Directionally solidified investment casting with improved filling

Abstract: A method of making a directionally solidified casting by casting a melt in a mold cavity of an investment mold having a core therein to form an internal casting surface feature involves evacuating the mold cavity while the investment mold is disposed on a chill member with the mold cavity communicating to the chill member, and introducing the melt into the evacuated mold cavity about the core so that the melt contacts the chill member for unidirectional heat removal and directional solidification. Then, gaseous pressure is applied to the melt cast in the mold cavity rapidly enough after introduction in the mold cavity to reduce localized void regions present in the cast melt as a result of surface tension effects between the melt and the core.

Description: The present invention relates to a method of casting a melt in a mold in a manner that improves filling of one or more mold cavities with the melt, especially about a ceramic core disposed in the mold cavity to form internal casting surface features. In the manufacture of components, such as nickel base superalloy turbine blades and vanes, for gas turbine engines, directional solidification investment casting techniques have been employed in the past to produce single crystal or columnar grain castings having improved mechanical properties at high temperatures encountered in the turbine section of the engine. In the manufacture of turbine blades and vanes for modern, high thrust gas turbine engines, there has been a continuing demand by gas turbine manufacturers for internally cooled blades and vanes having complex, internal cooling passages including such features as pedestals, turbulators, and turning vanes in the passages to control the flow of air through the passages in a manner to provide desired cooling of the blade or vane. These small cast internal surface features typically are formed by including a complex ceramic core in the mold cavity in which the melt is cast. The presence of the complex core having small dimensioned surface features to form pedestals, turbulators, turning vanes or other internal surface features renders filling of the mold cavity about the core with melt more difficult and more prone to inconsistency. Wettable ceramics and increased metallostatic head on the mold have been used in an attempt to improve mold filling and reduce localized voids in such situations, but these are costly and may be restricted by physical size of the casting apparatus. EP-A-0 293 960 disclosed an apparatus for producing directionally solidified castings with a casting chamber, an adjacent pressurization chamber communicated to the casting chamber by a closeable passage and a mold heating chamber located in the casting chamber and being adapted to having a mold disposed in and withdrawn from this mold heating chamber. In the process disclosed by EP-A-0 293 960, the casting chamber is evacuated, whereupon a melt is cast into the mold residing in the mold heating chamber; then, the mold is transferred to the pressurization chamber, the passage is closed and the pressurization chamber is filled with pressurized argon gas in order to apply gaseous pressure to the melt introduced into the mold. It is said that the molten metal is thus allowed to solidify under gas pressure to preclude shrinkage porosity void formation by pressurization. In using this known apparatus, substantial time is required for transfer of the filled mold from the mold heating chamber located in the casting chamber into the pressurization chamber, and for closing the passage before pressurized gas is introduced into the pressurization chamber. During this time period, the mold and the melt contained therein start to cool, and the cooling down continues while the pressurization chamber is filled with pressurized gas and while the gaseous pressure acts upon the melt. JP-A-59 01 459 (Abstract) discloses an apparatus with a single chamber housing a mold and a crucible being provided with heating means and containing a melt which is poured into the mold after the chamber was evacuated. Then, gaseous pressure is applied to the melt contained in the mold by introducing compressed air into the chamber. The invention relates to a method of producing castings as disclosed by EP-A-0 293 960, i. e. to a method of producing castings by means of a mold having a mold cavity, a casting chamber and a furnace located in the casting chamber, said furnace being adapted to having the mold disposed in and withdrawn from the furnace, said method comprising the steps of introducing a melt under an initial relative vacuum into the cavity of the mold residing in said furnace, and applying gaseous pressure to the melt introduced in the mold cavity. It is an object of the invention to provide such a method which improves filling of one or more mold cavities with the melt. In accordance with the present invention, this object is achieved by applying gaseous pressure to the melt introduced in the mold cavity while the mold resides in said furnace and prior to withdrawal of the mold from the furnace so that gaseous pressure can be applied to the melt rapidly enough after casting the melt in said mold to reduce localized void regions present in the cast melt as a result of surface tension effects between the melt and a mold component. In a preferred embodiment of the inventive method, the melt is cast into a mold cavity provided with a preferably ceramic core disposed therein and having a surface feature for forming an internal casting feature, wherein filling of the core surface feature is improved by said application of gaseous pressure to the melt introduced in the mold cavity. The cast internal surface features are especially fine or small dimensioned surface features, such as the pedestals, turbulators, and turning vanes described hereabove for internally cooled turbine blades and vanes. By the present invention it is possible to substantially decrease the level of internal porosity formed during solidification of the melt, and to improve filling of the mold cavity about a core disposed therein because the rapidly applied gaseous pressure is able to overcome the results of surface tension effects between the melt and a mold component, such as a mold cavity surface and/or a core surface. The gaseous pressure is applied rapidly enough to collapse one or more such localized void regions in the melt, particularly prior to gas pressure equalization within the void regions by virtue of the gas permeation through the mold. The inventive method can also be used for making a directionally solidified casting by disposing a preferably ceramic investment shell mold on a chill member with a mold cavity communicating to the chill member so that the melt can contact the chill member for unidirectional heat removal. Claim 10 is directed to a preferred embodiment of such method for making directionally solidified castings. Further, the invention relates to an apparatus for rapidly pressurizing a casting chamber (e. g. in about 2 seconds or less), said apparatus being defined by claim 13. The pressure vessel used for rapidly pressurizing the casting chamber may be a surge tank, and the valve disposed between said pressure vessel and the casting chamber shall be designed to be completely openable in rapid manner. Further improvements of the inventive method and apparatus are defined by claims 2 to 12, 14 and 15 resp.. A preferred embodiment of the present invention is shown in the enclosed drawings and described in the following; the figures of the drawings show the following: Figure 1 is a schematic view of apparatus of an embodiment of the invention for making single crystal castings pursuant to a method embodiment of the invention, the mold assembly being shown schematically for purposes of convenience. Figure 2 is an enlarged, sectional view of the investment shell mold assembly of Figure 1. Figures 3A and 3B are photographs at 1.5X of single crystal test panels having turbolator features cast pursuant to conventional practice, Figure 3A, and pursuant to the invention, Figure 3B. Referring to the Figures 1 and 2, casting apparatus for practicing an embodiment of the invention to produce a plurality of superalloy single crystal castings is illustrated for purposes of describing the invention, although the invention is not limited to the particular casting apparatus shown or to the casting of single crystal castings. The invention can be practiced in conjunction with a wide variety of casting equipment to produce equiaxed grain castings and directionally solidified castings having a single crystal, columnar grain, or directional eutectic microstructure of a variety of metals and alloys. The apparatus includes a vacuum casting chamber 10 in which a ceramic investment shell mold assembly 12 is disposed on a chill member (plate) 14 in conventional manner. A portion of the mold assembly 12 is shown in more detail in Figure 2 where it is apparent that each mold cavity 16 of the mold assembly 12 communicates to the chill member 14 via a mold cavity opening 16a at the lowermost or bottom thereof. The mold assembly 12 includes a plurality of mold cavities 16 disposed about the pour cup 30 as shown, for example, in U.S. Patent 3 763 926, the teachings of which are incorporated herein by reference with respect to an exemplary mold assembly configuration. The chill member 14 is disposed on a movable shaft 17 that effects withdrawal of the mold assembly 12 from a furnace 20 after the mold assembly 12 is filled with melt, such as a nickel or cobalt base superalloy, to effect directional solidification of the melt in the mold. The furnace 20 is of conventional construction and includes a tubular susceptor 22 typically comprising a graphite sleeve and an induction coil 24 disposed about the susceptor 22 by which the susceptor is heated for in turn heating the mold assembly 12 prior to filling with the melt. Heat shields 26 are positioned at the lower end of the susceptor sleeve about and proximate the periphery of the chill member 14. A removable heat shield cover 28 is disposed on the top of susceptor 22 and may include an opening for receiving a melt which is introduced to an upper pour cup 30 of the mold assembly 12, Figure 2. The pour cup 30 of the mold assembly 12 communicates to filling passages 34 that in turn communicate to each mold cavity 16 for feeding of the mold with melt. An alternative melt filling passage 35 shown in dashed lines can be provided from the pour cup 30 to each growth cavity 36 to feed melt thereto such as shown in U.S. Patent 3 763 926. The growth cavity 36 communicates with the mold cavity via a crystal selector passage 38, such as a pigtail or helical passage, such that one of the many crystals or grains propagating upwardly in the growth cavity 36 from the chill member is selected for further propagation through the mold cavity 16 thereabove to form a single crystal casting therein having a configuration complementary to the shape of the mold cavity, all as is well known. Above each mold cavity 16 is a riser cavity 32 that provides a source of melt to the mold cavity 16 to fill shrinkage during solidification as well as metallostatic pressure or head on the melt as it solidifies in the mold cavity 16. The mold assembly 12 typically comprises a ceramic investment shell mold assembly having the features described and formed by the well known lost wax process wherein a wax or other fugitive pattern of the mold assembly is dipped repeatedly in ceramic slurry, drained, and then stuccoed with coarse ceramic stucco to build up the desired shell mold thickness on the pattern. The pattern then is removed from the invested shell mold, and the shell mold is fired at elevated temperature to develop adequate mold strength for casting. In the manufacture of internally cooled turbine blades or vanes, each mold cavity 16 will have the outer configuration of the desired blade or vane casting shape. The internal cooling passage and related surface features of the blade or vane casting are formed by a ceramic core 45 disposed in each mold cavity 16 by chaplets, pins, and other known techniques which form no part of the present invention. As mentioned above, in the manufacture of turbine blades and vanes for modern, high thrust gas turbine engines, there has been a continuing demand by gas turbine manufacturers for internally cooled blades and vanes having complex, internal cooling passages including such features as pedestals, turbulators, and turning vanes in the passages to control the flow of air through the passages in a manner to provide desired cooling of the blade or vane. These small internal cast passage surface features are formed by including the complex ceramic core 45 in each mold cavity 16. The presence of the complex core 45 having small dimensional surface features to form pedestals, turbulators, turning vanes or other internal cast surface features, however, renders filling of the mold cavities 16 and the small dimensioned core surface features completely with melt more difficult and prone to inconsistency. In particular, the inventors have discovered that the small dimensions of the cooling passages to be formed in the blade or vane as well as the small dimensions of the core surface features can promote surface tension effects between the melt and core and/or mold surfaces that result in localized void regions in the melt and thus in the resultant solidified castings. That is, the melt incompletely fills small dimensioned cavities between the core and adjacent mold surfaces and small dimensioned surface features on the core itself; for example, core surfaces configured to form pedestals, turbulators, and turning vanes in the solidified casting. For purposes of illustration, small cavities between the core and adjacent mold surfaces having a width dimension (wall thickness) of only 0,03 cm - 0,051 cm (0.012 inch to 0.020 inch) can be present to form external and internal wall thicknesses in the cast internally cooled blade or vane. Moreover, core surface features, such as circular cross-section pedestals, have diameters of only 0,051 cm - 0,076 cm (0.020 inch to 0.030 inch). Such small dimensioned cavities and core surface features tend to exaggerate surface tension effects between the melt and the core and/or mold surfaces that prevent complete filling thereof with melt, resulting in localized void regions in the melt and thus in the solidified casting where there is incomplete melt filling. Use of such techniques as particular ceramics selected to improve metallurgical wetting and increased metallostatic pressure to overcome the localized surface tension effects are costly and may be restricted by physical size constraints in the casting furnace. In practicing an embodiment of the present invention using the apparatus illustrated in the Figure 1, the vacuum casting chamber 10 initially is evacuated by a vacuum pump 50 to a vacuum level of 5 microns or less. The mold cavities 16 likewise will be evacuated as a result of the mold assembly 12 being disposed in the vacuum chamber and being gas permeable. Also prior to introduction of melt, the mold assembly 12 is preheated to an elevated casting temperature (e.g. 1538°C (2800 degrees F) for a nickel base superalloy melt) by energization of the induction coil 24 disposed about the tubular susceptor 22. The preheat temperature for the mold assembly 12 depends on the type of melt being cast. The nickel base superalloy melt is provided by melting a charge C of the superalloy in a crucible 54 disposed in the evacuated vacuum chamber 10 by energization of an induction coil 56 about the crucible pursuant to conventional practice. The superalloy melt is heated to an appropriate superheat and then introduced to the mold assembly 12 by pouring from the crucible 54 into the pour cup 30 by suitable rotation of the crucible in known manner. The superheated melt flows down the filling passages 34 to each mold cavity 16 and then into each growth cavity 36. Filling is complete when each riser cavity 32 is full to a level corresponding to the level of melt in the pour cup 30. After the melt is poured into the mold assembly, fills the mold assembly and enters the riser cavities 32, the vacuum chamber 10 is backfilled with gas, such as typically inert gas (e.g. argon) or other gas that is substantially non-reactive with the superalloy melt in the mold assembly 12. Gaseous pressure thereby is applied to the melt introduced in the mold cavities 16. The gas pressure is ramped up rapidly enough to a sufficiently high pressure level after introduction and filling of the mold assembly with the melt to overcome and collapse localized void regions present in the cast melt as a result of surface tension effects between the melt and the core and/or mold surfaces, such as at the small dimensioned cavities and core surface features described above. The time of gas pressurization typically is determined by the gas permeation rate of the gas permeable investment shell mold 12. In particular, the gaseous pressure is ramped up rapidly enough to collapse one or more localized void regions in the melt before gas pressure equalization within the void regions occurs as a result of gas permeation through the mold 12. Otherwise, gas pressure equalization within void regions in the melt can occur by virtue of gas permeation through the mold walls before collapse of void regions in the melt. The degree or magnitude of gas pressure applied typically is determined by the dimensions of the core features to be filled or contacted with melt. In casting nickel base superalloy melts in the manner described above in the production of single crystal turbine blade castings, the vacuum chamber was backfilled with high purity argon at different times (e.g. at times that ranged from greater than 0 to 20 seconds) following the time the riser cavities were observed visually to be filled with the melt during casting trials. Gas pressurization was established prior to withdrawal of the melt filled mold assembly 12 from the furnace 20 for melt directional solidification. As mentioned, gas pressurization is effected prior to gas pressure equalization within the void regions of the melt due to gas permeation through the gas permeable mold walls. For example, in casting trials, gas pressurization after 2 minutes following the time the riser cavities were observed to be filled with melt was ineffective to collapse void regions in the melt. The argon was introduced into the vacuum chamber 10 from a pressure vessel 62, such as a surge tank, having an appropriate internal volume (e.g. 454 ℓ (120 gallons) for a vacuum chamber volume of 2,83 m 3 (100 cubic foot)) and having argon gas pressure therein (e.g. ranging from 5 psig to 50 psig) selected to establish the desired argon backpressure in the chamber 10 pursuant to the invention. The gas pressure is supplied from the vessel 62 through an electrically actuated, fast acting ball valve 64 that is able to open (or close) completely in very rapid manner (e.g. in less than one second) and a large diameter (e.g. 7,62 cm (3 inches) diameter) copper or other tube 65 communicated to the chamber 10. A gas diffuser 67 (shown schematically) is fastened to the top of the chamber 10 at the inlet of the tube 65 to the chamber 10 to reduce the velocity of the argon gas entering the chamber 10. The gas diffuser 67 comprises a stack of stainless steel rods of 0.5 inch diameter and 8 inches length arranged in three layers one atop the other and criss-crossed relative to one another, wherein the top layer includes 5 rods arranged parallel to one another and spaced about 1,27 cm (0.5 inch) apart, the middle layer includes 5 rods arranged parallel to one another and spaced about 1,27 cm (0.5 inch) apart yet perpendicular to the rods of the top layer, and the bottom layer includes 4 rods arranged parallel to one another and spaced about 1,27 cm (0.5 inch) apart yet perpendicular to the rods of the middle layer and located beneath the spaces between the rods of the top layer. The stacked, criss-crossed arrangement of rods provides a nearly optically opaque gas diffuser when viewing the diffuser perpendicular to the top layer thereof. In lieu of using a gas diffuser 67 to control velocity of argon gas entering the chamber 10, the diameter of the tube 65 can be substantially increased to this end, such as from 3 inches to 6 to 8 inches in diameter. A predetermined argon backfill pressure can be provided rapidly in the chamber 10 using the apparatus described and shown in Figure 1. Typical backfill pressures of 0.5 to 0.9 atmospheres of argon can be achieved or established in the chamber 10 nearly instantaneously using the apparatus; e.g. in slightly more than one second, by the apparatus operator's pushing an electrical valve actuator button to open the fast acting valve 64 when the riser cavities are observed to be filled. The final gas pressure in the chamber 10 is predetermined by controlling the initial gas pressure and volume of the pressure vessel 62. The pressure vessel 62 is filled from an argon gas source 60 via a shutoff valve 61 prior to discharging the pressure vessel 62 into the discharge tube 65 to ramp up gas pressure in the chamber 10. In different casting trials, the backpressure of argon gas was maintained in the chamber 10 at the predetermined level for different times ranging from 0.1 minutes up to the time for complete mold withdrawal from the furnace 20. Alternately, the argon backpressure can be rapidly established after mold filling for a short time (e.g. .1-3 seconds) followed by evacuation of the chamber 10 to return to the initial vacuum level during subsequent mold withdrawal. In casting trials, cored single crystal nickel base superalloy castings produced using such argon backpressure immediately after filling the mold assembly with melt yielded single crystal castings having reduced non-fill of 0,051 cm (0.020 inch) diameter pedestals as compared to single crystal castings produced using the same casting procedures but maintaining a vacuum in the vacuum chamber; i.e. without establishing the argon backpressure in the vacuum chamber pursuant to the invention. X-ray analysis revealed that none of the single crystal castings produced pursuant to the invention exhibited non-fill, whereas all of the single crystal castings produced without argon backpressure exhibited non-fill. In other casting trials of single crystal test panels (shown in Figure 3) containing various sizes of ceramic core details, commonly called turbulators, using argon backpressure in the vacuum chamber 10 pursuant to the invention immediately after filling of the mold assembly with melt yielded castings with 100% completeness (i.e. complete filling of the turbolator features with sharp turbolator edge detail as illustrated in Figure 3B) as compared to castings made in a conventional manner as shown in Figure 3A. Improved filling of the core details and a reduction in macroshrinkage were observed for the castings made pursuant to the invention as compared to conventional castings. Further casting trials were conducted to make cored directionally solidified nickel based superalloy castings having columnar grain structure using a ceramic core with circular cross-section pedestals of size range of 0,051 cm - 0,064 cm (0.020 to 0.025 inch) diameter. In these trials, the final backpressure in the chamber pursuant to the invention was 0.5 atmosphere argon. These trials resulted in a casting rejection rate for incomplete filling of the smallest dimensional core pedestal features of only 3% as compared to similar castings made using conventional casting practice where the rejection rate for incomplete fill of the pedestal features was 17%. It is believed that a higher final backpressure of argon pursuant to the invention would result in further reduction of the casting rejection percentage to near zero. It is to be understood that the invention has been described with respect to certain specific embodiments thereof for purposes of illustration and not limitation. The present invention envisions modifications, changes and the like can be made therein without departing from the spirit and scope of the invention as set forth in the following claims.

Claims: Method of producing castings by means of a mold having a mold cavity, a casting chamber and a furnace located in the casting chamber, said furnace being adapted to having the mold disposed in and withdrawn from the furnace, said method comprising the steps of introducing a melt under an initial relative vacuum into the cavity of the mold residing in said furnace, and applying gaseous pressure to the melt introduced in the mold cavity, characterized in that gaseous pressure is applied to the melt introduced in the mold cavity while the mold resides in said furnace and prior to withdrawal of the mold from the furnace, so that gaseous pressure can be applied to the melt rapidly enough after casting the melt in said mold to reduce localized void regions present in the cast melt as a result of surface tension effects between the melt and a mold component. The method of claim 1, wherein the mold cavity initially is evacuated, the melt is cast in the evacuated mold cavity, and said gaseous pressure is applied to the melt in said mold cavity immediately after it fills the mold cavity. The method of claim 1 or 2, wherein for applying said gaseous pressure a pressurized gas is used that is substantially nonreactive with the melt. The method of claim 3, wherein said pressurized gas comprises an inert gas. The method of one of claims 1 to 4, wherein the melt is cast into a mold cavity provided with a core disposed therein and having a surface feature for forming an internal casting feature, and wherein filling of the core surface feature is improved by said application of gaseous pressure to the melt introduced in the mold cavity. The method of claim 5, wherein an investment mold is used as said mold. The method of claim 5 or 6, wherein a refractory core is used. The method of one of claims 1 to 7, wherein for evacuating the mold cavity prior to casting the casting chamber is evacuated while the mold resides in said chamber, and wherein the gaseous pressure is applied by backfilling the casting chamber with a pressurized gas. The method of one of claims 1 to 8, wherein gaseous pressure of about 0,5 to about 0,9 atmosphere is applied to the melt introduced in the mold cavity. The method of one of claims 1 to 9, wherein for making directionally solidified castings from a superalloy melt the mold comprises a mold cavity having a configuration complementary to the shape of the castings to be produced and a crystal growth cavity communicating to said mold cavity, and wherein the mold is disposed with said crystal growth cavity on a chill member while the mold cavity and crystal growth cavity are evacuated and the melt is introduced into the evacuated cavities, and wherein the melt contained in said crystal growth cavity is brought into contact with said chill member for unidirectional heat removal. The method of one of claims 1 to 10 including the further step of evacuating the casting chamber after the gaseous pressure is applied to the melt in the mold cavity to return the casting chamber to a relative vacuum during solidification of the melt in the mold cavity. The method of one of claims 1 to 11, wherein a mold with gas permeable mold walls is used and gas pressurization of the melt in said mold is effected before gas pressure equalization within void regions of the melt occurs as a result of gas permeation through the mold walls. Apparatus for applying gaseous pressure to a melt cast into a mold cavity (16) of a mold (12), said apparatus comprising a casting chamber (10), a furnace (20) located in said casting chamber and being adapted to having the mold (12) disposed in and withdrawn from said furnace, and a source of gas (60), characterized by a pressure vessel (62) communicated to said gas source (60) and having appropriate volume and gas pressure therein selected in dependence on the volume of said casting chamber (10) to provide a predetermined gas pressure in said casting chamber, a fast acting valve (64) disposed between said pressure vessel (62) and said casting chamber (10) and a gas supply tube (65) between said valve (64) and said casting chamber (10). The apparatus of claim 13 including a gas diffuser (67) proximate an inlet of said gas supply tube (65) to said casting chamber (10) to reduce the velocity of the gas entering the casting chamber. The apparatus of claim 13 or 14, wherein the cross sectional area of said gas supply tube (65) is selected to reduce the velocity of the gas entering the casting chamber (12).

Inventors: RAUGUTH BRAD L, SCHMIEDEKNECHT DEAN L, STRASZHEIM MARK J, THOMPSON DENNIS J, RAUGUTH, BRAD L., SCHMIEDEKNECHT, DEAN L., STRASZHEIM, MARK J., THOMPSON, DENNIS J.
Applicants: HOWMET CORP, HOWMET CORPORATION
Application year: 1996
Main classification: B22D27
IPC codes: B22D27