Judul: Optimasi Nisbah Mol Pati Tapioka - Butanol dan Nisbah Mol Pati Tapioka - Fatty Alcohol C10 pada Proses Pembuatan Surfaktan Nonionik Alkil Poliglikosida (APG)
Abstrak: Nowadays, industries grow rapidly to produce assorted goods that are necessary to fulfill human needs. Industrial raw material requirement demands renewable raw material to guarantee industrial availability and sustainability. Therefore, assorted renewable raw materials are needed. Besides that, industries are demanded to pay attention for the environment preservation and ecosystem. Alkyl polyglycosides (APG) is a surfactant safe to environment because it is synthesized from natural raw materials based on carbohydrate likes sago, cassava, corn and vegetable oil such as coconut oil, palm oil, kapok seed oil and rubber seed oil. The main raw materials for producing APG is starch (sago, tapioca, etc.) or dextrose (based on starch) and fatty alcohol (based on vegetable oil). The objectives of this research were to obtain the optimum condition of the molar ratio of starch-butanol and the molar ratio of starch-fatty alcohol C10 on interfacial tension value, and to compare characterististics of APG produced from this research to APG commercial. Optimization used response surface method with central composite design. The variables were the molar ratio of starch-buthanol of 1: 6 - 1: 10 and starch-fatty alcohol C10 of 1: 2,5 - 1: 6. The result of optimum condition, based on interfacial tension value of water and xylene as parameter shows that surface model response was minimum. The optimum condition from validation result was interfacial tension value of water and xylene of 9 dynes/cm with the molar ratio of starch-butanol of 1 : 8,49 and and the molar ratio of starch-fatty alcohol of 1 : 4,66. The response surface model was Y = 9,354561 – 0,398990 X1 – 0,411616 X2 + 0,809388 X12 + 0,025000 X1X2 + 0,855307 X22. Characteristics of APG produced in optimum condition had similarity with those of APG commercial in their performances physicochemical properties, i.e. interfacial tension (9,75 dynes/cm and CMC value of 0,9 g/L), surface tension (34,55 dynes/cm and CMC value of 0,6 g/L), foam stability (87 %), emulsion stability (64%), pH (7,98) and HLB (13,8). FTIR analysis shows that the APG produced from this research had similar functional groups with those at the commercial product.
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Judul: Pemurnian surfaktan nonionik alkil poliglikosida (APG) berbasis tapioka dan dodekanol
Abstrak: Alkyl polyglycosides (APG) , a nonionic surfactant, has got some green labels such as Ecocert, EU Eco-flower and Green Seal as environmentally friendly surfactant. Sugar as APG's raw material, supplied the hydrophilic group, and fatty alcohol acted as hydrophobic group. Some undesirable compounds formed during the APG production had caused low quality. The research aimed to increase the quality and performance of APG, by controlling its process. The catalyst of p-toluene sulfonic acid (PTSA) was added and investigated the effect of catalysis concentration (0,018-0,036 mole per mole of starch) to enhance the butanolysis of starch. Addition 0-10% of activated carbon and 0-0,3% of NaBH4 in APG pre-purification process; 2% (w/w) of H2O2 35% and 500 ppm of MgO in the bleaching process were examined to process high quality and high performance of APG. The results showed that 0.027 mole of PTSA per mole starch and process temperature of 140 OC could minimize the residual sugars after butanolysis. The best APG was obtained from purification step by addition 0% of activated carbon and 0,2% of NaBH4, with the characteristics of clarity of 59,02(%T); the ability to reduce surface and interfacial tensions at 1% concentration were 61,98% and 95,60% respectively; 81,71% of stability of emulsion, 62,5% of foam height and stable up to 315 minutes.
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Judul: Etno-ornitologi Burung Kancilan Flores (Pachycephala nudigula nudigula Hartert 1897) pada Masyarakat Lio di Taman Nasional Kelimutu
Abstrak: Bare-throathed whistler is one of several wild birds in Kelimutu National Park (TNKL) that is believed to have correlation with Lio Community‟s belief. The estimation of Bare-throated whistler‟s population in Kelimutu National Park was about 186.41-1668.07 individual by the density about 0.0389-0.3481 ind/ha with the sex ratio 6.2:1 that spreaded on area with height of 1100 – 1600 masl. The characteristic of Bare-throated whistler‟s habitat is a natural forest with various canopy level, high plant species diversity and high density. The habitat characteristics related to the availability of food in the form of insects, cover, safety and a nesting site. Generally the most of Lio community knew the existence of Bare-throated whistler directly or from their parents‟ stories. The perceptions of Lio Community to the Bare-throated whistler‟s existence is generally support the conservation efforts. The perceptions construct the Lio Community‟s atitude that tend to be conservative to the existence of Bare-throated whistler. The attitude shown by their behavior that not cathing the Bare-throated whistler from the TNKL‟s area or the outside. The attitude have an important role to the existence of Bare-throated whistler in Kelimutu National Park‟s area.
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