bluuebunny/crossref_metadata_2025 huggingface dataset:
RANK and RANKL expression as markers of dendritic cell–t cell interactions in paired samples of rheumatoid synovium and lymph nodes
Authors: Page Guillaume , Miossec Pierre
Published: July 2005

Objective

The RANK/RANKL pathway is critical in bone destruction in conditions such as rheumatoid arthritis (RA). Since RANK/RANKL‐deficient mice show major lymph node (LN) abnormalities, undertook this study to investigate the expression of RANK/RANKL in paired samples of synovium and LNs from RA patients.

Methods

Using immunohistochemistry, RANK/RANKL expression by dendritic cell (DC) and T cell subsets was studied in this unique set of samples and in RA synoviocytes stimulated with interleukin‐1β (IL‐1β), tumor necrosis factor α (TNFα), and IL‐17.

Results

In RA synovium, RANKL+ cells were detected in the lining layer and the lymphocytic infiltrates, whereas RANK expression was restricted to the perivascular infiltrates. In LNs, RANK+ and RANKL+ cells were diffusely expressed in the T cell zone and in germinal centers. Double staining of paired RA synovium and LN sections showed that some immature CD1a+ DCs expressed RANK and RANKL, while some mature DC‐LAMP+ DCs expressed only RANK. Some CD3+, CD4+, interferon‐γ+, and IL‐17+ cells expressed RANKL, while none expressed RANK. Treatment of synoviocytes with TNFα or IL‐1β in combination with IL‐17 was particularly potent at inducing RANKL expression.

Conclusion

This study shows the involvement of RANK/RANKL in DC–T cell interactions during an inflammatory process. RANK expression appears to be limited to the sites of immune reaction, both in the synovium and in LNs. Therapeutic control of these targets may have both positive and negative consequences for the immune system.
Comparison of human stem cells derived from various mesenchymal tissues: Superiority of synovium as a cell source
Authors: Sakaguchi Yusuke , Sekiya Ichiro , Yagishita Kazuyoshi , Muneta Takeshi
Published: July 2005

Objective

To compare the properties of human mesenchymal stem cells (MSCs) isolated from bone marrow, synovium, periosteum, skeletal muscle, and adipose tissue.

Methods

Human mesenchymal tissues were obtained from 8 donors during knee surgery for ligament injury. After collagenase digestion or gradient‐density separation, nucleated cells were plated at an appropriate density for expansion at the maximum rate without colony‐to‐colony contact. Yield, expandability, differentiation potential, and epitope profile were compared among MSCs from the 5 different tissue sources.

Results

Colony number per 103 nucleated cells was lower, and cell number per colony was higher, in bone marrow than in other mesenchymal tissues. When the cells were replated at low density every 14 days, bone marrow–, synovium‐, and periosteum‐derived cells retained their proliferation ability even at passage 10. In chondrogenesis studies in which the cells were pelleted and cultured in vitro, pellets from bone marrow–, synovium‐, and periosteum‐derived cells were shown to be larger and stained more extensively for cartilage matrix. Synovium‐derived cells, in particular, had the greatest ability for chondrogenesis. In adipogenesis experiments, the frequency of oil red O–positive colonies was highest in synovium‐ and adipose tissue–derived cells. In studies of osteogenesis, the rate of alizarin red–positive colonies was highest in bone marrow–, synovium‐, and periosteum‐derived cells. For epitope profiling, 15 surface antigens were measured. Most appeared to have similar epitope profiles irrespective of cell source.

Conclusion

Our findings indicate that there are significant differences in MSC properties according to tissue source, beyond donor and experimental variation. Superiority of synovium as a potential source of MSCs for clinical applications was demonstrated.
“Pain elsewhere” and the impact of knee pain in older people
Authors: Croft Peter , Jordan Kelvin , Jinks Clare
Published: July 2005

Objective

To investigate how often knee pain is accompanied by pain elsewhere and to determine whether the presence of “pain elsewhere” than the knee influences either knee‐related disability or the impact of knee pain on health and psychological status.

Methods

A survey was mailed to 8,995 individuals (age ≥50 years) registered with 3 general practices in North Staffordshire in the UK. Patients recorded pain on a manikin and completed the Short‐Form 36 health survey, the Hospital Anxiety and Depression Scale, and the Western Ontario and McMaster Universities Osteoarthritis Index. Responders were categorized as having no pain, knee pain with or without pain elsewhere, or other pain (no knee pain, but pain elsewhere). Those with knee pain or other pain were subdivided by the extent of pain elsewhere.

Results

The adjusted survey response rate was 70%. Fifty‐seven percent of responders with knee pain had pain in at least 2 other joint areas. Pain elsewhere was associated with lower physical function and with anxiety and depression both in the knee‐pain group and in the other‐pain group (associations were stronger in the knee‐pain group). Knee pain and disability were less severe in those with knee pain alone than in those with knee pain and pain elsewhere, even after adjusting for age, sex, obesity, laterality of pain, and depression.

Conclusion

Most people with knee pain have multiple joint site pain. The importance of this to clinicians and researchers is that the severity of knee pain and related disability is worse in the presence of pain elsewhere. This finding has implications for the management and treatment of older people with knee pain.
Synovial intracellular citrullinated proteins colocalizing with peptidyl arginine deiminase as pathophysiologically relevant antigenic determinants of rheumatoid arthritis–specific humoral autoimmunity
Authors: De Rycke Leen , Nicholas Anthony P. , Cantaert Tineke , Kruithof Elli , Echols Joshua D. , Vandekerckhove Bart , Veys Eric M. , De Keyser Filip , Baeten Dominique
Published: July 2005

Objective

To address the ongoing debate concerning the specificity of synovial citrullinated proteins for rheumatoid arthritis (RA) and to analyze their pathophysiologic relevance to the induction or perpetuation of the RA‐specific anti–citrullinated protein antibodies (ACPAs).

Methods

Synovium of 19 RA patients and 19 non‐RA controls was immunostained for the presence of citrullinated proteins with a mouse monoclonal antibody (F95), for the citrullinating enzyme peptidyl arginine deiminase type 2 (PAD‐2), and for the free citrulline–producing enzyme inducible nitric oxide synthase (iNOS). Extending the RA cohort to 61 patients, the findings of anticitrulline staining in synovium were related to serum and synovial fluid ACPA levels, as measured by enzyme‐linked immunosorbent assay.

Results

F95 staining indicated the presence of synovial intracellular citrullinated proteins in 53% of RA samples versus 5% of control samples, whereas extracellular staining was not RA specific. Immunoblotting and inhibition experiments confirmed that the antibody recognized citrullinated proteins but not free citrulline. Accordingly, iNOS was equally found in RA and control synovium and in intracellular citrullinated protein–positive and intracellular citrullinated protein–negative samples. In contrast, intracellular citrullinated proteins colocalized with PAD‐2, which was found in 59% of RA samples versus 17% of control samples. Independent of local disease activity, the presence of the RA‐specific synovial intracellular citrullinated proteins was associated with significantly higher systemic and local ACPA levels and with local ACPA production in the joint.

Conclusion

These data confirm the presence of RA‐specific intracellular citrullinated proteins in synovium. The link with PAD‐2 and local and systemic ACPA levels emphasizes their pathophysiologic relevance for RA‐specific humoral autoimmunity.
Induction of a CXCL8 binding site on endothelial syndecan‐3 in rheumatoid synovium
Authors: Patterson Angela M. , Gardner Lucy , Shaw Jennifer , David Guido , Loreau Emilie , Aguilar Luc , Ashton Brian A. , Jim Middleton
Published: July 2005

Objective

To identify and characterize which endothelial heparan sulfate proteoglycans (HSPGs) bind the chemokine CXCL8 (interleukin‐8) in human rheumatoid arthritis (RA) and nonrheumatoid synovia.

Method

CXCL8 binding to endothelial HSPGs in RA and nonrheumatoid synovia was determined by heparinase treatment followed by an in situ binding assay and autoradiography. Endothelial HSPGs were characterized by immunohistochemical analysis and quantitative reverse transcriptase–polymerase chain reaction (RT‐PCR). Phosphatidyinositol‐specific phospholipase C (PI‐PLC) and antibodies to HSPGs were used in in situ binding experiments to identify which HSPGs bound CXCL8.

Results

The expression of heparan sulfate on microvascular endothelial cells was demonstrated in RA and nonrheumatoid synovia. Using antibodies to syndecan‐1–4 and glypican‐1, ‐3, and ‐4, the selective expression of syndecan‐3 by endothelial cells was detected in RA and nonrheumatoid synovia. In addition, RT‐PCR showed the presence of syndecan‐3 messenger RNA in endothelial cells extracted from RA and nonrheumatoid synovia. 125I‐CXCL8 bound to venular endothelial cells; treatment with heparinases I and III significantly reduced this binding in RA but not nonrheumatoid synovia. 125I‐CXCL8 binding was not reduced after treatment with PI‐PLC, which cleaves glycosyl phosphatidylinositol linkages, suggesting that CXCL8 did not bind to glypicans. Treatment of synovia with a syndecan‐3 antibody reduced CXCL8 binding to RA but not nonrheumatoid endothelial cells; however, no reduction in binding was observed with syndecan‐2 or glypican‐4 antibodies.

Conclusion

Our results show the selective induction of a CXCL8 binding site on endothelial syndecan‐3 in RA synovium. This site may be involved in leukocyte trafficking into RA synovial tissue.
Risk of malignancy in scleroderma: A population‐based cohort study
Authors: Chatterjee Soumya , Dombi George W. , Severson Richard K. , Mayes Maureen D.
Published: July 2005

Objective

To determine the incidence of cancer in patients with scleroderma (systemic sclerosis) and to compare those rates with cancer rates in the local population.

Methods

Cancer risk in scleroderma patients in the Detroit metropolitan area was assessed by linking patient identification codes of the Michigan Scleroderma Registry to the Metropolitan Detroit Cancer Surveillance System database. Patients were screened between the years 1973 and 2002, with additional followup to 2004. Standardized incidence ratios (SIRs) were calculated for selected malignancies (lung, liver, colon, breast, cervical, and prostate cancers, and non‐Hodgkin's lymphomas), with stratification by sex and race.

Results

Of 934 patients in the Scleroderma Registry, 538 were included in the study based on tri‐county residency (436 females and 102 males). Of these, 45 first malignancies were noted (37 females and 8 males). Lung cancer (10 cases) was found to be the most common cancer in scleroderma patients. However, its incidence was not significantly different from that in the general population of metropolitan Detroit (SIR 1.23). Other types of cancer were examined, and no significant differences were found as compared with the rates in the local population, with 1 exception: black females with scleroderma had significantly higher rates of liver cancer (SIR 45.8).

Conclusion

Contrary to previous studies, this study did not find statistical evidence of an increased incidence of cancer in scleroderma patients, except for liver cancer. One possible reason is the high background rates of certain cancers in the metropolitan Detroit area. It may be necessary to consider local cancer rates when comparing different scleroderma cohorts.
Assessment of the cranial involvement pattern of giant cell arteritis with 3t magnetic resonance imaging
Authors: Bley T. A. , Weiben O. , Uhl M. , Vaith P. , Schmidt D. , Warnatz K. , Langer M.
Published: July 2005

Objective

To noninvasively determine the involvement pattern of the cranial arteries in giant cell arteritis (GCA), with high‐resolution magnetic resonance imaging (MRI).

Methods

The superficial cranial arteries of 21 patients with suspected GCA were examined using a 3T high‐field MRI scanner. Postcontrast T1‐weighted spin‐echo images were acquired with submillimeter spatial resolution, to assess mural thickness and lumen diameter of the major cranial arteries on both sides of the head. In all cases, MRI results were compared with findings of clinical examination and laboratory tests. In addition, temporal artery biopsy specimens from 10 patients were examined by histology.

Results

MRI sharply revealed all of the major superficial cranial arteries, allowing for an evaluation of their lumen and vessel wall. Nine of the 21 patients were diagnosed as having GCA according to the criteria of the American College of Rheumatology. In all of these patients with clinically diagnosed GCA, multiple cranial arteries showed signs of inflammation on MRI. In 1 patient, the occipital arteries were inflamed, while the temporal arteries were spared.

Conclusion

Postcontrast high‐resolution MRI visualizes the major cranial arteries on both sides of the head within a single examination. The cranial involvement pattern in GCA can be assessed precisely and noninvasively. In the majority of GCA patients, several cranial arteries were affected simultaneously, with a predominance of involvement of the frontal branch of the superficial temporal artery. Inflammation of the occipital arteries, with sparing of the temporal arteries, was also encountered.
Impact of disease severity and gastrointestinal side effects on the health state preferences of patients with osteoarthritis
Authors: Chang Jane , Kauf Teresa L. , Mahajan Shibani , Jordan Joanne M. , Kraus Virginia B. , Vail T. Parker , Reed Shelby D. , Omar Mohamed A. , Kahler Kristijan H. , Schulman Kevin A.
Published: July 2005

Objective

To describe the health state preferences of patients with osteoarthritis (OA) according to the level of pain and disability and the extent of gastrointestinal side effects from nonsteroidal antiinflammatory drugs (NSAIDs).

Methods

Using combinations of 5 OA health states (4 specifying medication use) and 6 gastrointestinal side effect profiles, we developed 25 scenarios. In an Internet survey, adults with OA evaluated 5 randomly chosen health state–side effect scenarios (in addition to scenarios for congestive heart failure and wearing dentures, as benchmarks). They rated the scenarios on a 0–100 scale, in which 100 corresponds to best imaginable health. Unadjusted mean ratings were calculated using a difference‐in‐difference approach. A generalized linear model was used to estimate the effects of disease severity and side effect severity on the ratings, after controlling for patient characteristics.

Results

A total of 4,386 respondents whose mean age was 55.3 years, of whom 3,107 (70.8%) were women and 4,007 (91.4%) were white, completed the survey. Mean adjusted ratings for health state–side effect scenarios ranged from 94.9 for the mildest scenario to 25.3 for the most severe scenario. Severity of NSAID side effects had a greater negative influence on the ratings in milder OA states than in more severe OA states. Ratings were lower among men (P < 0.001) and among respondents with OA pain in the previous 24 hours (P < 0.001). Disease severity had a greater effect on ratings than did side effect severity.

Conclusion

Patients consider pain and functional limitations associated with OA to be important determinants of well‐being. Future research should attempt to determine whether patients prefer reductions in their OA‐related pain and disability over improvements in treatment side effect profiles.
Efficacy of infliximab in the treatment of uveitis that is resistant to treatment with the combination of azathioprine, cyclosporine, and corticosteroids in behçet's disease: An open‐label trial
Authors: Tugal‐Tutkun Ilknur , Mudun Abdulbaki , Urgancioglu Meri , Kamali Sevil , Kasapoglu Esen , Inanc Murat , Gül Ahmet
Published: July 2005

Objective

To investigate the effect of infliximab on the frequency of uveitis attacks and the visual prognosis in male patients with Behçet's disease in whom uveitis was resistant to combination therapy with corticosteroids, azathioprine, and cyclosporine.

Methods

The study group comprised patients who were receiving combination therapy but experienced at least 2 attacks of posterior uveitis/panuveitis or retinal vasculitis during the 6‐month period prior to enrollment. Infliximab infusions (5 mg/kg) were administered at weeks 0, 2, 6, and 14. Weeks 0–22 were defined as the infusion period, and weeks 23–54 were defined as the observation period. Patients continued to receive azathioprine and corticosteroids, but cyclosporine was discontinued after the screening visit. The primary outcome measures were the absence of uveitis attacks during the infusion period (remission), and the absence of uveitis attacks throughout the study period (sustained remission).

Results

Thirteen patients were enrolled in the study. Thirty‐two uveitis attacks involving the posterior segment occurred during the previous‐treatment period. During the infusion period, 4 patients (30.8%) remained attack‐free, and 9 patients had a total of 13 uveitis attacks. Ten of these attacks (76.9%) occurred at either week 14 or week 22. One of 13 patients fulfilled the definition of sustained remission, and the remaining 12 patients had a total of 36 uveitis attacks during the observation period. The mean number of uveitis attacks and daily corticosteroid doses were significantly lower during the infusion period than during the previous‐treatment period or the observation period. Although potential visual acuity was regained following infliximab infusion, this beneficial effect was not preserved until week 54. None of the patients experienced a serious adverse event.

Conclusion

The results of this trial suggest that infliximab is effective in suppressing the occurrence of uveitis attacks, has a corticosteroid‐sparing effect, and has favorable implications for the visual prognosis of patients with resistant Behçet's uveitis.
Psoriasis induced by anti–tumor necrosis factor therapy: A paradoxical adverse reaction
Authors: Sfikakis P. P. , Iliopoulos A. , Elezoglou A. , Kittas C. , Stratigos A.
Published: July 2005

Administration of anti–tumor necrosis factor (anti‐TNF) agents is beneficial in a variety of chronic inflammatory conditions, including psoriasis. We describe 5 patients in whom psoriasiform skin lesions developed 6–9 months after the initiation of anti‐TNF therapy for longstanding, seropositive rheumatoid arthritis (etanercept or adalimumab), typical ankylosing spondylitis (infliximab), and Adamantiades‐Behçet's disease (infliximab). In all 5 patients, the underlying disease had responded well to anti‐TNF therapy. Four patients developed a striking pustular eruption on the palms and/or soles accompanied by plaque‐type psoriasis at other skin sites, while 1 patient developed thick erythematous scaly plaques localized to the scalp. In 3 patients there was nail involvement with onycholysis, yellow discoloration, and subungual keratosis. Histologic findings from skin biopsies were consistent with psoriasis. None of these patients had a personal or family history of psoriasis. In all patients, skin lesions subsided either with topical treatment alone, or after discontinuation of the responsible anti‐TNF agent. The interpretation of this paradoxical side effect of anti‐TNF therapy remains unclear but may relate to altered immunity induced by the inhibition of TNF activity in predisposed individuals.
The expression of toll‐like receptors 3 and 7 in rheumatoid arthritis synovium is increased and costimulation of toll‐like receptors 3, 4, and 7/8 results in synergistic cytokine production by dendritic cells
Authors: Roelofs M. F. , Joosten L. A. B. , Abdollahi‐Roodsaz S. , Van Lieshout A. W. T. , Sprong T. , van den Hoogen F. H. , Van Den Berg W. B. , Radstake T. R. D. J.
Published: July 2005

Objective

To evaluate the expression of Toll‐like receptors (TLRs) 3 and 7 in synovium and to study potential differences in the maturation and cytokine production mediated by TLR‐2, TLR‐3, TLR‐4, and TLR‐7/8 by dendritic cells (DCs) from rheumatoid arthritis (RA) patients and DCs from healthy controls.

Methods

Synovial expression of TLR‐3 and TLR‐7 in RA was studied using immunohistochemistry. Monocyte‐derived DCs from RA patients and healthy controls were cultured for 6 days and subsequently stimulated for 48 hours via TLR‐mediated pathways (lipoteichoic acid, Pam3Cys, and fibroblast‐stimulating lipopeptide 1 for TLR‐2, poly[I‐C] for TLR‐3, lipopolysaccharide and extra domain A for TLR‐4, and R848 for TLR‐7/8). Phenotypic DC maturation was measured using flow cytometry. The secretion of tumor necrosis factor α (TNFα), interleukin‐6 (IL‐6), IL‐10, and IL‐12 was measured using the Bio‐Plex system. Cell lines expressing TLR‐2 and TLR‐4 were used for the detection of TLR‐2 and TLR‐4 ligands in serum and synovial fluid from RA patients.

Results

TLR‐3 and TLR‐7 were highly expressed in RA synovium. All TLR ligands elicited phenotypic DC maturation equally between DCs from RA patients and those from healthy controls. TLR‐2– and TLR‐4–mediated stimulation of DCs from RA patients resulted in markedly higher production of inflammatory mediators (TNFα and IL‐6) compared with DCs from healthy controls. In contrast, upon stimulation of TLR‐3 and TLR‐7/8, the level of cytokine production was equal between DCs from RA patients and those from healthy controls. Remarkably, both TLR‐3 and TLR‐7/8 stimulation resulted in a skewed balance toward IL‐12. Intriguingly, the combined stimulation of TLR‐4 and TLR‐3–7/8 resulted in a marked synergy with respect to the production of inflammatory mediators. As a proof of concept, TLR‐4 ligands were increased in the serum and synovial fluid of RA patients.

Conclusion

TLRs are involved in the regulation of DC activation and cytokine production. We hypothesize that various TLR ligands in the joint trigger multiple TLRs simultaneously, favoring the breakthrough of tolerance in RA.
Sodium Trithiophosphate(V): Crystal Structure and Sodium Ionic Conductivity.
Authors: Pompetzki M. , Jansen M.
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
A New Modification of the Laves Phase CaLi2.
Authors: Fischer Dieter , Jansen Martin
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
The Crystal Structure of Ba3Cu2Al2F16: A Relative of Ba4Cu2Al3F21.
Authors: Gredin Patrick , Corbel Gwenael , Wright Jonathan P. , Dupont Nathalie , de Kozak Ariel
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
The Structure of Magnesium Alanate.
Authors: Fichtner Maximillian , Engel Jens , Fuhr Olaf , Gloess Andreas , Rubner Oliver , Ahlrichs Reinhart
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
Tropochemical Cell‐Twinning in the New Quaternary Bismuth Selenides KxSn6‐2xBi2+xSe9 and KSn5Bi5Se13.
Authors: Mrotzek Antje , Kanatzidis Mercouri G.
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
β‐Y2Si2O7, a New Thortveitite‐Type Compound, Determined at 100 and 280 K.
Authors: Redhammer Guenther J. , Roth Georg
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
Valence State of Iron in the Sr2Fe(Mo,W,Ta)O6.0 Double‐Perovskite System: An Fe K‐Edge and L2,3‐Edge XANES Study.
Authors: Karppinen M. , Yamauchi H. , Yasukawa Y. , Linden J. , Chan T. S. , Liu R. S. , Chen J. M.
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
Synthesis and Luminescent Properties of a New Yellowish‐Orange Afterglow Phosphor Y2O2S:Ti,Mg.
Authors: Kang Chia‐Cheng , Liu Ru‐Shi , Chang Jiin‐Chyuan , Lee Biing‐Jye
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
La1‐xBa1+xGaO4‐x/2: A Novel High Temperature Proton Conductor.
Authors: Li Sara , Schoenberger Frank , Slater Peter
Published: July 2005

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Electrochemistry of Niobium(V) in Sulfuric and Methanesulfonic Acids: Formation of the Nb3O2(SO4)6 (H2O)35‐ Cluster and Designed Electrochemical Generation of “Nb3O2” Core Clusters by Double Potential Pulse Electrolysis.
Authors: May Michael , Gantt Melissa , Hoadley Caroline , Batten Thomas , Sayers William , Katovic Vladimir
Published: July 2005

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Gas‐Phase Hydration of U(IV), U(V), and U(VI) Dioxo Monocations.
Authors: Gresham Garold L. , Gianotto Anita K. , de B. Harrington Peter , Cao Libo , Scott Jill R. , Olsen John E. , Appelhans Anthony D. , Van Stipdonk Michael J. , Groenewold Gary S.
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
Crystal Structure and Spectroscopic Characterization of K8(VO)2O(SO4)6.
Authors: Rasmussen Soeren B. , Rasmussen Rikke Mattsson , Fehrmann Rasmus , Nielsen Kurt
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
2‐(3‐Pyridyl)‐1,3,8‐triazanaphthalene, a Product of the Catalytic Transformation of 3‐Cyanopyridine.
Authors: Janczak Jan , Kubiak Ryszard
Published: July 2005

For Abstract see ChemInform Abstract in Full Text.
Binaphthyldiamine‐Based Diazaphospholines as a New Class of Chiral Monodentate P‐Ligands.
Authors: Reetz Manfred T. , Oka Hiromasa , Goddard Richard
Published: July 2005

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Asymmetric Diels—Alder Reaction Using Pyrazole Derivatives as a Chiral Catalyst.
Authors: Kashima Choji , Miwa Yohei , Shibata Saori , Nakazono Hiroyuki
Published: July 2005

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One‐Pot Synthesis and Resolution of Chiral Allylic Alcohols.
Authors: Kamal Ahmed , Sandbhor Mahendra , Shaik Ahmad Ali , Sravanthi V.
Published: July 2005

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Lipase Catalyzed Preparation of Optically Active α‐Phenylethanol and the Related Substrates under Solvent Free Conditions.
Authors: Mamaghani Manouchehr , Tabatabaeian Khalil , Bahrami Behnaz
Published: July 2005

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A Novel Montmorillonite‐Enwrapped Scandium as a Heterogeneous Catalyst for Michael Reaction.
Authors: Kawabata Tomonori , Mizugaki Tomoo , Ebitani Kohki , Kaneda Kiyotomi
Published: July 2005

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Synthesis of Cyclic cis‐Enediynes from Manganese Carbyne Complexes and α,ω‐Diynes.
Authors: Casey Charles P. , Dzwiniel Trevor L. , Kraft Stefan , Guzei Ilia A.
Published: July 2005

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1,2,3‐ and 1,2,4‐Triazolium Salts, Pyrazoles, and Quinoxalines from Diarylnitrilimines and Isocyanides: A Study of the Scope.
Authors: Moderhack Dietrich , Daoud Ali
Published: July 2005

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The Co(I) Induced Methylmalonyl‐Succinyl Rearrangement in a Model for the Coenzyme B12 Dependent Methylmalonyl‐CoA Mutase.
Authors: Sun Fangping , Darbre Tamis
Published: July 2005

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Mixed Phosphite‐Phosphine and Phosphinite‐Phosphine Palladacyclic Complexes as Highly Active Catalysts for the Amination of Aryl Chlorides.
Authors: Bedford Robin B. , Blake Michael E.
Published: July 2005

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Highly Diastereoselective Addition of Et2AlCN to β‐Keto Amides Derived from (S)‐4‐Isopropyl‐2‐oxazolidinone.
Authors: Flores‐Morales Virginia , Fernandez‐Zertuche Mario , Ordonez Mario
Published: July 2005

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Reaction of Catalytic Olefination of Hydrazones with Polyhaloalkanes. Investigation of Alkene Formation Chemoselectivity.
Authors: Korotchenko V. N. , Shastin A. V. , Nenaidenko V. G. , Balenkova E. S.
Published: July 2005

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Gold‐Catalyzed Hydroarylation of Alkynes.
Authors: Reetz Manfred T. , Sommer Knut
Published: July 2005

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A General Model for Selectivity in Olefin Cross Metathesis.
Authors: Chatterjee Arnab K. , Choi Tae‐Lim , Sanders Daniel P. , Grubbs Robert H.
Published: July 2005

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Electrostatic Catalysis by Ionic Aggregates: Scope and Limitations of Mg(ClO4)2 as Acylation Catalyst.
Authors: Chakraborti Asit K. , Sharma Lalima , Gulhane Rajesh , Shivani Shivani
Published: July 2005

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An Efficient and Rapid Synthesis of β‐Carboxamide Derivatives Using 2,2‐Dimethyl‐2H,4H‐1,3‐dioxin‐4‐ones by Microwave Irradiation.
Authors: Miriyala Bruhaspathy , Williamson John S.
Published: July 2005

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Microwave‐Assisted in situ Deprotection and ω‐Methoxylation of TMS‐Protected Aryl Alkynes.
Authors: Wettergren Jenny , Minidis Alexander B. E.
Published: July 2005

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Solution‐Phase Parallel Synthesis of Substituted 1,2‐Ethyl and 1,3‐Propyl Diamines.
Authors: Dagan Ido D. , Lowden Christopher T.
Published: July 2005

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Synthesis of anti‐[2.2](2‐Phenylthiazolophane): A New Heterocyclic Biphenylophane.
Authors: Mashraqui Sabir Hussain , Kumar Sukeerthi
Published: July 2005

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A General Procedure for the One‐Pot Preparation of Polyfunctionalized Nitrocyclopropanes.
Authors: Ballini Roberto , Fiorini Dennis , Palmieri Alessandro
Published: July 2005

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Regioselective 1,4‐Trifluoromethylation of α,β‐Enones Using “Protect‐in‐situ” Methodology.
Authors: Sevenard Dmitri V. , Sosnovskikh Vyacheslav Ya. , Kolomeitsev Alexander A. , Koenigsmann Martin H. , Roeschenthaler Gerd‐Volker
Published: July 2005

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Highly Enantioselective Hydrogenation of Enamides Catalyzed by Rhodium‐Monodentate Phosphoramidite Complex Derived from H8‐BINOL.
Authors: Li Xingshu , Jia Xian , Lu Gui , Au‐Yeung Terry T.‐L. , Lam Kim‐Hung , Lo Thomas W. H. , Chan Albert S. C.
Published: July 2005

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A New “One‐Pot” Synthesis of Hydrazides by Reduction of Hydrazones.
Authors: Perdicchia Dario , Licandro Emanuela , Maiorana Stefano , Baldoli Clara , Giannini Clelia
Published: July 2005

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Fluorinated Hydrazones. Part 1. Reductive Coupling Reactions of Chlorodifluoroacetylated Dialkylhydrazones Using Tetrakis(dimethylamino)ethylene (TDAE).
Authors: Medebielle Maurice , Kato Katsuya , Dolbier William R. Jr.
Published: July 2005

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1,5‐Asymmetric Induction in Boron‐Mediated β‐Alkoxy Methyl Ketone Aldol Addition Reactions.
Authors: Evans David A. , Cote Bernard , Coleman Paul J. , Connell Brian T.
Published: July 2005

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Diastereoselective Allylations and Crotylations under Phase‐Transfer Conditions Using Trifluoroborate Salts: An Application to the Total Synthesis of (‐)‐Tetrahydrolipstatin.
Authors: Thadani Avinash N. , Batey Robert A.
Published: July 2005

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A Catalytic Asymmetric Method for the Synthesis of γ‐Unsaturated β‐Amino Acid Derivatives.
Authors: Lurain Alice E. , Walsh Patrick J.
Published: July 2005

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Formation of 1,4‐Diketones via Bis‐acylation of the Conjugated Carbon—Carbon Double Bonds in Acrylates, Acrylamides, Methyl Vinyl Ketone and Styrenes with Aroyl Chlorides Promoted by Samarium Metal in DMF.
Authors: Liu Yongjun , Zhang Yongmin
Published: July 2005

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A Convenient Method for the Preparation of Inverted tert‐Alkyl Carboxylates from Chiral tert‐Alcohols by a New Type of Oxidation—Reduction Condensation Using 2,6‐Dimethyl‐1,4‐benzoquinone.
Authors: Mukaiyama Teruaki , Shintou Taichi , Fukumoto Kentaro
Published: July 2005

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Halosulfenylation of Conjugated Dienes with Arylsulfenamides in the Presence of Phosphorus Oxyhalides.
Authors: Beloglazkina E. K. , Belova M. A. , Antipin R. L. , Zyk N. V. , Buryak A. K.
Published: July 2005

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In vitro anti‐Acanthamoeba Action by Thioureidic Derivatives.
Authors: Saturnino Carmela , Buonerba Mariafrancesca , Paesano Nicola , Lancelot Jean‐Charles , De Martino Giovanni
Published: July 2005

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trans‐Pd(OAc)2(Cy2NH)2 Catalyzed Suzuki Coupling Reactions and Its Temperature‐Dependent Activities Toward Aryl Bromides.
Authors: Tao Bin , Boykin David W.
Published: July 2005

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Highly Chemoselective Crossed Imino Pinacol Coupling Reaction Using the Synergetic Effect of Boron Trifluoride Etherate and Trichloromethylsilane.
Authors: Shimizu Makoto , Suzuki Ikuhiro , Makino Hiroaki
Published: July 2005

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Cyclodimerization of α,β‐Unsaturated Ketones Promoted by the TiCl4/Sm System.
Authors: Shi Daqing , Rong Liangce , Wang Juxian , Zhuang Qiya , Wang Xiangshan , Tu Shujiang , Hu Hongwen
Published: July 2005

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Stereoselective Synthesis of Tetralins Using Cationic Cyclizations.
Authors: Appelbe Ruth , Casey Mike , Dunne Aideen , Pascarella Enrica
Published: July 2005

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An Unexpected Result in an Intramolecular Ritter Reaction Induced by Triflic Anhydride.
Authors: Justribo Valeria , Colombo Maria I.
Published: July 2005

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A New Protocol for the in situ Generation of Aromatic, Heteroaromatic, and Unsaturated Diazo Compounds and Its Application in Catalytic and Asymmetric Epoxidation of Carbonyl Compounds. Extensive Studies to Map Out Scope and Limitations, and Rationalization of Diastereo‐ and Enantioselectivities.
Authors: Aggarwal Varinder K. , et al. et al.
Published: July 2005

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Synthesis and Root Growth‐Inhibitory Activity of 2‐ and 3‐(Haloacetylamino)‐3‐(2‐furyl)propanoic Acids.
Authors: Kitagawa Tokujiro , Nakamura Mizuki , Masai Katunori
Published: July 2005

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Efficient Synthesis and Photochromic Properties of 2,3‐Position Hybrid Diarylethylene Derivatives.
Authors: Sun Fan , Zhang Fushi , Guo Haobo , Zhou Xinhong , Wang Ruji , Zhao Fuqun
Published: July 2005

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Copper(I)‐Catalyzed Intramolecular Addition of N‐Chloroamides to Double Bonds: An Efficient Synthesis of Lactams from Unsaturated Amides.
Authors: Schulte‐Wuelwer Iris Anne , Helaja Juho , Goettlich Richard
Published: July 2005

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2‐Aryl‐3‐phenylamino‐4,5‐dihydro‐2H‐benz[g]indazoles with Analgesic Activity.
Authors: Schenone Silvia , Bruno Olga , Ranise Angelo , Brullo Chiara , Bondavalli Francesco , Filippelli Walter , Mazzeo Filomena , Capuano Annalisa , Falcone Giuseppe
Published: July 2005

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Studying the Synthesis of 4‐tert‐Butyl‐1,3‐dihydroimidazol‐2‐ones and Their Corresponding Thiones.
Authors: Loksha Yasser M. , Pedersen Erik B. , El‐Barbary Ahmed A. , El‐Badawi Mahmoud A. , Nielsen Claus
Published: July 2005

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Solventless Reactions of 5(4H)‐Oxazolones with Umbelliferones and Selected Enolcarbonyl Compounds.
Authors: Cordaro Massimiliano , Di Donna Leonardo , Foti Francesco , Grassi Giovanni , Napoli Anna , Risitano Francesco , Sindona Giovanni
Published: July 2005

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Synthesis and in vitro Pharmacology of Novel Heterocyclic Muscarinic Ligands.
Authors: De Amici Marco , Conti Paola , Fasoli Ezio , Barocelli Elisabetta , Ballabeni Vigilio , Bertoni Simona , Impicciatore Mariannina , Roth Bryan L. , Ernsberger Paul , De Micheli Carlo
Published: July 2005

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A Convenient Preparation of 3‐Acetyl‐5‐methylisoxazole.
Authors: Sauers Ronald R. , Van Arnum Susan D.
Published: July 2005

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Regio‐ and Stereoselective Preparation of γ‐Alkylidenebutenolides or α‐Pyrones Using a Stille Reaction and Palladium‐Catalyzed Oxacyclization Sequence.
Authors: Rousset Severine , Abarbri Mohamed , Thibonnet Jerome , Parrain Jean‐Luc , Duchene Alain
Published: July 2005

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2‐(Dialkylamino)‐4H‐1‐benzopyran‐4‐one Derivatives Modify Chloride Conductance in CFTR Expressing Cells.
Authors: Mazzei Mauro , Nieddu Erika , Folli Chiara , Caci Emanuela , Galietta Louis V. J.
Published: July 2005

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The Aza‐Silyl‐Prins Reaction: A Novel Method for the Synthesis of trans‐2,6‐Tetrahydropyridines.
Authors: Dobbs Adrian P. , Guesne Sebastien J. J. , Hursthouse Michael B. , Coles Simon J.
Published: July 2005

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New Synthesis of 3‐Fluoropyridine Derivatives.
Authors: Dolbier William R. Jr. , Xu Yu‐Lian
Published: July 2005

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Highly Enantioselective Iridium‐Catalyzed Hydrogenation of Heteroaromatic Compounds: Quinolines.
Authors: Wang Wen‐Bo , Lu Sheng‐Mei , Yang Peng‐Yu , Han Xiu‐Wen , Zhou Yong‐Gui
Published: July 2005

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Novel “Quinolone” Metal Complexes: Synthesis and Spectroscopic Studies of Mg(II), Zn(II), and Ba(II) Complexes with N‐Methyl (or NH)‐3‐Acetyl‐4‐hydroxy Quinolin‐2‐one Ligands.
Authors: Athanasellis Giorgos , Gavrielatos Efstathios , Igglessi‐Markopoulou Olga , Markopoulos John
Published: July 2005

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Towards New Neuroprotective Agents: Design and Synthesis of 4H‐Thieno[2,3‐c]isoquinolin‐5‐one Derivatives as Potent PARP‐1 Inhibitors.
Authors: Pellicciari Roberto , Camaioni Emidio , Constantino Gabriele , Marinozzi Maura , Macchiarulo Antonio , Moroni Flavio , Natalini Benedetto
Published: July 2005

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Synthesis of 3‐ or 4‐Phenyl‐1,8‐naphthyridine Derivatives and Evaluation of Antimycobacterial and Antimicrobial Activity.
Authors: Badawneh Muwaffag , Bellini Laura , Cavallini Tiziana , Al Jamal Jalal , Manera Clementina , Saccomanni Giuseppe , Ferrarini Pier Luigi
Published: July 2005

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Aromatic Nucleophilic Substitution in 1,2,4‐Triazine 4‐Oxides with Grignard Reagents.
Authors: Prokhorov A. M. , Kozhevnikov D. N. , Rusinov V. L. , Chupakhin O. N.
Published: July 2005

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4,4,6‐Trimethyl‐2‐vinyl‐1,3,2‐dioxaborinane: A Superior 2‐Carbon Building Block for Vinylboronate Heck Couplings.
Authors: Lightfoot Andrew P. , Maw Graham , Thirsk Carl , Twiddle Steven J. R. , Whiting Andrew
Published: July 2005

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CsOH‐Promoted Epoxide Ring‐Opening with Phosphines: Mild and Efficient Synthesis of Monohydroxyphosphines.
Authors: Fox Daniel L. , Robinson Ashlee A. , Frank James B. , Salvatore Ralph Nicholas
Published: July 2005

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Antifungal Isopimaranes from Hypoestes serpens.
Authors: Rasoamiaranjanahary L. , Guilet D. , Marston A. , Randimbivololona F. , Hostettmann K.
Published: July 2005

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seco‐Iridoids from Calycophyllum spruceanum (Rubiaceae).
Authors: Zuleta Luz Margarita Cardona , Cavalheiro Alberto Jose , Silva Dulce Helena Siqueira , Furlan Maysa , Young Maria Claudia Marx , Albuquerque Sergio , Castro‐Gamboa Ian , da Silva Bolzani Vanderlan
Published: July 2005

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Selective Epoxidation of Monoterpenes with H2O2 and Polymer‐Supported Methylrheniumtrioxide Systems.
Authors: Saladino Raffaele , Neri Veronica , Pelliccia Anna Rita , Mincione Enrico
Published: July 2005

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Synthesis and Crystal Structure of a New Methoxytrichloro Derivative of Achillin.
Authors: Alebastrov O. V. , Raldugin V. A. , Bagryanskaya I. Yu. , Gatilov Yu. V. , Shakirov M. M. , Kulyjasov A. T. , Adekenov S. M.
Published: July 2005

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Synthetic Study of Optically Active 3‐Azabicyclo[3.3.0]octane‐2,6,8‐tricarboxylic Acid.
Authors: Arakawa Yasushi , Ohnishi Masafumi , Yoshimura Norikazu , Yoshifuji Shigeyuki
Published: July 2005

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Microwave‐Induced, InCl3‐Catalyzed Ferrier Rearrangement of Acetylglycals: Synthesis of 2,3‐Unsaturated Glycopyranosides.
Authors: Das Saibal Kumar , Reddy K. Anantha , Roy Joyita
Published: July 2005

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The Synthesis of Isoquinoline Alkaloid and Its Related Compounds Using Alanine Derivatives as Chiral Auxiliaries.
Authors: Itoh Takashi , Nagata Kazuhiro , Yokoya Masashi , Miyazaki Michiko , Kameoka Keiko , Nakamura Shigeru , Ohsawa Akio
Published: July 2005

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Synthesis of (+/‐) Mappicine and Mappicine Ketone.
Authors: Henegar Kevin E. , Baughman Ted A.
Published: July 2005

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Oligonucleotides and Derivatives as Gene‐Specific Control Agents
Authors: Sun Jiang‐Sheng , Helene Claude
Published: July 2005

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Inhibition of Transcription by bisPNA‐Peptide Conjugates
Authors: Zhao Xin , Kaihatsu Kunihiro , Corey David R.
Published: July 2005

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Oligonucleotide N3′→P5′ Thio‐phosphoramidate Telomerase Template Antagonists as Potential Anticancer Agents
Authors: Gryaznov Sergei , et al. et al.
Published: July 2005

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MDPSCL2: A New Protecting Group for Chemoselective Synthesis of 2′‐O‐Alkylated Guanosines
Authors: Chow Suetying , Wen Ke , Sanghvi Yogesh S. , Theodorakis Emmanuel A.
Published: July 2005

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Phosphono Peptide Nucleic Acids with a Constrained Hydroxyproline‐Based Backbone
Authors: Efimov Vladimir A. , Klykov Valeryi N. , Chakhmakhcheva Oksana G.
Published: July 2005

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Developing Synthetic Methods for Bioactive Phosphorus Compounds Using H‐Phosphonate Chemistry: A Progress Report
Authors: Kraszewski Adam , et al. et al.
Published: July 2005

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Properties of Triple Helices Formed by Oligonucleotides Containing 8‐Aminopurines
Authors: Avino A. , Frieden M. , Morales J. C. , de la Torre B. G. , Gueimil‐Garcia R. , Orozco M. , Gonzalez C. , Eritja R.
Published: July 2005

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Labeling During Cleavage of Nucleic Acids for Their Detection on DNA Chips
Authors: Laayoun A. , Sothier I. , Menou L. , Bernal‐Mendez E. , Kotera M. , Bourget C. , Trevisiol E. , Lhomme J. , Troesch A.
Published: July 2005

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Synthesis of (Z)‐(1‐Fluoro‐2‐hydroxymethylcyclopropylmethyl)purines
Authors: Park Ju‐Hyun , Lee Young Rang , Chun Moon Woo , Jeong Lak Shin , Lee Chong‐Kyo , Kim Hee‐Doo
Published: July 2005

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Synthesis of New Pseudonucleosides Containing Chiral Cyclosulfamides as Agycone
Authors: Berredjem Malika , Aouf Nour‐Eddine
Published: July 2005

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Pterocarpans from Bituminaria morisiana and Bituminaria bituminosa.
Authors: Pistelli Luisa , Noccioli Cecilia , Appendino Giovanni , Bianchi Federica , Sterner Olov , Ballero Mauro
Published: July 2005

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Curtisians E—H: Four p‐Terphenyl Derivatives from the Inedible Mushroom Paxillus curtisii.
Authors: Quang Dang Ngoc , Hashimoto Toshihiro , Nukada Makiko , Yamamoto Isao , Tanaka Masami , Asakawa Yoshinori
Published: July 2005

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Flavonoids of Ochna afzelii.
Authors: Pegnyemb Dieudonne Emmanuel , Tih Raphael Ghogomu , Sondengam Beibam Lucas , Blond Alain , Bodo Bernard
Published: July 2005

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Biologically Active Alkylated Coumarins from Kayea assamica.
Authors: Lee Kyung‐Hee , Chai Hee‐Byung , Tamez Pamela A. , Pezzuto John M. , Cordell Geoffrey A. , Win Khin Khin , Thin‐Wa Maung
Published: July 2005

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Antifungal Flavanones and Prenylated Hydroquinones from Piper crassinervium Kunth.
Authors: Danelutte Ana Paula , Lago Joao Henrique G. , Young Maria Claudia M. , Kato Massuo J.
Published: July 2005

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Microwave‐Assisted Polyol Synthesis of CuInTe2 and CuInSe2 Nanoparticles.
Authors: Grisaru Haviv , Palchik Oleg , Gedanken Aharon , Palchik Valery , Slifkin Michael A. , Weiss Arie M.
Published: July 2005

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Considering Chlorine Dioxide
Authors: Layman Curtis M. , Burkle Jeffrey R.
Published: July 2005

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Molecular Aspects of Halide Ion Hydration: The Cluster Approach
Authors: Robertson William H. , Johnson Mark A.
Published: July 2005

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Lower Rare‐Earth Molybdates
Authors: Tkachenko E. A. , Fedorov P. P.
Published: July 2005

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Structure and Reactivity of Ziegler—Natta Catalyst Intermediates.
Authors: Sobota Piotr
Published: July 2005

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Ionic Liquids and Chirality: Opportunities and Challenges
Authors: Baudequin Christine , Baudoux Jerome , Levillain Jocelyne , Cahard Dominique , Gaumont Annie‐Claude , Plaquevent Jean‐Christophe
Published: July 2005

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Imidoylstannanes, Diazoalkylstannanes, Tin Isocyanates, and Tin Isothiocyanates
Authors: Wyatt P. B.
Published: July 2005

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Tin Carboxylates and Phosphates
Authors: Jousseaume B.
Published: July 2005

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Iminostannanes
Authors: Takeda N. , Tokitoh N. , Okazaki R.
Published: July 2005

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Tin Compounds
Authors: Thomas E. J.
Published: July 2005

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Aryl‐ and Heteroarylgermanes
Authors: Spivey A. C. , Diaper C. M.
Published: July 2005

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Imidoylgermanes (α‐Iminoalkylgermanes) and α‐Diazoalkylgermanes
Authors: Spivey A. C. , Diaper C. M.
Published: July 2005

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Acylgermanes
Authors: Spivey A. C. , Diaper C. M.
Published: July 2005

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Germanium Cyanides
Authors: Spivey A. C. , Diaper C. M.
Published: July 2005

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Gold Is Noble but Gold Hydride Anions Are Stable.
Authors: Wang Xuefeng , Andrews Lester
Published: July 2005

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Tetraaquacobalt(II) Bis[vanadyl(IV)phosphate], [Co(H2O)4][VO(PO4)]2.
Authors: Lin Bi‐Zhou , Pei Xiao‐Ke , Liu Pei‐De
Published: July 2005

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Novel Indigo Light Emitting Long‐Lasting Phosphors CdSiO3: Ln3+ (Ln: Y, La, Gd, Lu).
Authors: Lei Bingfu , Liu Yingliang , Ye Zeren , Shi Chunshan
Published: July 2005

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Synthesis, X‐Ray Data, and Hall Effect Measurements of Li‐Doped Tl—Ba—Ca—Cu—O Superconductor.
Authors: Kayed T. S.
Published: July 2005

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Cooling‐Rate Dependent Ferromagnetism in a Two‐Dimensional Cyano‐Bridged Sm(III)—W(V) Complex.
Authors: Hozumi Toshiya , Ohkoshi Shin‐ichi , Arimoto Yoichi , Seino Hidetake , Mizobe Yasushi , Hashimoto Kazuhito
Published: July 2005

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