Judul: Grafting degree Measurement of acrylamide onto polysaccharide using Infrared Spectrometry
Abstrak: Utilization of carbohydrate-based agricultural wastes has been carried out with the manufacture of derivatives by grafting and crosslinking with acrylamide. The success of the process is monitored by setting the levels of nitrogen in the product. This research work is trying to look for possible use of spectrometry Fourier Transform Infrared technique to determine level of nitrogen in the products. Preparation of powder with a reflectance technique gives satisfactory results for grafting product, also for saponified products very satisfactory. ANOVA test of the PLS for each processing the data on IR spectral of the grafted-crosslinked product and its saponified showed a smaller probability value of 0.05, it is indicate the model developed by the independent variable (wave number) is significant effect on nitrogen content at 95% confidence level. Results of Partial Least Square (PLS) model for each treatment to give the coefficient of determination (R2) ranged from 0.961-0.998, it is the model with the wave number of independent variables can predict nitrogen content as well. Results of PLS analysis also provide information that the processing of IR spectrum data does not affect the difference between the predictions and the values of the nitrogen content.
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Judul: Modifikasi selulosa dengan teknik pencangkokan dan penautan silang menggunakan akrilamida
Abstrak: Modification of cellulose was carried out by grafting and crosslinking copolymerization using acrylamide as monomer, N,N’-methylene-bis-acrylamide as crosslinker, and ammonium peroxydisulfate as initiator. The chemical structure of monomer will affect the properties of modified cellulose such as hydrophilic and hydrophobic characters, elasticity, ion exchange capability, absorptivity, and heat resistance. Infrared spectra showed that cellulose has been modified. It could be seen from C=O streching absorption at 1650 cm-1 and –NH2 streching at 3182.55 cm-1. Both absorption peaks indicated that grafting and crosslinking had been carried out. Modified product had been 31–50% grafted. The final product also weighed 69 times higher than its initial weight with percentage of absorbed water to initial sample weight of 6755% after for 24 hours and became 93 times and 9187%, respectively, after 48 hours.
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Judul: Karakteristik Anatomi Skelet Kepala Buaya senyulong (Tomistoma schlegelii).
Abstrak: Buaya sepit atau senyulong (Tomistoma schlegelii) merupakan jenis buaya asli Indonesia yang berhabitat di sungai-sungai Sumatera, Kalimantan, dan juga pedalaman Sulawesi. Salah satu ciri khas buaya senyulong adalah bentuk moncong yang runcing dan sempit, namun hingga saat ini informasi mengenai struktur skelet kepala buaya senyulong sangat terbatas. Penelitian ini bertujuan untuk mempelajari karakteristik anatomi skelet kepala buaya senyulong yang dikatikan dengan fungsi dan perilakunya. Penelitian dilakukan secara eksploratif dengan melakukan pengamatan, pencatatan, dan pengambilan gambar dari skelet kepala buaya senyulong. Skelet kepala berukuran panjang 70 cm, lebar 29 cm, dan tingggi 17 cm dengan permukaan kasar pada os nasale, os frontale, os maxilla, os mandibula, os lacrimale, os jugale. Jumlah gigi pada buaya ini sebanyak 78 buah, terdiri dari 4 buah gigi premaxila, 16 buah gigi maxila, dan 19 buah gigi mandibula. Pada regio orbitalis ditemukan dua pasang fenestrae temporales yang berkembang baik. Fenestra supratemporale merupakan lubang oval yang membentang di sepanjang os parietale. Fenestra infratemporale berbentuk segitiga dan dibatasi oleh os squamosum, os postorbitale, os jugulare, dan os quadratum. Os mandibula hewan ini mempunyai symphysis mandibularis yang panjang yaitu garis yang melintang di corpus mandibulae. Secara fungsional ukuran symphysis mandibularis berkaitan dengan adaptasi hewan terhadap diet makan.
Keyword: kepala, moncong, Tomistoma schlegelii