MEANS AND METHOD FOR DETERMINING THE TENSILE STRENGTH OF CERAMIC MATERIAL

Abstract: Means and method for determining the tensile strength of ceramic material. The means comprises a pressure chamber (1), two cylindrical bodies (13, 14) axially displace­ able therein, and having bore holes (24, 25) for insertion and securing, by means of adhesion, of a test rod (12) having substantially the same diameter along its entire length. Sealing means (6a, 6b) are provided between the pressure chamber wall and said cylindrical bodies (13, 14). A source of pressure medium (20) and a pressure meter (23) com­ municate with a space between the bodies (13, 14) in the pressure chamber (1). The method according to the inven­ tion comprises combining two cylindrical bodies (13, 14) and a test rod (12) to form a unit with the aid of an adhesive, inserting this unit into a pressure chamber (1) and sealing the gap between the bodies (13, 14) and the pressure cham­ ber wall with seals (6a, 6b), pressurizing the space defined between the pressure chamber wall and said bodies (13, 14), measuring the pressure in said space, and recording the pressure at which the test rod (12) fractures.

Description: Apparatus and method for determining the tensile strength of ceramic material The invention relates to an apparatus for determining the tensile strength of ceramic material or material having similar properties according to the precharacterising part of Claim 1. Such an apparatus, which is not specifically designed for determining the strength of ceramic material, is known from the US-A-3 610 031. The invention also relates to a method for determining the tensile strength of a ceramic material with the help of the afore-mentioned means. It is extremely expensive to produce test rods of ceramic material, such as silicon nitride, or material having similar properties in the same form as for testing the tensile strength of metallic material having end portions which are larger in diameter than an intermediate portion. Furthermore, the poor ductility of ceramic material, and its brittleness means that flexural stress in the test rods has a far greater falsifying impact on the test results than when testing material of high elasticity which stretch considerably before breaking, as is the case with most metals. It is thus scarcely possible to use the usual types of machines for determining the tensile strength of ceramic materials. From the US-A-3 610 031 an apparatus for determining the tensile strength of materials is known which exhibits a pressure chamber which is defined by a cylinder and two end portions with cylindrical holes which are provided with threads. The test body consists of a rod that has end portions of an increased diameter, these end portions being provided with threads. The two bodies to which the test rods secured by threading fit closely into the pressure chamber. The measurements are taken by a strain gage that is fitted to the test rod and is connected to measuring wires that are conducted through a bore in one of the two end portions, this end portion being permanently fixed to the pressure chamber. US-PS-3 492 862 discloses a similar test apparatus as the afore-mentioned US-A-3 610 031. In this case, besides connecting the test rod to the end bodies by threads, a test body is suggested consisting of the proper test rod and end portion integral therewith which end portion are formed with several flanges spaced apart by circular slots which accommodating sealing means. In this test device also one of the end portions is secured to the pressure chamber. The invention aims at developing an apparatus and a method for determining the tensile strength of ceramic material which enables testing the tensile strength of ceramic material at lower costs and with more reliable results than this is possible with the conventional means and methods. To achieve this aim the invention suggests an apparatus for determining the tensile strength of ceramic material according to the introductory part of claim 1, which is characterized by the features of the characterizing part of claim 1. A method for determining the tensile strength of a ceramic material is, according to the invention, characterized by the features of Claim 2. Further developments of this method are characterized by the features of the additional claims 3 to 5. The invention thus utilizes a hydraulic testing apparatus and a cylindrical test rod having the same cross section along its entire length. A test rod and two cylindrical bodies with bore holes fitting the test rod are joined together with an adhesive, preferably a cured glue, to form a unit. This unit is inserted into a cylindrical pressure chamber. Between the wall of the pressure chamber and the bodies seals are provided to produce a closed space which is defined by the wall of the pressure chamber and said two cylindrical bodies. This space communicates with a pressure medium source and pressure meter. Tensile strength measuring is performed as follows: A test rod and two cylindrical bodies are joined together with adhesive. A suitable quantity of adhesive, preferably a cured glue such as ARALDIT R , is inserted into the bore holes in the cylindrical bodies. The test rod is then inserted into the bodies and the glue allowed to set. Cured glue is preferably cured at an increased temperature, in the vicinity of 100°C, for instance. The unit thus formed is inserted into the pressure chamber, whereupon the space defined between the cylindrical bodies and the wall of the pressure chamber is filled with pressure medium, at gradually increasing pressure until the test rod fractures. The pressure at rupture is indicated. The invention allows entirely cylindrical test rods to be used. A test rod produced from powder by hot isostatic pressing is suitably used, with the surface as obtained by the pressing. The unfinished surface after pressing has the same structure as the surface of a product. Since the surface structure of the test rod is the same as that of a product, the test result will be more reliable than in the case of using a test rod which has been machined, for instance by grinding. The cost of such test rods and of the testing amounts only to a fraction of the cost entailed when using test rods of conventional design. The results will be substantially more reliable than with the use of rods of conventional design and conventional machines for testing tensile strength. The invention will now be described in greater detail with reference to the accompanying drawings showing ― by way of example ― an embodiment of a means according to the invention. The pressure chamber 1 comprises a cylinder 2 and two end plugs 3 and 4 screwed into the cylinder 2. An adjustment screw 5 is provided in the end plug 4. The cylinder 2 contains sealing rings 6a, 6b, which are supported by support rings 7, 8 with triangular cross-section, and support cylinders 10, 11 for transmitting axial forces exerted on the sealing rings to the end plugs 3, 4. The two sealing rings 6a, 6b seal a space 15 which is defined by the wall 16 of the cylinder 2 and the bodies 13, 14. The space 15 communicates through an opening 17 in the wall of the cylinder 2, and a pipe 18, with a pressure medium source 20 supplying a pressure medium to the space 15. A pressure of 60 MPa (600 bar) is used in the example shown, but equipment for considerably greater pressure is feasible. A pressure meter 23 is connected to the space 15 via an opening 21 and a pipe 22. The bodies 13, 14 are suitably made of steel. When the glue is cured at temperatures above room temperature, a strong grip is obtained on the test rod since steel has a higher coefficient of thermal expansion than ceramic. The adhesive force of the joint is thus increased. The pressure medium acts on the outer surface of the bodies and this, too, improves the grip. The test rod and end bodies are glued in a jig to ensure that they are completely parallel. To ensure high strength in the adhesive joint, the clearance between test rod 12 and the walls of the bore holes 24, 25 in the bodies 13 and 14 should be slight. The unit 9 formed by test rod 12 and bodies 13 and 14 will be self-centering in the pressure chamber, so that no flexural forces arise thanks to the perfect geometrical shape. Deviations from a perfect geometrical shape would inevitably give rise of flexural stresses in the test rod. Any curvature or deviation from the central axis must be measured before testing, with the combined unit of the test rod and end bodies 13, 14 placed on two V-blocks at exactly the same distance from each other as that between the seals 6a, 6b in the pressure chamber 2, and with one resting point the same distance from the end surface of the body 13 as the distance between the sealing ring 6b and the end plug 3 in the cylinder 2. The position of the test rod in relation to the centre line is measured. The unit formed by test rod 12 and end bodies 13, 14, is then inserted into the pressure chamber 1 with the end body 13 in contact with the end plug 3 so that the seals 6a, 6b, abut at the prior resting points in the V-blocks. The screw 5 is used to check the position of the unit 9 in the pressure chamber before the testing begins. The stress is nominally δo = P A₁ - A₂ A₂ where P = the pressure in the space 15, A₁ = the cross-sectional area of the end bodies, A₂ = the cross-sectional area of the test rods. If the point of fracture initiation can be localized, the fracture stress can be compensated Δδ δ o = r · e · 16 d² where r = the distance from the centre line of the test rod to the fracture initiation point with positive sign towards the flexural centre, e = half the centre deviation, d = the diameter of the test rod. The fracture stress is δ t = δ o + Δδ When determining the tensile strength of a cylindrical test rod in the manner proposed according to the invention, the test rod used can have a surface as obtained by producing the test rod by hot isostatic pressing of powder (HIP-compression) and subsequent sand-blasting to remove the casing. The surface has not been affected by grinding and the test rod therefore has a surface corresponding to the surface of an industrial product, thus ensuring reliable and correct test values.

Claims: 1. Apparatus for determining the tensile strength of ceramic material or material having similar properties comprising a pressure chamber (1) having a cylindrical inner wall with two cylindrical bodies (13, 14) fitting therein, one at each end and sealing means between the circumferences of said bodies and said cylindrical inner wall, said bodies being provided with cylindrical bore holes (24, 25) for insertion and securing of respective ends of a test rod, whereby at least one of said bodies is axially displaceable in the pressure chamber (1), a pressure medium source (20) and a pressure meter (23) being connected to the space which is defined by said cylindrical inner wall of the pressure chamber (1), said sealing means, the surface of said test rod and the surface of said two bodies (13, 14), characterized in that the connection between respective ends of the test body and the two bodies (13, 14) is effected by means of adhesion, and in that the test body has the same diameter along its entire length. 2. Method for determining the tensile strength of ceramic material or material having similar properties wherein a test rod, formed of said material is inserted into a pressure chamber with a cylindrical inner wall in which the test rod is held between two cylindrical bodies (13, 14), positioned inside and at opposite ends of said chamber, which seal around their circumferences against the inner cylindrical wall of the pressure chamber, whereby at least one of said bodies is axially displaceable in said pressure chamber and whereafter a pressure medium is supplied to the space (15) formed between the wall of the pressure chamber (1) and said two bodies (13, 14), wherein test rod (12), which has the same diameter along its entire length, is inserted at its respective ends into bore holes (24, 25) in the two cylindrical bodies (13, 14) which bore holes fit the test rod, so that the test rod and the two cylindrical bodies are combined to form a unit with the aid of an adhesive between the test rod (12) and the bore holes (24, 25), and wherein the unit thus formed is placed in said pressure chamber (1), whereafter the pressure medium is admitted to the pressure chamber and the pressure at which the test rod fractures is recorded. 3. Method according to claim 2, characterized in that the test rod (12) and the cylindrical bodies (13, 14) are joined by means of a cured glue. 4. Method according to claim 3, characterized in that the glue is cured at a temperature between 50°C and 120°C. 5. Method according to claim 2 or 3, characterized in that the test rod is produced by hot isostatic pressing of powder, its surface remaining as obtained by the hot isostatic pressing process.

Inventors: MATTSSON, BERTIL, NILSSON, JAN
Applicants: ASEA CERAMA AB
Application year: 1987
Main classification: G01N3
IPC codes: G01N33, G01N3