METHOD OF REDUCING THE OIL CONTENT OF CUTTINGS AND APPARATUS FOR THE APPLICATION OF SAID METHOD

Abstract: A method of reducing the oil content of cuttings, in which the cuttings are introduced into a drum-shaped space, where an elevated temperature is predominant and subjected to a hammering treatment in that space and the drum-shaped space is permanently heated from without so that during the performance of the hammering treatment the temperature in the interior is maintained in the vicinity of, but below, the cracking temperature of the oil in the cuttings to be treated, while further the pressure in the spaces is maintained at a value of at least 0.3 bar gauge. An apparatus for the application of such a method comprises a hammer mill and a dust cyclone, the hammer mill comprising a drum-shaped body, a rotary shaft passed through a side wall of the drum and extending axially through the drum, which shaft can be connected to suitable driving means outside the drum, onto which rotary shaft hammers are mounted which extend into a direction substantially transverse to the shaft reaching up to the vicinity of the inner wall of the drum, the drum further comprises an inlet for feeding cuttings to the drum and outlets for discharging the mist formed in the apparatus in operation and the purified cuttings respectively, the outlet for the mist being connected to the dust cyclone and means being provided around the drum for continuously supplying heat to the drum wall and maintaining it at a high temperature.

Description: Title: . Method of reducing the oil content of cuttings and apparatus for the application of said method. The invention relates to a method of reducing the oil content of cuttings, which have been removed from a drilling mud consisting essentially of oil or containing oil, in which the cuttings are treated for oil to be extracted from them, to effect which the cuttings are fed to a drum-shaped space in which an elevated temperature obtains and then subjected to a hammering treatment in that space, the temperature being selected so high that oil and water present in the cuttings are substantially converted to corresponding mist and/or vapour, which mist and/or vapour is removed from the drum- shaped space and passed to another space, where any residual dust is removed from the mist and/or vapour, the cuttings being removed from the drum-shaped space in more or less dry form. The invention further relates to an apparatus for the application of the method. A similar method and apparatus are known from GB patent application 2 165 259. In the known method the elevated temperature in the drum-shaped space is brought about by the heat of friction, which is produced by the rotation of the hammers provided in the drum for carrying out the hammering treatment and by the hammers' beating the cuttings. The publication mentioned does not specify what temperature is required in the drum. It is merely observed that the temperature is permitted to be substantially lower than in the then known methods, where temperatures of 260° C and over were utilized. In its discussion of test results the GB publication mentions a temperature of 172° C, beyond which it is suggested no further changes occur. Practice has shown that the known method does not lead to satisfactory results. It appears, in particular, that it is difficult to maintain a desired temperature. If the heat of friction generated in the drum brings about a desired high temperature at all, that temperature cannot be controlled. The object of the present invention is to provide a method which does not exhibit the drawback described above and an apparatus for applying that method. The object contemplated is achieved in accordance with the invention by the method of the type described in the preamble being characterized in that the drum-shaped space is permanently heated from without, so that during the performance of the hammering treatment the temperature in the interior is maintained throughout in the vicinity of, but below, the cracking temperature of the oil in the cuttings being treated, and further the pressure in the spaces is maintained at a value of at least 0.3 bar above atmospheric pressure. In the method according to the invention the drum-shaped space is continuously heated from without in a suitable manner, so that in the interior an elevated temperature of for instance at least 185° C or even more obtains. In accordance with the invention the temperature in the interior is just below the cracking temperature of the oil present in the cuttings. At such a high temperature the water present in the cuttings will, as it were, explode to form superheated steam, this process being enhanced by the hammering treatment applied to the cuttings. Residual oil in the cuttings will be entrained, so that a fine oil mist or vapour will be formed. The cuttings themselves are pulverized by the hammering treatment, so that a fine and quite homogeneous dust is formed. Pulverizing the cuttings allows the largest possible amount of oil and water to pass from the cuttings. By externally heating the drum-shaped space in which the hammering treatment is conducted, the temperature within the drum can be maintained at a required high level quite accurately, so that the explosive formation of steam entraining with it oil particles from the cuttings, continues without interruption. In practising the method according to the invention a gauge pressure of at least 0.3 bar is maintained in the drum and in the space connected to it for separating dust from the water vapour and the oil mist . Such a pressure will be brought about by the generated steam itself if the spaces referred to are kept closed off to a reasonable extent. In addition, the pressure in the system can optionally be maintained at a slightly higher value by introducing nitrogen via a duct connected to the hammer mill. An additional advantage of this option is that the risk of fire in the system is reduced in this way. Typically the gauge pressure will not exceed 1.3 bar. Partly due to the superatmospheric pressure and the action of the hammers the pulverized and purified cuttings will be carried through the drum from the location of supply to a location where the purified and virtually dry cuttings can be carried off. In the dry product the oil content is significantly lower than 5%, amounting to about 2% or less, which is permissible from environmental considerations if they are to be dumped as waste. The apparatus according to the invention, suitable for applying the method according to the invention, comprises a hammer mill and a dust cyclone, which hammer mill comprises a drum-shaped body, a rotary shaft passed through a side wall of the drum and extending axially through the drum, which shaft can be connected to suitable driving means outside the drum, hammers being mounted onto the rotary shaft, which hammers extend in a direction substantially transverse to the shaft and extend up to the vicinity of the inner wall of the drum, the drum further comprising an inlet for introducing into the drum cuttings containing oil and water and outlets for the mist containing oil, steam and dust, formed during the operation of the apparatus, and the purified cuttings, respectively, the outlet for the mist being connected to the dust cyclone and means being provided around the drum for continuously supplying heat to the drum wall and maintaining it at a high temperature. Preferably, the means for supplying heat to the drum wall and maintaining it at a high temperature comprise a system of chambers provided in or on the drum wall, which are connected to each other in such a way that a fluid passsed through these chambers from a location of supply to a location of discharge will pass along by far the greater part of said wall, the system of chambers being connected to a system in which heated thermal oil is circulated so that the thermal oil is introduced into the system of chambers at the location of supply and is removed from the system at the location of discharge. In a suitable embodiment of the apparatus according to the invention the shaft of the hammer mill, which is bearing- mounted on opposite sides, comprises a plurality of flanges secured to the shaft in spaced interrelationship and extending in a direction substantially transverse to the shaft, a plurality of evenly spaced hammer heads being arranged along the circumference of each flange, the hammer heads of consecutive flanges having a staggered arrangement in a direction parallel to the shaft. In such an arrangement the hammers of consecutive flanges are out of alignment with ach other as viewed in the longitudinal direction of the drum. Thus the accumulation of cuttings between the flanges is avoided. Six hammer heads, for instance, are arranged symmetrically along the circumference of each flange. Preferably, the hammer heads are provided on two opposite sides with a layer of very hard material. Hammer heads thus provided on opposite sides with a "hard facing", for instance of tungsten carbide, can in the course of time, be turned around, so that they can be employed longer. Further, the apparatus according to the invention is preferably constructed in such a way that in the hammer mill the shaft has its greatest diameter in the middle of the drum and is step-wise reduced on opposite sides towards its ends, each flange being welded to the shaft in the vicinity of such a step-wise reduction in such a way that the welds on opposite sides of each flange are at a different distance from the longitudinal axis of the shaft. The advantage of such welds at different levels is that the tendency for the flange secured in this way to become warped will be less . In addition to providing for the optimal connection of the flanges with their hammers, a reduction in opposite directions as described also provides for an improved balance of the shaft and a better distribution of forces in operation. The drum of the hammer mill may further be internally provided with semi-circular profiles extending in a direction parallel to the drum axis and secured to the inner surface in spaced interrelationship. Such semi-circular profiles offer additional protection to the drum, since during operation a "cake" of cuttings and drilling dust is formed on and between such profiles . Further, in the apparatus according to the invention the dust cyclone, too, may suitably comprise means for maintaining in its interior a temperature which is hardly lower, if at all, than the temperature in the hammer mill. In a preferred embodiment in which the dust cyclone is vertically positioned and essentially comprises an upper cylindrical part and a lower conical part, the wall of the conical part makes an angle not exceeding 20° with the vertical, while the height of the conical part is conventional, so that the dust cyclone has a bigger opening at the lower end than is conventional. The advantage of this is that the dust cyclone is substantially prevented from becoming silted up. If provided, the opening at the lower end of the dust cyclone is preferably closed off by a rotary valve. By means of such a rotary dosaging valve, the pressure in the system of hammer mill and dust cyclone can be maintained. The apparatus according to the invention may be part of a system of purifying stations which collectively form a complete treatment system for cuttings. A conventional treatment system comprises a main washing tank in which cuttings are washed using agitating gear and a washing fluid. The mixture of washing fluid and cuttings is pumped from the main washing tank to two centrifuges in parallel. The cuttings leaving the centrifuges after centrifugation have an oil content of about 8% and are pumped to the apparatus according to the invention via a collecting tank. The washing fluid coming from the two centrifuges referred to is, via a service tank, fed to a third centrifuge, where the residual solid particles are removed down to 2%. These residual solid particles are also fed to the collecting tank of the present apparatus. The washing fluid is used again in the main washing tank. In the hammer mill of the apparatus according to the invention the oil content of the cuttings is reduced to far below 5%, and the cuttings themselves are pulverized and dried. The dry material is carried off at one end of the hammer mill at the lower end thereof. In the dust cyclone of the apparatus substantially all dust is removed from the water vapour and oil mist. The steam/oil mist is discharged at the top via an outlet. The outlet connected to the dust cyclone for discharging the mist or vapour purified of dust is preferably arranged in a heat exchange relationship with a supply pipe for feeding the cuttings to be purified to the hammer mill. In- this way the steam/oil mist is condensed to a mixture of water and oil, while the cuttings to be treated are thus pre-heated in an inexpensive manner. This can be done in a screw condenser, in which a screw conveyor provides for the transport of the cuttings to be purified, while in the casing channels are provided for the steam/oil mist to be passed through, the steam/oil mist cooling down in those channels to a mixture of water and oil of about 60° C. Finally, the water and the oil are readily separated by removing the water by suction. In yet another suitable embodiment of the apparatus acording to the invention, the shaft of the hammer mill comprises a channel provided with openings terminating between the respective flanges for optionally introducing water and/or chemicals into the hammer mill. This embodiment allows water to be injected if more steam is to be generated in types of cuttings having a low water content. Chemicals may optionally be fed to the apparatus for various purposes. In certain cases, for instance, it is desirable that a de-emulsifier is introduced. The invention will now be further explained with reference to the accompanying drawings, in which Figure 1 shows the hammer mill in one embodiment of the apparatus according to the invention, partly in side view and partly in cross-section; Figure 2 is a cross-sectional view of the apparatus according to Fig 1 taken on the line II-II; and Figure 3 is a schematical cross-sectional view of the dust cyclone in one embodiment of the apparatus according to the invention. The hammer mill of the apparatus according to the invention shown in Figs 1 and 2 comprises an essentially drum- shaped body 1, which is positioned horizontally. At the top of the drum 1 in the vicinity of one end thereof, a suitable inlet 2 is provided for introducing the cuttings to be purified into the drum. The inlet 2 can be connected to a supply pipe (not shown) . In the vicinity of the opposite end of the drum 1, in the lower part thereof, an outlet 3 is provided for removing purified and for the greater part pulverized cuttings from the drum. In the top part of the drum 1, above the outlet 3, an outlet 4 is provided for discharging the steam/oil mist generated in the drum during operation. The inlet 2 and the outlet 3 are provided with suitable valves, so that during operation the pressure ' in the hammer mill and the dust cyclone connected to it via the outlet 4 can be maintained at a desired value of at least 0.3 bar gauge pressure. A shaft 5 extends axially through the drum 1, the shaft 5 having been passed through the opposite side walls of the drum 1 and being bearing-mounted on opposite sides outside the drum 1 in tubular members 6 and 7 which are fixedly attached to the drum 1. Shaft 5 may, for instance in the part outside the drum 1, optionally comprise a system of channels (not shown) for cooling the shaft 5 in operation by means of a cooling liquid circulated through this system of channels. The shaft 5 further comprises a channel 8, which at one end terminates outside the drum 1 and at the other end terminates at a number of points 9 within the drum 1 at the surface of the shaft 5. During operation water or another fluid, containing chemicals for instance, may optionally be introduced into the interior of the drum 1 via such a channel 8. The shaft 5 is adapted to be connected to a motor, for instance a diesel engine (not shown) . If such is the case, the existing lubricating oil system of the diesel engine may suitably be used for lubricating and cooling the main bearings and the shaft 5 of the hammer mill of the apparatus according to the invention. As indicated in Fig 1 the shaft 5 has its greatest diameter in the middle of the drum 1 and the diameter is step- wise reduced in opposite directions. In the vicinity of each reduction a flange 10 is welded onto shaft 5, in such a way that the welds 11 and 12 are situated at different levels. This is to say that the weld 11 of each flange 10 is situated "before" the reduction and the weld 12 of each flange 10 is situated "after" that reduction. Such a construction prevents the flanges 10 from becoming warped in operation and effects a better distribution of forces during the rotation of the shaft with the flanges, so that the hammer mill will be more balanced. Further it is ensured that the flanges 10 with the hammers attached to them are optimally connected. Each flange 10 is provided with pairs of through bores at a plurality of points, for instance six, which are evenly spaced along the circumference of the flange. At those points hammer blocks 13 are mounted onto the flange 10 and securely attached to it using bolts 14 extending through the bores and nuts 15. At the front and the back the hammer heads are provided with a hard layer, for instance of tungsten carbide. The hammers on consecutive flanges are arranged in a staggered relation relatively to each other, so that the hammers of consecutive flanges are not in one line when viewed in a straight line parallel to the shaft. Such a staggered configuration substantially prevents accumulation of cuttings between the flanges. Along the inner wall of the drum 1 semi-circular profiles 16 extending in a direction parallel to the shaft in evenly spaced relation relatively to each other, are secured to that inner wall, for instance by welding. Such semi-circular profiles protect the inner wall against wear and the like. In operation a protective layer of cuttings and drilling dust forms between the semi-circular profiles 16. On the side of the outlets 3 and 4 a screen plate 17 is positioned in the drum body. The screen plate 17 prevents pulverized cuttings which are carried along in the apparatus from being entrained into the outlet 4 along with the water vapour or steam and the oil mist formed in the drum 1. Any dust that is swept along with the steam and oil mist is removed from the mist in the dust cyclone, which is connected to the drum 1 via the outlet 4 and, along with the hammer mill, is part of the apparatus according to the invention. On the outer wall of the drum 1, all round the drum, a large number of elongate channels or chambers 18 are provided, which chambers 18 are connected in pairs with each other at their ends by means of transverse channels 19, in such a way that the system of chambers 18 and transverse channels 19 forms a zig-zag pattern of channels round the drum 1. As illustrated in Figure 2 in particular, a supply duct 20 and a discharge duct 21 respectively are connected to a pair of adjacent channels 18, which ducts 20 and 21 communicate with an installation 22 for thermal oil, which installation 22 comprises in known manner means for heating a thermal oil contained in the installation 22, maintaining the oil at a desired temperature, and pumping it via the supply duct 20 through the system.of channels 18 and 19 and discharging it via the discharge duct 21. In operation this provision enables the exterior of the casing of the drum 1 to be maintained at a desired high temperature of, for instance, 300° C, so that in the interior a high temperature is permanently maintained of, for instance, about 225°C, just below the cracking temperature of the oil to be removed from the cuttings in the apparatus. Further, at the bottom of the drum 1 a lock 23 is provided which can be opened in order to rapidly empty the drum in case of an emergency or to gain access to the interior if any repairs are to be carried out. Figure 3 schematically shows a cross-section of an embodiment of the dust cyclone of the apparatus according to the invention. This dust cyclone comprises in conventional manner a cylindrical upper part 24 and a conical lower part 25 connected to it (dust cyclones are usually positioned vertically) . In the present dust cyclone the wall of the conical part makes an angle of less than 20° with the vertical, unlike known dust cyclones, in which this angle is larger. The heights of the cylindrical part and the conical part are comparable to those of the corresponding measurements of the known dust cyclones, so that the opening at the bottom of the dust cyclone has a greater diameter than is usual. Thus clogging during operation is substantially prevented. On the side wall of the cylindrical part 24 an inlet 26 is provided. To this inlet a duct is connected (not shown) , which at its other end is connected to the outlet 4 of the hammer mill. At the top the dust cyclone is provided with an outlet 27 for discharging from the apparatus the steam and oil mist purified of dust. Connected to the outlet 27 is a discharge duct is connected (not shown) , which is preferably connected to a heat exchanger, in which the supply of the cuttings to be purified comes into heat exchanging contact with the purified steam and oil mist discharged, for instance by passing the steam and mist through channels in the casing of a screw conveyor for the cuttings. In this way the temperature of the. cuttings is raised even before the cuttings are introduced into the hammer mill. The temperature of the steam and the oil mist is lowered to about 60° C, so that at the end of the heat exchanger a mixture of water and oil comes out that is easy to separate. The dust cyclone is closed off at the bottom by a rotary dosaging valve 28 of known construction. Since in the duct between the hammer mill and the dust cyclone no further valves are disposed, the pressure in the entire system can be controlled using the dosaging valve 28. According to the invention the pressure should be at least 0.3 bar gauge. The dust cyclone further comprises means for keeping the interior of the cyclone at a high temperature. These means comprise for instance a system of channels 29 extending around the wall of the cyclone, through which system thermal oil is pumped. In this way the temperature in the dust cyclone is maintained at a value which is comparable with that of the temperature in the hammer mill, i.e. a temperature just below the cracking temperature of the oil in the steam and oil mist . All this highly promotes an effective separation of dust and solid particles from the steam and oil mist .

Claims: "■AIMS 1. A method of reducing the oil content of cuttings, which have been removed from a drilling mud consisting essentially of oil or containing oil, in which the cuttings are treated for oil to be extracted from them, to effect which the cuttings are-fed_to a drum-shaped space in which an elevated temperature obtains and then subjected to a hammering treatment in that space, the temperature being selected so high that oil and water present in the cuttings are substantially converted to corresponding mist and/or vapour, which mist and/or vapour is removed from the drum-shaped space and passed to another space, where any residual dust is removed from the mist and/or vapour, while the cuttings are removed from the drum-shaped space in more or less dry form, characterized in that the drum-shaped space is permanently heated from without, so that during the performance of the hammering treatment the temperature in the interior is maintained throughout in the vicinity of, but below, the cracking temperature of the oil in the cuttings being treated, and further the pressure in the spaces is maintained at a value of at least 0.3 bar gauge pressure. 2. An apparatus for the application of the method according to claim 1, comprising a hammer mill and a dust cyclone, which hammer mill comprises a drum-shaped body, a rotary shaft passed through a side wall of the drum and extending axially through the drum, which shaft can be connected to suitable driving means outside the drum, hammers being mounted onto the rotary shaft, which hammers extend in a direction substantially transverse to the shaft and reach up to the vicinity of the inner wall of the drum, the drum further comprising an inlet for introducing into the drum cuttings containing oil and water and outlets for the mist containing oil, steam and dust, formed during the operation of the apparatus, and the purified cuttings, respectively, and the outlet for the mist being connected to the dust cyclone and means being provided around the drum for continuously supplying heat to the drum wall and maintaining it at a high temperature. 3. An apparatus according to claim 2, characterized in that the means for supplying heat to the wall of the drum and maintaining it at a high temperature consists of a system of chambers provided on or in the drum wall and connected with each other in such a way that a fluid passed through these chambers from a location of supply to a location of discharge will travel along by far the greater part of the wall, said system of chambers being connected to a system in which heated thermal oil is circulated in order to feed the thermal oil into the system of chambers at the location of supply and to remove it from that system at the location of discharge. 4. An apparatus according to claims 2-3, characterized in that the shaft of the hammer mill, which is bearing-mounted on opposite sides, comprises a plurality of flanges secured to said shaft in spaced interrelationship, said flanges extending in a direction substantially transverse to the shaft, a plurality of hammer heads being arranged on each of the flanges in evenly spaced interrelationship along the circumference of the flange, the hammer heads of successive flanges being arranged in a staggered configuration relatively to each other in a direction parallel to the shaft . 5. An apparatus according to claim 4, characterized in that the hammer heads are provided on two opposite sides with a layer of very hard material. 6. An apparatus according to claims 4 - 5, characterized in that the shaft has its greatest diameter in the middle of the drum and on opposite sides is step-wise reduced towards its ends, each flange being welded to the shaft in the vicinity of such a stepped reduction in such a way that the welds on opposite sides of each flange are differently spaced from the axis of the shaft. 7. An apparatus according to claims 2 - 6, characterized in that the dust cyclone comprises means for causing a temperature to obtain in the interior of the dust cyclone which is hardly lower, if at all, than the temperature in the hammer mill. 8. An apparatus according to claims 2 - 7, characterized in that in the dust cyclone, which is vertically positioned and essentially consists of a cylindrical upper part and a subjacent conical part, the wall of the conical part makes an angle not exceeding 20° with the vertical, while the height of the conical part is conventional, so that the dust cyclone has a bigger opening at the bottom than is conventional. 9. An apparatus according to claim 8, characterized in that the opening of the dust cyclone is closed off at the bottom by means of a rotary valve. 10. An apparatus according to claims 2 - 9, characterized in that an outlet line connected to the dust cyclone for discharging the vapour or mist purified of dust is disposed in a heat exchanging arrangement with a supply pipe for feeding the cuttings to be purified to the hammer mill. 11. An apparatus according to claims 2 - 10, characterized in that the shaft of the hammer mill comprises a channel having openings terminating between the respective flanges, for optionally introducing water and/or chemicals into the hammer mill. 12. An apparatus according to claims 2 - 11, charcaterized in that the drum of the hammer mill is internally provided with semi-circular profiles secured to the inner surface in spaced interrelationship and extending in a direction parallel to the axis of the shaft.

Inventors: VAN DIJK TOM, VAN DIJK, TOM
Applicants: SCS ENVIRONMENTAL BV, SCS ENVIRONMENTAL B.V.
Application year: 1990
Main classification: C10G1
IPC codes: C10G1