bluuebunny/crossref_metadata_2025 huggingface dataset:
Initiating Research into Adapting Rural Hedging Techniques, Hedge Types, and Hedgerow Networks as Novel Urban Green Systems
Authors: Höpfl Lisa , Sunguroğlu Hensel Defne , Hensel Michael , Ludwig Ferdinand
Published: May 2021

This article seeks to initiate research into traditional rural hedging techniques, hedge types, and hedgerow networks for the purpose of their potential adaptation as urban green systems (UGS). The research involves three scales: (1) the plant scale and related manipulation techniques; (2) hedgerows and their context-specific types, ecosystem function, and ecosystem services; and (3) hedgerow networks as continuous green systems that characterize and support specific landscapes. This research required an interdisciplinary approach. The analysis was conducted by applying different modes of research including: (a) an extensive literature review, (b) analysis and systematization of hedge types and manipulation methods, (c) field experiments, (d) design experiments, and (e) examination of real-life projects that use hedges or hedging techniques as distinct design features. The initial research indicates that traditional hedges can be adapted to vitally contribute to UGS by providing a broad range of urban ecosystem services. Furthermore, the research includes initial proposals on future applications of adapted rural hedge types and techniques. On the larger scale, anticipated difficulties regarding implementation, such as land allocation in cities and resource-intensive planting, management, and maintenance, are discussed and further research questions are outlined.
Exploring the Relationship between Locational and Household Characteristics and E-Commerce Home Delivery Demand
Authors: Cheng Cheng , Sakai Takanori , Alho André , Cheah Lynette , Ben-Akiva Moshe
Published: May 2021

The rapid growth in online shopping and associated parcel deliveries prompts investigation of the factors that contribute to parcel delivery demand. In this study, we evaluated the influence of locational and household characteristics on e-commerce home delivery demand. While past research has largely focused on the impacts of the adoption of online shopping using individual/household survey data, we made use of data from an e-commerce carrier. A linear regression model was estimated considering factors such as degree of urbanization, transit and shopping accessibility, and household attributes. The results both confirm and contradict prior research findings, highlighting the potential for a non-negligible influence of the local context on demand for parcel deliveries.
(E)-3-((2-Fluorophenyl)(hydroxy)methylene)imidazo[1,2-a]pyridin-2(3H)-one
Authors: Tenti Giammarco , Cores Ángel , Ramos María Teresa , Menéndez J. Carlos
Published: May 2021

Treatment of a N-2-pyridyl-β-ketoamide precursor with bromine afforded the first example of the 3-aryl(α-hydroxy)methylenelimidazo[1,2-a]pyridin-2(3H)-one framework. This transformation proceeded through a domino process comprising an initial bromination, cyclization via an intramolecular SN reaction, and a final keto-enol tautomerism, and allows generation of the fused heterocyclic system and installation of the acyl substituent in a single operation.
Thermal Stability and Decomposition Kinetics of 1-Alkyl-2,3-Dimethylimidazolium Nitrate Ionic Liquids: TGA and DFT Study
Authors: Meng Jianwen , Pan Yong , Yang Fan , Wang Yanjun , Zheng Zhongyu , Jiang Juncheng
Published: May 2021

The thermal stability and decomposition kinetics analysis of 1-alkyl-2,3-dimethylimidazole nitrate ionic liquids with different alkyl chains (ethyl, butyl, hexyl, octyl and decyl) were investigated by using isothermal and nonisothermal thermogravimetric analysis combined with thermoanalytical kinetics calculations (Kissinger, Friedman and Flynn-Wall-Ozawa) and density functional theory (DFT) calculations. Isothermal experiments were performed in a nitrogen atmosphere at 240, 250, 260 and 270 °C. In addition, the nonisothermal experiments were carried out in nitrogen and air atmospheres from 30 to 600 °C with heating rates of 5, 10, 15, 20 and 25 °C/min. The results of two heating modes, three activation energy calculations and density functional theory calculations consistently showed that the thermal stability of 1-alkyl-2,3-dimethylimidazolium nitrate ionic liquids decreases with the increasing length of the alkyl chain of the substituent on the cation, and then the thermal hazard increases. This study could provide some guidance for the safety design and use of imidazolium nitrate ionic liquids for engineering.
Simultaneous Micro-Structuring and Surface Smoothing of Additive Manufactured Parts Using DLIP Technique and Its Influence on the Wetting Behaviour
Authors: Kuisat Florian , Ränke Fabian , Lasagni Fernando , Lasagni Andrés Fabián
Published: May 2021

It is well known that the surface topography of a part can affect its function as well as its mechanical performance. In this context, we report on the surface modification of additive manufactured components made of Titanium 64 and Scalmalloy®, using Direct Laser Interference Patterning technique. In our experiments, a nanosecond-pulsed near-infrared laser source with a pulse duration of 10 ns was used. By varying the process parameters, periodic structures with different depths and associated roughness values are produced. Additionally, the influence of the resultant morphological characteristics on the wettability behaviour of the fabricated textures is investigated by means of contact angle measurements. The results demonstrated a reduction of the surface roughness of the additive manufactured parts (in the order of some tens of micrometres) and simultaneously the production of well-defined micro-patterns (in the micrometre range), which allow the wettability of the surfaces from 26° and 16° up to 93° and 131° to be tuned for Titanium 6Al 4V and Al-Mg-Sc (Scalmalloy®), respectively.
Thermal and Thermo-Mechanical Properties of Poly(L-lactic Acid) Biocomposites Containing β-Cyclodextrin/d-Limonene Inclusion Complex
Authors: Dobrzyńska-Mizera Monika , Knitter Monika , Mallardo Salvatore , Del Barone Maria Cristina , Santagata Gabriella , Di Lorenzo Maria Laura
Published: May 2021

Bio-based composites made of poly(L-lactic acid) (PLLA) and β-cyclodextrin/d-limonene inclusion complex (CD-Lim) were prepared by melt extrusion. Encapsulation of volatile d-limonene molecules within β-cyclodextrin cages was proven to be a successful strategy to prevent evaporation during high-temperature processing. However, small amounts of limonene were released upon processing, resulting in the plasticization of the polymeric matrix. Morphological analysis revealed good dispersion of the filler, which acted as a nucleating agent, favoring the growth of PLLA crystals. The composites′ lowered glass transition temperature upon the addition of CD-Lim was also proved by thermomechanical analysis (DMA). Moreover, DMA revealed constant stiffness of modified materials at room temperature, which is crucial in PLLA-based formulations.
Some Aspects of Shear Behavior of Soft Soil–Concrete Interfaces and Its Consequences in Pile Shaft Friction Modeling
Authors: Konkol Jakub , Mikina Kamila
Published: May 2021

This paper examines the stiffness degradation and interface failure load on soft soil–concrete interface. The friction behavior and its variability is investigated. The direct shear tests under constant normal load were used to establish parameters to hyperbolic interface model which provided a good approximation of the data from instrumented piles. Four instrumented piles were used to obtain reference soil–concrete interface behavior. It was found that the variability of the friction characteristics is the highest for organic clays and the lowest for organic silts. The intact samples exhibit lower shear strength than reconstituted ones. The adhesion varies significantly depending on interface and soil type, which can result in high scatter of the skin friction prediction. The analysis of parameters variability can be used to determine the upper and lower bound of friction behavior on the interface at constant normal load condition. The backward shearing results in decrease in shear strength up to 40% of the precedent forward phase but higher initial stiffness by a factor of between 2 and 3. Presented research provides basic shear and stiffness parameters for four soft soils (organic clay, organic silt, peat, and silty loam) and gives information about variability of interface characteristics.
Electrical Property Analysis of Textured Ferroelectric Polycrystalline Antimony Sulfoiodide Using Complex Impedance Spectroscopy
Authors: Starczewska Anna , Toroń Bartłomiej , Szperlich Piotr , Nowak Marian
Published: May 2021

Antimony sulfoiodide (SbSI) is a ferroelectric semiconductor with many interesting physical properties (optical, photoconductive, ferroelectric, piezoelectric, etc.). The electrical properties of textured polycrystalline SbSI obtained by the rapid cooling of a melted mass in liquid nitrogen are presented in this work using ac impedance spectroscopy over a wide temperature range (275–500 K) in the frequency range of 1 Hz to 100 kHz. Detailed studies of the impedance Z*(ω), conductivity σ*(ω), electric modulus M*(ω), and dielectric permittivity ε*(ω) of this material were performed using complex impedance spectroscopy for the first time. This study showed that the impedance and related parameters are strongly dependent on temperature. The internal domain structure and the presence of grain boundaries in textured polycrystalline SbSI explain the obtained results.
Special Issue: Layered Double Hydroxides (LDH) and LDH-Based Hybrid Composites
Authors: Matusik Jakub
Published: May 2021

LDHs are a class of two-dimensional layered anionic structures with unique properties [...]
Wear Behavior of Conventionally and Directly Aged Maraging 18Ni-300 Steel Produced by Laser Powder Bed Fusion
Authors: Bae Kichang , Kim Dohyung , Lee Wookjin , Park Yongho
Published: May 2021

This study aims to explore the wear performance of maraging 18Ni-300 steel, fabricated via laser powder bed fusion (LPBF). The building direction dependence of wear resistance was investigated with various wear loads and in terms of ball-on-disk wear tests. The effect of direct aging heat treatment, i.e., aging without solution heat treatment, on the wear performance was investigated by comparing the wear rates of directly aged samples, followed by solution heat treatment. The effect of counterpart material on the wear performance of the maraging steel was studied using two counterpart materials of bearing steel and ZrO2 balls. When the bearing steel ball was used as the counterpart material, both the as-built and heat-treated maraging steel produced by the LPBF showed pronounced building direction dependence on their wear performance when the applied wear load was sufficiently high. However, when the ZrO2 ball was used as the counterpart material, isotropic wear resistance was reported. The maraging steel produced by the LPBF demonstrated excellent wear resistance, particularly when it was aging heat-treated and the counterpart material was ZrO2. The directly aged sample showed wear performance almost the same as the sample solution heat-treated and then aged, indicating that direct aging can be used as an alternative post heat treatment for tribological applications of the maraging steels produced by LPBF.
Design Optimization of Explosion-Resistant System Consisting of Steel Slab and CFRP Frame
Authors: Kim Jung J.
Published: May 2021

This study presents an explosion-resistant hybrid system containing a steel slab and a carbon fiber-reinforced polymer (CFRP) frame. CFRP, which is a high-strength material, acts as an impact reflection part. Steel slab, which is a high-ductility material, plays a role as an impact energy absorption part. Based on the elastoplastic behavior of steel, a numerical model is proposed to simulate the dynamic responses of the hybrid system under the air pressure from an explosion. Based on this, a case study is conducted to analyze and identify the optimal design of the proposed hybrid system, which is subjected to an impact load condition. The observations from the case study show the optimal thicknesses of 8.2 and 7 mm for a steel slab and a ϕ100 mm CFRP pipe for the hybrid system, respectively. In addition, the ability of the proposed hybrid system to resist an uncertain explosion is demonstrated in the case study based on the reliability methodology.
Effects of Loading and Boundary Conditions on the Performance of Ultrasound Compressional Viscoelastography: A Computational Simulation Study to Guide Experimental Design
Authors: Lin Che-Yu , Chang Ke-Vin
Published: May 2021

Most biomaterials and tissues are viscoelastic; thus, evaluating viscoelastic properties is important for numerous biomedical applications. Compressional viscoelastography is an ultrasound imaging technique used for measuring the viscoelastic properties of biomaterials and tissues. It analyzes the creep behavior of a material under an external mechanical compression. The aim of this study is to use finite element analysis to investigate how loading conditions (the distribution of the applied compressional pressure on the surface of the sample) and boundary conditions (the fixation method used to stabilize the sample) can affect the measurement accuracy of compressional viscoelastography. The results show that loading and boundary conditions in computational simulations of compressional viscoelastography can severely affect the measurement accuracy of the viscoelastic properties of materials. The measurement can only be accurate if the compressional pressure is exerted on the entire top surface of the sample, as well as if the bottom of the sample is fixed only along the vertical direction. These findings imply that, in an experimental validation study, the phantom design should take into account that the surface area of the pressure plate must be equal to or larger than that of the top surface of the sample, and the sample should be placed directly on the testing platform without any fixation (such as a sample container). The findings indicate that when applying compressional viscoelastography to real tissues in vivo, consideration should be given to the representative loading and boundary conditions. The findings of the present simulation study will provide a reference for experimental phantom designs regarding loading and boundary conditions, as well as guidance towards validating the experimental results of compressional viscoelastography.
Approximately Model of the Maximum Temperature on the Chip Surface
Authors: Bartoszuk Marian
Published: May 2021

This article presents an approximately model that allows for the determination of the maximum temperature of the chip surface in dry orthogonal turning. The mathematical formula describing the maximum temperature of the chip surface was formulated based on experimental data. The experiments were carried out for orthogonal cutting of austenitic steel AISI 321 with flat rake face carbide inserts that were made of tungsten carbide H10F, both uncoated and coated, with coatings of varied arrangement. Thermographic images of the cutting zone were used to verify the correctness of the approximately model. The obtained results show good agreement between the modelling results and experimental studies. The discrepancy of the maximum temperature values of the top surface of the chip does not exceed 6.4%.
The Analysis of Deformability, Structure and Properties of AZ61 Cast Magnesium Alloy in a New Hammer Forging Process for Aircraft Mounts
Authors: Dziubińska Anna , Surdacki Piotr , Majerski Krzysztof
Published: May 2021

This article presents the analysis of the deformability, structure and properties of the AZ61 cast magnesium alloy on the example of a new forging process of aircraft mount forgings. It was assumed that their production process would be based on drop forging on a die hammer. Two geometries of preforms, differing in forging degree, were used as the billet for the forging process. It was assumed that using a cast, unformed preform positively affects the deformability of hard-deformable magnesium alloys and flow kinematics during their forging and reduces the number of operations necessary to obtain the correct product. Numerical analysis of the proposed new technology was carried out using DEFORM 3D v.11, a commercial program dedicated to analyzing metal forming processes. The simulations were performed in the conditions of spatial strain, considering the full thermomechanical analysis. The obtained results of numerical tests confirmed the possibility of forming the forgings of aviation mounts from the AZ61 cast magnesium alloy with the proposed technology. They also allowed us to obtain information about the kinematics of the material flow during forming and process parameters, such as strain intensity distribution, temperatures, Cockcroft–Latham criterion and forming energy. The proposed forging process on a die hammer was verified in industrial conditions. The manufactured forgings of aircraft mounts made of AZ61 magnesium alloy were subjected to qualitative tests in terms of their structure, conductivity and mechanical properties.
Graphene-Based Two-Dimensional Mesoporous Materials: Synthesis and Electrochemical Energy Storage Applications
Authors: Park Jongyoon , Lee Jiyun , Kim Seongseop , Hwang Jongkook
Published: May 2021

Graphene (G)-based two dimensional (2D) mesoporous materials combine the advantages of G, ultrathin 2D morphology, and mesoporous structures, greatly contributing to the improvement of power and energy densities of energy storage devices. Despite considerable research progress made in the past decade, a complete overview of G-based 2D mesoporous materials has not yet been provided. In this review, we summarize the synthesis strategies for G-based 2D mesoporous materials and their applications in supercapacitors (SCs) and lithium-ion batteries (LIBs). The general aspect of synthesis procedures and underlying mechanisms are discussed in detail. The structural and compositional advantages of G-based 2D mesoporous materials as electrodes for SCs and LIBs are highlighted. We provide our perspective on the opportunities and challenges for development of G-based 2D mesoporous materials. Therefore, we believe that this review will offer fruitful guidance for fabricating G-based 2D mesoporous materials as well as the other types of 2D heterostructures for electrochemical energy storage applications.
Sustained Release of Bone Morphogenetic Protein-2 through Alginate Microbeads Enhances Bone Regeneration in Rabbit Tibial Metaphyseal Defect Model
Authors: Kim Junhyung , Lee Seoyun , Choi Yonghyun , Choi Jonghoon , Kang Byung-Jae
Published: May 2021

Bone morphogenetic protein-2 (BMP-2) is widely used to enhance bone regeneration. However, because of its short half-life and rapid disappearance, large amounts of BMP-2 are needed, leading to unintended side effects. In this study, BMP-2-encapsulated alginate microbeads (AM) were used to enhance bone regeneration. Enzyme-linked immunosorbent assay confirmed the sustained release of BMP-2 from AM. Vascular endothelial growth factor (VEGF)-adsorbing aptamer-conjugated hydroxyapatite (Apt-HA) was used for osteoconduction and dual delivery of VEGF and BMP-2. For in vivo bone regeneration evaluation, the grafts (1) Apt-HA + phosphate-buffered saline (PBS), (2) Apt-HA + AM without BMP-2, (3) Apt-HA + BMP-2, and (4) Apt-HA + AM encapsulated with BMP-2 were implanted into rabbit tibial metaphyseal defects. After four weeks, micro-computed tomography (CT), histological, and histomorphometric analyses were performed to evaluate bone regeneration. The Apt-HA + AM with BMP-2 group revealed a significantly higher new bone volume and bone volume/total volume (BV/TV) in both cortical and trabecular bone than the others. Furthermore, as evaluated by histomorphometric analysis, BMP-2 AM exhibited a significantly higher bone formation area than the others, indicating that AM could be used to efficiently deliver BMP-2 through sustained release. Moreover, the combined application of BMP-2-encapsulated Apt-HA + AM may effectively promote bone regeneration.
Magnetic Anisotropy and Damping Constant of Ferrimagnetic GdCo Alloy near Compensation Point
Authors: Joo Sungjung , Alemayehu Rekikua Sahilu , Choi Jong-Guk , Park Byong-Guk , Choi Gyung-Min
Published: May 2021

Metallic ferrimagnets with rare earth-transition metal alloys can provide novel properties that cannot be obtained using conventional ferromagnets. Recently, the compensation point of ferrimagnets, where the net magnetization or net angular momentum vanishes, has been considered a key aspect for memory device applications. For such applications, the magnetic anisotropy energy and damping constant are crucial. In this study, we investigate the magnetic anisotropy and damping constant of a GdCo alloy, with a Gd concentration of 12–27%. By analyzing the equilibrium tilting of magnetization as a function of the applied magnetic field, we estimate the uniaxial anisotropy to be 1–3 × 104 J m−3. By analyzing the transient dynamics of magnetization as a function of time, we estimate the damping constant to be 0.08–0.22.
Exposure to Iron Oxide Nanoparticles Coated with Phospholipid-Based Polymeric Micelles Induces Renal Transitory Biochemical and Histopathological Changes in Mice
Authors: Balas Mihaela , Popescu Din Ioana Mihaela , Hermenean Anca , Cinteza Ludmila Otilia , Dinischiotu Anca
Published: May 2021

The renal toxicity induced by the intravenously injected iron oxide nanoparticles (IONPs) encapsulated in phospholipid-based polymeric micelles was studied in CD1 mice for 2 weeks. Two doses of 5 and 15 mg of Fe/kg bodyweight of NPs or saline solution (control) were tested, and the levels of antioxidant enzyme activities, oxidative stress parameters, and the expressions of kidney fibrosis biomarkers were analyzed. The enzymatic activities of superoxide dismutase, catalase, glutathione peroxidase, glutathione-S-transferase, glutathione reductase, and glucose-6-phosphate dehydrogenase in the kidney were significantly decreased compared to the control in the first 3 days followed by a recovery up to 14 days. Concomitantly, a significant increase in lipid peroxidation (malondialdehyde) levels and a decrease in protein thiol groups were recorded. Moreover, increases in the expressions of T cell immunoglobulin and mucin domain 1 (TIM-1) and transforming growth factor-β (TGF-β) were observed in mouse tissue samples in the first week, which were more pronounced for the higher dose. The results suggested the role of oxidative stress as a mechanism for induced toxicity in mice kidneys after the IV administration of IONPs encapsulated in phospholipid-based polymeric micelles but also the capacity of the kidneys’ defense systems to revert efficiently the biochemical modifications that were moderate and for short duration.
Effect of Surface Roughness Characteristics on Structural Performance of Hollow Core Slabs
Authors: Lee Yong-Jun , Kim Hyeong-Gook , Jeong Chan-Yu , Kim Dong-Hwan , Han Sang-Pil , Kim Kil-Hee
Published: May 2021

This study was conducted to evaluate the flexural performance of hollow core slabs (HCS) incorporating the effect of surface roughness. The HCSs are suitable for long span structures due to reduced self-weight. The specimens were HCS with topping concrete and the variables were cross sectional height and surface roughness. The tests were conducted on simply supported beams under four-point loads. The results showed that specimens with interface roughness applied in the lengthwise direction of members exhibited ductile flexural behavior up to peak load than those with interface roughness applied in the member width direction. Their flexural strength was also higher by 1–7% on average, indicating that they are advantageous in improving structural performance.
Incorporation of Copper-Doped Mesoporous Bioactive Glass Nanospheres in Experimental Dental Composites: Chemical and Mechanical Characterization
Authors: Marovic Danijela , Haugen Håvard J. , Negovetic Mandic Visnja , Par Matej , Zheng Kai , Tarle Zrinka , Boccaccini Aldo R.
Published: May 2021

Experimental dental resin composites incorporating copper-doped mesoporous bioactive glass nanospheres (Cu-MBGN) were designed to impart antibacterial and remineralizing properties. The study evaluated the influence of Cu-MBGN on the mechanical properties and photopolymerization of resin composites. Cu-MBGN were synthesized using a microemulsion-assisted sol–gel method. Increasing amounts of Cu-MBGN (0, 1, 5, and 10 wt %) were added to the organic polymer matrix with inert glass micro- and nanofillers while maintaining a constant resin/filler ratio. Six tests were performed: X-ray diffraction, scanning electron microscopy, flexural strength (FS), flexural modulus (FM), Vickers microhardness (MH), and degree of conversion (DC). FS and MH of Cu-MBGN composites with silica fillers showed no deterioration with aging, with statistically similar results at 1 and 28 days. FM was not influenced by the addition of Cu-MBGN but was reduced for all tested materials after 28 days. The specimens with 1 and 5% Cu-MBGN had the highest FS, FM, MH, and DC values at 28 days, while controls with 45S5 bioactive glass had the lowest FM, FS, and MH. DC was high for all materials (83.7–93.0%). Cu-MBGN composites with silica have a potential for clinical implementation due to high DC and good mechanical properties with adequate resistance to aging.
Preparation of Ultrafiltration Membrane by Polyethylene Glycol Non-Covalent Functionalized Multi-Walled Carbon Nanotubes: Application for HA Removal and Fouling Control
Authors: Wang Yu , Dong Mengchan , Xiong Xinya , Gai Xiaoli , Zeng Jia , Luan Guirong , Wang Yufei , Wu Yaochen , Guo Jin
Published: May 2021

Polyethylene glycol (PEG) non-covalent-functionalized multi-walled carbon nanotubes (MWCNT) membrane were prepared by vacuum filtration. The dispersion and stability of MWCNT non-covalent functionalized with PEG were all improved. TEM characterization and XPS quantitative analysis proved that the use of PEG to non-covalent functionalize MWCNT was successful. SEM image analysis confirmed that the pore size of PEG–MWCNT membrane was more concentrated and distributed in a narrower range of diameter. Contact angle measurement demonstrated that PEG non-covalent functionalization greatly enhanced the hydrophilicity of MWCNT membranes. The results of pure water flux showed that the PEG–MWCNT membranes could be categorized into low pressure membrane. PEG-MWCNT membrane had a better effect on the removal of humic acid (HA) and a lower TMP growth rate compared with a commercial 0.01-μm PVDF ultrafiltration membrane. During the filtration of bovine serum albumin (BSA), the antifouling ability of PEG-MWCNT membranes were obviously better than the raw MWCNT membranes. The TMP recovery rate of PEG–MWCNT membrane after cross flushing was 79.4%, while that of raw MWCNT–COOH and MWCNT membrane were only 14.9% and 28.3%, respectively. PEG non-covalent functionalization improved the antifouling ability of the raw MWCNT membranes and reduced the irreversible fouling, which effectively prolonged the service life of MWCNT membrane.
Transformation of the Microstructure of Fe-Cr Steel during Its Production
Authors: Núñez Andrés , Collado Irene , Almagro Juan F. , Sales David L.
Published: May 2021

EN 1.4016 stainless steels combine good corrosion resistance with good formability and ductility. As such, their most popular applications are related to sheet forming. During re-crystallisation of Fe-Cr steels, deviations from the desired γ-fibre (gamma fibre, <111>||ND) texture promote a decrease in deep drawability. Additionally, α-fibre (alpha fibre, <110>||RD) has been found to be damaging to formability. In this study, an EN 1.4016 basic material and a modified one with optimised settings as regards to chemical composition and manufacturing process, in order to improve the formability properties, are characterised. The phase diagram, microstructure, Lankford coefficients and Electron Backscatter Diffraction (EBSD) (results confirm the evolution of texture during the processing of ferritic stainless steel. Texture is analysed by the interpretation of Orientation Distribution Function (ODF), using orientation density results for each sample obtained in the processing route. The cube ({001} <100>) and rotated cube ({001} <110>) textures dominate the crystal orientation from the slab until the intermediate annealing stage. After final annealing, there is a texture evolution in both materials; the γ-fibre component dominates the texture, which is much more intense in modified material supported by components that show good deep drawability, {554} <225>, and good transition from hot to cold rolling, {332} <113>. The modified composition and process material delivers a better re-crystallisation status and, therefore, the best drawability performance.
Deformation Characteristics and Microstructure Analysis of Aluminum Alloy Component with Complex Shape by Cold Orbital Forming
Authors: Feng Wei , Jin Chaoyi , Deng Jiadong , Zhuang Wuhao
Published: May 2021

This work aimed to study the deformation characteristics and microstructure of AA6063 aluminum alloy component with complex shape manufactured by cold orbital forming processing. The material flowing behavior was analyzed by Finite Element (FE) simulation and forming experiments were carried out using bar blank with different lengths. The microstructure of the boss zone cut from the formed samples was observed using scanning electron microscopy (SEM) and electron back-scatter diffraction (EBSD). FE simulation and experiment results both showed the aluminum base can be formed using cold orbital forming process. The distributions of the effective strain of the component with different blank lengths were almost the same, and the effective strain was bigger at the boss and the flash as the forming finished. The material flow is complex, especially in the boss, and the folding defect was observed at the root of the boss. The distribution of Mg2Si strengthening precipitate is more homogeneous in the matrix, has a different shape, and shows directivity at different position of boss zone. The grains are elongated, and the extent is different at different positions of the boss zone after cold orbital forming, and the crystal orientation discrepancy is smaller in the component main body and bigger in the boss zone. Subsequent forming process and blank optimization need to be further researched to improve forming quality.
Metallurgical and Mechanical Characterization of Low Carbon Steel—Stainless Steel Dissimilar Joints Made by Laser Autogenous Welding
Authors: Scutelnicu Elena , Iordachescu Mihaela , Rusu Carmen Catalina , Mihailescu Danut , Ocaña José Luis
Published: May 2021

This paper addresses the metallurgical and mechanical characterization of dissimilar joints made by laser autogenous welding between thin sheets of low-carbon steel (CS) and austenitic stainless steel (SS). The welding technology applied, previously optimized to produce sound dissimilar joints, is based on the heat source displacement from the weld gap centerline towards CS, in order to reduce the SS overheating. The research includes optical microscopy observations, energy dispersive X-ray analysis (EDX) to assess the wt% of Cr, Ni, and Fe in all regions of the dissimilar welded joint, hardness measurements, and tensile tests of transverse-welded flat specimens. In comparison with classical determination of the joint overall mechanical characteristics, the novelty of this research consists of experimental assessment of the local mechanical behavior of the fusion and heat affected zones by using a digital image correlation technique (VIC-2D). This is an efficient tool for determining the constitutive properties of the joint, useful for modelling the mechanical behavior of materials and for verifying the engineering predictions. The results show that the positive difference in yielding between the weld metal and the base materials protects the joint from being plastically deformed. As a consequence, the tensile loading of flat transverse specimens generates the strain localization and failure in CS, far away from the weld.
Influence of Morphology of Intermetallic Particles on the Microstructure and Properties Evolution in Severely Deformed Al-Fe Alloys
Authors: Medvedev Andrey , Murashkin Maxim , Enikeev Nariman , Medvedev Evgeniy , Sauvage Xavier
Published: May 2021

This study focuses on the difference in microstructural features and physical properties of Al-2Fe and Al-4Fe alloys subjected to large plastic straining. The difference in the intermetallic particle morphology in the initial state is shown to be a key parameter influencing the particle and grain fragmentation process and, as a result, the properties of these two alloys. We demonstrate that the shape and average size of Al-Fe intermetallic particles provide stronger effect on the microstructure evolution during high pressure torsion (HPT) than their volume fraction. The formation of Fe supersaturated solid solution in Al in these two alloys during deformation is discussed in connection to the morphology of the intermetallic phase. The major microstructural attributes, responsible for the solid solution formation, are highlighted.
Controlling Capillary Flow Rate on Lateral Flow Test Substrates by Tape
Authors: Xiao Zhiqing , Yang Yuqian , Zhang Xingwei , Guo Weijin
Published: May 2021

Controlling capillary flow rate of sample liquid is of high interest for lateral flow tests, since the flow rate can affect the dissolution and mixing of the immunoreagents and the efficiency of immunoreactions. Here we develop a facile method to adjust the capillary flow rate on lateral flow test substrates by using tape to cover the surface of substrates. We test this method on the traditional lateral flow test substrate—nitrocellulose and a novel lateral flow test substrate—synthetic paper, which is a porous media made by interlocked off-stoichiometry thiol-ene (OSTE) micropillars. We found that after the surface was covered by tape, the average flow rate decreased to 61% of the original flow rate on nitrocellulose, while the average flow rate increased to at least 320% of the original flow rate on synthetic paper. More interesting, besides the increase of flow rate, the volume capacity of synthetic paper also increases after covered by tape. Furthermore, we investigated the influence of length and position of tape on the capillary flow rate for nitrocellulose. A longer tape will lead to a smaller flow rate. The influence of tape of same length on the flow rate is bigger when the tape is placed closer to the loading pad. These results can help in the flow rate control on lateral flow test substrates, and potentially improve the performance of lateral flow tests.
Study of the Absorption of Electromagnetic Radiation by 3D, Vacuum-Packaged, Nano-Machined CMOS Transistors for Uncooled IR Sensing
Authors: Cherniak Gil , Avraham Moshe , Bar-Lev Sharon , Golan Gady , Nemirovsky Yael
Published: May 2021

There is an ongoing effort to fabricate miniature, low-cost, and sensitive thermal sensors for domestic and industrial uses. This paper presents a miniature thermal sensor (dubbed TMOS) that is fabricated in advanced CMOS FABs, where the micromachined CMOS-SOI transistor, implemented with a 130-nm technology node, acts as a sensing element. This study puts emphasis on the study of electromagnetic absorption via the vacuum-packaged TMOS and how to optimize it. The regular CMOS transistor is transformed to a high-performance sensor by the micro- or nano-machining process that releases it from the silicon substrate by wafer-level processing and vacuum packaging. Since the TMOS is processed in a CMOS-SOI FAB and is comprised of multiple thin layers that follow strict FAB design rules, the absorbed electromagnetic radiation cannot be modeled accurately and a simulation tool is required. This paper presents modeling and simulations based on the LUMERICAL software package of the vacuum-packaged TMOS. A very high absorption coefficient may be achieved by understanding the physics, as well as the role of each layer.
Effect of Solution and Aging Temperatures on Microstructure and Mechanical Properties of 10Cr13Co13Mo5Ni3W1VE(S280) Steel
Authors: Zhong Jinyan , Chen Zun , Yang Shanglin , Li Songmei , Liu Jianhua , Yu Mei
Published: May 2021

The article investigated the effects of solution and ging temperatures on microstructure and mechanical properties of ultra-high strength stainless steel 10Cr13Co13Mo5Ni3W1VE(S280). Higher solution temperatures can improve impact toughness because of the quantity reduction of submicron-sized particles which act as microporous nucleation sites. S280 has the best mechanical properties at 1080 °C solution temperature. After quenching, the steel is completely martensite with almost no retained austenite. Aging at 560 °C results in peak strength due to the precipitation of fine carbides coherent zones. The loss of precipitates/matrix coherency and precipitates coarsening cause a decrease in strength at higher aging temperatures. Good strength and toughness obtained at 540 °C aging temperature are attributed to fine and dispersed strengthening phases such as Cr2C and Fe2Mo, and the recovery of austenite in high-density dislocation martensite matrix. The details of electron microscopy research, strengthening and toughening mechanisms are discussed.
Femtosecond Laser Trimming with Simultaneous Nanostructuring to Fine Piercing Punch to Electrical Amorphous Steel Sheets
Authors: Aizawa Tatsuhiko , Shiratori Tomomi , Kira Yoshihiro , Yoshino Tomoaki , Suzuki Yohei
Published: May 2021

A CVD (Chemical Vapor Deposition) diamond coated tungsten carbide (WC) and cobalt (Co) sintered alloy punch was trimmed by the femtosecond laser machining to sharpen its edge with about 2 μm and to simultaneously make nanostructuring to its side surface. In addition to the sharpened edge, its edge profile was formed to be homogeneous enough to reduce the damage layer width by piercing the electrical amorphous steel sheet stack. Each brittle sheet in the stacked work was damaged to have three kinds of defects by piercing; e.g., the droop-like cracking in the thickness and at the vicinity of hole, the wrinkling in peak-to-valley with partial cracking on the peaks, and the circumferential cracking. When using the WC (Co) punch with the inhomogeneous edge profile in the sharpened edge width, these three damages were induced into each sheet and the maximum damage width exceeded 80 μm. When using the punch with the sharpened edge and homogeneous edge profile, the wrinkling mode was saved and the total affected layer width was significantly reduced to less than 20 μm. Through the precise embossing experiments, this effect of punch edge profile condition to the induced damages was discussed with a statement on the nanostructuring effect on the reduction of damaged width in electrical amorphous steel sheets. The developed tool with the sharpened edge and homogenous edge condition contributes to the realization of a low iron loss motor with a reduced affected layer width.
Three-Dimensional Arterial Pulse Signal Acquisition in Time Domain Using Flexible Pressure-Sensor Dense Arrays
Authors: Chen Jianzhong , Sun Ke , Zheng Rong , Sun Yi , Yang Heng , Zhong Yifei , Li Xinxin
Published: May 2021

In this study, we developed a radial artery pulse acquisition system based on finger-worn dense pressure sensor arrays to enable three-dimensional pulse signals acquisition. The finger-worn dense pressure-sensor arrays were fabricated by packaging 18 ultra-small MEMS pressure sensors (0.4 mm × 0.4 mm × 0.2 mm each) with a pitch of 0.65 mm on flexible printed circuit boards. Pulse signals are measured and recorded simultaneously when traditional Chinese medicine practitioners wear the arrays on the fingers while palpating the radial pulse. Given that the pitches are much smaller than the diameter of the human radial artery, three-dimensional pulse envelope images can be measured with the system, as can the width and the dynamic width of the pulse signals. Furthermore, the array has an effective span of 11.6 mm—3–5 times the diameter of the radial artery—which enables easy and accurate positioning of the sensor array on the radial artery. This study also outlines proposed methods for measuring the pulse width and dynamic pulse width. The dynamic pulse widths of three volunteers were measured, and the dynamic pulse width measurements were consistent with those obtained by color Doppler ultrasound. The pulse wave velocity can also be measured with the system by measuring the pulse transit time between the pulse signals at the brachial and radial arteries using the finger-worn sensor arrays.
Enhanced Signal-to-Noise and Fast Calibration of Optical Tweezers Using Single Trapping Events
Authors: Stilgoe Alexander B. , Armstrong Declan J. , Rubinsztein-Dunlop Halina
Published: May 2021

The trap stiffness us the key property in using optical tweezers as a force transducer. Force reconstruction via maximum-likelihood-estimator analysis (FORMA) determines the optical trap stiffness based on estimation of the particle velocity from statistical trajectories. Using a modification of this technique, we determine the trap stiffness for a two micron particle within 2 ms to a precision of ∼10% using camera measurements at 10 kfps with the contribution of pixel noise to the signal being larger the level Brownian motion. This is done by observing a particle fall into an optical trap once at a high stiffness. This type of calibration is attractive, as it avoids the use of a nanopositioning stage, which makes it ideal for systems of large numbers of particles, e.g., micro-fluidics or active matter systems.
Taloe—Sedimentation in an Intermittent Lake (Russian Federation, Republic of Khakassia)
Authors: Khrushcheva Maria O. , Dutova Ekaterina M. , Tishin Platon A. , Arkhipov Alexander L. , Nikitenkov Alexei N. , Chernyshov Alexei I.
Published: May 2021

This paper examines the mineral and geochemical features of lake sediments and waters in intermittent Lake Taloe, located in a semiarid climate. Minerals that belong to groups of oxides, sulfides, aluminosilicates, carbonates, sulfates, and halides are identified through the use of precision methods. The resulting mineral species are divided by genetic features into two associations: terrigenous and hydrogenic. The terrigenous association includes water-insoluble minerals, while the hydrogenic association combines typical hydrogenic minerals. The regularities of the accumulation and distribution of minerals along the lake laterally and to a depth of up to one meter are also examined. The order of deposition of hydrogenous association minerals from sulfate-chloride lake waters was established. The obtained results are confirmed and supplemented by physicochemical calculations, which show the equilibrium of lake waters with hydroxides, oxides, aluminosilicates, carbonates, and sulfates. It has been established that the formation of minerals mainly occurs through evaporative concentration in conjunction with bedrock weathering.
Low Temperature Illitization through Illite-Dioctahedral Vermiculite Mixed Layers in a Tropical Saline Lake Rich in Hydrothermal Fluids (Sochagota Lake, Colombia)
Authors: Cifuentes Gabriel Ricardo , Jiménez-Millán Juan , Quevedo Claudia Patricia , Nieto Fernando , Cuadros Javier , Jiménez-Espinosa Rosario
Published: May 2021

In this investigation, we showed that high salinity promoted by hydrothermal inputs, reducing conditions of sediments with high content in organic matter, and the occurrence of an appropriate clay mineral precursor provide a suitable framework for low-temperature illitization processes. We studied the sedimentary illitization process that occurs in carbonaceous sediments from a lake with saline waters (Sochagota Lake, Colombia) located at a tropical latitude. Water isotopic composition suggests that high salinity was produced by hydrothermal contribution. Materials accumulated in the Sochagota Lake’s southern entrance are organic matter-poor sediments that contain detrital kaolinite and quartz. On the other hand, materials formed at the central segment and near the lake exit (north portion) are enriched in organic matter and characterized by the crystallization of Fe-sulfides. X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), high resolution transmission electron microscopy (HRTEM), and energy dispersive X-ray spectrometry (EDX) data allowed for the identification of illite and illite-dioctahedral vermiculite mixed layers (I-DV), which are absent in the southern sediments. High humidity and temperate climate caused the formation of small-sized metastable intermediates of I-DV particles by the weathering of the source rocks in the Sochagota Lake Basin. These particles were deposited in the low-energy lake environments (middle and north part). The interaction of these sediments enriched in organic matter with the saline waters of the lake enriched in hydrothermal K caused a reducing environment that favored Fe mobilization processes and its incorporation to I-DV mixed layers that acted as mineral precursor for fast low temperature illitization, revealing that in geothermal areas clays in lakes favor a hydrothermal K uptake.
Geochronological and Paleomagnetic Constraints on the Lower Cretaceous Dalazi Formation from the Yanji Basin, NE China, and its Tectonic Implication
Authors: Shen Zhongshan , Yu Zhiqiang , Ye Hanqing , Qin Zuohuan , Xi Dangpeng
Published: May 2021

The Lower Cretaceous Dalazi Formation in the Yanji Basin, eastern Jilin Province is of particular interest because it contains key fresh water fossil taxa, oil and gas resources, a potential terrestrial Albian–Cenomanian boundary, and regional unconformities. However, the lack of a precise chronology for the non-marine strata has precluded a better understanding of the regional stratigraphic correlation and terrestrial processes. Here, we report magnetostratigraphic and U–Pb geochronologic results of a sedimentary sequence from the Xing’antun section in the Yanji Basin. Thirty-two zircons from the tuff sample were analyzed by secondary ion mass spectrometry (SIMS); the U–Pb zircon dating method yielded a weighted mean of 206Pb/238U age of 105.7 ± 0.8 Ma (2σ, internal error). Paleomagnetic results show that the Dalazi Formation is of normal polarity, which was correlated to the early chron C34n constrained by the SIMS U–Pb zircon geochronologic data, further demonstrating that the terrestrial sedimentary sequence of the upper Dalazi Formation is of late Albian age. The established geochronologic framework allows the regional correlation of the Dalazi Formation in the Yanji Basin to the strata from other terrestrial sequences in northeastern China. The similar geodynamic and geologic background between the Yanji Basin and other terrestrial rift basins in northeastern China suggests that the unconformity between the Dalazi and Longjing formations may represent syn-rift and post-rift stages in the Yanji Basin, and thus the switch from extension to contraction during the mid-Cretaceous, precisely constrained to ~106–101 Ma based on our new chronology and previously published high-precision U–Pb dating of the lower Longjing Formation. It is most likely attributable to the docking of the west Pacific plate along the East Asian continental margin.