MATRIX TREATMENT PROCESS FOR OIL EXTRACTION APPLICATIONS

Abstract: Using the invented procedure, a curve representing pressure as a function of time is recorded in real time and then compared with the theoretical curve. The difference is attributed to the skin factor and the matrix treatment can thus be adjusted in real time until it reaches the desired skin value. High treatment efficiency and precision.

Description: The sector concerned by this invention is that of oil and oil-related industry, more specifically treatment of matrices or reservoirs (subterranean formations containing various fluids used by the oil industry, whether natural or injected). This sector covers injection, production and geothermal wells, gas and water wells, etc.... One skilled in the art is perfectly aware of the various fluids used for purposes related to the above: acids, concentrated or variously diluted acid mixtures (especially HF, HCl, H₃BO₃, HBF₄, H₃PO₄ and various organic acids or acid precursors such as esters,...) diluted in known proportions, temporary or permanent plugging fluids, gelled polymers, water, diesel oil, gas oil, solvents, etc... It is entirely useless here to repeat their nature and the classical uses to which they are put. It is also known to try and determine the evolution of the skin factor (degree of damage of the formation within a short radius of the well) with time. The interest is, reaching a zero skin factor shows the point in time when the treatment can be stopped. In that matter, one can refer to US-A-4,607,524. However, this patent uses a prior well testing (col. 3), and is also using calculated parameters (therefore not totally accurate) to reach the "skin effect" value (col. 8). In fact, the invention does not involve a new treatment fluid, but a new treatment process using known treatment fluids, the process using known treatment fluids, the process being more efficient and precise, thus minimising damage. The invented process consists of two main stages: A. Definition of the reservoir type and parameters. The reservoir type and parameters may have been defined by preceding classic analyses (highly expensive well testing). If this is the case, the invention uses these data. If such data are not available, one is often content or constrained (for various technical and economical reasons) to use mean values stemming from more or less rough approximations as initial parameters. Such approximations are described for example in US-A-4,558,592. That document teaches the calculation of the variation of the skin factor S with time, using the flowrate, the surface pressure and the bottomhole pressure, as well as the permeability of the reservoir, as parameters for the calculation. One major drawback of that technique lies in the fact that permeability and bottomhole pressure, especially, are estimated through data like geometry of the well which is inaccurately known. This inaccuracy is incorporated in S as a result. Conversely, the invention proposes to determine these parameters through a simple procedure immediately before the treatment itself. This procedure is described below and has the definite advantages of: a) using the equipment already designed for the treatment, b) hardly increasing the treatment cost at all, c) leading directly into the treatment, and d) enabling initial parameters to be obtained which, for the first time, are precisely known. This important improvement in precision has a significant effect on the treatment's precision and quality. The procedure above consists of the injection of an inert preflush fluid, which is non-damaging and non-stimulating to the formation. This fluid can be a gas oil type, methylbenzene, dimethylbenzene or even KCl, NH₄Cl or NaCl brine or filtered sea water with or without mutual solvents and other known additives. Of the brines, NH₄Cl is to be preferred. However, the invention is characterized in that it especially recommends direct use of the oil formation fluid which has pervaded the well or has been produced by the formation and collected and stored at the surface. By reinjecting this oil into the formation as preflush, a remarkably practical and economical test is realised, giving rise to considerably more exact results than those out produces by preceding techniques as they are based on fact. Moreover, these results have the advantage of immediately preceding the treatment and the use of oil (natural formation fluid) has the advantage of not being likely to disturb measurement of the initial state of the reservoir, unlike other exogenous fluids which could disturb measurement. These results give: the reservoir type: homogeneous, fissured, faulted, stratified,... its basic parameters, notably the kh (hydraulic conductivity or premeability x thickness) which indicates the permeability and the initial skin. It should be remembered that the skin factor indicates the degree of damage undergone by the formation in the immediate proximity of the well (most often from 0 to 1 m). To obtain the above results, the preflush fluid (preferably oil, in accordance with the invention) is injected, a shut-in is carried out (pumping stoppage) and the resulting pressure drop is observed as a function of time. In some cases, where reservoir pressure is insufficient to the point of not enabling the pressure drop curve to be registered at the surface (and if there is no pressure gauge below) shut-in is replaced by violent variation in injection flow rate (rise or fall) and the resulting pressure variation is then examined as above. These procedures are known by their general designation of "Injection/Fall-off Test" or injection/shut-in test and a pressure variation curve analysis enables the reservoir data to be obtained. Other known analysis techniques could also be used, such as the Horner and analogous methods. Study of the data obtained above facilitates participation in determining the details of the treatment procedure applied to the reservoir in question (type and sequence of fluids injected, volumes, pressures, possible injection of ball-sealers, use of diverters, etc..), commonly known as treatment "design". B. Treatment: The initial skin (and the other reservoir specificities and parameters) are known from stage A. The invention is characterised in that the "design" is implemented by recording essential phase parameters (output, pumping duration, fluid rheology, pressure, etc.), for each design, phase. The Psim curve is then drawn (this comprises a theoretical curve representing the well-head or bottom pressure variation as a function of time), from actual pumping sequence data. The "theoretical" nature of the curve stems from the fact that it represents the pressure variation that would occur if the physical state of the reservoir remained unchanged in its original state (notably, damage) as determined in stage A, i.e. ignoring injection fluid reactivity and rock reaction. However, treatment causes the reservoir to change. The originality of this invention consists in comparing the Psim curve with the Pmeas curve (actual pressure variation as a function of time, measured in real tim using familiar data acquisition and recording devices, themselves linked to equally familiar surface or bottom sensors and gauges), then drawing the curve of skin factor variation as a function of time. The latter operation is made possible due to the new approach which is the basis of the invention. This approach consists in considering that the difference between the Psim (t) curve and the Pmeas (t) curve is solely due to the skin variation, a conclusion resulting from the precision with which the reservoir parameters and thus the Psim (t) curve are known using the invention. Thia approach is completely original and permits reliable and precise operation for the first time. Using the invented process, it is therefore possible to draw the skin = f (t) curve precisely, which enables: 1) skin evolution (and so reservoir reaction to current treatment) to be monitored in real time, and therefore treatment to be adjusted and optimised, even modified, for exact adherence to the design, and 2) a precise treatment stopping time to be determined: this time is reached when the skin value reaches a certain value, and depends on the reservoir characteristics (in homogeneous reservoirs, it is reached when the skin value reaches zero). In figure 1 annexed, the curves of Psim and Pmeas as a function of time are shown.

Claims: 1. Method for performing a matrix treatment of a formation surrounding an oil well or analogous well, wherein the skin factor is calculated as a function of time, and the treatment is stopped when the skin factor reaches zero or a value close to zero, characterised in that: A. immediately preceding the treatment, an "injection fall-off test" is performed, consisting of injection of an inert, non-damaging and non-stimulating fluid into the formation for purposes of determining the reservoir's initial characteristics, notably the kh (hydraulic conductivity) and skin (skin factor) values; followed by a shut-in of the well and measurement of the pressure drop; B. and in that, during the subsequent treatment: 1) the theoretical pressure as a function of time curve Psim (t) obtained from the actual pumping sequence applied to the reservoir in step A of the method, which is assumed static in its initial state, is compared with the pressure as a function of time curve Pmeas (t), obtained from the same sequence, but measured in real time using surface and/or bottom data acquisition devices, taking account of the reservoir's reaction to the treatment, 2) the real time skin = f (time) curve is drawn by calculating the divergence between the Psim (t) and Pmeas (t) curves and, 3) the treatment is precisely adapted to the result sought through examination of the skin = f (t) curve, and the treatment is terminated when the skin = f (t) curve shows that the desired result has been achieved. 2. Method in accordance with claim 1, characterised in that the inert fluids is a solvent such as gas oil, toluene, xylene, or a KCl, NH₄Cl or NaCl brine, or filtered sea water with or without mutual solvents and other recognised additives. 3. Method in accordance with claim 1, characterised in that the inert fluid consists of the formation oil which has pervaded the well or has been produced by the formation and collected at the surface.

Inventors: ECONOMIDES, MICHAEL, PROUVOST, LAURENT
Applicants: PUMPTECH N.V.
Application year: 1988
Main classification: E21B49
IPC codes: E21B49, E21B43