Judul: Pengaruh Lama Reaksi dan Laju Alir SO3 pada Produksi Surfaktan Methyl Ester Sulfonate Acid (Mesa) dari Metil Ester Jarak Pagar (Jatropha curcas L)
Abstrak: Surfactant is an active agent which could reduce surface tension. Surfactant could be found in cleaning agent, emulsifier, and homogenizer. Applications of surfactant are in detergent industry, food and beverage industry, and oil industry. According to its hydrophilic complex we could divide surfactant into four groups which is anionic surfactant, cationic surfactant, amphoteric surfactant, and non-ionic surfactant. Anionic surfactant is the most needed surfactant in the world Methyl ester sulfonates Acid (MESA) are one of the anionic surfactant which is renewable. One of the prospective feedstock of MESA is jatropha curcas. The dominant fatty acid of jatropha curcas oil is C16 unti 18. This fatty acid will have good detergency if it converted to surfactant. Jatropha curcas also doesn’t compete with food as a industry feedstock. Sulfonation method to produce MESA are falling film method with Single Tube Falling Film Reactor (STFR) 5 liter scale. The feedstock are jatropha curcas oil which is converted to methyl ester trough esterification process and continued with trans-esterification process (es-trans). The reactant which is used is sulfur trioxide (SO3). This reactant is chosen because it more reactive and produce less sludge than H2SO4 or Na2SO3 reactant. This research scope is only cover MESA production. MESA is an intermediate product for MES which is not purified yet. The goal of this research is to know the effect of reaction time and reactant flow rate to physic-chemical characteristic of MESA. The levels of reaction time are 30, 45, 60, 75, and 90 minutes. The SO3 reactant flow rate levels are 2,2, 2,8 dan 3,0 kg/hour. Analyses of MESA cover interfacial tension, surface tension reduction, iodine value, active matter content, acid value, and pH. . The range of interfacial tension of MESA are 1,1-4,43 dyne/cm. The
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Judul: Kajian Pengaruh Laju Alir Gas So3 dan Suhu Reaksi Sulfonasi pada Karakteristik Surfaktan Methyl Ester Sulfonates Acid dari Jarak Pagar (Jatropha curcas L.) dengan Menggunakan Single Tube Falling Film Reactor
Abstrak: Surfactant is surface active agent that has ability to reduce surface and interfacial tension. Based on its ability, surfactant is used almost in all sectors of industries. It can be synthesized from petroleum, microorganism, and vegetable oil. Based on the hydrophilic part, it is divided into four groups: cationic, anionic, non-ionic, and amphoteric. Anionic surfactant is the most produced compared to other groups. Methyl Ester Sulfonates (MES) is the anionic surfactant made from vegetable oil that is now being developed. MES has the similar, or even better, than Linear Alkylbenzene Sulfonates that is now the most produced anionic surfactant synthesized from petroleum. Jatropha curcas is potential to be developed as MES feedstock because it has high productivity and oil contain. Sulfonation process is the main process in MES production. There are some reactants can be used in sulfonation process but SO3 in the form of gas is the most common reactant used in industry. The sulfonation process of this research uses the Single Tube Falling Film Reactor. This research has purposes to find the effect of reactant flow rate and temperature to the characteristics of Methyl Ester Sulfonates Acid produced and also to find the best process condition. This research used factorial completely randomized design with two replications. The treatments used are reactant flow rate with levels 0.8, 0.9, 1.0, and 1.1 kg SO3/hr and temperature with levels 80, 100, and 120°C. Performance test shows that the reactant flow rate and temperature have significant effect in the surface tension value, inter-facial tension value, iodine number, acid number, pH, and active matter of MESA produced. MESA produced in this research could reduce the water surface tension from 41.88% up to 50.22%, has inter-facial tension value from 2.57 dyne/cm to 46.88 dyne/cm, iodine value from 50.96 mg I2/g MESA, acid value from 3.43 up to 10.79 mg NaOH/g MESA, pH from 1.42 to 1.73, and active matter from 0.08 to 13.66 percent. Based on this research, it is found that the MESA produced by 1.1 kg SO3 reactant flow rate/hr and 100°C temperature condition shows the best characteristic, especially in the inter-facial tension value.
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Judul: Isolasi dan Identifikasi Virus Newcatle Disease Pada Burung yang terdapat di Pasar-pasar Burung Wilayah Bogor.
Abstrak: Burung adalah satu jenis hewan kesayangan yang dipelihara karena burung bisa mengeluarkan suara-suara yang indah dan mempunyai warna bulu yang indah pula. Jenis burung yang ada di Indonesia kurang lebih 300 dan 118 jenis dari burung-burung tersebut terancam kepunahan. Kepunahan merupakan proses alami, dari catatan fosil menunjukkan rata-rata hanya satu jenis burung yang punah setiap 100 tahun. Dalam 200 tahun terakhir, tingkat kepunahan sedikitnya 40 kali lebih besar dari rata-rata angka kepunahan. Lalu kepunahan spesies burung yang sangat cepat tersebut berhubungan langsung dengan perusakan yang dilakukan oleh manusia dan pemanfaatan yang tidak lestari juga disebabkan oleh terserangya suatu penyakit yang akan mengakibatkan kematian sehingga menyebabkan kepunahan.
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