Minute step height measuring method and apparatus therefor

Abstract: Apparatus and method for measuring a minute step height on an object to be examined are disclosed. The apparatus comprises a laser source, an illuminating optical system for focusing a light beam from said laser source and forming a light spot on said object, a focusing optical system for focusing the light beam from said object on a detecting surface, detecting means for detecting the light beam focused on said detecting surface. The detecting means has a substrate formed with a channel waveguide which is constituted of a double mode channel waveguide region having an entrance end on said detecting surface and at least two branch channel waveguide regions branched from said double mode channel waveguide region. The detecting means further has respective detecting elements for detecting lights propagated through said branch channel waveguide regions, adding means for obtaining the sum of signals from the detecting elements, subtracting means for obtaining the difference of signals from the detecting elements and calculating means for outputting data of the minute step height on the object based on outputs of the adding means and the substracting means.

Description: BACKGROUND OF THE INVENTION Field of the Invention This invention relates to a method of measuring minute step heights on an object and an apparatus with a confocal laser scanning differential interference contrast microscope therefor. Related Background Art Generally, there have been utilized scan-type electron microscopes or probe-type microscopes in order to quantifiably measure minute step heights formed on an object in nanometer order. Also, atomic force microscopes (AFM) have been started to be utilized recently. However, the scan-type electron microscopes and atomic force microscopes are expensive and the handling of those is difficult. In the probe-type microscopes, a probe is brought into contact with the surface of the object for the measurement, so the object is liable to be damaged and the probe is often broken, necessitating replacement of the probe often. Consequently, it is also disadvantageous from the viewpoint of the cost. Therefore, the inventors of the present invention utilized a phase contrast microscope and a differential interference contrast microscope and tried to obtain the amount of step heights from image outputs of these microscopes quantifiably. This method is not impossible in principle but it is very difficult to establish a formula for the method from the wave optical image formation theory. Also, the principle for measuring step heights by utilizing the differential interference contrast microscope is disclosed at page 70 in O plus E (a Japanese publication) published in October, 1992, wherein a signal corresponding to the slope of the step structure is obtained when the width (not height) of the step structure on the object (phase object) is sufficiently larger than a light spot. That is, the method is applicable to the object having the step heights with gentle slopes, in which the measurement of the step heights can be performed without taking the effect of diffraction into consideration. Also, the effect of diffraction of the optical system is not taken into consideration. Accordingly, the resolution to an object having minute and narrow step heights is considerably reduced. Optic Communications, 85 (1991), P177 discloses a double mode channel waveguide in an interference contrast microscope. SUMMARY OF THE INVENTION It would be desirable to provide a method and an apparatus capable of measuring on an object step heights having a narrower width than a light spot with high resolution, without being in contact with the object. The present invention is set out in the appended claims. The inventors of the present invention found that minute step heights cn an object (a phase object) can be measured by image signals of a microscope even though the width of the minute step heights is smaller than that of a light spot. Thereby, it is possible to obtain a measuring apparatus which is capable of measuring minute step heights without being in contact with the object and inexpensive and easy to handle as compared with scan-type electron microscopes and atomic force microscopes. Further, it was found that if a confocal laser scanning differential interference contrast microscope provided with a waveguide in the detecting system is utilized, by utilizing two detecting devices, a step height can be calculated from output signals from the detecting devices without carrying out measurement in various points. Also, in the present invention, its quantification was endorsed definitely by the wave optical image formation theory and so it is possible to measure step heights from image signals quantifiably. For measuring a minute step height on an object to be examined, an embodiment of the present invention basically comprises a laser source, an illuminating optical system for focusing a light beam from the laser source and forming a light spot on the object, an optical system for focusing the light beam from the object on a detecting surface, and detecting means for detecting the light beam focused on the detecting surface. The detecting means has a substrate formed with a channel waveguide. The channel waveguide has a double mode channel waveguide region having an entrance end on the detecting surface and at least two branch channel waveguide regions branched from said double mode channel waveguide region. The detecting means further has respective detecting elements for detecting lights propagated through the branch channel waveguides, adding means for adding signals from the detecting elements, subtracting means for obtaining the difference of signals from the detecting elements and calculating means for outputting data of the step height on the object on the basis of the outputs of the adding and subtracting means. In the above structure, when the fully coupled length of two modes of the double mode region of the channel waveguide is Lc, it is effective that the length L of the double mode channel waveguide is L = Lc (2m + 1) / 2. (m = 0, 1, 2, ....) The minute step height measuring apparatus is preferably provided with scanning means for relatively shifting the light spot with respect to the object to be examined. Also, based on the output information S(s 0 ) of the adding means and the output information W(s 0 ) of the subtracting means, it is effective to obtain the minute step height  0 by the following equation:  0 = C A · S(s 0 )/W(s 0 ), wherein C A is the constant which depends on the apparatus. The method of measuring the minute step height on the object to be examined comprises the steps of forming the light spot on the object by focusing light from the laser source, focusing the light from the object on the detecting surface and detecting the focused light on the detecting surface. Further, the detecting step comprises the steps of detecting the respective intensity of lights from the branch channel waveguides propagated through the double mode channel waveguide from the entrance end surface on the detecting surface, obtaining the difference and the sum of the respective intensity signals and calculating a signal for the minute step height on the object based on the difference signal and the sum signal. The minute step height measuring method may further comprise the step of relatively shifting the light spot with respect to the object. Although the detecting principle in a confocal laser scanning mode interference contrast microscope using a waveguide is already disclosed by the inventors (Optics communications, 85 (1991), P177), a quantitative relationship between the minute step height on the object and the image signal will be described hereinafter. For simplicity, the description will be restricted to one-dimensional case, but two-dimentionalization is easy. Of course, the discovery of the quantitative relationship is the chief meaning of the present invention. If the amplitude distribution function of the object is o(x), the amplitude distribution function of the laser spot for illuminating the object (even function) is u(x) and the amplitude distribution function of the point image in the image formation optical system from the object to the entrance end surface of the channel waveguide is K(x), the amplitude distribution function of the laser spot at the entrance end surface of the channel waveguide h(x, x 0 ) is given by h(x, x 0 ) = ∫o(s)u(s-x 0 )K(s-x 0 -x)ds, wherein s and x are coordinates on the object and the entrance end surface of the channel waveguide respectively and x 0 is the distance between the origin of the coordinates on the object and the center of the laser spot. That is, x 0 is varied according to scanning. If the field distribution functions of the zeroth and first modes of the double mode channel waveguide are f 0 (x) and f 1 (x) respectively, the coupling coefficients of the zeroth and first modes η o , η 1 are η 0 (x 0 ) = ∫h(x, x 0 )f 0 *(x)dx and η 1 (x 0 ) = ∫h(x, x 0 )f 1 *(x)dx. Here, f 0 (x) is an even function and f 1 (x) is an odd function. Now, the light intensity distribution I(x 0 , t) in the double mode channel waveguide is expressed as I(x 0 , t) = η 0 x 0 f 0 t+exp i η 1 x 0 f 1 t 2 . Here, t is a coordinate system taken in the double mode waveguide so as to be parallel to the X-coordinate.  is a phase difference between the zeroth and first modes. Note that  = π/2 + mπ is optimum when observing a phase object, which is already disclosed in the foregoing reference (Optical Communication, 85 (1991), 177). Let it be assumed that the angle of inclination is  and sin  = α. If the amplitude distribution of the laser spot when the inclination is O is u(x) and the field distribution of each eigen mode of the double mode waveguide is fe(x) and fo(x) with respect to the even and odd modes, respectively, u(x) and fe(x) are eve functions and fo(x) is an odd function. With k = 2π/λ (λ: wavelength), the amplitude distribution of the laser spot uα(x) when there is an inclination is expressed as uα(x) ≃ u(x)exp(ikαx) = u(x)[cos(kαx) + i sin(kαx)]. (a) Here, the coupling efficiency ηe of the even mode is η e = ∫ u x cos kαx fe * x dx ∫ u x 2 dx ∫ fe x 2 dx (b) while the coupling efficiency η o of the odd mode is η o = i ∫ u x sin kαx fo * x dx ∫ u x 2 dx ∫ fo x 2 dx . (c) if the integration range is suitably chosen and |kαx| « 2π within this range, cos(kαx) ≃ 1, sin(kαx) ≃ kαx and hence, from the fact that u(x), fo(x) and fe(x) are predetermined functions, it can be seen that ηe ≃ constant, ηo ∝ iα. If C 1 and C 2 are real constants and  is the phase difference between the even and odd modes at the point of branch-off, the variation in the intensity of light by the interference between the even mode and the odd mode is I∝ ηe ± iηo exp i 2 = C 1 ± iαC 2 exp i 2 . Consequently, if exp{i} is selected to exp{i} = ± i, the equation (e) substantially becomes I = C 1 2 ± 2αC 1 C 2 and a variation in the intensity proportional to α is obtained, and a so-called differential image can be obtained. Accordingly, to obtain such a differential image, it is necessary that at the point of branch-off between the double mode and the single mode, a phase difference an odd number times as great as 90° be brought about between the two modes. For this reason, if the well-known fully coupled length of the two modes (the length for which the phase difference between the even and odd modes is 180°) is Lc, it is preferable that the length L of the double mode region be L = Lc (2m + 1) / 2. (m = 0, 1, 2, ....). Note that the expression (a) takes the inclination of the object into consideration and thus, supposes a phase object. The length of the double mode channel waveguide determined in the equation (g) is not limited to the length determined mechanically. That is, when the substrate with the double mode channel waveguide has electro-optical effect, the fully coupled length Lc can be varied by applying a voltage to electrodes disposed on the double mode region of the channel waveguide. Therefore, even when the mechanical length of the double mode region is a certain fixed length, the equation (g) can be satisfied by the regulation of the voltage. When the length L of the double mode region is L = mLc (m = 0, 1, 2, ....), it is possible to detect the variation in the intensity of the light of the object. However, in order to measure the step heights, the equation (g) needs to be satisfied. Next, the object is assumed to be a minute phase object as follows: o(x) = a·exp[i(x)] ≃ a{1 + i(x)}. Here, a 2 is the reflectivity of the object and (x) is the phase distribution of the object due to the uneven surface (unit: radian). From the equations (1) to (5), I (x 0 , t) is obtained by I (x 0 , t) ={aC 0 f 0 (t)} 2 - 2a 2 C 0 f 0 (t)f 1 (t) · ∫∫(s)u(s-x 0 )K(s-x 0 -x)f 1 (x)dsdx. Here, the coefficient C 0 is C 0 = ∫∫u(s-x 0 )K(s-x 0 -x)f 0 (x)dsdx. When obtaining the equation (6), quadratic or more terms as to  are neglected. The difference signal output S(x 0 ) is given by The fact that f 0 (x), f 1 (x) are the even and odd functions respectively is taken into consideration and then, from the equations (6) and (8), S(x 0 ) becomes Here, C t and G(x) are and Thereby, the equation (9) becomes Of course, PSF(x) is PSF(x) = u(x)G(x). On the other hand, the sum signal output W(x 0 ) is given by From the equation (6), W(x 0 ) becomes W(x 0 ) = a 2 C 0 2 C w . Here, Now, the minute step height on the object (s) is defined as follows: (s) = 0 s < s 0  0 s ≥ s 0 The equation (17) is substituted for the equation (12) to be Thereby, On the other hand, the sum signal output does not depend on , therefore, W(s) = a 2 C 0 2 C w . Then, from the equations (19) and (20),  0 is obtained by That is,  0 can be simply expressed as  0 = C p · S(s 0 )/W(s 0 ) wherein C P = C w C 0 /{4C t PSF(s)ds}. Thus,  0 can be obtained simply by multiplying a ratio of the difference signal output S(s 0 ) to the sum signal output W(s 0 ) by the constant C P determined by the apparatus. BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a schematic diagram of a minute step height measuring apparatus according to an embodiment of the present invention; Figure 2 is a sectional view of a standard sample to be used in the apparatus; and Figures 3A and 3B are examples of difference signal outputs of the apparatus. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Embodiments of the present invention will be described concretely with reference to drawings now. Embodiments of present invention are structured to have a confocal laser scanning differential interference contrast microscope and memory means and calculating means both annexed to the microscope. The memory means has a constant of the apparatus. The calculating means is for obtaining the step height of an object by the apparatus constant and difference and sum signal outputs from the microscope. Separate apparatuses for the respective memory and calculating means may be combined to be a single step height measuring machine but practically it is preferable to make one computer have both functions. Figure 1 is a schematic diagram showing a step height measuring apparatus of an embodiment of the present invention. Light emitted from a laser source 1 is reflected by a half mirror 2 and focused on the surface of an object 5 via X-Y two-dimensional scanning means 3 and an objective lens 4. The light reflected by the surface of the object and transmitted again through the objective lens 4, the X-Y two-dimensional scanning means 3 and the half mirror 2 is incident on the entrance end surface of a double mode channel waveguide 7 formed on the substrate 6. The length of the double mode channel waveguide 7 is chosen to be optimum for observing phase objects, so that the light propagated through the double mode channel waveguide 7 is distributed at a branch-off region 8 into two channel waveguides 9 and 10 in the optimum distribution ratio for reflecting the step heights on the surface of the object 5 strongly. The respective lights propagated through the channel waveguides 9 and 10 are subjected to the intensity measurement by photodetectors 11 and 12 provided at the exit ends of the channel waveguides 9 and 10. Signals output from the photodetectors 11 and 12 are simultaneously supplied to a subtracting circuit 13 and an adding circuit 14. The signals output from the subtracting and adding circuits 13 and 14 are respectively sent to A/D converters 15 and 16 to be quantized. The quantized difference and sum signals are input in a computer 19 from respective input ports 17 and 18. The computer 19 stores in an internal memory unit an apparatus constant which was preliminarily and experimentally obtained for the minute step height measuring machine in this embodiment. The computer 19 calculates a step height on the surface of the object 5 within the laser light spot from the apparatus constant and the quantized difference and sum signals based on the equation (21). The result of the calculation is displayed on a monitor 20 as a cross section of the object 5 together with a scale indicating the absolute value of the step height based on the positional information of the laser light spot on the surface of the object from the X-Y two-dimentional scanning means 3. The apparatus constant in this embodiment was determined as follows. First, a standard sample was formed on an Si substrate by means of a reactive dry etching technique. A step height of the standard sample was measured by an interferometer. The result as a specimen was measured by the step height measuring machine of this invention to obtain difference and sum signals. An apparatus constant was calculated from these difference and sum signals by using the equation (21). A plurality of standard samples having various step heights were formed to reduce the error and apparatus constants obtained from the respective standard samples were averaged to determine the apparatus constant for the step height measuring machine in this embodiment. Figure 2 is a sectional view of a standard sample. Figures 3A and 3B show portions of difference signal outputs obtained from standard samples with step heights of 12 nm and step heights of 30 nm respectively relative to the surfaces of the respective standard samples. Thus, the difference signal outputs are varied in accordance with the largeness of the step heights. If not the absolute values of the step heights but only the relative configuration of the step heights is required, the procedure of obtaining the apparatus constant is omitted. Although the apparatus constant is determined prior to the measurement in this embodiment, only the relative configuration of the step heights may be obtained at the time of the measurement and stored in an external memory unit and thereafter, the absolute configuration of the step heights may be obtained by calculation with the obtained apparatus constant. In this embodiment, the measurement of the step heights is possible only in one axial direction of the X-Y plane on the surface of the object. However, if the present invention is applied to a confocal laser scanning differential interference contrast microscope proposed in Japanese Patent Application Nos. 3-290293 and 4-159722 wherein a differential image can be obtained in two axial directions, the configuration of the surface of the object can be reproduced completely. According to the present invention, as above, it is possible to measure the step heights of the surface of the object without damaging the object and without being in contact with the object. Also, therein no need to provide a plurality of detecting devices as conventional and the apparatus can be provided with only one detecting device consisting of a substrate with a channel waveguide, making it possible to form the apparatus at low cost. Further, its quantification is endorsed by the wave optical image formation theory, so that it is possible to quantifiably measure the minute step heights on the object with high resolution and with ease even though the width of the minute step heights is fairly smaller than that of the laser light spot.

Claims: Apparatus for measuring a minute step height on an object (5) to be examined, comprising: a source (1) of coherent radiation for irradiating said object (5) with a light spot; and detecting means for detecting the radiation from the irradiated object (5), the detecting means comprising a double-mode channel waveguide (7) for receiving the radiation, two channel waveguide regions (9, 10) branched from said double mode channel waveguide (7) and two respective detecting elements (11, 12) for detecting radiation propagated in said channel waveguide regions (9, 10) and for generating two respective detection signals, characterised in that said apparatus further comprises calculating means (13, 14, 19) for outputting data of a minute step height on said object (5) based on a ratio of the sum of and the difference between said signals when said light spot is at the same position on said object (5). An apparatus according to claim 1, where in said radiation source (1) is a laser source (1), wherein said detecting means has a substrate formed with said channel waveguide (7) which is constituted of a double mode channel waveguide region having an entrance end on a detecting surface and said two branch channel waveguide regions branched from said double mode channel waveguide, and wherein said apparatus further comprises: an illuminating optical system (2, 4) for focusing a light beam from said laser source (1) and forming said light spot on said object (5); and a focusing optical system (4) for condensing the light beam from said object (5) on said detecting surface. An apparatus according to claim 2, wherein when the fully coupled length of both modes in said double mode channel waveguide region is Lc, the length of said double mode channel waveguide region L is given by L = Lc (2m + 1) / 2. (m = 0, 1, 2 ....) An apparatus according to claim 1, 2 or 3, further comprising scanning means (3) for relatively shifting the light spot with respect to the object (5). An apparatus according to any preceding claim, wherein said calculating means obtains the minute step height  0 on said object based on the sum S(s 0 ) of said signals and the difference W(s 0 ) of said signals by the following equation:  0 = C P ·S(s 0 )/W(s 0 ), wherein C P is an eigen constant of said apparatus. A method of measuring a minute step height on an object (5) to be examined, comprising the steps of: forming a light spot on said object (5) by focusing a light beam from a laser source (1); focusing the light beam from said object (5) on a detecting surface; and detecting the light beam focused on said detecting surface, said detecting step comprising the step of: detecting the intensities of light which are propagated from an entrance end of said detecting surface through a double mode channel waveguide region and at least two branch channel waveguide regions (9, 10) branched from said double mode channel waveguide region, characterised by the step of calculating a value representation of said minute step height on the object based on a ratio of the sum of and the difference between said intensities when said light spot is at the same position on said object (5). A method according to claim 6, wherein when the fully coupled length of both modes in said double mode channel waveguide region is Lc, the length of said double mode channel waveguide region L is given by L = Lc (2m + 1) / 2. (m = 0, 1, 2 ....) A method according to claim 6 or 7, further comprising the step of relatively shifting said light spot with respect to said object (5). A method according to any of claims 6, 7 or 8 wherein said calculating step obtains the minute step height  0 on said object based on the difference data S(s 0 ) and the sum data W(s 0 ) by the following equation:  0 = C P ·S(s 0 )/W(s 0 ), wherein C P is an eigen constant of an apparatus for performing said method.

Inventors: IWASAKI JUN, IWASAKI YUTAKA, OKI HIROSHI, IWASAKI, JUN, IWASAKI, YUTAKA, OKI, HIROSHI, IWASAKI, JUN, DAISAN OHFUNA PAKUTAUN G-710, IWASAKI, YUTAKA, KOSUMO YOKOHAMA KOZUKUE, OKI, HIROSHI, AZAMINO RIIBERU B-204
Applicants: NIPPON KOGAKU KK, NIKON CORPORATION
Application year: 1994
Main classification: G01B11
IPC codes: G01B11, G02B21, G01B9