CYROSTAT ASSEMBLY

Abstract: A cryostat assembly comprises at least one substantially heat insulating wall (3) surrounding a cooled region for restricting heat flow into the cooled region. A refrigeration system (8) is provided having a heat absorbing portion coupled with the wall (3) to enable heat to transfer to the heat absorbing portion, the refrigeration system also having a heat evacuating portion to enable absorbed heat to be evacuated from the cryostat assembly.

Description: The invention relates to cryostat assemblies comprising at least one substantially heat insulating wall surrounding a cooled region for restricting heat flow into the region. Such assemblies are hereinafter referred to as of the kind described. Cryostat assemblies of the kind described are used in a variety of fields one of which is the field of nuclear magnetic resonance (NMR) imaging wherein superconducting coils of an electromagnet are sitatuated within the cryostat. In order that the coils of the magnet take up a superconducting state it is necessary to cool them to very low temperatures in the order of 4K and conventionally this is achieved by making use of a liquid helium vessel within which the coils are mounted, the helium vessel being sandwiched within a radiation shield, the radiation shield being sandwiched within a liquid nitrogen vessel, and the liquid nitrogen vessel being sandwiched within an evacuated vessel. This series of insulating jackets enables the coils to be maintained at the required low temperature. One of the problems with these cryostat assemblies is that there is a continuous vapourising of the liquid helium and liquid nitrogen which is boiled off and fresh helium and nitrogen has to be supplied to the respective vessels. This degree of boil off is expensive and generally undesirable. An attempt to make use of the vapourising liquid coolant is described in FR-A-2568350 disclosing the features of the preamble of claim 1.In that case, one or more slotted plates were positioned in the turret through which liquid helium escaped so as to maximize heat transfer between the various walls of the cryostat and the liquid helium thereby cooling the walls. In a modification of that arrangement, a refrigerator was positioned in the turret coupled with the heat exchange plates. EP-A-116364 also discloses the use of a refrigerator which is sealed to the cryostat and extends through a number of evacuated vessels. A number of difficulties arise with the arrangement shown in the French specification. Firstly, the problem of boil off is not solved and indeed the intention is to promote the use of such boil off. Furthermore, the effectiveness of the refrigerator is significantly reduced by the action of the boiling off coolant. Thus, the boiling off vapour will effectively short circuit the two stage capability of the refrigerator. The main problem with the disclosure in EP-A-ll6364 is that the refrigerator cannot be disassembled from the cryostat without purging the evacuated vessels. This leads to considerable expense if refrigerator removal is required and also a lengthy "down time". In accordance with the present invention, a cryostat assembly comprises at least one substantially heat insulating wall and at least one coolant containing or evacuated vessel surrounding a cooled region for restricting heat flow into the cooled region; a refrigeration system comprising a support housing, and a refrigeration unit having a heat absorbing portion and a heat evacuating portion to enable absorbed heat to be evacuated from the cryostat assembly, the refrigeration unit being removably mounted in the support housing, cooperating heat conducting contacts being provided on the unit and in the support housing whereby when the unit is fully mounted in the support housing the contacts engage one another to provide a path for heat to flow between the support housing and the heat absorbing portion; and coupling means connected between the support housing and the wall to conduct heat from the wall to the support housing, the arrangement being such that the refrigeration unit can be dissassembled from the rest of the cryostat assembly without purging the evacuated vessel, and is characterised in that the interior of the support housing is isolated from the interior of all the coolant containing and evacuated vessels. With this cryostat assembly, the refrigeration system is provided in a support housing which is isolated from the interior of all the coolant containing and evacuated vessels. In contrast to the concept described in FR-A-2568350, the invention seeks instead to minimize boil off by providing the refrigeration system in a separate support housing. Not only does this minimize boil off but also avoids the undesirable affects of boiling off coolant on the efficiency of the refigerator system itself. The invention also enables more freedom of choice to be achieved in the selection and positioning of refrigeration systems which are no longer constrained by the dimensions of the main coolant turret. Furthermore, in contrast to EP-A-0116364, the refrigeration unit can be removed or disassembled from the rest of the cryostat assembly without having to purge the evacuated vessels. This arrangement enables the refrigeration unit to be removed and inserted either for replacement or for repair without having to dissassemble the remainder of the cryostat and in particular without having to empty or purge the coolant or evacuated vessel or vessels. It has been found that the invention considerably reduces the liquid coolant consumption where the system includes a coolant vessel. For example, in one system it has been found that liquid nitrogen consumption has been reduced by about 1 litre per hour while liquid helium consumption is reduced by about 200 cc per hour. In some cases, the refrigeration system can reduce liquid nitrogen consumption to substantially zero. It will be appreciated that the substantially heat insulating wall could comprise part of a wall of a coolant vessel or a heat radiation shield. The refrigeration unit may be of any suitable conventional type such as of the Gifford McMahon type using a closed helium gas cycle. Conveniently, the refrigeration unit is a two-stage system, each stage being connected with a different part of the remainder of the assembly. For example, a first (higher temperature) stage of the system may be coupled for heat transfer with an outer radiation shield or coolant vessel and a second (lower temperature) stage may be coupled for heat transfer with an inner radiation shield. In other examples, a single stage refrigeration unit could be used which would typically be coupled for heat transfer with a wall defined by at least part of a coolant vessel. In many conventional cryostat assemblies, the elements of the assembly are supported by a plurality of support rods. These provide an undesirable source of heat supply to the vessel or shield to which they are connected and are conventionally made of low heat conductivity material. However, some heat conduction does take place and it is particularly convenient if the refrigeration system is coupled for heat transfer with at least one of the support rods. This coupling may be direct in the sense that the coupling means extends between the support and the refrigeration system, but would typically be indirect. Thus, at least one of the support rods is coupled with another wall or vessel which itself is coupled with the refrigeration system whereby a heat flow path exists from the rod via the wall or vessel to the refrigeration system. Preferably, the or each coupling means comprises a flexible, highly heat conductive linkage. Flexibility is desirable to cope with relative movement between the refrigeration system and the element to which it is connected and high heat conductivity is required for rapid dissipation of heat. Conveniently, the coupling means comprises copper braid. The precise dimensions of the braid depends on the powers available at the refrigeration system and on the other properties of the cryostat assembly. It is particularly convenient if the walls of the support housing are insulated against heat flow. An example of a cryostat in accordance with the present invention will now be described with reference to the accompanying drawings, in which:- Figure 1 is a partly cut away side elevation of a cryostat with the refrigeration system omitted; Figure 2 is a partial cross-section through an example of a cryostat assembly for use in nuclear magnetic resonance apparatus to assist an understanding of the invention; Figure 3 is a view similar to Figure 2 but of an example of the invention; Figure 4 is a partial perspective view from one end with some parts removed of a cryostat assembly illustrating support rods; and, Figure 5 illstrates the coupling of a support rod within an inner radiation shield. Figure 1 illustrates the general form of a cryostat assembly which comprises a number of cylindrical, aluminium alloy, or stainless steel walls which are connected to define liquid coolant vessels and radiation shields as will be explained. A central wall 1 defines with another, coaxial wall 1' and end walls 1" a liquid helium vessel 2. The vessel 2 on one side is surrounded by a cylindrical wall 3 defining an inner radiation shield and by another radiation shield 3' on its other side connected with end walls 3". A liquid nitrogen vessel defined by two pairs of cylindrical walls 4,5 and its extension 4' connected to end wall extension 4" sandwiches the radiation shields. An outer vacuum jacket 6 surrounds the liquid nitrogen vessel and extension. A cylindrical bore 60 is defined by the innermost cylindrical wall defining part of the wall of the inner vacuum jacket. In addition, in nuclear magnetic resonance apparatus, coils of a main superconducting magnet 61 are situated within the helium vessel 2 which constitutes a cooled region. A turret 62 is positioned on top of the cryostat assembly through which a helium boil-off port 63 and one or more nitrogen boil-off ports 64 extend. Figure 2 illustrates part of the cryostat assembly shown in Figure 1 and in particular the section indicated at A in Figure 1. In Figure 1 the refrigeration elements shown in Figure 2 have been omitted. A turret 7 having a vacuum jacket is bolted to the wall of the jacket 6. A two stage refrigerator unit 8 of the Gifford McMahon type (such as manufactured by Leybold Heraeus) is bolted to the turret 7 via flanges 9, 10 and a seal 11. The first (higher temperature) stage of the refrigerator 12 is bolted to a high conductivity copper flange 13 which in turn is bolted to an annular, auxiliary flange 14 to which one end of a number of flexible, high conductivity copper braid links 15 are soft soldered. The other end of each link 15 is soft soldered to an annular, high conductivity copper flange 16 bolted to an annular end wall 17 of the liquid nitrogen vessel 18. The second (lower temperature) stage 19 of the refrigerator 8 is bonded to a high conductivity copper flange 20 to which a number of further high conductivity copper braid links 21 are soft soldered. The other end of the links 21 are soft soldered to a copper flange 22 bolted via an intermediate copper flange 23 to the inner shield 3. The arrangement shown in Figure 2 enables the refrigeration power to be transferred from the first stage 12 to the liquid nitrogen vessel 18 via the flanges 13, 14 (which may be segmented) and the links 15 and to the inner shield 3 via the flanges 20, 22, 23 and the links 21. The links 15, 21 are of sufficient length, cross-sectional area, and number to provide for movement between the refrigerator and the parts to which it is connected and to adequately transfer the refrigerator power to the nitrogen vessel and shield. The precise dimensions of the braids depends on the powers available at each stage of the refrigerator used and on the cryostat system. It has been found that the system shown in Figure 2, when used in NMR apparatus, enables a reduction in liquid nitrogen consumption of about 1 litre per hour, compared with the unrefrigerated system, and a reduction in liqiud helium consumption of about 200 cc per hour. It will be seen from Figure 2 that if it is desired to remove the refrigeration unit 8 for the purposes of repair or replacement, it is necessary to destroy the vacuum within the vacuum jacket and this requires the preliminary removal of all liquid helium and liquid nitrogen coolant. Figure 3 shows an arrangement in accordance with the invention in which removal and replacement of the refrigeration unit 8 can be achieved very simply without coolant removal. Figure 3 illustrates only a part of the cryostat assembly including three concentric walls 24, 25, 26. The wall 24 defines the outer cylinder of the inner radiation shield and is surrounded by the wall 25 which constitutes the outer cylinder of the outer radiation shield. In this case there is no nitrogen vessel. The shield 25 is surrounded by an outer vacuum jacket 26. An anti-vibration mounting is provided part of which is shown at 27. In this example, the refrigeration unit 8 is mounted to the remainder of the cryostat assembly by insertion into a support housing 28. The support housing 28 has an outer flange 29 bolted to a turret flange 30. Flange 30 is supported from the lower bolted flange by a set of springs which are adjusted by means of screws and the intermediate flange so that the flange 30 is resiliently supported against the force of air pressure. The resiliency of this support considerably reduces the vibration from the refrigerator being transmitted to the outer vacuum wall 26, whence it would be re-radiated into the environment. A radially inner portion of the housing 28 is defined by a triple wall 31 comprising three concentric cylinders terminating in an inner flange 32 of highly conductive copper. The triple wall 31 is to increase the heat path length between room temperature and the outer shield 26. The flange 32 may be equated with the flange 13 in Figure 2 and links 33 of highly conductive copper braid are soft soldered between the flange 32 and another copper flange 34 coupled with the radiation shield 25. The housing 28 has a further inner, cylindrical wall part 35 sealed to a radially inner surface of the flange 32 and supporting at its lower end a copper nose 36 sealed to its outer surface. Copper braid links 37 are soft soldered between the nose 36 and a copper plate 38 coupled with the wall 24. The refrigeration unit 8 is mounted within the support housing 28 so that a copper flange 39 connected to the first stage 40 of the unit 8 is pressed against an indium metal pressure contact 42 to enable the first stage 40 to be coupled for heat transfer with the links 33. The second stage 43 of the refrigerator unit includes a copper cylinder 44 which forms a close fit within the nose 36. Contact between the cylinder 44 and the nose 36 is achieved by filling a cavity 45 within the housing 28 with helium gas at about 1 atmosphere (although much lower pressures are feasible). If it is desired to remove or replace the refrigeration unit 8, this is simply unbolted at its outer end and slid out of the support housing 28. This removal does not open any access to the jackets of the cryostat and so any vacuum within those jackets is not destroyed. In a typical cryostat assembly, the various vessels and shields are supported by means of elongate tension rods as partly shown in Figure 4. Figure 4 illustrates a coolant vessel 46 (such as a helium vessel) supported by a rod 47 extending between the vessel 46 and an outer vessel 48 (such as a nitrogen vessel) through an aperture 49 in an inner radiation shield 50. In a similar way the vessel 48 is supported by a tension rod 51 to an outer vacuum jacket 52. Since there may be some heat conduction along the rod 47 or 51, it is advantagous to couple the support rods with one of the walls of the cryostat to which the refrigeration unit 8 is coupled. As shown in Figure 5, a suitable connection may be achieved between the support rod 47 and the inner shield 3 which, as seen in Figure 2, is coupled to the second stage of the refrigerator unit 8. Coupling between the rod 47 and the shield 3 is achieved by connecting a flexible copper braid link 53 bolted to the inner shield 3 and whipped to the support rod by a brass wire. Other coupling methods are also possible.

Claims: A cryostat assembly comprising at least one substantially heat insulating wall (25) and at least one coolant containing or evacuated vessel surrounding a cooled region for restricting heat flow into the cooled region; a refrigeration system comprising a support housing (28), and a refrigeration unit (8) having a heat absorbing portion and a heat evacuating portion to enable absorbed heat to be evacuated from the cryostat assembly, the refrigeration unit being removably mounted in the support housing, cooperating heat conducting contacts (42) being provided on the unit and in the support housing whereby when the unit is fully mounted in the support housing the contacts engage one another to provide a path for heat to flow between the support housing and the heat absorbing portion; and coupling means (33,37) connected between the support housing and the wall (25) to conduct heat from the wall to the support housing, the arrangement being such that the refrigeration unit (8) can be dissassembled from the rest of the cryostat assembly without purging the evacuated vessel, characterised in that the interior of the support housing (28) is isolated from the interior of all the coolant containing and evacuated vessels. An assembly according to claim 1, wherein the vessel contains liquid nitrogen or liquid helium. An assembly according to claim 1 or claim 2, wherein the wall coupled to the refrigeration unit is defined by at least part of the coolant containing or evacuated vessel. An assembly according to any of claims 1 to 3, further comprising an inner heat radiation shield (24) surrounding the region, the refrigeration system comprising a two stage refigeration system, a first stage (40) of the system being coupled for heat transfer with the vessel and a second stage (43) being coupled for heat transfer with the inner radiation shield. An assembly according to claim 4, further comprising another evacuated or coolant containing vessel positioned within a volume defined by the inner radiation shield. An assembly according to any of the preceding claims, wherein the wall is supported by a plurality of support rods (47), the refrigeration system being coupled for heat transfer with at least one of the support rods. An assembly according to claim 6, wherein at least one of the support rods (47) is coupled with another wall or vessel which itself is coupled with the refrigeration system (8) whereby a heat flow path exists from the rod via the wall or vessel to the refrigeration system. An assembly according to any of the preceding claims, wherein the or each coupling means (21) comprises a flexible, highly heat conductive linkage. An assembly according to claim 8, wherein the coupling means (21) comprises copper braid. An assembly according to any of the preceding claims, wherein the support housing wall includes a section defined by three nested, spaced tubes (31).

Inventors: WHITE, KEITH
Applicants: OXFORD ADVANCED TECHNOLOGY LIMITED
Application year: 1987
Main classification: F17C3
IPC codes: F17C3, F25B9, H01L39, G01R33, F25D3, F25D19