Conclusions .
Airborne-particle abrasion and tribo-chemical silica coating are the pre-treatment methods with more evidence in the literature .
Increased adhesion could be expected after physico-chemical conditioning of zirconia .
Surface contamination has a negative effect on adhesion .
There is no evidence to support a universal adhesion protocol
Background .
Reliable bonding between resin composite cements and high strength ceramics is difficult to achieve because of their chemical inertness and lack of silica content that makes etching impossible .
The purpose of this review is to classify and analyze the existing methods and material s suggested to improve the adhesion of zirconia to dental substrate by using composite resins , in order to explore current trends in surface conditioning methods with predictable results .
Methods .
Silica-based nano-coating on zirconia surfaces using reactive magnetron sputtering: effect on chemical adhesion of resin cements.
PURPOSE To compare the effect of silica (Si)-based nano-coating deposited by reactive magnetron sputtering ( RMP ) with that of conventional surface conditioning using metal/zirconia primer alone or after air-particle abrasion on the adhesion of resin cements to zirconia ceramic . MATERIAL S AND METHODS Two hundred forty zirconia ceramic blocks ( Cercon ) were sintered , finished with 1200- grit SiC paper under water cooling , and cleaned ultrasonically in distilled water for 10 min . The blocks ( 4.5 mm x 3.5 mm x 4.5 mm ) were r and omly divided into 24 groups ( n = 10 ) according to 3 testing parameters : a ) resin cements ( Multilink , Panavia F , RelyX U100 ) , b ) surface conditioning ( no conditioning as control group ; Metal/Zirconia Primer ; air abrasion + Metal/Zirconia Primer ; Si-based nanofilm + Monobond s ) ; c ) aging ( no aging vs thermocycling at 5 ° C to 55 ° C , 6000 cycles ) . The nanofilm was deposited by direct current using argon/oxygen plasma ( 8:1 in flux ) on the zirconia surface . Resin cements were bonded to zirconia surfaces using polyethylene molds . The shear bond strength ( SBS ) test was performed using a universal testing machine ( 1 mm/min ) , and after debonding , the substrate and adherent surfaces were analyzed using optical and scanning electron microscopes to categorize the failure types . The data were statistically evaluated using 3-way ANOVA and Tukey 's test ( 5 % ) . RESULTS Resin cement type ( p < 0.05 ) , surface conditioning method ( p < 0.05 ) , and aging condition ( p < 0.05 ) had a significant effect on the bond strength results . Interactions were also significant ( p < 0.05 ) . In the nonaged condition , while control groups presented the lowest results with all cements ( 0 to 5.2 MPa ) , the airabraded group in combination with RelyX U100 result ed in the highest SBS ( 21.8 ± 6.7 MPa ) . After aging , the SBS results decreased in the air-abraded groups for all cements ( 4.54 to 9.44 MPa ) and showed no statistical significance compared to the Si-based nanocoated groups ( 4.24 to 6.44 MPa ) . After air-abrasion and primer application , only Panavia F and RelyX U100 cements showed exclusively mixed failures , but after nanofilm coating and silanization , all cements showed exclusively mixed failures with and without aging . CONCLUSION Chemical adhesion of the resin cements tested to zirconia was similar after silica-based nanofilm deposition and air abrasion followed by primer application
Conclusions .
Airborne-particle abrasion and tribo-chemical silica coating are the pre-treatment methods with more evidence in the literature .
Increased adhesion could be expected after physico-chemical conditioning of zirconia .
Surface contamination has a negative effect on adhesion .
There is no evidence to support a universal adhesion protocol
Background .
Reliable bonding between resin composite cements and high strength ceramics is difficult to achieve because of their chemical inertness and lack of silica content that makes etching impossible .
The purpose of this review is to classify and analyze the existing methods and material s suggested to improve the adhesion of zirconia to dental substrate by using composite resins , in order to explore current trends in surface conditioning methods with predictable results .
Methods .