APPARATUS AND METHOD FOR PERMEABILITY MEASUREMENT

Abstract: An apparatus and a method for determining the drainability by permeability measurements. The apparatus is provided for taking a sample of a suspension, particularly a fibre suspension, e.g. such as flows in a pipe (2), said apparatus including a sampling piston housing (4) connected to the pipe (2) and accomodating a sampling piston (5) which can be displaced into the pipe (2) and has a through hole for forming a sample chamber (9) for taking out a pulp sample. The housing (4) is in communication with a dilution and mixing chamber (35) including an agitation or mixing device (36), the lower portion of the chamber (35) being closed off by an end member (23) with a screening plate (22). In the method in accordance with the invention there first takes place measurement on the entire pulp sample, subsequent to which the sample is liberated from its fine fraction by a washing process in a mixing chamber (35), measurement on the proportion of fibre in the pulp sample then taking place, for which purpose the permeability of the pulp bed formed against the screening plate (22) is measured during one or more pressure drops, possibly with intermediate slushing with the aid of the mixing device (36) and reformation of the pulp bed.

Description: Apparatus and method for permeability measurement The present invention relates to an apparatus and a method for permeability measurement, said apparatus is provided f .sampling a suspension passing through a pipe, particularly a fibrous suspension, and comprises a sampling cylinder housing attachable round an opening made in the wall of th pipe, the housing being open towards the interior of the pipe and accommodating concentrically an axially displace- able sampling cylinder, adapted for taking a suspension sample from the pipe for the purpose of determining its permeability or freeness level and also the permeability of a sample impoverished of fines or smaller fibre fragmen Drainage transmitters or meters provided so far usually ha a very complicated structure, which results in expensive service, as well as the installation of these meters in a pulp line requiring special arrangements. Due to this the weight of this type of meter rarely falls below 50 kg, whi makes dismantling the meter more difficult when it is to b cleaned, for example. Other problems with this kind of met is that they are easily blocked up by fibers remaining fro the fiber suspension after sampling. These meters moreover lack the possibility of determining the permeability of the long fiber portion of the pulp sample. The present invention has the object of providing a draina rate transmitter of the kind mentioned in the introduction, which is substantially distinguished in that the sampling piston has a cylindrically formed through-hole at right angles to its longitudinal direction, the hole forming a sample chamber, such that when the sampling piston is in i retracted position inside the housing the chamber is in register with at least one hole of substantially the same diameter in the cylindrical surface of the housing, for connecting to it a preferably cylindrical casing defining a mixing and dilution chamber r in which there is an agitat ing or mixing device, the casing being provided with two opposing openings, of which one has the same diameter as the hole in the cylindrical surface of the housing and the ' other has a shape affording sealing connection to an end wall member carrying a screening plate, said member being provided with a drainage collection duct under the screeni plate for conveying measuring water passing through a fibr bed formed on the screening plate to measuring means for determining the drainage properties of the sample taken, a also of a sample which has been completely or partially liberated from smaller fibre fragments by a special separ tion method. By the sample-taking chamber being arranged i line with the spaces required for achieving a homogenous pulp bed from a suspension sample there is obtained accordi to the invention better formation or growth of the pulp on the screening plate, as well as complete flushing after ea sampling procedure, since there are no dead spaces where t remains of previous samples can catch and negatively affec the measuring result. The simple construction means that n heavy details need to be removed for inspecting the screen and neither are any tools required, since the cylindrical wall and the end wall member carrying the screening plate with the intermediate mixing chamber may be fastened to th housing with the aid of toggle catches. The present invention also relates to a method of determin ing the permeability,. particularly in a fibre suspension the method being substantially distinguished in that smalle fibre fragments in a pulp sample introduced into the measuring or mixing chamber, after filtering against the screening plate and subsequent permeation of water during one or more pressure drops, possibly after slushing by agitation of the pulp bed built up aginst the screening plate between the different measurements, are removed by once again bringing the pulp bed into suspension by slushi with the aid of the mixing or agitating means and a simultaneously applied flow of water, after which the fib suspension, substantially impoverished of fine material, once again filtered against the screening plate after .terminated agitation, the permeability of the pulp bed formed once again being measured during one or more press drops, possibly with intermediate slushing and reformatio of the bed. The invention is described in detail below with reference to the appended drawing, which illustrates an axial secti through a preferred embodiment of a drainage rate trans¬ mitter in accordance with the present invention. The drainage rate transmitter 1 illustrated on the drawin includes a cylindrical sampling piston housing 4, fixable an opening 3 made in a pipe 2 or a vessel with agitated contents. The housing 4 concentrically accommodates a sampling position and a retracted position with the aid o a piston rod means 7 attached to its outer end portion 6, the piston rod being associated with a pneumatic cylinder There is a sample chamber 9 in the piston 5 in the form of through-hole transverse the longitudinal direction of the piston 5, and when the piston is in its retracted position inside the housing 4 the chamber 9 forms part of a measuri space and has its axis coinciding with those of two holes and 11 in the cylindrical surface of the housing 4. As wit the sample chamber 9 these holes are also preferably cylindrically formed and of the same diameter as the chamb 9. The upper hole 10 continues into a space 13 defined by a cylindrical wall 14 of the same diameter as the hole 10 and by an end wall 12. The space 13, hole 10, sample chamb 9 and hole 11 thus form a continuous chamber, such as to avoid dead spaces which can give rise to collections of fibres from different samplings. A measuring water nozzle 15 opens out into the space 13, and the nozzle is in OΛIPI communication with a water supply via a valve 16. The space 13 is in communication with an outlet 17 via a hole in the end wall 12, this communication being regulated by an outle valve 18. For eliminating rotation of the sampling piston 5 in relat¬ ion to the housing 4, the piston rod 7 may be exchanged for two mutually parallel partial piston rods, or attached, as illustrated on the drawing, to the outward end portion 6 of the piston 5 at a point situated at a distance from the axi of the piston 5. The drainage rate transmitter in accordance with the presen invention is suitably used for sampling suspensions which have a concentration of about 1-10%, and for the cases wher the permeability of a sample, liberated from smaller fib fragments is to be determined. The lower hole 11 of the housing 4 opens out into a mixing and dilution chamber 35 formed by a casing 32 which has two opposing openings 33, 34, of which the upper 33 fits sealingly into the hole 11 and the lower 34 is adapted to seal against an end member 2 carrying a screening plate 22. The end member 23 includes a drainage collecting duct 24 arranged under the screening plate 22, the duct opening out conically in the area under the screening plate. Via a dewatering valve 25 the duct 24 is in communication with a measuring glass 26 containing tw electrodes 27, 28, and in an area directly under its conica portion is connected to a flushing water supply via a valve 29. The measuring glass 26 may be emptied via an outlet 31 and an outflow control valve 30. Depending on the pulp concentration, the length of the casing 32 may be varied with a variation in the volume of the mixing chamber as a result. Dilution of the suspension sample may be carried out to give it a suitable concentration level with the aid of the variation in volume of the mixing chamber 35 between the housing 4 and end member 23. The intention with the dilution is to arrive at a concentration level in the sample where the pulp flocking properties, are reduced, and also to facilitate separation of smaller fibre fragments. With higher concentrations the pulp sample is usually -heavily flocked, which affects the measurement procedure, since waterways are formed between the flocks, causing th measuring water to flow in the waterways between the flock and in turn cause an unsteady output signal, which may giv a faulty measuring result. The measuring result is considerably improved when the pulp is diluted down to abo 0,8% or lower, with the aid of a mixing and dilution chamb of appropriate volume. For mixing during the dilution of t sample to the desired concentration and also for achieving sufficient turbulence for taking away the fine fraction there is a mixing or agitating propeller 36 in the mixing chamber 35, the propeller being driven by a motor 37. The revolutionary speed of the motor and the implementation of the propeller 36 are such that during the simultaneous introduction of measuring water at a suitable pressure such large shearing forces may be achieved at the screening plat 22 that a pulp plug is not formed. Short fibre fragments ca thus be separated by passing through the perforations in th screening plate 22. It is desirable, inter alia for cleaning purposes, quickly and easily to remove the upper end wall 12, casing 32 and end member 23 with the screening plate 22. This is enabled with the end of suitably placed, unillustrated toggle catch The measuring prodedure in accordance with the present invention and using the equipment described hereinbefore, when the suspension sample has a pulp concentration of abou 1-10%, or when measurement of the drainability properties o the entire pulp as well as those of the long fibre content takes place, is performed in the following manner: A. Sampling The pneumatic cylinder 8 is activated so that the sampling piston 5 is thrust into the pipe 2 simultaneously as the outflow control valve 30 under the measuring glass 26 and outlet valve 18 are open and the flushing water valve 29, measuring water valve 16 and dewatering valve 25 under the screening plate 22 are closed. This means that the mixing chamber 35, which also serves as a measure chamber, is filled with water to the bottom edge of the piston 5. Supe fluous water runs out through a vent 38 in the outer end portion of the housing 4. When sampling is finished, the piston 5 has been completely retracted into its retracted position and mixing begins. B. Mixing All the valves have the same operational status as under A The sample taken out of the pipe 2 with the aid of the piston 5 is mixed with the water in the mixing chamber 35 with the aid of the propeller 36. Mixing conditions may ' vary depending on the pulp concentration, as mentioned previously. The intention with dilution is to obtain a concentration level in which the flocking properties of th pulp are heavily reduced, which is the case when the con¬ centration is at about 0,8% or less. C. Predrainage The outlet valve 18 is closed and the measuring water valv 16 and the dewatering valve 25 under the screening plate 2 are opened. The outflow control valve 30 under the measuri glass 26 is still open and the flushing water valve 29 st closed. This means that during draining, which takes place in the mixing chamber 35, the fibres in the suspension are deposited on the screening plate 22 to form a pulp bed, with the aid of the measuring water. The drained water goe through the pulp on the screening plate 22 via the outflow control valve 30 under the measuring glass and out through the outlet 31. D. Measuring Excepting the outflow control valve 30 under the measurin glass 26, all the valves have the same operational status as under C. The outflow control valve 30 is now closed. This means that the drainage which passes through the pul on the screening plate 22 is collected in the measuring glass 26, where the rising time between the electrodes 27 28 is measured for determining the permeability and/or th freeness level in the sample. This measurement can be re¬ peated at one or more different pressures, with possible intermediate slushing. E. Slushing All valves are closed. The propeller 36 is activated and fibre bed formed is slushed up again. F. Washing The smaller fibre fragments and fine material are separate by the valves being put into the operational state as in item C while the propeller 36 is still activated. There ar thus obtained sufficiently large shearing forces to preven the formation of a fibre bed. The perforations in the screening plate 22 therefore allow passage of fine materia which is thus removed from the sample. G. Measurement Measurement according to item D is carried out on the samp impoverished of fine material. When the measuring result h been registered the pressure can be varied, if so required and a new measurement carried out at a different pressure. This measurement can be carried out with or without an intermediate slushing according to item E. The measuring values now obtained are subsequently compared with the measuring value or values obtained according to item D to determine the content of fine fraction in the pulp suspension. H. Flushing ,The flushing water valve 29 and the outlet valve 18 are opened. Simultaneous with closing the measuring water valve 16 and the dewatering valve 25 under the screening plate 22, while the outflow control valve 30 under the measuring glas 26 is open so that the measuring water in the measuring glass 26 can be tapped off. When flushing is terminated, th flushing water valve 29 is closed and the water remaining i the chamber 35 is used to dilute the next sample. A new sample can now be taken.

Claims: CLAIMS 1. Apparatus, preferably a drainage rate meter (1) for sampling a suspension, particularly a fibre suspension flowing through such as a pipe (2) , comprising a cylindrical sampling piston housing (4) attachable round an opening (3) made in the wall of the pipe, the housing being open towards the interior of the pipe and accommodat ing concentrically an axially displaceable sampling piston (5) , adapted for taking out a suspension sample, c h a r- a c t e r i z e d i n that the sampling piston (5) has a .cylindrically formed through hole at right angles to its longitudinal direction, the hole forming a sample chamber (9) , such that when the sampling piston is in its retracte position inside the housing the chamber is in register wit at least one hole (11) of substantially the same diameter the cylindrical surface of the housing, for connecting to it a preferably cylindrical casing (32) defining a mixing and dilution chamber (35) in which there is an agitating o mixing device (36) , said casing being provided with two opposing openings (33, 34), of which one (33) has the same diameter as the hole (11) in the cylindrical surface of the housing and the other has a shape affording sealing connection to an end wall member (23) carrying a screening plate (22) , said member being provided with a drainage collection duct (24) under the screening plate (22) and a valve (29) which is connectable to a pressurized medium source for flushing after sampling in a manner known per se 2. Apparatus as claimed in claim 1, c h a r a c t e r¬ i z e d i that the cylindrical surface of the housing (4) is provided with two mutually opposing holes (10, 11) in register with the chamber in the piston (5) , the upper hole (10) merging into a space (13) defined by an end wall (12) integral with a cylinder wall (14) which is sealingly fixable over the hole (10) , in that an inlet (15) for the - wipo supply of measuring water and washing water opens out into the space (13) , and in that a flushing water outlet (17) , which can be put in communication with the space (13) via a hole in the end wall (12) , is arranged in the area adjacent the end wall. 3. Apparatus as claimed in claim 1, c h a r a c t e r¬ i z e d i n that the movement in the housing (4) " of the sampling piston (5) is provided with the aid of a pneumatic cylinder (8) , the piston rod (7) of which is attached to the outward end portion (6) of the sampling piston (5) at a point spaced from the axis (21) of the piston (5) . 4. Apparatus as claimed in any of the preceding claims, c h a r a c t e r i z e d i n that the agitating or mix¬ ing device arranged in the mixing chamber (35) consists of a motor-driven propeller (36) situated centrally inside the mixing chamber (35) with its axis of rotation horisont or transverse the longitudinal direction of the mixing chamber (35) . 5. Apparatus as claimed in any of the preceding claims, c h a r a c t e r i z e d i n that the end wall (12) wit its cylindrical wall (14) and the end member (23) with the intermediate mixing chamber casing (32) are removably fixable to the cylindrical surface of the housing (4) with the aid of toggle catches. 6. Method of determining the degree of permeability and the fine fraction content of a suspension flowing through such as a pipe (2) , particularly a fibre suspension, with the aid of a drainage rate transmitter including a samplin piston housing (4) attachable round an opening (3) made in the wall of the pipe (2) , the housing being open towards the interior of the pipe (2) and accommodating con¬ centrically an axially displaceable sampling piston (5) , sϋRE _ OMPI adapted for taking out a suspension sample, said piston (5) having a cylindrically formed through hole at right angles to its longitudinal direction, the hole forming a sample chamber (9), such that when the sampling piston (5) is in -its retracted position inside the housing (4) the chamber (9) is in register with at least one hole (11) of sub¬ stantially the same diameter in the cylindrical surface of the housing (4) , for connecting to it a preferably cylindrical casing (32) defining a mixing and dilution chamber (35) , in which there is an agitating or mixing device (36) , said casing being provided with two opposing openings (33, 34) , of which one has the same diameter as th hole (11) in the cylindrical surface of the housing (4) and the other has a shape affording sealing connection to an end wall member (23) carrying a screening plate (22) , c h a r a c t e r i z e d i n that smaller fibre frag¬ ments in a pulp sample introduced into the measuring or mixing chamber (35) are removed during filtering against th screening plate (22) and subsequent permeation of water - during one or more pressure drops, possibly after slushing of the pulp bed formed against the screening plate (22) by agitation between the different measurements, by the pulp bed once again being brought into suspension by slushing with the aid of the mixing or agitating device (36) and a simultaneously provided flow of water, subsequent to which the fibre suspension substantially impoverished of fine material is filtered against the screening plate (22) after terminated agitation, the drainability of the pulp bed formed being measured during one or more pressure drops, possibly with intermediate slushing and reformation. 7. Method as claimed in claim 6, c h a r a c t e r¬ i z e d i n that the permeability of the pulp bed is measured during a formation phase during the build-up of the pulp bed on the screening plate (22) .

Inventors: GREN URBAN, LJUNGKVIST KJELL, SKAOLLEN BENGT, GREN, URBAN, LJUNGKVIST, KJELL, SKAOLLEN, BENGT
Applicants: KAELLE EUR CONTROL, EUR-CONTROL KAELLE AB
Application year: 1984
Main classification: G01N1
IPC codes: G01N1, G01N15