Low temperature infrared source

Abstract: An infrared source suitable for use as a remote source for infrared interferometer spectrometers. This device is composed of a heat source (1), a black body radiating element (4) and a concave reflector (3). A support (2) to maintain the heat source and black body radiating element (4) in proper position is also preferably included. The device of the present invention enhances the accuracy and sensitivity of gas sensing devices based upon measurement of background infrared radiation, and allows the remote infrared source to be used in locations in which ignitable materials may be present.

Description: The present invention relates to a low temperature infrared radiation source, comprising a heat source, which is surrounded by a black medium and a concave reflector for collimating said radiation. Use of an infrared source to provide a radiation source which essentially matches the radiation of the source to the throughput radiation of an interferometer spectrometer is known. For example, U.S. Patent 4,724,329 discloses an infrared source which is composed of a radiating element positioned at the center of a hollow, inwardly reflecting sphere having a single aperture positioned to fill the entrance field of view of a spectrometer with infrared radiation. This infrared source is, however, contained in the disclosed interferometer and does not function as a remote source. Further, the temperatures present in this source are undesirably high, particularly if the device is to be located in an area in which significant amounts of volatile, ignitable materials are present. Another infrared radiation source is described in U.S. Patent 4,064,402 the radiation source being surrounded by a gas or a mixture of gases. The gas is selected for absorbing the visible light, but transmits the infrared portion of the light source and thus is acting as an absorption filter. Further this infrared radiation source comprises an enclosure type glass tube and a transparent envelope surrounding and spaced from the radiation source, the gas or gas mixture being enclosed in the interspace between the glass tube and said envelope. U.S. Patent 4,681,445 also discloses an interferometer in which a radiation source is incorporated. The details of this radiation source are not given but it is clear from the disclosure that use of the radiation source external to the interferometer was not contemplated. U.S. Patent 4,740,082 also discloses a spectrophotometer in which an infrared radiation source beam is employed. In this disclosure, it is taught that the source beam may be positioned within the enclosure of a spectrophotometry instrument or external to the instrument. This disclosure does not, however, teach a specific instrument which employs an infrared source external to the device. The radiation source employed is a heated wire which provides radiation between the wavelengths of 5000 and 50 wavenumbers in the infrared spectrum. Such heated wire could not, however, be used as an external remote infrared source in an area where volatile materials might be present in significant quantities without substantial risk of fire or explosion. In view of the greater flexibility of a remote source spectrophotometer, it would be advantageous to have an infrared radiation source which is external to the spectrophotometer that did not generate temperatures which would preclude its use in areas where volatile chemicals might be present in significant quantities. SUMMARY OF THE INVENTION It is an object of the present invention to provide a remote source of infrared radiation which may be used in any area to be monitored, even an area in which significant amounts of volatile, flammable materials may be present. This and other objects, which will be readily apparent to those skilled in the art are accomplished by a device in which the black medium surrounding the heat source is a black body radiating element acting as a heat sink for the heat generated by the heat source and wherein a concave reflector is provided for, which is positioned to reflect the radiant energy emitted from said radiating element. Further specific embodiments and improvements are apparent from the attached subclaims. BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 illustrates one embodiment of the remote source of the present invention. Figure 2 illustrates a convex black body radiating element suitable for use in the remote source of the present invention. DETAILED DESCRIPTION OF THE PRESENT INVENTION The present invention relates to a low temperature remote source of infrared radiation useful in connection with infrared spectrophotometers, particularly gas sensing devices such as those described in U.S. Patent 4,795,253. The device of the present invention is composed of a heat source, a black body radiating element, a concave reflector and if necessary, a support to hold the heat source in its proper position within the reflector. One embodiment of such a device is shown in Figure 1 in which heat source 1 is mounted on support 2 which is mounted on concave reflector 3 . Heat source 1 is completely surrounded or encased by black body radiating element 4 . Heat source 1 may be any device capable of raising the surface temperature of radiating element 4 to required levels. Specific examples of such devices include heating cartridges, wire heating elements, ceramic heating elements, quartz encased wire heaters and the like. The size of an appropriate heat generating device will of course depend upon the size of the black body radiating element 4 and the required power output of the source. The size of heat source 1 will also determine whether or not support 2 is needed. If support 2 is necessary, it is generally made of a durable material capable of withstanding the heat generated by heat source 1 without deterioration. Specific examples of suitable materials include stainless steel, ceramic, and chrome alloys. Where a support is employed, that support is generally long enough to maintain heat source 1 in the center of black body radiating element 4 and at the approximate focal point of concave reflector 3 . Reflector 3 may be parabolic, spherical or an approximation of these shapes. Reflector 3 is generally made of a material capable of withstanding a harsh environment such as rhodium plated electroformed nickel. The size of reflector 3 is dependent upon the area required for proper operation of the particular remote spectrometer employed, and will generally range from 3" to 36" in diameter. Heat source 1 and the surrounding radiating element 4 are generally positioned at the focal point of reflector 3 , so as to collimate the outgoing infrared beam. Black body radiating element 4 acts as a heat sink for the heat generated by heat source 1 . Black body radiating element 4 reduces the radiating surface temperature generated by heat source 1 but maintains the thermal output of heat source 1 . The black body element also shifts the spectral maximum from the visible and near infrared regions to longer infrared wavelengths. Black body radiating element 4 is generally made of a material capable of withstanding the temperatures generated by heat source 1 and the chemical environment of the area in which it is to be placed. Specific examples of suitable materials include brass, copper, stainless steel, and alloys having high thermal conductivity. The shape of black body radiating element 4 facing the reflector 3 is generally rounded or parabolic, preferably, with a diameter in the range of .5 to 0.028 of the diameter of reflector 3 . A particularly advantageous shape is illustrated in Figure 2. The inner surface of black body radiating element 4 is chemically blackened to improve emissivity. Techniques for blackening surfaces are known to those skilled in the art and any one of the known techniques may be employed. An example of such a technique is to treat the brass or copper with a solution containing 1 part copper carbonate, 2 parts aqueous ammonia, 5 parts water at 175°F followed by dipping in a 2½% solution of caustic soda. As has already been mentioned, the device of the present invention is advantageously used in combination with spectrophotometric devices such as the one disclosed in U.S. Patent 4,795,253. More specifically, the device of the present invention may be positioned at a location between 15 and 500 meters from the gas sensing device. The radiation emitted by the device of the present invention is picked up by the gas sensing device and absorption bands due to gases in the beam path between the devices and are used to determine the presence and amounts of each gas. Having thus described our invention, the following examples are given as being illustrative thereof. All parts and percentages given are parts by weight and percentages by weight, unless otherwise indicated. EXAMPLES EXAMPLE 1 A device corresponding to that illustrated in Figure 1 was constructed from the following: Heat source 1 : a 250 Volt Amp ½ inch diameter Cromolox heater cartridge. Support 2 : a 14 inch length of ½ inch diameter stainless steel tube. Concave reflector 3 : a rhodium plated 24 inch parabolic reflector (available from Optical Radiation Corp.) Black body radiating element 4 : machined brass element which was chemically blackened. This device was then positioned 60 meters from the gas sensing device described in Example 1 of U.S. Patent 4,795,253 which is herein incorporated by reference. A 100 milligram sample of dichlorodifluoromethane was released into the atmosphere between the infrared source and the instrument. A spectrum of the halocarbon was obtained in approximately 3 seconds. Although the invention has been described in detail in the foregoing for the purpose of illustration, it is to be understood that such detail is solely for that purpose and that variations can be made therein by those skilled in the art without departing from the scope of the invention except as it may be limited by the claims.

Claims: A low temperature infrared radiation source comprising a heat source (1) which is surrounded by a black medium and a concave reflector (3) for collimating said radiation characterized in that the black medium is a black body radiating element (4) acting as a heat sink for the heat generated by the heat source (1) and that the concave reflector (3) is positioned to reflect the radiant energy emitted from said radiating element (4). The source of claim 1 in which a support element (2) is employed to maintain the heat source (1) and the radiating element (4) in proper position with respect to the concave reflector (3). The source of claim 1 in which the heat source (1) is a heater cartridge. The source of claim 1 in which the radiating element (4) has a convex hemispheric or parabolic surface facing the reflector. The source of claim 1 in which the reflector (3) is a parabolic mirror. The source of claim 1 in which the reflector (3) is a hemispherical mirror.

Inventors: HUNT ROBERT N, SANDRIDGE ROBERT L, HUNT, ROBERT N., SANDRIDGE, ROBERT L.
Applicants: MILES INC, MILES INC.
Application year: 1990
Main classification: G01J3
IPC codes: G01J3, G01N21