Method and apparatus for the production of semi-solidified metal composition

Abstract: In a method and an apparatus for producing a solid-liquid metal mixture in which non-dendritic primary solid particles are dispersed into the remaining liquid matrix through electromagnetic induction system, a core member is arranged inside a cooling agitation tank provided with an electromagnetic induction coil therearound.

Description: This invention relates to a method for producing a solid-liquid metal mixture in which non-dendritic primary solid particles are dispersed into the remaining liquid matrix (hereinafter referred to as a semi-solidified metal composition) by electromagnetic induction agitation, and an apparatus used therefor. In methods for the production of a semi-solidified metal composition, agitation can be carried out mechanically or by electromagnetic induction. The electromagnetic induction agitating method (hereinafter referred to simply as electromagnetic agitation) is poor in agitating efficiency as compared with the mechanical agitating method, but is less restricted in the materials that can be used in the apparatus and is high in productivity. As a result, there have hitherto been proposed many improvements for the electromagnetic agitation. In Japanese Patent Applications Publication Nos. 61-7148 and No. 62-25464, there is disclosed a method of continuously or semi-continuously producing a metal slurry in a semi-solidified state by electromagnetic agitation and an apparatus used therefor. In this method, an electromagnetic agitation means producing a rotating magnetic field through a bipolar electric motor stator or the like is used and a mould provided with a cooling means is arranged inside the rotating magnetic field. Molten metal is then charged into the mould from above and cooled and agitated therein while being rotatably moved by the rotating magnetic field. As a result, a metal slurry of a semi-solidified state is obtained in which non-dendritic primary solid particles formed by breaking of dendrites are dispersed into the remaining liquid matrix. In order to provide a metal slurry having a good semi-solidified state, it is necessary to have strong cooling for forming sufficiently small solid particles and vigorous agitation strength for shearing dendrites. In the electromagnetic agitation system however, the above two conditions are conflicting, so that it can not necessarily be said to satisfy the above conventional method and apparatus. That is, there are the following problems in the conventional method and apparatus for the production of a semi-solidified metal composition by electromagnetic agitation: (1) In order to produce a good semi-solidified metal composition, it is necessary to provide vigorous agitation while cooling the molten metal. If it is intended to conduct vigorous agitation through the conventional electromagnetic agitation or high-speed rotating movement, a large eddy dent is created in the central portion of the rotating molten metal because of centrifugal force. In addition, the level of the outer peripheral portion of the molten metal becomes higher, and consequently the scattering of molten metal from the upper part of the cooling agitation tank and gas entrapment increase. As a result, stable operation is impossible. Therefore, the high-speed rotating movement or vigorous agitation effect can not be attained in the conventional electromagnetic agitation system. (2) Although the central portion of molten metal is rotated at a high speed, the agitation effect is less and hence the agitation effect, when considered in the horizontal section of the molten metal, is not uniform. On the other hand, the rotating speed or agitation effect is dependent upon the viscosity of the molten metal, so that as the apparent viscosity at the semi-solidified state becomes high, the agitation effect lowers and particularly the mixing effect is lost at the central portion and hence the risk of causing segregation increases. (3) In order to produce a good semi-solidified metal composition, it is necessary to conduct strong cooling for forming sufficiently small solid particles. In the conventional electromagnetic agitation system, the internal volume of the cooling agitation tank is large with respect to the area of the inner wall or cooling wall thereof and the heat capacity of the molten metal is large so that the cooling rate can not be made fairly high due to the heat generated by current produced through the rotating magnetic field. On the other hand, when strong cooling is carried out by using a water-cooled copper plate in the inner wall, a solidification shell adheres to the inner wall and gradually grows. This reduces the magnetic flux of the rotating magnetic field, whereby the agitation effect is considerably decreased, so that the cooling strength in the inner wall is critical. (4) In the conventional electromagnetic agitation system, the central portion of rotating movement of the molten metal or the central portion of the cooling agitation tank forms a dead space for the production of the semi-solidified metal composition and is harmful and useless. JP-A-1138044 discloses a method for producing a semi-solidified metal composition having the features of the preamble of claim 1. It is, therefore, an object of the invention to effectively solve the above problems of the conventional technique and to provide a method and an apparatus for the production of semi-solidified metal compositions by electromagnetic agitation which can eliminate the scattering of molten metal and the entrapment of gas and increase the agitation and cooling effects and attain stable operation. According to a first aspect of the invention, there is provided a method for producing a semi-solidified metal composition using electromagnetic agitation, comprising discharging molten metal into a cooling agitation tank cooling said molten metal via the inner wall of said cooling agitation tank, while agitating said molten metal by rotatably moving the molten metal between said inner wall of the tank and the outer wall of a core member arranged in the central portion of the tank by means of a magnetic field acting horizontally across the tank and discharging the resulting semi-solidified metal composition from a discharge port in the tank, characterised in that said molten metal is rotated between said inner wall of the tank and the outer wall of a cooled, non-magnetic, non-conductive core member. The inventors have found that it is most effective to remove molten metal from the central portion of the rotating molten metal or the central portion of the cooling agitation tank substantially not contributing to the cooling and agitation effects for solving the above problems and have made various studies, and as a result the invention has been accomplished. The use of a cooled body as the core member increases the cooling efficiency of molten metal. In a preferred embodiment in accordance with the first aspect of the invention, the core member is repeatedly lifted up and down inside the tank during the rotating movement of molten metal. According to a second aspect of the present invention, there is provided apparatus for producing a semi-solidified metal composition using electromagnetic agitation comprising a cooling agitation tank provided with means for cooling molten metal, an electromagnetic induction coil for producing a rotating magnetic field across a section of the tank to rotate the molten metal in the tank, a discharge port for discharging the resulting semi-solidified metal composition, and a core member arranged in the central portion of the tank the disposition of said core member relative to said port being adjustable, characterised in that said core member is a cooled, non-magnetic, non-conductive body. In a preferred embodiment in accordance with the second aspect of the invention, the core member is rotatably supported and fixed through a torque meter. The outer size of the core member may be within the range of 30-60% of the inner diameter of the cooling agitation tank. Furthermore, the shape of the inner wall face of the cooling agitation tank is preferably cylindrical, and the shape of the outer wall face of the core member is preferably cylindrical, but may be various forms for improvement of the agitation effect and the like. Moreover, the core member is preferably positioned in such a manner that its centre axis substantially meets with the centre axis of the cooling agitation tank. However, in some embodiments, the centre axis of the core member may be somewhat shifted from the centre axis of the tank. When the core member is required to act as a stopper, the shape of the portion of the core member adjacent the discharge port is preferably hemispherical or the like so as to conform with the shape of the discharge port in the cooling agitation tank. In another preferred embodiment of the invention, there are at least two cooled bodies, one of the cooled bodies being, in use, immersed in the molten metal and the or each other cooled body being cooled or preliminarily heated to a given cooling temperature at a waiting position. The cooled body may comprise ceramic, cermet, metal or a composite body thereof. For a better understanding of the invention, and to show how the same may be carried into effect, reference will now be made, by way of example only, to the accompanying drawings, in which:- Fig. 1 is schematic sectional view of a first embodiment of an apparatus for the production of semi-solidified metal composition in accordance with the invention; Fig. 2 is a theoretical view showing an agitating action in the conventional electromagnetic agitation system; Fig. 3 is a theoretical view showing an agitating action in the electromagnetic agitation system in accordance with the invention; Fig. 4 is a graph showing agitation effects in the electromagnetic agitation system according to the conventional technique and the invention; Figs. 5a and 5b are graphs showing relations between the radius of the core member and the shearing rates at inner wall face of the cooling agitation tank and outer wall face of the core member; Fig. 6 is a graph showing the relation between the radius of the core member and the eddy dent of molten metal; and Fig. 7 is a schematic sectional view of another embodiment of the apparatus for the production of semi-solidified metal composition in accordance with the invention. When semi-solidified metal compositions are produced from molten metal by cooling and agitating through rotating movement of molten metal in a rotating magnetic field according to the invention, the non-magnetic and non-conductive core member made of, for example, a refractory material or ceramics is arranged to be in the rotating centre portion of the molten metal or the central portion of the cooling agitation tank, whereby molten metal is removed from the rotating center portion as a dead space. Thus, the molten metal is agitated by rotating movement between the outer wall face of the core member and the inner wall face of the cooling agitation tank. In this case, the rotating speed of such a rotating movement is small compared to the case of using no core member. However the eddy dent of the surface level of the molten metal is decreased to a practical extent and hence stable operation can be attained without scattering of the molten metal. Furthermore, the lowering of the agitation effect can be prevented by properly selecting the size of the core member even though the rotating speed becomes small. Moreover, when the core member is lifted up and down, molten metal is moved up and down in addition to the rotating movement, whereby a more homogeneous semi-solidified metal composition can be produced. In the latter case, the core member acts as a stopper at the time of starting the operation. A first embodiment of an apparatus for the production of semi-solidified metal composition according to the invention will be described with reference to Fig. 1. As shown in Fig. 1, a cooling agitation tank 1 comprises a vertical cooling cylinder 2 and a water-cooled jacket 3, and an electromagnetic induction coil 4 is arranged around the outer periphery of the tank 1. Each of the cooling cylinder 2 and the water-cooled jacket 3 is made from thin and non-magnetic metal plate for reducing attenuation of the magnetic flux as far as possible. In the cooling agitation'tank 1, cooling water is supplied to a lower part 13 of the water-cooled jacket 3 and discharged from an upper part 13' thereof, during which cooling water passes over the outer surface of the cooling cylinder 2 at a high speed to give a proper cooling effect to molten metal held inside the cylinder 2. Moreover, the inner wall face of the cylinder 2 may be lined with a refractory material of a proper thickness. The stator coil of a bipolar, three-phase induction motor is frequently used as the electromagnetic induction coil 4, to which is supplied a three-phase alternating current 14 to provide a rotating magnetic field in the centre of the coil. As a result, molten metal is agitated in the cooling agitation tank 1 by rotating movement at a rotating torque in proportion to the magnetic flux density of the rotating magnetic field. A tundish 5 for molten metal lined with a refractory material 5' is arranged at the upper end of the cooling agitation tank 1, while a discharge nozzle 6 is arranged at the bottom portion of the tank 1. In the central portion of the cooling agitation tank 1 is arranged a cooled, non-magnetic and non-conductive core member 7 made from, for example, a refractory material. The core member 7 is rotatably supported by a support arm 8 through a bearing 9, as shown in Fig. 1. Furthermore, the support arm 8 is liftably mounted on a support base 10 by lifting means 11, such as hydraulic cylinder or the like. Moreover, a torque meter 16 is attached to the core member 7 through a connecting rod 15. In operation, molten metal 17 is continuously fed into the tundish 5, from which it flows into the cooling agitation tank 1. The molten metal is cooled by the cooling action of the cooling cylinder 2 in the tank 1 and of the cooled core member 7 and simultaneously agitated by rotating movement between the outer wall face of the core member 7 and the inner wall face of the cylinder 2 caused by the rotating magnetic field generated by the electromagnetic induction coil 4. As a result, the resulting dendrite is converted into such a state having a spheroidal or granular shape that dendritic branches are substantially eliminated or reduced and, at the same time, the resulting non-dendritic primary solid particles are dispersed into the remaining liquid matrix to form a semi-solidified metal composition 18. Then, the semi-solidified metal composition 18 is continuously discharged from the discharge nozzle 6 located at the bottom of the cooling agitation tank 1. In this case, the core member 7 may be set to a given position or may be moved in up and down directions in the tank 1 through the lifting means 11 to promote the agitating effect. Moreover, the properties and agitating state of the semi-solidified metal composition can be estimated by measuring the viscosity torque of the semi-solidified metal composition acting on the core member by means of the torque meter 16. After completion of the operation, the core member 7 is lifted upwards from the tank 1 through the support arm 8 by actuation of the lifting means 11 in the form of a hydraulic cylinder. Preferably, the support arm 8 is turned to enable easy maintenance and inspection of the cooling agitation tank 1. Fig. 2 shows a theory of the agitating action in the conventional electromagnetic agitation system, and Fig. 3 shows a theory of the agitating action in the electromagnetic agitation system according to the invention, and Fig. 4 is a graph representing the above agitating effect as a numerical value. In Figs. 2 and 3, the cooling agitation tank 1 comprising the cooling metal cylinder 2 and the water-cooled jacket 3 and the electromagnetic induction coil 4 arranged therearound are common, but the cooled core member 7 is arranged inside the tank 1 in the system of Fig. 3. In the conventional system of Fig. 2, as agitation through the rotating magnetic field becomes strong, molten metal 17 in the tank 1 is rotated at a high speed, in which the rotating speed (Ω) is maximum at the central portion of the tank 1 as shown in Fig. 4. Consequently a large eddy dent (H o ) is created at the centre by centrifugal force. If the eddy dent (H o ) becomes too large, problems are caused such as scattering of molten metal from the upper part of the tank, entrapment of gas and the like. Although the central portion of molten metal is rotated at a very high speed, the shearing force required for the conversion of dendrites is very small or the agitating effect is substantially zero. As shown in Fig. 3, according to the invention, the cooled cylindrical core member 7 having a radius r 1 is arranged in the central portion of the tank 1. If the rotating magnetic field having the same intensity as in the conventional system is applied to the system according to the invention, the rotating speed (Ω) of the rotating movement produced in molten metal 17 becomes zero at the inner wall face of the cooling cylinder 2 and the outer wall face of the core member 7, so that the maximum rotating speed becomes small. As a result, the eddy dent (H o ) produced through centrifugal force becomes fairly small, which solves problems in practical use. Furthermore, the agitating effect generated in the horizontal section of the molten metal or the shearing stress is on average substantially the same over such a section, even though the rotating speed is smaller than that of the conventional system, so that the agitating effect becomes very effective for molten metal. In the electromagnetic agitation system, molten metal itself rotates through rotating force of electromagnetic induction produced in molten metal, so that the rotating speed of molten metal or semi-solidified metal composition or the agitating effect of molten metal itself is dependent upon the viscosity of the molten metal or the semi-solidified metal composition. Although it is difficult to confirm the rotating speed or the agitating effect in the conventional system, according to the invention, the agitating effect is estimated by measuring the viscosity torque of molten metal by means of the torque meter 16 directly connected to the core member 7. The invention will now be described with respect to the relationship between the inner diameter of the cooling agitation tank (i.e. cooling cylinder 2) and the outer diameter of the core member 7 for providing the effective agitating effect. When a rotating magnetic field of 600 gauss is produced inside a cooling agitation tank having an inner diameter of 170 mm and the core member is arranged inside the tank so that the centre axis of the outer wall face of the core member is aligned with the centre axis of the inner wall face of the tank, the results measured on the agitating effect are shown in Figs. 5a, 5b and 6. In Figs. 5a and 5b, relationships of the radius (r 1 ) of the core member to the shearing strain rates at the inner wall face of the tank and outer wall face of the core member, respectively, are shown using the fraction solid (fs) as a parameter. The relationship between the radius (r 1 ) of the core member and the eddy dent (H o ) at the outer wall face of the core member is shown in Fig. 6 using the fraction solid (fs) as a parameter. In these graphs, the shaded portion is a practical region having a large shearing strain rate (agitating effect) and showing a small eddy dent and an optimum radius range of core member. This region shows that the outer diameter of the core member preferably corresponds to 30-60% of the inner diameter of the cooling agitation tank. When the semi-solidified metal composition is discharged from the discharge nozzle 6 located at the bottom of the cooling agitation tank 1, a known sliding gate system, rotary valve system, stopper system and the like can be used as a discharge nozzle. Among these systems, however, the sliding gate system and rotary valve system have drawbacks in that the flow of semi-solidified metal composition through the nozzle is apt to be disturbed and metal is apt to adhere to the nozzle. Restoring flow is difficult after adhesion of metal to the nozzle. On the contrary, the stopper system of lifting a stopper up and down to change the opening area of the nozzle is most suitable for controlling the discharge of the slurry of semi-solidified metal composition. According to one embodiment of the invention, the core member is utilized as a stopper. In this case, as shown in Fig. 1, the core member 7 is lifted down so as to contact with the bottom of the cooling agitation tank 1 by the actuation of the hydraulic cylinder 11 above the discharge nozzle 6 at the initial operation stage (shown by a phantom line in Fig. 1), whereby the core member 7 serves as a stopper for closing the opening of the discharge nozzle 6. Then, molten metal 17 is discharged into the cooling agitation tank 1 and cooled and agitated by the cooling cylinder 2 and the electromagnetic induction coil 4 to increase the fraction solid of the resulting slurry as a semi-solidified metal composition. When the fraction solid reaches a given value, the core member 7 is lifted upward by actuation of hydraulic cylinder 11 to adjust the opening degree of the stopper and discharge the semi-solidified metal composition from the nozzle 6. That is, the core member 7 is used to serve as a stopper when the molten metal charged into the cooling agitation tank is discharged out from the discharge nozzle 6 at the initial operation stage. In another preferred embodiment of the invention, as shown in Fig. 7, a cooled body composed of ceramics, cermet, metal or a composite material thereof is used as the core member 7 for enhancing the cooling of the molten metal 17. In this case, at least a pair of the cooled bodies 7 are suspended from the top portions of at least a pair of support arms 8 which can be lifted and rotated by support base 10, respectively. In use, one of the cooled bodies 7 is immersed into the molten metal 17 inside the cooling agitation tank 1, while the other cooled body 7 is placed at a waiting position. In this waiting position, the temperature of the cooled body is adjusted to a given initial cooling temperature by means of a temperature adjusting means comprising refrigerant spraying nozzles 19 arranged at both sides of the cooled body and a cylindrical preheating furnace 20 moved in up and down so as to surround the cooled body. When these cooled bodies 7 are alternately immersed into the molten metal 17, heat can rapidly be removed from the molten metal because the temperature difference between the cooled body and molten metal is large, whereby the semi-solidified metal composition in which fine non-dendritic primary solid particles are uniformly dispersed into the remaining liquid matrix can be produced by synergistic action with the agitating effect through electromagnetic induction. The invention will be further described with reference to the following examples. Example 1 This example shows a case in which molten metal is cooled and agitated in a cylindrical cooling agitation tank having an inner diameter of 170 mm (r 2 = 85 mm) provided with a bipolar, three-phase agitating coil under a rotating magnetic field showing a centre magnetic flux density of 800 gauss. In the conventional method as shown in Fig. 2, the maximum rotating speed of the molten metal was 1000 rpm in the central portion, and the eddy dent H o at the rotating central portion was 1200 mm. In the method of the invention using a cylindrical core member 7 with an outer diameter of 100 mm (r 1 = 50 mm) as shown in Fig. 3, the maximum rotating speed of the molten metal was about 200 rpm at a middle point between the outer wall face of the core member 7 and the inner wall face of the cooling agitation tank 1, and the eddy dent H o was reduced to 70 mm at the surface of the core member, so that the stable operation was made possible. When the theoretical calculation for representing the agitating effect as a shearing strain rate was conducted, it was found to be a maximum of 250 sec -1 at the inner wall face of the cooling agitation tank and zero in the rotating central portion according to the conventional method, while it was a maximum of 230 sec -1 at the inner wall face of the cooling agitation tank and the outer wall face of the core member according to the method of the invention. From this it was apparent that the invention provides an effective agitating effect. Example 2 A cylindrical bottomed vessel having an inner diameter of 170 mm and provided with a water-cooled jacket was set inside an electromagnetic induction coil of 1100 gauss, and then molten cast iron was filled in the vessel and agitated to a solid-liquid coexisting region. In case of using no core member, the cast iron was rotated at 600 rpm and the shape of the surface level was very deep concave at the center. When the core member was immersed into the cast iron, the rotating speed was reduced to 300 rpm and the shape of the surface was fairly gently concave. The cast iron was sampled at the solid-liquid coexisting temperature (fraction solid = 25%) and solidified by quenching, and thereafter the resulting solidified texture was observed. As a result, the texture was uniform because there was no great difference in the shearing strain rate. Then, a discharge nozzle was arranged in the bottom of the above cylindrical vessel and 500 kg of molten cast iron was continuously charged thereinto. When the core member was not used as a stopper, the cast iron was discharged from the discharge nozzle at substantially liquid state. On the other hand, when the core member was used as a stopper, the cast iron was filled in the vessel at an initial charging stage while closing the discharge nozzle with the core member and then the discharge of the resulting semi-solidified metal composition was controlled by gradually moving the core member upwards so as to balance the discharge rate with the charging rate. As a result, it was confirmed from the measurement of the discharging temperature that semi-solidified metal composition having a fraction solid of 20% could stably be produced from the initial charging stage to the last charging stage. For comparison, the discharge of semi-solidified composition was controlled by arranging a sliding gate on the bottom of the discharge nozzle without using the core member as a stopper. When the sliding gate was closed to fill the vessel with cast iron at the initial charging stage, if the gate was opened, discharge of the semi-solidified metal composition was impossible because the nozzle was clogged with solidified iron. In order to prevent such a phenomenon, the sliding gate was fully opened at the initial charging stage and gradually closed to control the discharging amount. However, a greater part of the cast iron (500 kg) was discharged in a liquid phase state when the nozzle was fully open to prevent the clogging of the nozzle, and discharge of the semi-solidified metal composition was first observed only at the last charging stage. As seen from the above, the use of the core member as a stopper stabilises the surface level and prevents gas entrapment, and also brings about stable production of the semi-solidified metal composition. Example 3 Cast iron was cooled and agitated by using an apparatus shown in Fig. 7 to produce a semi-solidified metal composition. In this case, cooling water was passed through the water-cooled jacket 3 at a rate of 600 l/min, and hence the temperature of the cooling water was raised by 1°C. Due to using a cooled body as the core member 7 the cooling capacity of the cooling agitation tank 1 was about 600 kcal.min. When cast iron (C content: 2.58) was passed through the cooling agitation tank at a rate of 34 kg.min (5 l/min), if a cooled body was not used as the core member, the cast iron was substantially discharged from the discharge nozzle 6 in a liquid phase state even after about 5 minutes. On the other hand, when the cooled body 7 was immersed into the cast iron inside the cooling agitation tank 1, the semi-solidified metal composition having a fraction solid of 5-10% could stably be produced. In the latter case, the cooled body 7 was made from alumina graphite and had an outer diameter of 100 mm and had been previously heated to a temperature of 400°C. During the charging of cast iron, the cooled body 7 had a cooling capacity of about 2000-2500 kcal/min, so that the cast iron was cooled by about 4-5 times as compared with the case of using only water cooling. Furthermore, the fraction solid of the semi-solidified metal composition could be changed by changing the outer diameter of the cooled body even at the same charging rate. In the production of semi-solidified metal compositions by the electromagnetic agitation according to the invention, the following merits are expected: (1) Even when molten metal is agitated through strong turning movement by electromagnetic induction agitation, the eddy dent is small and there is no risk of scattering molten metal from the upper part of the cooling agitation tank, so that a stable, practical operation is made possible. (2) Under the same rotating magnetic field, the agitating effect is same even when the rotating speed lowers. In the conventional method, the rotating centre portion forms a dead space providing substantially no agitating effect, while according to the invention, a substantially uniform agitating effect is obtained. (3) An amount of molten metal corresponding to the volume of the core member is eliminated from the cooling agitation tank, so that heat capacity is reduced by a quantity corresponding to such an amount and hence the cooling rate for molten metal is increased even at the same cooling capacity, and thus semi-solidified metal compositions having a smaller particle size can be produced. (4) When the core member is used as a stopper at the initial charging stage, the semi-solidified metal composition can stably be produced by controlling the discharging amount while preventing gas entrapment. (5) Using a cooled body as the core member means that the cooling capacity against molten metal can largely be increased in a relatively simple manner. Furthermore, when a plurality of cooled bodies are used alternately, the semi-solidified metal composition can continuously be produced over a long period of time. Moreover, the cooling capacity substantially determined by the structure of the apparatus itself can be changed by changing the size of the cooled body. As mentioned above, the invention considerably contributes to the practical use of the electromagnetic induction agitating system for the production of semi-solidified compositions.

Claims: A method for producing a semi-solidified metal composition using electromagnetic agitation, comprising discharging molten metal (17) into a cooling agitation tank (1), cooling said molten metal (17) via the inner wall of said cooling agitation tank (1), while agitating said molten metal (17) by rotatably moving the molten metal (17) between said inner wall of the tank (1) and the outer wall of a core member (7) arranged in the central portion of the tank (1) by means of a magnetic field acting horizontally across the tank (1), and discharging the resulting semi-solidified metal composition from a discharge port (6) in the tank (1), characterised in that said molten metal (17) is rotated between said inner wall of the tank (1) and the outer wall of a cooled, non-magnetic, non-conductive core member (7). A method as claimed in claim 1, wherein said core member (7) is repeatedly lifted up and down inside the tank (1) during the rotating movement of the molten metal (17). A method as claimed in claim 1 or claim 2, wherein, in order to fill said cooling agitation tank (1) with molten metal (17) at the start of operation, the core member (7) is moved to block said discharge port (6) and prevent flow of molten metal (17) therefrom. A method as claimed in claim 1, 2 or 3, wherein said molten metal (17) is continuously discharged into said cooling agitation tank (1) and the resulting semi-solidified metal composition is continuously discharged from said discharge port (6) at a rate of discharge which is controlled by the disposition of said core member (7) relative to said discharge port (6). Apparatus for producing a semi-solidified metal composition using electromagnetic agitation, comprising a cooling agitation tank (1) provided with means for cooling molten metal (2, 3), an electromagnetic induction coil (4) for producing a rotating magnetic field across a section of the tank (1) to rotate the molten metal (17) in the tank (1), a discharge port (6) for discharging the resulting semi-solidified metal composition, and a core member (7) arranged in the central portion of the tank (1), the disposition of said core member (7) relative to said port (6) being adjustable, characterised in that said core member (7) is a cooled, non-magnetic, non-conductive body. Apparatus as claimed in claim 5, wherein said core member (7) is rotatably supported by and fixed to a support arm (8) having a torque meter (16). Apparatus as claimed in claim 5 or claim 6, wherein the outer diameter of said core member (7) is in the range of 30-60% of the inner diameter of said cooling agitation tank (1). Apparatus as claimed in claim 5, 6 or 7, wherein the inner wall face of said cooling agitation tank (1) and the outer wall face of said core member (7) are cylindrical. Apparatus as claimed in any one of claims 5 to 8, wherein said core member (7) is positioned in such a manner that the centre axis thereof substantially meets with the centre axis of said cooling agitation tank (1). Apparatus as claimed in any one of claims 5 to 9, wherein the shape of the discharge port (6) and the shape of the portion of said core member (7) adjacent the discharge port (6) are hemispherical. Apparatus as claimed in any one of claims 5 to 10, comprising at least two cooled bodies, one of the cooled bodies being, in use, immersed in said molten metal and the or each other body being cooled or preliminarily heated to a given cooling temperature at a waiting position. Apparatus as claimed in any one of claims 5 to 11, wherein said cooled body (7) comprises ceramic, cermet, metal or a composite thereof.

Inventors: FUJIKAWA YASUO, TAKEBAYASHI KATSUHIRO, YOSHIKAWA YUJI, FUJIKAWA, YASUO, TAKEBAYASHI, KATSUHIRO, YOSHIKAWA, YUJI, FUJIKAWA, YASUO, C/O RHEO-TECHNOLOGY, LTD., TAKEBAYASHI, KATSUHIRO, C/O RHEO-TECHNOLOGY, LTD., Yoshikawa, Yuji, c/o Rheo-Technology, Ltd.
Applicants: RHEO TECHNOLOGY LTD, RHEO-TECHNOLOGY, LTD
Application year: 1991
Main classification: C22C1
IPC codes: C22C1, B22D11