GLASS ENCAPSULATED QUARTZ OSCILLATOR

Abstract: A quartz crystal (1) is encapsulated in a glass tube (4) by bonding lead-in wires (3) to the crystal, press sealing one end of the glass tube onto the lead-in wires, and then heating and sealing the other end of the glass tube.

Description: GLASS ENCAPSULATED QUARTZ OSCILLATOR This invention is concerned with quartz crystal oscillators. Such crystals are shown in U. S. Patents 3,483,402, 3,877,122 and 4,183,126. The crystals are often encapsulated in order to protect them from the environment, for example, humidity, in order to prevent a shift of electrical characteristics throughout the operating life of the crystal. In the prior art, such encapsulation generally consisted of preformed containers which were relatively expensive and did not readily lend themselves to high speed manufacturing processes. For example, a commonly used prior art encapsulating process employed a preformed rectangular glass container, a preformed glass base, two rigid lead-in wires and two preformed metal springs. First, the lead-in wires were embedded in the glass base and the metal springs were then welded to the lead-in wires. Next, the quartz crystal was conductively bonded to the springs so that one electrode (metallized surface) of the crystal was in electrical contact with one of the springs, and the other metallized surface of the crystal was in electrical contact with the other spring. Finally the mounted crystal was inserted into the glass container, the glass base being a reasonably close fit within the open end of the glass container, and the glass base and the end of the glass container were heated to their soldering point, and fused together to seal the container. This process does not readily lend itself to high speed manufacture. This invention discloses an encapsulation process which does not require preformed parts and is suitable for high speed. manufacture. The only parts required are two lead-in wires and a glass tube. First, the quartz crystal is conductively bonded to the lead-in wires, that is to say, one electrode is electrically and physically connected to one of the lead-in wires and the other electrode is electrically and physically connected to the other lead-in wire. The conductive bond may be made, for example, by electrically conductive bonding material, for example, silver-filled epoxy. Or it may be made by soldering, welding and the like. The quartz crystal is then inserted into an openended glass tube-of suitable diameter and length. The extremities of the lead-in wires protrude outside the glass tube and are secured in a suitable external holder to properly position the quartz crystal within the glass tube. The end of the glass tube is then heated to its EMI2.1 softening point and pressed together to seal the end by forming a press seal, the lead-in wires being embedded in the press seal. For this purpose, the lead-in wires are of a type readily sealable to glass, for example, dumet wire for sealing to soft glass. Dumet comprises a nickel-iron core.within a copper sheath. Upon cooling, the press seal solidifies and rigidly holds the lead-in wires and quartz crystal. Next, a circumferential section of the glass tube near the other end thereof is heated to its softening point and the end is then drawn apart from the main body of the glass tube to form a necked-down portion in the glass tube. Said end is then cut off or otherwise removed, leaving the necked-down portion which is of smaller diameter than the glass tube and is suitable as an exhaust tubulation to exhaust, tip-off and seal the glass tube with the quartz crystal therewithin. After exhausting (by vacuum) the atmosphere within the glass tube, the exhaust tubulation may be tipped off under vacuum, to maintain a vacuum within the glass tube. Or an inert gas, for example, dry nitrogen, may be introduced into the glass tube prior to tip-off of the exhaust tube. If necessary, a cooling gas, e.g. nitrogen, may be flowed into the glass tube during the sealing steps in order to cool the quartz crystal and prevent it from being heated above the curie point of the quartz material. The drawing shows one embodiment of an encapsulated quartz crystal in accordance with this invention. Quartz crystal 1 comprised a flat circular disk about 8mm in diameter by 0.5mm thick. The metallized portion 2 of each surface was about 6mm in diameter. Lead-in wires 3 were made of dumet, 0.35mm thick, and were fastened to electrodes 2. Glass tube 4 was 1lmm outside diameter by 20mm long (internal length). Press seal 5 was about 9mm wide by about 7mm long and was about 2.5mm thick. After exhausting and filling with nitrogen, glass tube 4 was sealed at tip-off 6. If desired, lead-in wires 3 could be embedded in glass bead 7 prior to press sealing in order to bend and hold wires 3 in the correct position for fastening crystal 1 thereto. Also, if necessary, the frequency of quartz crystal 1 can be adjusted prior to the top end sealing by techniques known to the art, for example, by an Iodine trimming system. Or crystal 1 can be trimmed to its final frequency by means of a laser after complete sealing of the glass tube. In some cases, it may be desirable for glass tube 4 to be flattened into, say a flat substantially rectangular shape, instead of being circular, in order to reduce the size of glass tube 4 or in order to accommodate a rectangular quartz crystal 1. In such a case, the openended round glass tube would be heated and flattened prior to mounting of the quartz crystal/lead-in wire assembly therein. After embedment of said assembly in a press seal at one end of the flattened glass tube, the other end could also be sealed by a press seal without the need of an exhaust tubulation. In such a case, nitrogen, for example, could be introduced into the interior of the flattened glass tube by means of a small diameter hollow metal needle inserted therein while the glass was heated to its softening point. At the proper time, the needle would be removed and the press seal made immediately, thereby providing the desired nitrogen fill within the -glass tube.

Claims: 1. The method of encapsulating a flat quartz crys tal having an electrode on each surface comprising the steps of: connecting a lead-in wire by means of an electrically conductive bond to one electrode of the quartz crystal; connecting a second lead-in wire.by means of an electrically conductive bond to the other electrode; disposing the lead-in wires in a holder and inserting the quartz crystal into one end of an open-ended glass tube; heating said end of the glass tube to its softening point; pressing the softened end of the glass tube together with the lead-in wires therebetween to form a press seal in which the lead-in wires are embedded; and heating and sealing the other end of the glass tube. 2. The method of claim 1 wherein the glass tube is circular and the other end is sealed by heating a circumferential section of the glass tube near said other end thereof to its softening point; drawing out the softened section to form a necked down portion; removing enough of said other end of the glass tube to permit the necked down portion to be used as an exhaust tubulation; exhausting the glass tube through the exhaust tubulation; and sealing the glass tube by tipping off the exhaust tubula tion. 3. The process of claim l wherein the lead-in wires are embedded in a glass bead prior to press sealing. 4. The process of claim 1 wherein an inert gas is introduced into the glass tube after the exhausting step. 5. The process of claim 1 including the step of adjusting the frequency of the quartz crystal prior to the necking step. 6. The method of claim 1 wherein the open-ended glass tube has a flat substantially rectangular shape and the other end of the glass tube is sealed by a press seal. 7. The process of claim 1 including the step of adjusting the frequency of the quartz crystal after the glass tube is completely sealed. 8. An encapsulated quartz crystal made in accordance with claim 1. 9. An encapsulated quartz crystal comprising: a flat quartz crystal having an electrode on each surface and disposed within a sealed glass tube having a press seal at one end thereof and a tip-off at the other end; two lead-in wires, one bonded to each electrode of the quartz crystal, the lead-in wires being embedded in, and extending through, the press seal. 10. The quartz crystal of claim 9 comprising, in addition, a glass bead in which the lead-in wires are embedded, the glass bead being disposed between the quartz crystal and the press seal.

Inventors: BUCKINX, POL, HOEBER, HENRI, VAN NOPPEN, JEAN
Applicants: GTE PRODUCTS CORPORATION
Application year: 1982
Main classification: H03H9
IPC codes: H03H9, H03H3