Patent GB-1208963-A (GB)
Title: Apparatus for detecting or measuring the amount or concentration of a liquid or gaseous fluid in fluid mixture
Inventor: ETZLINGER LUCIEN
IPC: G01N35/00
Filed: 1968-10-08
Abstract: 1,208,963. Sampling for analysis. L. ETZLINGER. 8 Oct., 1968 [9 Oct., 1967], No. 47648/68. Heading B1X. [Also in Division G1] Apparatus for the analysis of a gaseous, or liquid, fluid comprises a coiled duct 1, which in a cycle of operation is automatically rinsed out with an inert fluid, filled with the fluid to be analysed and then subsequently emptied through an analyser, the filling of the duct being checked by a valve 14' which is operated by the pressure of fluid to be analysed fed into the duct so that it operates only whilst such fluid is fed in, the valve being rendered ineffective after a predetermined time interval chosen such that the duct will contain only fluid to be analysed, so that this fluid may then pass to the analyser. The apparatus is specifically described for the analysis of alcohol in breath and the analyser consists of a light source 103 from which light passes separately to two selenum photo-electric cells 101, 102 connected in a bridge circuit with an ammeter 104, the two light beams to the cells 101, 102 passing respectively through ampoules 14, 16 containing a colorimetric reagent for the alcohol, e.g. bichromate or chromic acid, the ampoul 16 serving as a reference and the gas to be analysed being passed through the ampoule 14 so that any alcohol present therein will cause a change in colour and thus a change in the intensity of the light received by the cells 101, 102, which will register on the ammeter. The duct 1 is machined in a block of material which may 'be heated by a heater 11 controlled by a thermostatic switch to maintain a constant temperature. Solenoid operated valves 2, 3 are disposed at each end of the duct 1, and the apparatus is controlled by rotation of an electric motor 8 with cams 71, 72, 73, 74 operating associated control contacts. The cycle of operation is started by energising the motor 8 by closing a switch 18. Rotation of the cams then produces the following sequence:-With the valves 2, 3 in the positions shown a motor 63 driving a diaphragm pump 6 is energised to pump air through the duct 1 and out through an opening 21 thus flushing the duct. The two valves 3 are then operated to connect the duct 1 with the valve 14' and a subject blows into the opening 21 displacing the air in the duct 1 out through the valve 14' causing contacts 15 to close, maintaining rotation of the motor 8. The cam 74 is such that after the motor has rotated under the control of the contact 15 for a predetermined length of time, the cam 74 again closes the motor circuit and the valve 3 is returned to its initial position rendering the valve 14' ineffective. This time period is such as to allow complete filling of the duct 1 with breath from the subject. Actuation of the contacts 15 far too short a length of time will prevent further rotation of the motor 8 until the duct contains only gas to be analysed. The pump 6 now operates to pump the sample from the duct through an opening 22 and into the analyser with the valve 2 disposed so as to connect the duct 1 with the opening 22.