DYNAMICALLY LOADING SOLID MATERIALS OR POWDERS OF SOLID MATERIALS

Abstract: Solid materials are dynamically loaded by impact with a piston (10) fired at the material (11) in a suitable support (12) wherein a ''punch'', which is a body (22) of material introducing a shock wave impedance mismatch, is inserted between the piston (10) and the material (11). The preferred embodiment relates to a gas fired piston which is propelled onto a powder constrained in a die and uses a steel punch. The punch provides a highly reflective surface for stress waves in the powder and modifies the pressure-time history of the initial shock wave propagating in the powder.

Description: Title; "DYNAMICALLY LOADING SOLID MATERIALS OR POWDERS OF SOLID MATERIALS" * FIELD OF THE INVENTION This invention relates to the addition of an extra element into the path of stress waves present during the working or compaction of solid phase materials. BACKGROUND ART It is well established that materials can be shaped or compacted by impacting them with either a hammer or piston or punch or similar, e.g. see U.S. Patent No. 4255374 issued 10 March, 1981, to Bo Lemcke et al and assigned to Institut Cerac S.A. The operation of this type of equipment is described in greater detail below. OBJECT OF THE INVENTION It is an object of. the present invention to mo.dify the propagation of stress waves in a material which is being dynamically loaded so as to gain greater control over the way in which the material is loaded compared to prior techniques. Other objects and advant¬ ages of the invention will hereinafter become apparent. NATURE OF THE INVENTION The invention provides a method of dynamically loading materials such as solid materials, or powders of solid materials, wherein the material is loaded in a support means and is impacted by a means generating a stress wave therein, characterised by the provision of an impedance means between the material and the means generating a stress wave, the impedance means being effective to cause reflection of stress waves within the material being dynamically loaded. The invention also provides an apparatus for dynamically loading materials such as solid materials, or powders of solid materials, comprising a support means wherein the material is loaded, and a means generating stress waves therein characterised in that an impedance means is provided between the material and the means generating stress waves. The impedance means may be applied directly to the means which generates stress waves or it may be located adjacent the material being stressed. The purpose of the impedance means is to modify the propagation of stress waves by either (a) changing the way in which the stress (pressure) varies with time, or (b) producing higher compressive stresses (pressures) by changing the nature of stress wave reflections in the materials being worked, or both. In the present specification the term 'solid phase' merely denotes a solid phase as distinct from a liquid or gas phase. Typical materials include metals, plastics, and ceramics. The ' term'high shock impedance' merely implies that an impedance mismatch exists. * BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a schematic of an apparatus of a type to which the invention may be applied. FIG.2a is a wave diagram setting out the characteristic stresses to be encountered in a material being worked in the apparatus of FIG. 1. FIG.2b graphically shows the pressure exper¬ ienced by a powder under impact. FIGS. 3 and 4 show two ways in which the invention may be applied in the working of powders. FIGS. 5a and 5b show wave diagrams correspond¬ ing to the situation arising in operation of the apparatus of FIGS. 3 and 4 respectively. FIGS. 6a and 6b show the pressure variations arising in the material being worked in the apparatus of FIGS. 3 and 4 respectively. DESCRIPTION OF PREFERRED EMBODIMENTS For simplicity in the subsequent description, the invention will be described in terms of its applic¬ ation to the dynamic compaction (consolidation) of powdered materials but in principal it could also be applied to other processes utilizing stress waves caused by the impact of one body on another. One method of dynamic powder compaction that lends itself to simple description of the invention utilizes a gas driven piston which is fired into powder constrained in a die (FIG. 1). On impact, an initial shock wave is formed in the powder. This is a compressive stress wave across which there is an abrupt increase in pressure. This propagates through the powder compressing it. Simultaneously there is a com¬ pressive stress wave formed in the piston which propa¬ gates back into the piston away from the piston/powder interface. This and subsequent wave behaviour is illustrated in FIG. 2. ' In the apparatus of FIG. 1, a piston 10 is fired down a launch tube 14 at a powder 11 contained in a die insert 12 in a die block 13. The piston 10 is propelled by a high pressure gas in a reservoir 16 supplied from a valved supply 17. The piston is sel- ectively operated by a fast acting valve 15 controlling an orifice 21 communicating the reservoir 16 with the launch tube 14. The fast acting valve is switched by pressurised gas in valved lines 18 and 19. Operation of valve 18 closes the fast acting valve and operation of valve 19 opens it. The strength of the initial shock wave depends on the shock impedance of the piston material, the piston speed on impact and the pressure-density relation for the powder. To maximise the strength of the initial shock it is usually found that the best strategy is to maximise the piston speed on impact. However, given a fixed energy in the driver gas behind the piston, this means that, for a given kinetic energy in the piston, the lower the mass the higher is the speed. Thus, it is usual for the piston to be made of low density material. The passage of the initial shock wave raises the powder from state 1 to state 2 with state 2 being characterised by high pressure ( as seen in FIG. 2). When the initial shock wave reaches the base of the die there is a reflected wave and a transmitted wave. Depending on the relative shock impedances of the powder and die materials, both the reflected and transmitted waves are usually compressive and there is a further com- pression of the powder to state 3 as the reflected wave propagates back towards the piston face. When the reflected wave arrives back at the -piston face, there is a further reflection. In some situations it would be desirable for this reflected wave to also be compress- ive in nature leading to a further increase in pressure in the powder. However, with the light piston materials chosen to maximise the strength of the initial shock, the shock impedance of the piston is usually lower than that in the powder at state 2 and thus a tensile wave is reflected. One consequence of this is that the top layers of the resulting compact (i.e. those adjacent to the piston) do not weld adequately and have a loose flakey appearance. This occurs regularly when metal powders are being consolidated. For a compressive wave to be reflected at this stage, the shock impedance of the piston face materials must be higher than that in the powder. The invention described herein resides in the insertion of a relatively thin layer of high shock impedance material (which will be referred to as a "punch") between the piston and the powder so that the advantage of low piston mass is retained while the apparent shock impedance is raised. As will become more clear below, the thick¬ ness of the "'punch ■, affects the time scale of events with thicker punches lengthening the time scale. The "punch" 22 could initially be fixed to the piston 10, as shown in FIG. 3 or adjacent to the powder 11 as shown in FIG. 4. The resulting stress wave diagrams for both these cases are qualitatively similar but with the stress/shock waves starting at the punch/powder interface in case of the punch fixed to the front of the piston, and at the piston/punch interface for the case when the punch was initially adjacent to the powder. These two cases are shown in FIGS. 5a and 5b respectively. The main differences between the two cases lies in the different strength of the waves. Because of the addition of a layer of much higher shock impedance material to the front of the piston, the impact of the punch faced piston onto the powder causes the generation of a much higher strength shock wav ' e in the -powder. However, the multiple reflections that sub¬ sequently take place in the punch sends a series of tensile waves into the powder unloading it down to a pressure below that which would have been attained had no punch been present (i.e. as in FIG. 2b). The result- ing pressure time history in the powder adjacent to the punch is shown in FIG. 6a in the absence of any reflected waves from the back of the die. Each step in pressure is separated by a time increment corresponding to the time taken for two traverses of the punch length by the stress wave (one in each direction). The corresponding pressure history for the second case with the punch initially adjacent to the powder is shown in FIG. 6b. In this case the pressure in the powder is initially low and, through the series of wave reflections in the punch, builds up to a value higher than that which would have been achieved had there been no punch present (i.e. as in FIG. 2b). The dotted line indicated at 23 indicates the result where no punch is present. So, in addition to providing a highly reflect¬ ive surface for stress waves in the powder, the punch also modifies the pressure-time history of the initial shock wave propagating into the powder. If the punch is attached to the piston, a much higher peak pressure is achieved in the powder but the pressure drops at a rate dependent on the thickness of the punch. If the highest possible pressures are desired in the powder, the punch should be attached to the piston. However, the high pressures correspond to high particle velocities which may be undesirable in applications such as those involving powder flow into dies of complex shape. In such applications low powder velocities are desirable, and these can be achieved, also with high peak pressures, this time build up over a period of time by means 'of multiple stress wave reflections within the powder arid punch, by placing the punch initially adjacent to the powder. The range of shapes which is possible is limited only by the need for a surface which is impacted so that die shapes with an opening of suitable dimension can be employed. EXAMPLE ' Two compacts were made from iron powder using a gas driven piston apparatus of the kind shown in FIG. 1. The compacts were simple cylindrical shapes about 25 mm. in diameter and 10 mm. deep. A piston made from PVC was employed and impacted at about 280 m/s in both cases. Compact (a) was directly impacted by the piston. It had a flakey top surface characteristic of all compacts made in this way. Its density was about 83% of the theoretical density for iron. Compact (b) had a steel punch of about 6 mm. length initially adjacent to the powder, as in FIG. 4. Otherwise it was an identical experiment to that producing compact (a). Compact (b) had an excellent top surface, indis¬ tinguishable from that on the bottom where the powder had been in contact with a fixed steel die. Compact (b) also had a density of about 88% of the theoretical density of iron. The conclusion to be reached is that the extra compressive wave reflection, to state 4 in FIG. 2a, lead to the superior compact in case (b). It will be readily apparent to the skilled addressee that the relative densities, masses and materials of the piston and punch, the impact velocity of the piston and the other design parameters of the apparatus will be determined to provide the most approp- riate operating conditions for the particular application, However, the .inclusion of the "punch" of the present invention produces marked improvement over the known apparatus referred to e.g. in the cited U.S. Patent. Under certain conditions materials will flow and it is possible to cause solid blocks of material to flow under impact to fill out a die cavity. For example, where conditions are appropriate, some plastics can be moulded under impaction in a suitable die. Various changes and modifications may be made to the embodiments described without departing from the present invention.

Claims: CLAIMS 1. A method of dynamically loading material such as solid materials, or powders of solid materials, wherein the material is loaded in a support means and is impacted by a means generating a stress wave therein characterised by the provision of an impedance means between the material and the means generating a stress wave, the impedance means being effective to cause reflection of stress waves within the material being dynamically loaded. 2. The method of claim 1 wherein the means gener¬ ating a stress wave is a selectively driven impact means and the impedance means is interposed between the impact means and the material. 3. The method of claim 2 wherein the impedance means is attached to the impact means to be carried thereby into contact with the material, thereby generat¬ ing an initial shock wave and subsequent reflections thereof which unload the material down to a pressure below that which would exist without the impedance means. 4. The method of claim 3 wherein the material being dynamically loaded is a powder, the support means is a die, the impact means is a piston and the impedance means is a plate-like body fixed to the forward face of the piston. 5. The method of claim 2 wherein the impedance means abuts the material, between it and the impact means, to generate, when struck by the impact means, an initial shock wave in the material at a pressure lower than that which would exist without the impedance means, which pressure is stepped upwardly by subsequent reflect¬ ions in the material. 6. The method of claim 5 wherein the material being dyanmically loaded is a powder, the support means is a die, the impact means is a piston, and the impedance means is a plate-like body. 7. The method of claim 1 wherein the material being dynamically loaded comprises powders of at' least two solid materials. 8. The method of claim 7 wherein the support means is a die, the means generating a stress wave is a piston projected along a launch tube, and the impedance means is a plate-like body between the powder and the piston, the piston being driven into contact with the powder thereby generating a shock wave therein which is reflected internally of the powder off the powder/die and powder/plate-like body interfaces. 9. The method of claim 8 wherein the plate-like body is attached to, and carried by, the piston. 10. The method of claim 8 wherein the plate-like body abuts the powder and is struck by the piston. 11. An apparatus for dynamically loading materials such as solid materials, or powders of solid materials, comprising a support means wherein the material is loaded, and a means generating stress waves therein characterised in that an impedance means is provided between the material and the means generating stress waves. 12. The apparatus of claim 11 wherein the support means is a die which is open into a launch tube and the means generating stress waves is a piston contained in said launch tube and operative to be selectively projected towards said die. 13- The apparatus of claim 12 wherein the impedance means is a plate-like body attached to the face of the piston directed towards the die. 14. The apparatus of claim 12 wherein the impedance means is a platelike body inserted into the opening of the die between the material therein and the piston. 15. The apparatus of claim 14 wherein the piston is projected towards said die by a high pressure gas from a supply thereof, the high pressure gas being selectively switched into said launch tube, behind said piston by a valve means. 16. The apparatus of claim 14 wherein the piston is projected towards said die by a high pressure gas from a supply thereof, the high pressure gas being selectively switched into said launch tube, behind said piston by a valve means. 17. The apparatus of claim 11 wherein the means generating a stress wave is a PVC piston projected down a launch tube by a pressurized gas which is selectively switched by a valve therefor and the impedance means is a steel plate. 18. The apparatus of claim 17 wherein the steel plate is bonded to the PVC piston. 19. The apparatus of claim 17 wherein the steel plate is located adjacent the material to be struck by the PVC piston.

Inventors: PAGE NEIL W, PAGE, NEIL, W.
Applicants: UNIV QUEENSLAND, UNIVERSITY OF QUEENSLAND
Application year: 1986
Main classification: B22F3
IPC codes: B01J3, B22F3, B29C43, B30B11