epithelium architecture damaged by 5-FU. These ameliorative effects were associated with a downregulation of inflammatory markers (Tlr2, Nfkb1, Il12, Il17a, Il1b, Tnf), and upregulation of immunoregulatory Il10 cytokine and the epithelial barrier markers Ocln, Cldn1, 2, 5, Hp and Muc2. Thus, heat-killed L. delbrueckii CIDCA 133 and supernatants derived from this strain were shown to be effective in reducing 5-FU-induced inflammatory damage, demonstrating them to be an alternative approach to the problems arising from the use of live beneficial microorganisms in clinical practice.
Antibiotic Resistance Properties among Pseudomonas spp. Associated with Salmon Processing Environments
Authors: Thomassen Gunn Merethe Bjørge , Reiche Thorben , Tennfjord Christine Eikås , Mehli Lisbeth
Published: July 2022

Continuous monitoring of antimicrobial resistance in bacteria along the food chain is crucial for the assessment of human health risks. Uncritical use of antibiotics in farming over years can be one of the main reasons for increased antibiotic resistance in bacteria. In this study, we aimed to classify 222 presumptive Pseudomonas isolates originating from a salmon processing environment, and to examine the phenotypic and genotypic antibiotic resistance profiles of these isolates. Of all the analyzed isolates 68% belonged to Pseudomonas, and the most abundant species were Pseudomonas fluorescens, Pseudomonas azotoformans, Pseudomonas gessardii, Pseudomonas libanesis, Pseudomonas lundensis, Pseudomonas cedrina and Pseudomonas extremaustralis based on sequencing of the rpoD gene. As many as 27% of Pseudomonas isolates could not be classified to species level. Phenotypic susceptibility analysis by disc diffusion method revealed a high level of resistance towards the antibiotics ampicillin, amoxicillin, cefotaxime, ceftriaxone, imipenem, and the fish farming relevant antibiotics florfenicol and oxolinic acid among the Pseudomonas isolates. Whole genome sequencing and subsequent analysis of AMR determinants by ResFinder and CARD revealed that no isolates harbored any acquired resistance determinants, but all isolates carried variants of genes known from P. aeruginosa to be involved in multidrug efflux pump systems.
Nitrate Addition Increases the Activity of Microbial Nitrogen Removal in Freshwater Sediment
Authors: Cai Min , Hong Yiguo , Wu Jiapeng , Moore Selina Sterup , Vamerali Teofilo , Ye Fei , Wang Yu
Published: July 2022

Denitrification and anammox occur widely in aquatic ecosystems serving vital roles in nitrogen pollution removal. However, small waterbodies are sensitive to external influences; stormwater runoff carrying nutrients and oxygen, flows into waterbodies resulting in a disruption of geochemical and microbial processes. Nonetheless, little is known about how these short-term external inputs affect the microbial processes of nitrogen removal in small waterbodies. To investigate the effects of NO3−, NH4+, dissolved oxygen (DO) and organic C on microbial nitrogen removal in pond sediments, regulation experiments have been conducted using slurry incubation experiments and 15N tracer techniques in this study. It was demonstrated the addition of NO3− (50 to 800 μmol L−1) significantly promoted denitrification rates, as expected by Michaelis-Menten kinetics. Ponds with higher NO3− concentrations in the overlying water responded more greatly to NO3− additions. Moreover, N2O production was also promoted by such an addition of NO3−. Denitrification was significantly inhibited by the elevation of DO concentration from 0 to 2 mg L−1, after which no significant increase in inhibition was observed. Denitrification rates increased when organic C was introduced. Due to the abundant NH4+ in pond sediments, the addition demonstrated little influence on nitrogen removal. Moreover, anammox rates showed no significant changes to any amendment.
Determination of Benzocaine in Pharmaceutical Formulations by Indirect SERRS Assay Combined with Azo Coupling
Authors: Zhao Chao-Yang , Sui Huimin , Xue Endi , Li Li , Zhang Jie , Xu Tao , Liang Xin , Yang Ying
Published: July 2022

Coupled with an azo coupling reaction, a simple, rapid, sensitive, and effective surface-enhanced resonance Raman scattering (SERRS) detection method for benzocaine was developed. In our study, benzocaine which is used clinically as a local anesthetic was derived with p-aminothiophenol into a corresponding azo product within 5 min, resulting in a strong SERRS response with the simple addition of Ag NPs excited with a 532 nm laser. The linear correlation between SERRS intensity of dominant bands and logarithm of benzocaine concentration was investigated for quantitative determination. The method reached a limit of detection (LOD) down to 0.139 and 0.0788 μg/mL calculated with two peak intensity ratios (I1568/I2260 and I1331/I2260), which is comparable to most studies reported previously, and meanwhile had superiority in simplicity and rapidness. The quantitative measurements for pharmaceutical preparations with benzocaine were conducted without complex extraction and enrichment processes. It was indicated that the SERRS assay combined with azo derivatization reaction has implications for practical applications in more complicated systems involving biological samples, in which appropriate and simplified pretreatments were conducted to remove interfering components.
Cloning, Expression, Purification, and Characterization of β-Galactosidase from Bifidobacterium longum and Bifidobacterium pseudocatenulatum
Authors: Du Mingzhu , Yang Shuanghong , Jiang Tong , Liang Tingting , Li Ying , Cai Shuzhen , Wu Qingping , Zhang Jumei , Chen Wei , Xie Xinqiang
Published: July 2022

Expression and purification of β-galactosidases derived from Bifidobacterium provide a new resource for efficient lactose hydrolysis and lactose intolerance alleviation. Here, we cloned and expressed two β-galactosidases derived from Bifidobacterium. The optimal pH for BLGLB1 was 5.5, and the optimal temperature was 45 °C, at which the enzyme activity of BLGLB1 was higher than that of commercial enzyme E (300 ± 3.6 U/mg) under its optimal conditions, reaching 2200 ± 15 U/mg. The optimal pH and temperature for BPGLB1 were 6.0 and 45 °C, respectively, and the enzyme activity (0.58 ± 0.03 U/mg) under optimum conditions was significantly lower than that of BLGLB1. The structures of the two β-galactosidase were similar, with all known key sites conserved. When o-nitrophenyl-β-D-galactoside (oNPG) was used as an enzyme reaction substrate, the maximum reaction velocity (Vmax) for BLGLB1 and BPGLB1 was 3700 ± 100 U/mg and 1.1 ± 0.1 U/mg, respectively. The kinetic constant (Km) of BLGLB1 and BPGLB1 was 1.9 ± 0.1 and 1.3 ± 0.3 mmol/L, respectively. The respective catalytic constant (kcat) of BLGLB1 and BPGLB1 was 1700 ± 40 s−1 and 0.5 ± 0.02 s−1, respectively; the respective kcat/Km value of BLGLB1 and BPGLB1 was 870 L/(mmol∙s) and 0.36 L/(mmol∙s), respectively. The Km, kcat and Vmax values of BLGLB1 were superior to those of earlier reported β-galactosidase derived from Bifidobacterium. Overall, BLGLB1 has potential application in the food industry.
Effect of Antimicrobial and Antioxidant Rich Pomegranate Peel Based Edible Coatings on Quality and Functional Properties of Chicken Nuggets
Authors: Bashir Sadaf , Arshad Muhammad Sajid , Khalid Waseem , Nayik Gulzar Ahmad , Al Obaid Sami , Ansari Mohammad Javed , Moreno Andres , Karabagias Ioannis K.
Published: July 2022

The current study evaluated the effect of pomegranate peel-based edible coating on chicken nuggets in order to develop a functional and safe product, high in nutritional value. For this purpose, 2,2-diphenyl-1-picrylhydrazyl (DPPH) and total phenolic content (TPC) assays were performed to check the potential antioxidant activity of chicken nuggets; microbial control, including total aerobic count and coliforms population, was performed for quality and safety purposes; and thiobarbituric acid reactive substances (TBARS) and peroxide value (POV) were performed to determine the oxidative stability of chicken nuggets. Different treatments were applied at different storage periods (0th, 7th, 14th and 21st day). The higher value of total aerobic count (5.09 ± 0.05 log CFU/g) and coliforms (3.91 ± 0.06 log CFU/g) were obtained for the uncoated samples, while the lower population was enumerated in the combination of sodium alginate (SA) and pomegranate peel powder (PPP). However, DPPH (64.65 ± 2.15%) and TPC (135.66 ± 3.07 GAE/100 g) values were higher in the coated chicken nuggets (SA (1.5%) and PPP (1.5%)) and lowest in the control samples. The higher value of TBARS (1.62 ± 0.03 MDA/kg) and POV (0.92 ± 0.03 meq peroxide/kg) were observed in the uncoated chicken nuggets. In the Hunter color system, L*, a*, and b* peak values were determined in the coated chicken nuggets with SA (1.5%) + PPP (1.5%) at the 21st day of storage. The uncoated chicken nuggets had different sensory characteristics (appearance, color, taste, texture, and overall acceptability) compared to the coated samples. Conclusively, coating based on the combination of SA (1.5%) and PPP (1.5%) increased the quality, safety, and nutritional properties of chicken nuggets.
Comparative Effect of UV, UV/H2O2 and UV/H2O2/Fe on Terbuthylazine Degradation in Natural and Ultrapure Water
Authors: Andrades José Antonio , Lojo-López Manuel , Egea-Corbacho Agata , Quiroga José María
Published: July 2022

Different advanced oxidation processes (AOPs) (ultraviolet radiation, hydrogen peroxide photolysis and photo-Fenton) were applied to test the degradation of terbuthylazine in three types of water: (a) ultrapure water, (b) surface water from the Gaditana area (Los Hurones reservoir, Cádiz, Spain) and (c) groundwater from the Tempul spring in Jerez de la Frontera (Cádiz, Spain). The experiments were carried out on a laboratory scale, using two different types of reactors, batch and semi-continuous. In batch reactors, the most efficient process for the experiments carried out with both ultrapure water and underground groundwater was ultraviolet radiation, whereas for surface water from the Gaditana area, the process that obtained the best results was the photolysis of hydrogen peroxide with 2.5 mg L−1 of H2O2. In semi-continuous reactors, the most efficient process was the photolysis of hydrogen peroxide with 2.5 mg L−1 of H2O2 for all the matrices studied. In both types of reactors, terbuthylazine degradation percentages higher than 90% were achieved; the main difference was in the reaction time, which varied from minutes in the batch reactor to seconds in the semi-continuous reactor. In all the applied AOPs, N-terbutyl-6-hydroxy-N′ethyl-1,3,5-triazine-2,4-diamine (TBA-212) was generated as a reaction intermediate.
Effects of Seed Roasting Temperature on Sesame Oil Fatty Acid Composition, Lignan, Sterol and Tocopherol Contents, Oxidative Stability and Antioxidant Potential for Food Applications
Authors: Arab Radia , Casal Susana , Pinho Teresa , Cruz Rebeca , Freidja Mohamed Lamine , Lorenzo José Manuel , Hano Christophe , Madani Khodir , Boulekbache-Makhlouf Lila
Published: July 2022

Roasting is a key step for preparing sesame oil that leads to important changes in its organoleptic properties and quality. In this study, white sesame seeds were roasted for 20 min in an electric oven at different temperatures (120, 150, 180, 210, 250 and 300 °C). The oils extracted from unroasted and roasted seeds were compared for their chemical composition: fatty acids (including trans isomers), phytosterols, lignans (sesamin and sesamolin), tocopherols and total phenolic compounds, as well as their oxidative stability and antiradical capacity. There were no obvious differences in the oil densities, refractive indexes or iodine values, but the saponification values were affected by temperature. Relevant primary and secondary lipid oxidation were observed at T > 250 °C, resulting in a higher p-anisidine value and K232 as well as K268 values. Roasting improved oil yield (from 33.5 to 62.6%), increased its induction period (from 5.5 to 10.5 h) and enhanced the total phenolic content (from 152 to 194 mg/100 g) and antiradical activity of the extracted oil. Depending on roasting temperature, a gradual decline was recorded in total amounts of phytosterols (up to 17.4%), γ-tocopherol (up to 10.6%), sesamolin (maximum of 27.5%) and sesamin (maximum of 12.5%). All the investigated oils presented a low quantity in triglyceride polymers, clearly below the maximum tolerated quantity according to the European regulation. The optimal roasting temperature for obtaining high nutritional grade oil within the permissible values was 210 °C. The unsaponifiable components (including lignans and sterols) extracted from roasted seeds have been shown to be natural additives to fresh meatball products to extend shelf life. The results of this study may help to boost the nutritional content of plant-based diets by allowing for the use of roasted sesame seed oil and its components.
Tropaeolin OO as a Chemical Sensor for a Trace Amount of Pd(II) Ions Determination
Authors: Pach Adrianna , Podborska Agnieszka , Csapo Edit , Luty-Błocho Magdalena
Published: July 2022

The selective determination of metals in waste solutions is a very important aspect of the industry and environmental protection. Knowledge of the contents and composition of the waste can contribute to design an efficient process separation and recovery of valuable metals. The problematic issue is primarily the correct determination of metals with similar properties such as palladium and platinum. Thus this paper focuses on the development of a selective method that enables Pd(II) determination in the presence of Pt(IV) ions using the azo-dye tropaeolin OO (TR). For this purpose, the process of the metalorganic complex formation and Pd(II) ions determination were studied by using UV–Vis spectrophotometry under different conditions: solvents (water and B-R buffer), pH (2.09–6.09), temperature (20–60 °C), anions and cations concentrations. The formed metalorganic complex between Pd and tropaeolin OO allows for distinguishing Pd(II) ions from both platinum complexes, i.e. Pt(II), Pt(IV). Moreover, the proposed method can be applied to solutions containing both chloride and chlorate ions. The obtained characteristic spectrum with two maxima allows the determination of palladium even in the presence of other cations (Na, K, Mg, Zn, Co, Ni, Al) and changed concentrations of Pt(IV) ions. Furthermore, the developed spectrophotometric method for the Pd(II) ions determination using tropaeolin OO is characterized by high selectivity towards palladium ions.
Facile Synthesis of Nitrogen Self-Doped Porous Carbon Derived from Cicada Shell via KOH Activation for Simultaneous Detection and Removal of Cu2+
Authors: Zou Jin , Liu Jiawei , Yu Qi , Gao Yansha , Chen Shangxing , Huang Xigen , Hu Dongnan , Liu Shuwu , Lu Limin
Published: July 2022

Sensitive detection and efficient removal of heavy metal ions with high toxicity and mobility are of great importance for environmental monitoring and control. Although several kinds of functional materials have been reported for this purpose, their preparation processes are complicated. Herein, nitrogen self-doped activated porous biochar (NAC) was synthesized in a facile process via an activation–carbonization strategy from cicada shell rich in chitin, and subsequently employed as an effective functional material for the simultaneous determination and removal of Cu2+ from aqueous media. With its unique porous structure and abundant oxygen-containing functional groups, along with the presence of heteroatoms, NAC exhibits high sensitivity for the electrochemical sensing of Cu2+ in concentrations ranging from 0.001 to 1000 μg·L−1, with a low detection limit of 0.3 ng·L−1. Additionally, NAC presents an excellent removal efficiency of over 78%. The maximum adsorption capacity is estimated at 110.4 mg/g. These excellent performances demonstrate that NAC could serve as an efficient platform for the detection and removal of Cu2+ in real environmental areas.
Provision of Energy- and Wavelength-Efficient Traffic Grooming for Sparse WDM-Enabled Distributed Satellite Cluster Networks
Authors: Peng Cong , He Yuanzhi , Yan Di , Fu Huajun , Zhao Shanghong
Published: July 2022

Sparse wavelength division multiplex (WDM) enabled distributed satellite cluster networks (DSCNs) have emerged as a promising architecture to accommodate future extensive applications. Networking of the DSCNs will face the challenges of explosively increasing traffic requests, the limited number of wavelengths, and restricted energy provisioning. To address these issues, a novel approach, the two-phase traffic grooming based on the matching algorithm (TPTG_MA), is proposed in this paper. To analyze resource utilization, energy- and wavelength- minimized models are established. After that, we develop the MA to tackle the traffic grooming problem in two phases, including the first phase for traffic aggregation and sub-wavelength assignment (TAASA) and the second phase for sub-wavelength grooming (SG). To evaluate the performance of the proposed TPTG_MA, the direct lightpath grooming (DLG) heuristic and the genetic algorithm (GA) are simulated for comparison. The results demonstrate that the TPTG_MA and DLG_GA outperform TPTG and DLG in the average wavelength utilization ratio (AWUR), the energy consumption saving (ESC), and the blocking probability. Compared with the DLG_GA, the TPTG_MA achieves at most 18% and 23% higher AWUR in the 12-node and 22-node topologies, respectively. In addition, the TPTG_MA can actualize at most 10% ECS improvement over the DLG_GA. At last, the influence of the network size, the number of wavelengths, and the number of hops are discussed.
A Primary Support Design for Deep Shaft Construction Based on the Mechanism of Advanced Sequential Geopressure Release
Authors: Zhao Xingdong , Deng Lei , Zhou Xin , Zhao Yifan , Guo Zhenpeng
Published: July 2022

The construction of 1500 m depth shaft in Xincheng Gold Mine, China, faces complex stress conditions such as high geostress (>50 MPa), high ground temperature (>50 °C), high water-pressure (>9 MPa), and highly corrosive. Traditional deep shafts excavated by the sinking and lining method cannot adapt to high geostress problems, such as rock bursts and large deformations, etc., in the deep shaft construction process. To avoid and adjust the high geostress induced the rockburst and large deformations, the mechanism of the advanced sequential geopressure release (ASGR) has been proposed for the ground control in deep shaft construction. In this paper, the safe distance between the concrete lining and the shaft excavation face is determined based on the ASGR mechanism, which can provide the space for geopressure release, and primary support based on rock mass quality and numerical simulation was employed to control the geopressure and deformation. A new support scheme for the deep shaft is proposed, using long bolts to restrain severe deformations, metal mesh, and a double reinforcement bar to improve the induced stress distribution. According to the results, the construction scheme of deep shaft has been improved, and the safe support distance of the proposed scheme is determined to be 12 m, with an interval of three excavation cycles. Compared to the original scheme of shaft lining after excavation, the proposed scheme based on the ASGR mechanism can effectively improve the geopressure release and benefit from controlling the rockburst and large deformation of deep shaft induced by high geostress conditions. The stress distribution in the lining is more uniform, and safety factor of the lining is increased to 2.0, which is benefit the long-term stability of deep shaft.
Separation and Analytical Techniques Used in Snake Venomics: A Review Article
Authors: Sahyoun Christina , Rima Mohamad , Mattei César , Sabatier Jean-Marc , Fajloun Ziad , Legros Christian
Published: July 2022

The deleterious consequences of snake envenomation are due to the extreme protein complexity of snake venoms. Therefore, the identification of their components is crucial for understanding the clinical manifestations of envenomation pathophysiology and for the development of effective antivenoms. In addition, snake venoms are considered as libraries of bioactive molecules that can be used to develop innovative drugs. Numerous separation and analytical techniques are combined to study snake venom composition including chromatographic techniques such as size exclusion and RP-HPLC and electrophoretic techniques. Herein, we present in detail these existing techniques and their applications in snake venom research. In the first part, we discuss the different possible technical combinations that could be used to isolate and purify SV proteins using what is known as bioassay-guided fractionation. In the second part, we describe four different proteomic strategies that could be applied for venomics studies to evaluate whole venom composition, including the mostly used technique: RP-HPLC. Eventually, we show that to date, there is no standard technique used for the separation of all snake venoms. Thus, different combinations might be developed, taking into consideration the main objective of the study, the available resources, and the properties of the target molecules to be isolated.
The Comparison of InSb-Based Thin Films and Graphene on SiC for Magnetic Diagnostics under Extreme Conditions
Authors: El-Ahmar Semir , Przychodnia Marta , Jankowski Jakub , Prokopowicz Rafał , Ziemba Maciej , Szary Maciej J. , Reddig Wiktoria , Jagiełło Jakub , Dobrowolski Artur , Ciuk Tymoteusz
Published: July 2022

The ability to precisely measure magnetic fields under extreme operating conditions is becoming increasingly important as a result of the advent of modern diagnostics for future magnetic-confinement fusion devices. These conditions are recognized as strong neutron radiation and high temperatures (up to 350 °C). We report on the first experimental comparison of the impact of neutron radiation on graphene and indium antimonide thin films. For this purpose, a 2D-material-based structure was fabricated in the form of hydrogen-intercalated quasi-free-standing graphene on semi-insulating high-purity on-axis 4H-SiC(0001), passivated with an Al2O3 layer. InSb-based thin films, donor doped to varying degrees, were deposited on a monocrystalline gallium arsenide or a polycrystalline ceramic substrate. The thin films were covered with a SiO2 insulating layer. All samples were exposed to a fast-neutron fluence of ≈7×1017 cm−2. The results have shown that the graphene sheet is only moderately affected by neutron radiation compared to the InSb-based structures. The low structural damage allowed the graphene/SiC system to retain its electrical properties and excellent sensitivity to magnetic fields. However, InSb-based structures proved to have significantly more post-irradiation self-healing capabilities when subject to proper temperature treatment. This property has been tested depending on the doping level and type of the substrate.
Lightweight Indoor Multi-Object Tracking in Overlapping FOV Multi-Camera Environments
Authors: Jang Jungik , Seon Minjae , Choi Jaehyuk
Published: July 2022

Multi-Target Multi-Camera Tracking (MTMCT), which aims to track multiple targets within a multi-camera network, has recently attracted considerable attention due to its wide range of applications. The main challenge of MTMCT is to match local tracklets (i.e., sub-trajectories) obtained by different cameras and to combine them into global trajectories across the multi-camera network. This paper addresses the cross-camera tracklet matching problem in scenarios with partially overlapping fields of view (FOVs), such as indoor multi-camera environments. We present a new lightweight matching method for the MTMC task that employs similarity analysis for location features. The proposed approach comprises two steps: (i) extracting the motion information of targets based on a ground projection method and (ii) matching the tracklets using similarity analysis based on the Dynamic Time Warping (DTW) algorithm. We use a Kanade–Lucas–Tomasi (KLT) algorithm-based frame-skipping method to reduce the computational overhead in object detection and to produce a smooth estimate of the target’s local tracklets. To improve matching accuracy, we also investigate three different location features to determine the most appropriate feature for similarity analysis. The effectiveness of the proposed method has been evaluated through real experiments, demonstrating its ability to accurately match local tracklets.
Tracking Missing Person in Large Crowd Gathering Using Intelligent Video Surveillance
Authors: Nadeem Adnan , Ashraf Muhammad , Qadeer Nauman , Rizwan Kashif , Mehmood Amir , AlZahrani Ali , Noor Fazal , Abbasi Qammer H.
Published: July 2022

Locating a missing child or elderly person in a large gathering through face recognition in videos is still challenging because of various dynamic factors. In this paper, we present an intelligent mechanism for tracking missing persons in an unconstrained large gathering scenario of Al-Nabawi Mosque, Madinah, KSA. The proposed mechanism in this paper is unique in two aspects. First, there are various proposals existing in the literature that deal with face detection and recognition in high-quality images of a large crowd but none of them tested tracking of a missing person in low resolution images of a large gathering scenario. Secondly, our proposed mechanism is unique in the sense that it employs four phases: (a) report missing person online through web and mobile app based on spatio-temporal features; (b) geo fence set estimation for reducing search space; (c) face detection using the fusion of Viola Jones cascades LBP, CART, and HAAR to optimize the results of the localization of face regions; and (d) face recognition to find a missing person based on the profile image of reported missing person. The overall results of our proposed intelligent tracking mechanism suggest good performance when tested on a challenging dataset of 2208 low resolution images of large crowd gathering.