Patent GB-763152-A (GB)
Title: Improvements relating to apparatus for use in the examination of materials by x-ray diffraction
IPC: G01N23/205
Filed: 1954-10-14
Abstract: 763,152. Recording-apparatus. GENERAL ELECTRIC CO. Oct. 14, 1954 [Oct. 15, 1953], No. 29648/54. Class 106 (4). [Also in Groups XX and XL (b)] In apparatus for producing an X-ray diffraction pole figure a specimen which may be moved about two perpendicular axes is impinged by a beam of X-rays, and the diffracted rays are received by a device producing an electric signal in response to their intensity and compensated for geometrical effects produced by different specimen positions and are used to select one of a number of different indicia to print a chart rotating in synchronism with the movement of the specimen about one of its axes the printing means being moved radially with respect to the chart in co-ordination with the movement of the specimen about its other axis. General operation (Fig. 2). -As shown, a specimen to be examined is mounted on a holder 102 supported for continuous rotation about a horizontal axis and intermittent rotation about a vertical axis. The horizontal motion is effected by a motor M, the vertical by a solenoid 110. The output of a Geiger tube receiving the diffracted X-rays is applied to terminals 121, passed through one of correcting resistors 127-169 selected in accordance with the rotation of the specimen about the vertical axis by means of a stepping switch 124 and used to operate a strip recorder consisting of a pen moved across the strip to a position determined by the magnitude of the input signal. As the pen moves, cams coupled to it actuate sequentially switches 187 to 192 which apply potential to contacts 223 to 229 in contact with a gapped conducting disc 211 thus completing the circuit of a solenoid motor 45 which step around the disc and opens its own contacts at 52. At the same time a printing drum 38 carrying seven possible printing g characters is stepped around 45 degrees. The solenoid motor relapses closing contacts 52. This continues until the energized contact is opposite the gap when the current through a solenoid 70 energized by contact 238 is sufficient to bring the printing drum into contact with a continuously rotating chart driven by motor M<SP>1</SP> and to print one of a series of circumferential dots on the chart and print the character related by the rotation of the disc. A time delay solenoid 242 then short circuits the printing drum solenoid 70 and the printing drum lifts from the chart. The circuit of solenoid 203 is still made and the disc is stepped around until the gap is opposite contact 238. After one complete rotation of the specimen contacts 105 are closed by the specimen holder 102, energizing solenoids 117, 106 and solenoid motor 113. Solenoid 106 alters the position of the specimen about its vertical axis; solenoid 117 moves contacts 124 to the next resistor of the series 127-169 to make the correction of the input signal appropriate to the new specimen position and solenoid 113 moves the printing head radially over the chart so that a new set of dots are printed inside the outer ring and parallel to it. Wiper 252 is also stepped by solenoid motor 113 the effect being to reverse the chart drive. Thus if the specimen holder is arranged to close contacts 105 each quarter revolution of the specimen a chart of the type shown in Fig. 5. is obtained. Strip printer (Fig. 3).-The pen 171 of the strip printer is shown diagrammatically as driven by a motor 179 to a position indicative of the size of the input signal. On the shaft of the motor are cams 181 which operate switches 186 to 192 one at a time and in sequence. Chart and chart printer (Fig. 1).-The circular chart is positioned on a disc 10 and clamped by a screw 12. As described, the disc rotates continuously and a series of circumferential lines of dots is printed on it. The printing head comprises an octagonal drum 34 which is stepped around by solenoid motor 45 through shaft 18 and gearing 56, 57, 58 and maintained in the position to which it is stepped by a ratchet and pawl mechanism 59. Geared to the head is a holder 39 in which are differently coloured ink pads 40. The head and pad holder are so connected by gearing 42, 43, 44 that each face of the head receives ink from one of its associated pads only and thus prints always the same colour. The printing head is attached to a carriage 17 sliding on guide rods 19, 20 and biased towards the centre of the chart by a spring-loaded pulley arrangement 23, 25, 26. The printing head is urged towards the chart by a spring 60 but.is unable to move because of the contact of member 62 with a cam 61. The cam is biased to hold the head away from the paper by springs 65, 69. Energization of printing solenoid 70 rotates the cam to allow the printing of the appropriate dot in the lower position on the printing head so that the entire head may be moved along a radius to allow of printing a further circumferential row of dots (see Fig. 5), a series of cams 30 is provided on a shaft each having'an aperture 31 spaced by 45 degrees from its neighbour. Thus stop 27 on carriage 17 is urged by the spring-loaded pulley already described into engagement with the side of the cam. Motion of shaft 29 by solenoid motor 113 allows the stop to pass through the gaps in the cam with which it is in contact and contact the side of the next cam. Specification 726,886, [Group XL (b)] is referred to.