Method and apparatus to prepare a suspension for measuring

Abstract: Method and apparatus for preparing a suspension for sample taking in a measurement section formed as a gap. The suspension provided with energy in a gap (10) immediately preceding the measurement section (11), which is enabled by the gap (10) being formed between a part (9) of a rotational body (4) and a part (5) surrounding it. These parts (9,5) are movable in relation to each other.

Description: The present invention relates to a method and apparatus for preparing a suspension for sample taking according to the preamble of claim 1 and 2. In handling suspensions, there is a need of continuously checking the composition of a suspension, e.g. measuring size distribution in it, separating different kinds of particles or measuring the concentration of one kind of particle. Conventionally, in the technique in question here, an optical method ordinarily with the aid of photocells is used to carry out this checking, monitoring or measurement of the suspension. From the laboratory aspect, there are no substantial problems in such measurement, even in the case where the particles flocculate easily, e.g. in suspensions containing artificial or natural fibres. The problems occur in the intermittent or continuous measurement of a suspension directly in the industrial process, e.g. paper manufacturing. In these cases there is a pressing requirement of being able to measure the fibre concentration in such as papermaking stock. For this purpose it is at present necessary to process and measure samples of the suspension taken intermittently from the process. Measurement difficulties increase with dense or concentrated suspensions, and in such cases it is very often necessary to dilute the suspension before measurement. The measurement process is at present distinguished by complicated apparatus, which even so does not permit taking measurements directly in the process. Through DE-A-27 42 229 a method and an apparatus to be used for continous measuring of a suspension during the process by using the viscous resistance between a gap between a rotor and a stator as a test result. It is possible with the aid of the present invention readily to analyse, either intermittently or continuously, the suspension being treated in the process at the place and time required, thus to obtain a picture of the appearance of the suspension at that moment. For this purpose the invention has been given the distinguishing features disclosed in the claims. The invention will now be described in the form of an example, and with reference to the drawing, schematically illustrating in section an embodiment of the apparatus in accordance with the invention. In the Figure, the numeral 1 denotes a casing, carrying via bearings a shaft 2 driven by a motor 3. On the end of the shaft remote from the motor there is disposed an impeller 4 which, when driven by the motor, rotates in a housing formed in two parts 5 and 6. Further to the shaft bearings in the casing 1, the shaft is also sealed by suitably arranged seals, although neither seals or bearings will be dealt with here, since they are included in the known state of the art. The impeller 4 is provided with blades 7 on its side facing towards an inlet 8. The impeller 4 also has a peripheral part 9 formed as the curved surface of a trucated cone. Together with the housing part 5 this peripheral part 9 forms a narrow gap 10. Similarly, when the parts have been assembled with the aid of screws or the like, indicated by the numeral 14, a second gap 11 is formed. This gap 11 is the measurement gap of the apparatus, and can have a width of 1 mm for example. It will be understood that it is in this measurement gap that measurement of the suspension is performed. An optical measurement means is illustrated in the Figure, and includes a light source and photocell, generally denoted by 12. In order to measure suspensions of different kinds, particularly in the case where the suspension particles tend to flocculate, e.g in artificial or natural fibre suspensions, it is necessary to disintegrate the flocculations and distribute the fibres as uniformly as possible in the suspension, if reliable measurement of desired parameters is to be possible. However, it is not sufficient with this disintegration and uniform distribution; measurement must take place before flocculation reoccurs, which can happen very rapidly, particularly with heavy concentrations. The consequence of this has been that it has so far not been possible to measure the suspension directly in a process, e.g. that of producing paper pulp, and samples have had to be taken from the process for preparation, dilution etc. By the present invention it has become possible also to measure concentrated suspensions taken directly from the process, e.g. by the suspension being drawn off via a shunt connection. Connection of the apparatus into the process is not discussed in more detail other than that a fibre suspension flows through the inlet 8 in the direction of the arrows A in the Figure. The impeller 4 with its blades 7 urges the suspension through the gap 10. In this gap the suspension has a relatively high pressure and the fibres are sujected to beating and slushing, which takes places immediately prior to the suspension reaching the measurement gap 11. In the latter there is thus a homogenous suspension in which the fibres are distributed optimally. A very good measurement result is thus obtained. For the apparatus to function well, the gap between the peripheral part of the wheel 4 and the housing part 5 should be narrower than the actual measurement gap 11. The suspension leaves the housing 5,6 via peripherally distributed outlets 13, as indicated by the arrows B. The peripheral part of the impeller 4 can be smooth, or it can be provided with a plurality of fine flutes or ridges, as indicated on one half of the impeller and denoted 15. A further supply of energy to the suspension for disintegrating flocculation is also acheived by the measurement gap 11 forming an angle to the other gap 10 between the housing part 5 and impeller 4. The measuring methods themselves as such do not form any part of this invention, and measurement may concern such as size distribution of particles, separation of different kinds of particles, concentration of one kind of particle, photographing of particles etc. It will also be understood that several measurement means can be distributed round the housing and measurement gap 11, for registering different parameters, if so desired. However, for the sake of simplicity only one measurement means has been depicted on the drawing.

Claims: Method of preparing a suspension for measurement comprising the steps of :- a) Flowing a fibre suspension through an inlet (8) in a first part (5) of a housing formed in two parts (5,6), which houses an impeller (4) b) Urging the suspension through a first gap formed between a peripheral part of the impeller (4) and said first part (5) of the housing (5,6) by rotating the impeller (4) and thus simultaneously disintegrating the flocculations and distributing the fibres as uniformly as possible in the suspension, c) immediately thereafter passing the suspension into a measurement gap (11) which is formed in the housing between the two parts thereof as a part of the outlet from the impeller (4), and downstream and adjacent the first gap (10), the suspension being measured in the measurement gap (11). Apparatus for preparing a suspension for measurement according to claim 1 , comprising :- a housing formed in two parts (5,6), a housing inlet (8) through which fibre suspension flows, an impeller (4) rotatably mounted in the housing (5,6), a first gap (10) formed between a peripheral part of the impeller and a first part (5) of the said housing (5,6), and in connection with said inlet (8), a measurement gap (11) formed in the housing between the two parts thereof, downstream and adjacent the first gap (10), and formed as a part of the outlet from the impeller (4). Apparatus as claimed in claim 2, charaterised in that the first gap (10) has a width less than that of the measurement gap (11). Apparatus as claimed in claim 2 or 3, characterised in that the width of the measurement gap (11) is about 1 mm. Apparatus as claimed in any one of claims 2 - 4, charaterised in that the peripheral part (9) of the impeller (4), forming one side of the first gap (10), is formed with flutes or ridges (15). Apparatus as claimed in any one of claims 2 - 5, characterised in that the measurement gap (11) together with the first gap (10) mutually form an angle. Apparatus as claimed in claim 6, charaterised in that the peripheral part (9) of the impeller (4) constitutes the curved surface of a truncated cone and in that the measurement gap (11) lies in a plane perpendicular to the rotational axis (2) of the impeller (4).

Inventors: SOEDERLING PETER, SOEDERLING, PETER, Söderling, Peter
Applicants: SVENSKA TRAEFORSKNINGSINST, STFI
Application year: 1988
Main classification: G01N1
IPC codes: G01N21, G01N33, G01N15, G01N1